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Superpave Asphalt Mix Design

Dr. Hozayen Ahmed Hozayen


Professor of Highway Engineering

Hozayena@yahoo.com

0020106044758

NCAT 1

A
Introduction to Superpave
Mix Design Concepts
Materials Selection – Aggregate
Materials Selection - Binder

NCAT 2

1
Mix (aggregate) Properties

Aggregate Gradation

Mix (aggregate) Gradations


* Uniformly graded
- Few points of contact
- Poor interlock (shape dependent)
- High permeability
* Well graded
- Good interlock
- Low permeability
* Gap graded
- Only limited sizes
- Good interlock
- Low permeability

2
Aggregate Gradation
• Use 0.45 Power Gradation
Chart
• Blend Size Definitions
– maximum size
– nominal maximum size
• Gradation Limits
– control points
– restricted zone

0.45 Power Grading Chart


Percent Passing
100

80

60 Example:

40 4.75 mm sieve plots at (4.75)0.45 = 2.02


20

0
0 1 2 3 4
Sieve Size (mm) Raised to 0.45 Power

3
0.45 Power Grading Chart
Percent Passing
100

80
max
60
size
40

20
maximum density line
0
0 .075 .3 .6 1.18 2.36 4.75 9.5 12.5 19.0
19.0
Sieve Size (mm) Raised to 0.45 Power

Aggregate Size
100 10a
100 Definitions 99
90 89
• Nominal Maximum
72 72
65 Aggregate Size 65
48 – one size larger than the first 48
36 sieve to retain more than 10% 36
22 22
15
• Maximum Aggregate Size 15
9 – one size larger than nominal 9
4 maximum size 4

4
Percent Passing
100
max density line

restricted zone

control point nom max


max size
size

0
.075 .3 2.36 4.75 9.5 12.5 19.0

Sieve Size (mm) Raised to 0.45 Power

Superpave Aggregate
Gradation
Percent Passing
100

Design Aggregate Structure

0
.075 .3 2.36 12.5 19.0
Sieve Size (mm) Raised to 0.45 Power

5
Superpave Mix Size
Designations
Superpave Nom Max Size Max Size
Designation (mm) (mm)

37.5 mm 37.5 50
25 mm 25 37.5
19 mm 19 25
12.5 mm 12.5 19
9.5 mm 9.5 12.5

Gradations
* Considerations:
- Max. size < 1/2 AC lift thickness
- Larger max size
+ Increases strength
+ Improves skid resistance
+ Increases volume and surface area of agg
which decreases required AC content
+ Improves rut resistance
+ Increases problem with segregation of particles
- Smaller max size
+ Reduces segregation
+ Reduces road noise
+ Decreases tire wear

6
Target Gradation
• Acceptable gradation band specified
• Mix design selects a job mix formula (JMF)
which falls within band and meets design
criteria
• Superpave
– 5 nominal sizes (37.5, 25, 19, 12.5, and 9.5 mm)
– Four sieve sizes used to set upper and lower limits
– Staying out of the restricted zone in suggested to
minimize problems with natural sands

Blending Stockpiles

• Basic formula for combining


stockpiles to achieve a target
gradation is:

p = Aa + Bb + Cc + ….
where:
p = percent of material passing given sieve size
A, B, C, .. = percent passing given sieve for each agg.
a, b, c, … = decimal fraction of A, B, C, … to be used

7
Blending Stockpiles

• Plot individual gradations


• Plot specification limits
• Can be used for initial
assessment
– Can blend be made from available
materials?
– Identification of critical sieves
– Est. trial proportions

All possible combinations fall between A and B

Percent Passing, %

100
100
90
90 Gradation B
80
80 Control points for
70
70 12. 5 nominal max. size
60
60
50
50
40 Gradation A
40
30 30
20 20
10 10
0 0
0.075 0.3 1 .18 4.75 9.5 12.5 19

Sieve Size, mm

8
No poss. combination of A and B will meet spec.

Percent Passing, %
100
Gradation B Gradation A
90
80
70
60
50 Control points for
12. 5 nominal max. size
40
30
20
10
0
0.075 0.3 1 .18 4.75 9.5 12.5 19

Sieve Size, mm

All poss. combinations pass through cross-over point


Blends containing more A than B will be closer to A
Percent Passing, %
100 Gradation A
90
80
70
60
Gradation B
50
40
30
20 Control points for
12. 5 nominal max. size
10
0
0.075 0.3 1 .18 4.75 9.5 12.5 19

Sieve Size, mm

9
Trial and Error Steps

• Select critical sieves in blend


• Determine initial proportions which
will meet critical sieves
• Check calc. blend against
specification
• Adjust if necessary and repeat above
steps

Blended Aggregate Specific


Gravities

• Once the percentages of the


stockpiles have been established,
the combined aggregate specific
gravities can also be calculated

10
Combined Specific Gravities

1
G=
P1 + P2 + ……. Pn
100 G1 100 G2 100 Gn

Blending of Aggregates
• Reasons for Blending
– Obtain desirable gradation
– Single natural or quarried material not
enough
– Economical to combine natural and
process materials

11
Blending of Aggregates
• Numerical Method
– Trial and Error
– Basic Formula

Blending of Aggregates
· P = Aa + Bb + Cc + ….
– Where:
• P = % of material passing a given sieve for
the blended aggregates A, B, C, …
• A, B, C, … = % material passing a given
sieve for each aggregate A, B, C, …..
• a, b, c, …. = Proportions (decimal fractions)
of aggregates A, B, C, … to be
used in Blend

12
Blending of Aggregates
Material Agg. #1 Agg. #2
% Used Blend Target
% % % %
U.S. Sieve
Passing Batch Passing Batch
3/8 “ 100 100
No. 4 90 100
No. 8 30 100
No. 16 7 88
No. 30 3 47
No. 50 1 32
No. 100 0 24
No. 200 0 10

Blending of Aggregates
Material Agg. #1 Agg. #2 First Try
(remember trial & error)
% Used 50 % 50 % Blend Target
% % % %
U.S. Sieve
Passing Batch Passing Batch
3/8 “ 100 50 100 100 * 0.5 = 50 100
No. 4 90 45 100 90 * 0.5 = 45 80 - 100
No. 8 30 15 100 30 * 0.5 = 15 65 - 100
No. 16 7 3.5 88 7 * 0.5 = 3.5 40 - 80
No. 30 3 1.5 47 3 * 0.5 = 1.5 20 - 65
No. 50 1 0.5 32 1 * 0.5 = 0.5 7 - 40
No. 100 0 0 24 0 * 0.5 = 50 3 - 20
No. 200 0 0 10 0 * 0.5 = 0 2 - 10

13
Blending of Aggregates
Material Agg. #1 Agg. #2
% Used 50 % 50 % Blend Target
% % % %
U.S. Sieve
Passing Batch Passing Batch
3/8 “ 100 50 100 50 100 100
No. 4 90 45 100 50 95 80 - 100
No. 8 30 15 100 50 65 65 - 100
No. 16 7 3.5 88 44 47.5 40 - 80
No. 30 3 1.5 47 23.5 25 20 - 65
No. 50 1 0.5 32 16 16.5 7 - 40
No. 100 0 0 24 12 12 3 - 20
No. 200 0 0 10 5 5 2 - 10

Blending of Aggregates
Material Agg. #1 Agg. #2
% Used 50 % 50 % Blend Target
% % % %
U.S. Sieve
Passing Batch Passing Batch
3/8 “ 100 50 100Let’s Try 50 100 100
No. 4 90 45 100 and get 50 95 80 - 100
No. 8 30 15 100a little closer
50 65 65 - 100
No. 16 7 3.5 to
88the middle44 of 47.5 40 - 80
the target values.
No. 30 3 1.5 47 23.5 25 20 - 65
No. 50 1 0.5 32 16 16.5 7 - 40
No. 100 0 0 24 12 12 3 - 20
No. 200 0 0 10 5 5 2 - 10

14
Blending of Aggregates
Material Agg. #1 Agg. #2
% Used 30 % 70 % Blend Target
% % % %
U.S. Sieve
Passing Batch Passing Batch
3/8 “ 100 30 100 70 100 100
No. 4 90 27 100 70 97 80 - 100
No. 8 30 9 100 70 79 65 - 100
No. 16 7 2.1 88 61.6 63.7 40 - 80
No. 30 3 0.9 47 32.9 33.8 20 - 65
No. 50 1 0.3 32 22.4 22.7 7 - 40
No. 100 0 0 24 16.8 16.8 3 - 20
No. 200 0 0 10 7 7 2 - 10

Aggregates

Usually refers to a soil that has in


some way been processed or sorted.

15
Aggregate Processing

• Excavation
• Transportatio
n
• Crushing
• Sizing
• Washing

Excavation
* Natural sands and gravels
- Underwater sources
+ Rivers & lakes
+ Barge-mounted dredges, draglines,
scoop, conveyors, or pumps
+ Relatively clean
- Land sources
+ Gravel or sand pits
+ Bucket loader

16
Excavation

Excavation
* Crushed stone and rock
- Rock depths < 50 ft., overburden washed
out during processing

- Rock depths > 50 ft., remove overburden


+ Soil stripped with bulldozers
and scrapers

- Blasting required

17
Excavation

Crushing

18
Crushing
River Gravel Partially Crushed
River Gravel

Transportation

19
Transportation

Transportation

20
Sizing

Stockpiling
* Prevent segregation and contamination
* Good stockpiling = uniform gradations
- Short drop distances
- Minimize moving
- Don't use "single cone" method
- Separate stockpiles

21
Stockpiling

Sampling
• Why Sampling Is Important
– To evaluate the potential quality of a
proposed aggregate source.
• Does new source meet aggregate
specifications?
– To determine compliance with project
specification requirements.
• Do current aggregates meet specifications?

22
Sampling from Stockpile

Sampling from Fine


Aggregate Stockpile

Sampling from Conveyor

23
Source Aggregate
Properties
Toughness
Soundness
Deleterious
Materials
Gradation

Definitions
* Coarse Aggregate
- Retained on 4.75 mm (No. 4) ASTM D692
- Retained on 2.38 mm (No. 8) Asphalt Institute
- Retained on 2.00 mm (No. 10) HMA Book

* Fine Aggregate.
- Passing 4.75 mm (No. 4) ASTM D1073
- Passing 2.38 mm (No. 8) Asphalt Institute

* Mineral Filler
- At least 70% Pass. 0.075 mm ASTM D242

24
Toughness
* Los Angeles Abrasion (AASHTO T96, ASTM C131):
Resistance of coarse agg to abrasion and
mechanical degradation during handling,
construction and use

* Aggregate at standard gradation subjected to


damage by rolling with prescribed number of steel
balls in large drum for a given number of rotations

* Result expressed as % changes in original weight

LA Abrasion Test

- Approx. 10% loss for extremely hard igneous rocks


- Approx. 60% loss for soft limestones and sandstones

25
Soundness
* Estimates resistance to weathering .

* Simulates freeze/thaw action by successively wetting


and drying aggregate in sodium sulfate or magnesium
sulfate solution
+ One immersion and drying is considered one
cycle

* Result is total percent loss over various sieve intervals


for a prescribed number of cycles
+ Max. loss values typically range from
10 to 20%per 5 cycles

Soundness

26
Soundness

Before After

Gradations

• Aggregate Gradation
– The distribution of particle sizes
expressed as a percent of total weight.
– Determined by sieve analysis

27
Steps in Gradation Analysis
Mechanical sieve analysis
– Place dry aggregate in standard
stack of sieves
– Place sieve stack in mechanical
shaker
– Determine mass of aggregate
retained on each sieve

Mechanical Sieve

Individual Sieve Stack of Sieves

28
Mechanical Sieve

Stack in
Mechanical
Shaker

Gradations - Computation
Sieve Mass Cumulative
Retained Mass Retained % Retained % Passing

9.5 0.0
4.75 6.5
2.36 127.4
1.18 103.4
0.60 72.8
0.30 64.2
0.15 60.0
0.075 83.0
Pan 22.4

29
Gradations - Computing

Cum. Wt Retained
% Retained = * 100
Original Dry Wt.

% Passing = [ 1- Cum. Wt Retained


Original Dry Wt.
] * 100

Gradations - Computation
Sieve Mass Cumulative
Retained Mass Retained % Retained % Passing

9.5 0.0 0.0 0.0 100.0


4.75 6.5 6.5 1.2 98.9
2.36 127.4 133.9 24.8 75.2
1.18 103.4 237.3 44.0 56.0
0.60 72.8 310.1 57.5 42.6
0.30 64.2 374.3 69.4 30.6
0.15 60.0 434.3 80.5 19.5
0.075 83.0 517.3 95.8 4.2
Pan 22.4 539.7 100.0 0.0

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Asphalt Cements

Background
History of Specifications

Background
• Asphalt • Tar
– Soluble in – Resistant to
petroleum petroleum
products products
– Generally a by- – Generally by-
product of product of coke
petroleum (from coal)
distillation process production
– Can be naturally
occurring

31
Background
• First US hot mix
asphalt (HMA)
constructed in
1870’s
– Pennsylvania Ave.
– Used naturally
occurring asphalt
from surface of lake
on Island of Trinidad
• Two sources
– Island of Trinadad

Background
• Each lake asphalt source very
consistent
– Used solubility test to determine source
• Insolubles differed substantially between
sources

• Demand for paved roads exceeded


the supply of lake asphalts in late
1800’s
– Led to use of petroleum asphalts

32
Petroleum-Based Asphalts
• Asphalt is waste product from
refinery processing of crude oil
– Sometimes called the “bottom of the
barrel”
• Properties depend on:
– Refinery operations
Gasoline
– Composition crude source-dependent
Kerosene
Barrel of Crude Oil
Lt. Gas Oil
Diesel
Motor Oils

Asphalt

Asphalt Cement Components


• Asphaltenes
– Large, discrete solid inclusions (black)
– High viscosity component
• Resins
– Semi-solid or solid at room
temperature
• Fluid when heated
• Brittle when cold
• Oils
– Colorless liquid
– Soluble in most solvents
– Allows asphalt to flow

33
Refinery Operation

LIGHT DISTILLATE

PUMPING MEDIUM DISTILLATE


FIELD STORAGE STATION

HEAVY DISTILLATE
TOWER
DISTILLATION
REFINERY

RESIDUUM
PROCESS
UNIT
OR
STORAGE TUBE CONDENSERS
HEATER AND ASPHALT
GAS COOLERS CEMENTS
AIR
PETROLEUM BLOWN FOR PROCESSING INTO
ASPHALT EMULSIFIED AND
CUTBACK ASPHALTS
SAND AND WATER AIR

STILL

Types
• Asphalt cements
– Generally refinery produced material
– Air blown asphalt cements
• Cutbacks
– Asphalt cements “cut” with petroleum
solvents
• Emulsions
– Mixture of asphalt cement, water, and
emulsifying agent

34
Air Blown Asphalt Cement

Cutbacks
• Rapid cure (RC) (Naphtha or
Gasoline)
– High volatility of solvent
– Tack coats, surface treatments
• Medium cure (MC) (Kerosene)
– Moderate volatility
– Stockpile patching mix
• Slow cure (SC) (Low viscosity
oil)
– Low volatility
– Prime coat, dust control

35
Emulsions
• Emulsifier gives surface charge to
asphalt droplets suspended in water
medium
– Anionic
• Negative charge
• Alkaline
• Good with limestones (positive charge)
– Cationic
• Positive charge
• Acid
• Good with silica gravels (negative charge)

Purchasing of Asphalt
Cements
• Need to be able to specify
desirable characteristics
• “Desirable characteristics” have
evolved over time and with
increasing technological
advances

• Purchasing requires
specifications

36
Early Specifications
• Lake Asphalts
– Appearance
– Solubility in carbon disulfide
• Petroleum asphalts (early
1900’s)
– Consistency
• Chewing
• Penetration machine
– Measure consistency

Penetration Testing
• Sewing machine needle
• Specified load, time, temperature

100 g Penetration in 0.1 mm

Initial After 5 seconds

37
Penetration Specification
• Five
Grades
• 40 - 50
• 60 - 70
• 85 - 100
• 120 - 150
• 200 - 300

Penetration Gradation
Specification
• Uses penetration results to
specify
• Adds
– Flash point test
– Ductility
– Solubility
– Thin film oven aging
• Penetration
• Ductility

38
Flash Point (Safety)

Thermometer

Cup filled with


asphalt

Wand attached
to gas line

Ductility

39
Solubility (Purity)

Thin Film Oven

Pan Thermometer

Rotating Shelf

Outside of Oven

40
Typical Penetration
Specifications
Penetration 40 - 50 200 - 300
Flash Point, C 450+ 350+
Ductility, cm 100+ 100+
Solubility, % 99.0+ 99.0+
Retained Pen., % 55+ 37+
Ductility, cm NA 100+

Penetration, 0.1 mm

Medium

Low

High

25C (77F)

Temperature

41
Advantages

• Grades asphalt near average in-


service temp.
• Fast
• Can be used in field labs
• Low capital costs
• Precision well established
• Temp. susceptibility can be
determined

Disadvantages
• Empirical test
• Shear rate
– High
– Variable
• Mixing and compaction temp.
information not available
• Similar penetrations at 25C (77F)
do not reflect wide differences in
asphalts

42
Viscosity Graded
Specifications

Definition
Viscosity: the ratio between the applied shear
stress and the rate of shear.

η=τ/γ

43
Types of Viscosity Tubes

Zietfuchs Cross-Arm
Asphalt Institute Tube
Tube

Testing
• Absolute viscosity
– U-shaped tube with
timing marks & filled
with asphalt
– Placed in 60C bath
– Vacuum used to pull
asphalt through tube
– Time to pass marks
– Visc. in Pa s (Poise)

44
Testing
• Kinematic viscosity
– Cross arm tube with
timing marks & filled with
asphalt
– Placed in 135C bath
– Once started gravity
moves asphalt through
tube
– Time to pass marks
– Visc. in mm2 / s
(centistoke)

Viscosity Grade
Specifications
• ASTM D3381
• Three specifications
– Table 1
• Original properties
– Table 2
• Original properties
– Table 3
• Rolling thin film oven aging

45
Table 1 & 2 Tests

• Viscosities at 60 and
135oC
• Penetrations at 25oC
• Flash point
• Solubility
• TFO aged residue
– Viscosity at 60oC
– Ductility at 25oC

Table 1 & 2 Grades


• Table 1
– AC 2.5, AC 5, AC 10, AC 20, AC 40
• Table 2
– AC 2.5, AC 5, AC 10, AC 20, AC 30, AC
40

46
Table 1 Example
AC 2.5 AC 40
Visc, 60C 250 + 50 4,000 + 800
Visc, 135C 80+ 300+
Penetration 200+ 20+
Visc, 60C <1,250 <20,000
Ductility 100+ 10+

Table 2 Example
AC 2.5 AC 40
Visc, 60C 250 + 50 4,000 + 800
Visc, 135C 125+ 400+
Penetration 220+ 40+
Visc, 60C <1,250 <20,000
Ductility 100+ 25+

47
Ave. Mixing
Hot
Service &
Summer
Temp. Compaction
Viscosity (Stiffness)

40 Pen

60 Pen
2400
Low
1600 Table 2
300
210
Table 1
25C (77F) 60C (140F) 135C (275F)
Temperature

Mixing/Compaction
Temps
Viscosity, Pa s
10
5

1
.5
.3 Compaction Range
.2 Mixing Range

.1
100 110 120 130 140 150 160 170 180 190 200
Temperature, C

48
Advantages
(Original AC Visc. Grade)
• Fundamental property
• Wide range of temperatures
• Based on max. pavement surface
temp.
• Wide range of instruments
• Test method precision
established
• Temperature susceptibility is
controlled

Disadvantages
(Original AC Visc. Grade)
• More expensive
• Longer testing time
• More technician skill needed
• Not applicable for Non-Newtonian
materials
• Wide range of properties for same
grade

49
Table 3
• AR Grades
– AR 1000, AR 2000, AR
4000, AR 8000, AR 16000

• Tests on RTFO aged residue


– Viscosities at 60 and 135oC
– Penetrations at 25oC
– % of Original Penetration
– Ductility
– Properties of unaged asphalt
• Flash point and solubility

Rolling Thin Film Oven

50
Table 3 Specification
AR 1000 AR 16,000
Visc, 60C 1,000 + 250 16,000 + 4,000
Visc, 135C 140+ 550+
Pen. 65+ 20+
% Orig. Pen NS 52+

Advantages
(AR Visc. Grade)

• Represents asphalt properties


after mixing
• Fundamental properties
• Covers wide range of
temperatures
• Limits aging

51
Disadvantages
(AR Visc. Grade)
• Highly regional
• Requires different testing
equipment
• Longer testing time
• No consistency test on original AC
• Not applicable for Non-Newtonian
materials
• Wide range of properties for same
grade

Penetration Grades
AC 40 AR 16000
40
Viscosity, 60C (140F)

100 50 AC 20
AR 8000
60
50 AC 10
70 AR 4000
85
100 AC 5
AR 2000
120
150 AC 2.5
10 200 AR 1000
300
5

52
B
Asphalt Binder Superpave Requirements
1. Performance Grade Superpave Grading
Grading Criteria
High Temperature Requirements
Low Temperature Requirements

2. Performance based specifications


Consistency Properties
Shear Reheometer Specification
Bending Beam Reohometer

PG Specifications

• Fundamental properties related to


pavement performance
• Environmental factors
• In-service & construction
temperatures
• Short and long term aging

53
PG Specifications

• Based on rheological testing


– Rheology: study of flow and deformation
• Asphalt cement is a viscoelastic
material
• Behavior depends on:
– Temperature
– Time of loading
– Aging (properties change with time)

High Temperature Behavior


• High in-service temperature
– Desert climates
– Summer temperatures Viscous Liquid
• Sustained loads
– Slow moving trucks
– Intersections

54
Pavement Behavior
(Warm Temperatures)
• Permanent deformation (rutting)
• Mixture is plastic
• Depends on asphalt source,
additives, and aggregate properties

Permanent Deformation

Courtesy of FHWA

Function of warm weather and traffic

55
Low Temperature Behavior
• Low Temperature
– Cold climates
– Winter Elastic Solid
• Rapid Loads
– Fast moving trucks

Hooke’s Law
σ=τE

Pavement Behavior
(Low Temperatures)
• Thermal cracks
– Stress generated by contraction due to
drop in temperature
– Crack forms when thermal stresses
exceed ability of material to relieve
stress through deformation
• Material is brittle
• Depends on source of asphalt and
aggregate properties

56
Thermal Cracking

Courtesy of FHWA

Aging
• Asphalt reacts with oxygen
– “oxidative” or “age hardening”
• Short term
– Volatilization of specific components
– During construction process
• Long term
– Over life of pavement (in-service)

57
Superpave Asphalt Binder
Specification
The grading system is based on Climate

PG 64 - 22

Min pavement
Performance temperature
Grade
Average 7-day max
pavement temperature

Pavement Temperatures are


Calculated

• Calculated by Superpave software


• High temperature
– 20 mm below the surface of mixture
• Low temperature
– at surface of mixture

Pave temp = f (air temp, depth, latitude)

58
Tests Used in PG
Specifications
Construction

RV DSR BBR

Concentric Cylinder Rheometers

‹ Concentric Cylinder
Mi
τ Rθ =
2 π Ri2 L

ΩR
γ=
Ro - Ri

59
Rotational Viscometer
(Brookfield)
Torque Motor

Inner Cylinder

Thermosel
Environmental
Chamber
Digital Temperature
Controller

Original Properties, Rutting, and Fatigue

DSR

RV BBR

60
Dynamic Shear Rheometer
(DSR)
Shear flow varies with
• Parallel Plate gap height and radius

Non-homogeneous flow

2M
τR =
π R3


γR =
h

Oscillating Plate
B C
A Fixed Plate

Test operates at 10 rad/sec


or 1.59 Hz
A Time
A
360o = 2 π radians per circle
1 rad = 57.3o
C
1 cycle

61
Elastic Viscous
B

Strain
A
Time
A

Strain in-phase Strain out-of-phase


δ = 0o δ = 90o

DSR Equipment
Computer Control DSR
and Data Equipment
Acquisition

62
Motor

Parallel Plates
with Sample

Area for
Liquid Bath

25 mm Plate with Sample

63
Rutting

RV BBR

DSR

Permanent
Deformation
Addressed by:
G*/sin δ on unaged binder > 1.00 kPa
G*/sin δ on RTFO aged binder >
2.20 kPa

For the early part


of the service life

64
Short Term Binder Aging
• Rolling Thin Film Oven
– Simulates aging from hot mixing and construction

Inside of RTFO

Fan

Rotating
Bottle
Carriage

Air Line

65
Bottles Before and After
Testing

Opening in
Bottle

Testing
• Calculate mass loss after RTFO
Original mass - Aged mass
Mass loss, % = x 100
Original mass

• Determine G*/sin δ for RTFO aged


material at same test temp. used for
original asphalt cement

66
Permanent
Deformation
Question: Why a minimum G*/sin δ to
address rutting
Answer: We want a stiff, elastic binder
to contribute to mix rutting
resistance
How: By increasing G* or decreasing δ

Fatigue

RV BBR

DSR

67
Fatigue Cracking
Function of repeated traffic loads over time
(in wheel paths)

Testing
• Aged binder
– Since long term performance problem,
include:
• Short term aging
• Long term aging
• Determine DSR parameters using 8
mm plate and intermediate test
temperature

68
Pressure Aging Vessel
(Long Term Aging)
• Simulates aging of an asphalt
binder for 7 to 10 years
• 50 gram sample is aged for 20
hours
• Pressure of 2,070 kPa (300 psi)
• At 90, 100 or 110 C

Pressure Aging Vessel


Rack of individual pans
(50g of asphalt / pan)

Bottom of
pressure aging
vessel

Vessel Lid Components

69
Pressure Aging Vessel

Courtesy of FHWA

Fatigue Cracking
• G* (sin δ) on RTFO and PAV aged
binder
• The parameter addresses the later
part of the fatigue life
• Value must be < 5000 kPa

70
Fatigue Cracking
• Question: Why a maximum G* sin δ
to address fatigue?

Answer: We want a soft elastic binder (to


sustain many loads without cracking)

How: By decreasing G* or decreasing δ

Thermal
Cracking

RV BBR
DSR

71
Bending Beam Rheometer

Deflection Transducer
Computer
Air Bearing

Load Cell Fluid Bath

Bending Beam Rheometer


Sample

72
Bending Beam Rheometer
Equipment

Fluid Bath
Loading
Ram

Cooling
System

Bending Beam Rheometer


• S(t) = P L3
4 b h3 δ (t)

Where:
S(t) = creep stiffness (M Pa) at time, t
P = applied constant load, N
L = distance between beam supports (102 mm)
b = beam width, 12.5 mm
h = beam thickness, 6.25 mm
d(t) = deflection (mm) at time, t

73
Bending Beam Rheometer
• Evaluates low temperature stiffness
properties
– Creep stiffness
– Slope of response (called m-value)

Log Creep
Stiffness, S(t)

8 15 30 60 120 240

Log Loading Time, t (sec)

Is Stiffness Enough?

• No. Need to assess strain needed to


break specimen.
– Thermal cracking occurs when strain is
too great
• Direct tension test
– Currently (1998) in specification
• New equipment is now available

74
Direct Tension Test
Load
Stress = σ = P / A

ΔL σf

Δ Le

εf
Strain

Direct Tension Test

FHWA

Courtesy of FHWA

75
Direct Tension Test

Courtesy of FHWA

Summary
Fatigue Low Temp
Cracking Cracking
Construction Rutting

[DTT]

[RV] [DSR] [BBR]

RTFO
No aging Short Term Aging
PAV
Long Term Aging

76
C
Performance-Based Specifications
Rutting Requirements
Aging Specifications
Fatigue Tests (for binders)
Low Temperature Tests
Selecting a PG Grade

Superpave Binder
Purchase Specification

NCAT 154

77
Superpave Asphalt Binder
Specification
The grading system is based on Climate

PG 64 - 22

Min pavement
Performance temperature
Grade
Average 7-day max
pavement temperature

Performance Grades
CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12 -
18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

78
How the PG Spec Works
CEC

Spec Requirement
Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
Remains Constant-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 5858 64
64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

Test Temperature (Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
Changes10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12 -
18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Permanent Deformation
CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

•Unaged (Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
•RTFO Aged 46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

79
Permanent
Deformation
• Addressed by high temp
stiffness
– G*/sin δ on unaged binder > 1.00 kPa
– G*/sin δ on RTFO aged binder > 2.20 kPa

Heavy Trucks
> Early part of
pavement
service life

Fatigue Cracking
CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

PAV Aged
S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

80
Fatigue Cracking

• Addressed by
intermediate temperature
stiffness
– G*sin δ on RTFO & PAV
aged binder < 5000 kPa
> Later part of
pavement service life

Low Temperature Cracking


CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value
PAV Aged -24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

81
Low Temperature Cracking
CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC
(Flash Point) FP
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO Mass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

PAV Aged -24 -30 -36


-18 -24
0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Miscellaneous Spec Requirements


CEC

Avg 7-day Max, oC PG 46 PG 52 PG 58 PG 64 PG 70 PG 76 PG 82

1-day Min, oC -34 -40 -46 -10 -16 -22 -28 -34 -40 -46 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -40 -10 -16 -22 -28 -34 -10 -16 -22
-28 -34

ORIGINAL
> 230 oC (Flash Point) FP
Flash
< 3 Pa.s @ 135 oC (Rotational Viscosity) RV
Point
(Dynamic Shear Rheometer) DSR G*/sin δ
> 1.00 kPa
46 52 58 64 70 76 82

(ROLLING THIN FILM OVEN) RTFO MassMass Loss < 1.00 %

(Dynamic Shear Rheometer) DSR G*/sin δ


Loss
> 2.20 kPa
46 52 58 64 70 76 82

(PRESSURE AGING VESSEL) PAV


20 Hours, 2.07 MPa 90 90 100 100 100 (110) 100 (110) 110 (110)

(Dynamic Shear Rheometer) DSR G* sin δ


< 5000 kPa
10 7 4 25 22 19 16 13 10 7 25 22 19 16 13 31 28 25 22 19 16 34 31 28 25 22 19 37 34 31 28 25 40 28 31
37 34

S < 300 MPa m > 0.300 ( Bending Beam Rheometer) BBR “S” Stiffness & “m”- value

-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

Report Value (Bending Beam Rheometer) BBR Physical Hardening

> 1.00 % (Direct Tension) DT


-24 -30 -36 0 -6 -12 -18 -24 -30 -36 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 -30 0 -6 -12 -18 -24 0 -6 -12
-18 -24

82
PG Binder Selection
> Many agencies have
PG 52-28 established zones

PG 58-22 PG 58-16
PG 64-10

Developed from Air


Temperatures > 20 years

• Superpave Weather Database SH


- 6 RP
A
– 6500 stations in U.S. and Canada 48A
• Annual air temperatures
– hottest seven-day temp (avg and std dev)
– coldest temp (avg and std dev)
• Calculated pavement temps used in PG
selection

83
Reliability
• Percent Probability of Not Exceeding
Design Temp > using Normal Distribution

frequency of Reliability is area under curve


observed temps to the left of Tdes
(Total area under
curve = 100 %)

Tavg Tdes

Observed Air Temperatures


Topeka, KS
50 % reliability average summer

very hot summer

98 % reliability

> this data - standard


36 40 deviation of 2°C
7-Day Maximum Air Temperatures

84
Observed Air
Temperatures
Topeka, KS 36
very cold winter 40

average winter

-31 -23
> standard
deviation of 4°C

-40 -30 -20 -10 0 10 20 30 40 50 60

Convert to Pavement
Temperature
• Calculated by Superpave
software
• High Temperature
– 20 mm below surface of
mixture
• Low Temperature
– at surface of mixture

Pavt Temp = f ( Air Temp, Depth, Latitude )

85
Calculated Pavement
Temperatures
Topeka, KS
56
pvt > air
60

-31 -23

pvt = air

-40 -30 -20 -10 0 10 20 30 40 50 60 70

PG Binder Grades
Topeka, KS
PG 64-34 (98% minimum reliability)

PG 58-28 (50 % minimum reliability)

PG grades- six degree


increments

-40 -30 -20 -10 0 10 20 30 40 50 60 70

86
Effect of Rounding to Standard
Grades

PG 58-28 (50 % minimum reliability)

PG 58 provides 85% reliability

PG -28 provides 90% reliability

-40 -30 -20 -10 0 10 20 30 40 50 60 70

Effect of Rounding to
Standard Grades
-16 -22 -28 needed grade
for 50% reliability

selected grade
for 50% reliability Rounding depends
on actual temps!

-28 -23
Minimum Pavement Temperatures

87
Effect of Loading Rate
on Binder Selection
90 kph
• Dilemma
– specified DSR loading rate is 10 rad/sec
– what about longer loading times ?
• Use binder with more stiffness at higher
temps
– slow- - increase one high temp grade
– stationary - - increase two high temp grades
– no effect on low temp grade

Effect of Loading Rate


on Binder Selection
90 kph
• Example
– for toll road PG 64
- 22
– for toll booth PG 70
- 22 Slow
– for weigh stations PG 76
- 22

Stopping

88
Effect of Traffic
Amount
on Binder Selection
80 kN ESALs

• 10 - 30 x 106 ESAL
– Consider increasing - - one high temp
grade
• 30 x 106 + ESAL
– Recommend increasing - - one high
temp grade
> Equivalent Single Axle Loads

ESAL Comparison
80 kN 100 kN 44 kN
18,000 lb. 22,000 lb. 10,000 lb.

1 2.2 .09
ESAL ESAL ESAL

89
Little Truck

67 kN 27 kN
15,000 lb + 6,000 lb = 0.49 ESALs
0.48 ESAL 0.01 ESAL

BIG TRUCK

151 kN 151 kN 54 kN
34,000 lb + 34,000 lb + 12,000 lb = 2.39 ESALs
1.10 1.10 0.19

Summary of How to Use


PG Specification
• Determine
– 7-day max pavement temperatures
– 1-day minimum pavement
temperature
• Use specification tables to select
test temperatures
• Determine asphalt cement
properties and compare to
specification limits

90
D
Superpave Mix Design Methods
Superpave vs. Marshall Criteria
Asphalt Mix Volumetric Properties
Gyratory Compactor and Refusal Density
Superpave Mix Design

NCAT 181

Asphalt Concrete Mix


Design
History

91
Hot Mix Asphalt Concrete
(HMA)
Mix Designs
• Objective:
– Develop an economical blend of
aggregates and asphalt that meet
design requirements
• Historical mix design methods
– Marshall
– Hveem
• New
– Superpave gyratory

Requirements in Common
• Sufficient asphalt to ensure a durable
pavement
• Sufficient stability under traffic loads
• Sufficient air voids
– Upper limit to prevent excessive
environmental damage
– Lower limit to allow room for initial
densification due to traffic
• Sufficient workability

92
MARSHALL
MIX
DESIGN

Marshall Mix Design


• Developed by Bruce Marshall for the
Mississippi Highway Department in
the late 30’s
• WES began to study it in 1943 for
WWII
– Evaluated compaction effort
• No. of blows, foot design, etc.
• Decided on 10 lb.. Hammer, 50 blows/side
• 4% voids after traffic
• Initial criteria were established and
upgraded for increased tire
pressures and loads

93
Automatic Marshall Hammer

Marshall Mix Design


• Select and test aggregate
• Select and test asphalt cement
– Establish mixing and compaction
temperatures
• Develop trial blends
– Heat and mix asphalt cement and
aggregates
– Compact specimen (100 mm
diameter)

94
Mixing/Compaction
Temps
Viscosity, Pa s
10
5

1
.5
.3 Compaction Range
.2 Mixing Range

.1
100 110 120 130 140 150 160 170 180 190 200
Temperature, C

Marshall Design Criteria


Light Traffic Medium Traffic Heavy Traffic
ESAL < 104 10 4 < ESAL< 10 ESAL > 106

Compaction 35 50 75

Stability N (lb.) 3336 (750) 5338 (1200) 8006 (1800)

Flow, 0.25 mm (0.1 in) 8 to 18 8 to 16 8 to 14

Air Voids, % 3 to 5 3 to 5 3 to 5

Voids in Mineral Agg.


(VMA) Varies with aggregate size

95
Minimum VMA
Requirements

Marshall Mix Design Tests


• Heights
– Used to correct stability measurements
• Bulk specific gravity of compacted sample
• Maximum specific gravity of loose mix
• Stability and flow
– 60oC water bath (30 to 40 minutes)
– 50 mm/min loading rate
– Max. load = uncorrected stability
– Corresponding vertical deformation = flow

96
Marshall Stability and Flow

Marshall Design Use of Data


Asphalt Institute Procedure
Air Voids,
% Stability Unit Wt.

4%

Asphalt Content, % Asphalt Content, % Asphalt Content, %

Target optimum asphalt content = average

97
Marshall Design Use of Data
Asphalt Institute Procedure
Flow VMA, %

Upper limit OK
OK
Minimum
Lower Limit

Asphalt Content, % Asphalt Content, %

Use target optimum asphalt content


to check if these criteria are met

Marshall Design Use of Data


NAPA Procedure
Air Voids,
%

4%

Asphalt Content, %

Target optimum asphalt content =


the asphalt content at 4% air voids

98
Marshall Design Use of Data
NAPA Procedure
Stability

OK

Asphalt Content, %

The target stability is checked

Marshall Design Use of Data


NAPA Procedure
Flow VMA, %

Upper limit OK
OK
Minimum
Lower Limit

Asphalt Content, % Asphalt Content, %

Use target optimum asphalt content


to check if these criteria are met

99
Marshall Design Method
• Advantages
– Attention on voids, strength, durability
– Inexpensive equipment
– Easy to use in process
control/acceptance

• Disadvantages
– Impact method of compaction
– Does not consider shear strength
– Load perpendicular to compaction axis

HVEEM MIX
DESIGN

100
Hveem Mix Design
Method
• Francis Hveem developed for
California DOT in mid 1920’s
• Limited use
– Primarily in West coast states
• Addresses similar design
considerations as Marshall
• Considers asphalt absorption by
aggregate

Hveem Mix Design


Method

• Selection and testing of


aggregates
• Selection and testing of binders
• Centrifuge kerosene equivalent
(CKE)
– Surface capacity of aggregate
– Estimate optimum asphalt content

101
Hveem Mix Design Method
• Use kneading compactor to prepare
specimens
• Determine stability with Hveem
stabilometer
– Evaluates horizontal deformation under axial
load
– Specimen loaded along axis of compaction
• Visual observation, volumetrics, and
stability used to select optimum asphalt
content

Hveem Kneading
Compactor

102
Hveem Stabilometer

Hveem Mix Design Method

Stability
Air
Minimum Voids,
%

Asphalt Content, % Asphalt Content, %

VMA
Minimum

Heavy traffic = 37 stability min. Asphalt Content, %


Medium = 35 min.
Light = 30 min.

103
Hveem Mix Design Method
Step 4
Max. AC with 4% Voids

Step 3
Min. Stability

Step 2
Flushing

Step 1
Design Series

Hveem Mix Design


• Advantages
– Attention to voids, strength, durability
– Kneading compaction similar to field
– Strength parameter direct indication of
internal friction component of shear
strength

• Disadvantages
– Equipment expensive and not easily
portable
– Not wide range in stability measurements

104
Asphalt Concrete Mix
Design
Superpave

Superpave Volumetric Mix


Design
• Goals
– Compaction method which simulates field
– Accommodates large size aggregates
– Measure of compactibility
– Able to use in field labs
– Address durability issues
• Film thickness
• Environmental

105
Specimen
Preparation
• Mechanical mixer
– 0.170 Pa-s binder viscosity
• Short term oven aging
– 4 hours at 135°C
– 2 hours at 135°C (optional)

Mixing/Compaction
Temps
Viscosity, Pa s
10
5

1
.5
.3 Compaction Range
.2 Mixing Range

.1
100 110 120 130 140 150 160 170 180 190 200
Temperature, C

106
Specimen
Preparation
• Specimen Height
– Mix Design - 115 mm (4700 g)
– Moisture Sens. - 95 mm (3500 g)

• Loose Specimen for Max. Theor.


(Rice) 150 mm
– varies with nominal max size
• 19 mm (2000 g)
• 12.5 mm (1500 g)

Mixing
Place pre-heated aggregate in
bowl and add hot asphalt

107
Mixing
Place bowl on mixer and mix until
aggregate is well-coated

Short Term Aging


Empty mix into pan and place in oven to
simulate short term aging

2 hours for low absorption aggregates


4 hours for high absorption aggregates

108
Short Term Aging
Important
• Allows time for aggregate to absorb
asphalt
• Helps minimize variability in volumetric
calculations
– Most terms dependent upon volumes which
change with changes in the amount
(volume) of absorbed asphalt

Compaction
Place funnel on top of mold and place mix in mold.
Take care not to allow the mix to segregate.

109
Compaction
Place another paper on top of mix
and place mold in compactor.

Compaction
Example of typical full-size compactors.

110
Compaction
Key Components of Gyratory Compactor

height control and data


measurement acquisition panel

reaction
frame loading
ram

tilt bar mold

rotating
base

Compaction
• Gyratory compactor
– Axial and shearing action
– 150 mm diameter molds
• Aggregate size up to 37.5 mm
• Height measurement during compaction
– Allows densification during compaction to be
evaluated

Ram pressure
600 kPa

1.25o

111
Compaction
After aging, take mix and preheated mold
from oven. Place paper in bottom of mold.

Compaction
Once compaction is finished, extrude
sample from mold.

112
Compaction
Remove the paper and label samples.

SGC Results
% Gmm

10 100 1000
Log Gyrations

113
Three Points on SGC Curve
% Gmm
Nmax
Ndes

Nini

10 100 1000
Log Gyrations

Design Compaction

% Gmm Nmax
• Ndes based on Ndes
– average design high
air temp Nini
– traffic level
• Log Nmax = 1.10 Log
Ndes 10 100 1000
• Log Nini = 0.45 Log Log Gyrations
Ndes

114
% Gmm Data Presentation
100
98
Nmax = 174
96
Ndes = 109
94
Nini = 8
92
90 Specimen 1
Specimen 2
88 Average
86
84
1 10 100 1000

Number of Gyrations

Superpave Mix Design


Analysis

115
Superpave Testing

• Specimen heights
• Mixture volumetrics
– Air voids
– Voids in mineral aggregate (VMA)
– Voids filled with asphalt (VFA)
– Mixture density characteristics
• Dust proportion
• Moisture sensitivity

Superpave Mix Design

• Gmb (estimated) = Wm
gw Vmx
Where:
Wm = mass of specimen, g
Vmx = volume of compaction mold (cm3)
gw = density of water, g/cm3

Assumption: specimen is smooth


- sided cylinder

116
Superpave Mix Design
• However, surface irregularities cause the
volume of the specimen to be slightly less
than volume of cylinder
• Actual bulk specific gravity measurement
of compacted sample used to determine
correction factor, C:

Gmb (measured)
C=
Gmb (estimated)

% Gmm = Gmb (estimated) C / Gmm (measured)

Superpave Mix Design

• Determine mix properties at NDesign and


compare to criteria

– Air voids 4% (or 96% Gmm)


– VMA See table
– VFA See table
– %Gmm at Nini < 89%
– %Gmmat Nmax < 98%
– Dust proportion 0.6 to 1.2

117
SGC Results
% Gmm

Increasing asphalt
96% cement content
(4% Voids)

Nini Ndes Nmax


10 100 1000
Log Gyrations

Each line = avg. of two samples

Superpave Mix Design

• VMA requirements:
– Nominal max agg size Min. VMA
» 9.5 mm 15
» 12.5 mm 14
» 19 mm 13
» 35 mm 12
» 37.5 mm 11

118
Superpave Mix Design
• VFA requirements:
– Traffic (millions of ESALs) Range of VFA

< 0.3 70 to 80
1 to 3 65 to 78
> 3.0 65 to 75

Superpave Mix Design

% weight of- 0.075 material


0.6 < < 1.2
% weight of effective asphalt

Effective asphalt content is asphalt on surface of aggregate


(asphalt not absorbed by aggregate)

119
Superpave Mix Design
• Moisture Sensitivity
– Prepare set of 6 specimens
• 6 to 8% voids
– Represents anticipated in-service voids
– Determine tensile strength of 3 of specimens
– Condition remaining 3 in water bath (60oC, 24 hr.)
• Option for freeze cycle
– Bring to test temperature (25oC) and determine
wet (conditioned) tensile strength

Moisture Sensitivity
AASHTO T 283
• Measured on proposed aggregate blend
and asphalt content
• Reduced compactive effort to increase
voids 3 Dry Specimens
3 Conditioned Specimens

Vacuum saturate specimens


Soak at 60oC for 24 hours
Soak at 25oC for 2 hours

120
Moisture Sensitivity
AASHTO T 283

Determine the tensile strengths


of both sets of 3 specimens

Calculate the Tensile


Strength Ratio (TSR)

Avg. wet tensile strength


TSR =
Avg. dry tensile strength

Minimum of 80% needed

Moisture Sensitivity
AASHTO T 283

Indirect tensile
strength apparatus
for 100 mm
specimens

121
Example of Superpave Mix
Design

Trial Gradations
19.0 mm Nominal Mixture

100.0
90.0
80.0
70.0
% PASSING

Trial Blend 3 Trial Blend 1


60.0
50.0
40.0
Trial Blend 2
30.0
20.0
10.0
0.0
0.075 2.36 19.0
Sieve Size (mm) raised to 0.45 power

122
Aggregate Consensus Properties
• Blended Aggregate properties are
determined
Property Criteria Blend 1 Blend 2
Blend 3
Coarse Ang. 95%/90% min. 96%/92% 95%/92%
97%/93%
Fine Ang. 45% min. 46% 46%
48%
FLat/Elong. 10% max. 0% 0% 0%
Sand Equiv. 45 min. 59 58 54
Combined Gsb n/a 2.699
2.697 2.701
Combined Gsa n/a 2.768
2.769 2.767

Compaction Characteristics

%Gmm

Blend %AC Nini Ndes Nmax


1 4.3% 86.9% 96.0% 97.4%
2 4.5% 85.9% 96.0% 97.7%
3 4.7% 87.1% 96.0% 97.3%

123
Volumetric
Properties

Blend %AC %Air %VMA %VFA DP


1 4.3% 4.0% 12.7% 68.5% 0.86
2 4.5% 4.0% 13.0% 69.2% 0.78
3 4.0% 4.0% 13.5% 70.1% 0.88

Selection of Design Asphalt


Binder Content
Va VMA

% binder Blend 3 % binder

VFA
DP

% binder
% binder

%Gmm at Nini %Gmm at Nmax

% binder % binder

124

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