Professional Documents
Culture Documents
Questions:
1. What is the rule in diluting acids? What is the basis of this rule?
When diluting acids, the guideline is to pour the water into a beaker first, then gently pour
the acid down a stirring rod into the water (when mixing them), not the other way around.
The basis for this rule is that if you pour the water in a beaker that has acids in it, the acids
would boil and may even spill out of the beaker. This is because heat is created when the two
are combined, causing it to boil. So, you must always Add the acid to the water
2. What are volatile chemicals? How do you handle volatile chemicals in the lab?
Volatile chemicals are chemicals that are give of vapors which can cause can irritation to the
eyes, nose and even throat, while also can cause difficulty breathing and nausea. To handle
volatile chemicals in the lab, one must be carefully and preform the experiment when dealing
with volatile chemicals in a fume hood which is an enclosure in which gases or vapors and fumes
are contained.
5. Why you should not wear contact lenses when performing chemistry experiments?
Wearing contact lenses in a lab can be a hazard since, wearing one may trap chemical vapors
against once eyes, if that does happen your eyelids may go into spasms that makes it impossible
to remove the lenses and wash out the chemicals, which can cause eye damage. Since some
vapors can be absorb by some lens which may cause irritation or even injury. Which is why
wearing contact lenses are advice to be removed to prevent such events. And why we have to
wear goggles.
6. In case chemicals was splattered on your eyes, how long should you use the eye shower?
In case an accident happened where a chemical was hit your eyes, you have to wash them
immediately in an eye wash fountain, they must wash there eyes thoroughly for at least 15 mins
however should they be wearing any contact lenses they have to remove the contact lenses as
soon as possible after giving your eyes a good rinsing, after which they should see a doctor
immediately to have a check up on whether their eyes were damage or not. Since chemical spills
and splashes are common lab accidents we should be carefully and prepared in case an accident
does happen.
7. What is the correct way of extinguishing fire on clothes
In case someone clothes catch on fire there are a couple of ways you can put out the fire. First, to
put out the fire by going to the safety shower however should there not be a safety shower or its
not close by you can do the “Stop, Drop, and Roll” this is where the victim stop immediately,
then drops to the ground, and cover their face with once hands. And roll then wait till the fire is
put out and a fire blanket put on the place of the fire and wait for it to extinguish after which
when the fire is put out they should get medical attention immediately.
Safety proceeds:
Thermometer Safety
Don’t shake the Thermometers
Use thermometers in suitable temperature range
Lay thermometers down on a towel or wire screen away from edge
Let your teacher clean up broken thermometers
Glass Tubing Safety.
Most common lab injuries are cuts from broken glass especially glass tubing a typical
accident comes form using too much force to push a tube through the hole in the stopper
one
One way to avoid this kind of accidents is to use an inserter
First dip the Teflon tip in glass lubricant such as glycerin
Then push it through the stopper then remove the tip and slide the tubing through the
hollow inserter shaft removing the shaft leaves the tubing behind make sure to wash the
lubricant off the tubing and stopper before using them and replace the Teflon tip so it
doesn’t get lost
To remove the tubing take out the tip and lubricate the end of the hollow shaft
Then push it through the stopper hole around the tubing then slide the tubing out through
the shaft and remove the inserter
Remember to wash the lubricant off before returning the stopper and tubing to the storage
and don’t forget to replace the tip
If you don’t have an inserter lubricate the tubing instead and protect your hands with
leather gloves push the tubing gently through rotate if there’s any resistance use the same
carer when removing it
And don’t forget to wash of the lubricant
Glass Tubing Safety
Use an inserter (to place glass tubing and a stopper or remove)
Lubricate the tubing and wear leather gloves
Centrifuge Safety.
A centrifuge spins mixtures around in test tubes to separate solids from liquids the solids
move towards the bottom of the tubes and the liquids stay in top
When the test tubes inside aren’t evenly distributed the centrifuge is unbalanced
It vibrates like a washing machine with an unbalanced load if the vibration is bad enough
it can fall off the bench top
To prevent vibration a centrifuge must be balance
If your only centrifuging one test tube place another one opposite it with an equal amount
of water
Once it is balanced you turn it on and when its finish turn it off and wait till it stops
spinning on its own never try to stop a centrifuge with your hand
Centrifuge Safety.
Place equalize test tubes for balance
Don’t try to stop it from spinning with your hand
Emergency Equipment.
In spite of safety precautions people get careless and accidents happen
That’s why a well-equipped chem lab jas emergency equipment
If you’ve cut yourself wash the wound to remove any chemical traces make sure
there are no pieces of glass in the cut
Dry your skin carefully so a bandage will stick
Notify your teacher whenever you have an accident and make sure to get
immediate medical attention after any injury in the lab
Chemical spills and splashes are also common lab accidents
If a chemical hit your eyes wash them immediately in an eye wash fountain
Hold your eyes open and roll them around so the water can wash them thoroughly
you shouldn’t be wearing contacts but if you are get them out as soon as you’ve
given your eyes a good initial rinsing continue washing for at least 15 mins then
see a doctor immediately to check your eyes for damage
Non corrosive chemical splashes on bare skin should be rinsed off in the lab sink
with plenty of water
Spills of corrosive materials require a lot more water don’t wait till you feel pain
from the chemical head for the safety shower immediately rinse your body
thoroughly as fast as possible take off all your clothes
Stay under the shower for at least 15 mins
Fires are always a potential hazard in chem lab especially when organic liquids
are involved small fires in containers can often be put out by covering them
Then turn off the burner so the fire wont reignite
Larger fires require a fire extinguisher (by teacher)
If the fire is too large to control clear out of the building call the fire department
when you’re safely outside and tell them what chemicals are involved
Clothing fires can be put out in a couple of ways as best way is In the safety
shower and if the showers not close by the rules is stop, drop, and roll the victims
wait on the fire put some of it out and a fire blanket gets the rest flames should be
kept away from the victims face anyone who’s been burned must get medical
attention immediately
Emergency Equipment.
Clean and dry cut
Rinse eyes in the eye wash fountain
Rinse hands and arms in sink
Remove clothes and rinse large spills in safety shower
Cover small fires (extinguish small fires in containers)
Let teacher handle larger fires (extinguisher)
Put out clothing fires in safety shower
(if there’s no other way to put out a clothing fire) use fire blankets carefully to
keep flames away from face and neck
https://www.youtube.com/watch?v=9o77QEeM-68
General apparatus
- Glass Rod: used to mix chemicals and liquids and dip a paper with a solution to
determine the pH
- Pestle & Mortar: is used for grinding and crashing samples into a powder the mortar
is the bowl and pestle is the object used for grinding and crashing samples
- Evaporation dish: is used for the evaporation of a solution
- Wire gauze: are placed between the beaker and the tripod to support the beaker while
heating the solution with a Bunsen Burner
- Thermometer: measures the temp of a solution the bulb of the thermometer should be
immersed in the solution and the bulb should not touch the bottom of the beaker, if
needed the thermometer can be secured with a clamp
- Glass funnel: has a wide mouth and narrow stem a glass funnel is used when a
solution of a solid needs to be added to a flask or period without spilling
- Watch Glass: is a circular concave piece of glass it can be used to cover the mouth of
the beaker or to weigh out a solid in the absence of a weighing bottle
- Test-tube peg: is a peg that has an extended handle it is used while heating the tube to
prevent burning oneself
https://www.youtube.com/watch?v=Bp2DI32X4wE
Techniques I
Measuring the mass of a substance using an Electronic Balance
(Use and operation)
Step 1: turn the balance on, or re-zeroing the balance (make sure that the balance is zero before using
it)
Step 2: place a weighing boat or plastic weighing boat on the balance (one rule never place a substance
directly on the metal) to prevent the substance coming contact with the pan
Step 3: Re-zero the balance (press the zero button the balance will automatically re-zero itself and
subtract the weight of the plastic weighing dish)
Step 4: begin adding substance into the weighing boat (when adding never use your hand but spoon or
some other apparatus )
Step 5: stop adding substance when you have reached the required amount needed (should you spill
any substance around the balance clean it up)
Technique 2
Important point: lots of glassware can measure volume… graduated cylinders do it better than beakers
and flasks
Step 1: Using a 100 milliliter graduated cylinder, measure exactly 95.0 milliliters of di-water
Step 2: use the Di-water wash bottle to “top off” the level of water in the graduated cylinder to 95.0 ml
(remember to carefully read the volume on the graduated cylinder at eye level and remember to
measure from the bottom of the meniscus formed by the surface of the water not the top)
At this point you should have 0.50 grams of salt and sand in beaker and 95.0ml of water measured (they
should be in a 250 milliliter beaker at this point you should be ready to combine those substances)
Step 3: Combine the water with the salt and sand… swirl until the salt dissolves (by combining the water
with the salt and sand you’ve created a mixture swirling will allow the salt to dissolve and the sand will
settle to the bottom of the beaker)
Technique 3
Step 1: Submerge a thermometer into the mixture of salt, sand, and water as far as possible without
touching the beaker (in order to obtain the most accurate temp reading possible thermometer must be
submerged as far as possible without touching the bottom or the walls of the container)
For quick measurements you can hold the thermometer by hand... or use a stand and clamp (but for
longer periods of time you can use the stand with a clamp)
Never allow a thermometer to rest in a beaker unsupported it can tip over (for if you bump into it it will
easily tip over after using it a thermometer make sure to set it down flat on the countertop when done
using)
Step 2: read the thermometer to the correct level of precision… in this case 20.0 Celsius (remember that
when using any instrument with a printed scale you must round to the nearest tenth) (remember to
record your findings)
Technique 4
Step 1: set up equipment as shown… a funnel supported by a ring and triangle with a clean empty flask
beneath ()
Step 2: obtain a piece of filter paper (use a filter paper to separate the sand from salt water)
Step 3: Fold the filter paper so it fits into the funnel… first in half (fold the filter paper in half then in half
again)
Then Finally grad three of the four layers of the fold and pull them to one side forming a cone
Step 4: place the paper cone into the funnel (then you can begin the process of filtration)
Step 5: prepare to decant the liquid into the funnel using a glass rod (to more carefully pour the salt
water into the funnel containing the filter paper were going to use a technique that called decanting
hold a glass rod against the top of beaker, the rod will serve as conduit for the flow of water so can aim
that flow of water directly where I want too)
Step 6: Decanting is a technique that allows you to control exactly where the water pours into the funnel
(this will keep me from spilling salt water in the lab table)
Step 7: To get all of the sand into the filter paper you may need to rinse the beaker with the di-water
wash bottle (collect all the sand in the filter paper and the salt water in the beaker)
Technique 5
Step 1 : gather the appropriate tools… including goggles, Bunsen burner, and striker (remove any
combustible materials, any long sleeves or loose clothing should be rolled up or secured)
Before lighting the burner, you should put on an apron and safety goggles
Step 2: turn the gas valve on the bottom of the burner off (clockwise) (before hooking the burner up to
the gas jet at your table please be sure to turn this valve off until its tight)
Step 3 : turn the combustion column down (clockwise) (should also adjust the combustion column
downward by turning it, this will prevent there from being too much oxygen mixing with the gas )
Step 4: hook up the burner to the gas at your lab table (valve is off) (please be sure that they are
connection of the rubber tube to the outlet of the gas jet is tight)
Step 6: open the gas valve on the bottom of the Bunsen burner and use a striker to light the gas ()
Step 7: turn the combustion column counterclockwise to increase the amount of oxygen… flame gets
blue and hot (the inner cone is the hottest most part of the Bunsen burner flame)
If time allows you can evaporate the water to separate it from the salt
Safety Data Sheets - GHS -Top Ten Things to Know - Hazcom Safety for Work & Home
Safety Data Sheets (SDS) = 16 sections
Formerly known as material safety data sheets (MSDS)
Section 1 – Identification (manufacturer or distributors name, address, and phone number in front of
section 1 along with 24/7 emergency phone)
Section 4 - first air measures (signs and symptoms of exposure to the chemicals )
Section 7 – handling & storage (provides information about where to store this)
Section 8 – exposure controls/personal protection (this tells us what we need to do to engineer a safe
environment when using)
Section 9 - physical & chemical properties (lists the chemical characteristics we should know)
Section 10 -stability & reactivity (outlines these cautions along with any known hazardous reactions)
Section 11 – toxicological information (could repeated exposure cause allergic reaction, any short or
long-term health effects to exposure)