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2020

Right Solutions • Right Partner


alsglobal.com

SCHEDULE OF SERVICES & FEES

Geochemistry
USD

ALS Geochemistry App —
track samples and
receive alerts.
Table of Contents
On-Site Services and Mine Site Services. . . . . . . . . . . . . . . . . . . . . . . . 1
Unrivalled detection limits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
ALS Geochemistry App. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Cutting Edge Hyperspectral Imaging & Processing. . . . . . . . . . . . . . . . 4

SAMPLE PREPARATION
Core Services . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
ALS CoreViewer™. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Sample Submission. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Sample Preparation Packages. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Individual Sample Preparation Methods. . . . . . . . . . . . . . . . . . . . . . . 11

PRECIOUS METALS ANALYSIS


Gold, Silver and PGEs in Rocks and Drill Core. . . . . . . . . . . . . . . . . . . 13
Concentrates, Bullions and Metallurgical Testing. . . . . . . . . . . . . . . . . 14
Gold in Soils and Stream Sediments. . . . . . . . . . . . . . . . . . . . . . . . . . 15

GENERATIVE EXPLORATION
Super Trace Analysis for Soils and Sediments. . . . . . . . . . . . . . . . . . . 18
Super Trace Analysis for Rocks and Drill Core. . . . . . . . . . . . . . . . . . . 19
Hydrogeochemistry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Biogeochemistry. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

TARGETED EXPLORATION
Ultra Trace Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Trace and Intermediate Level Methods. . . . . . . . . . . . . . . . . . . . . . . . 26
Isotopic Analysis and Geochronology. . . . . . . . . . . . . . . . . . . . . . . . . 28

WHOLE ROCK ANALYSIS AND LITHOGEOCHEMISTRY . . . . . . . . . . . . . 30

SPECIFIC ORES AND COMMODITIES


Copper and Iron Ore. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Lithium . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Uranium, Rare Earths and Rare Metals. . . . . . . . . . . . . . . . . . . . . . . . 36
Bauxites, Laterites, and Other Commodities. . . . . . . . . . . . . . . . . . . . 37
High Grade Methods and Refractory Ores. . . . . . . . . . . . . . . . . . . . . . 38

CARBON, SULPHUR, ARD AND CONCENTRATES


Carbon & Sulphur Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
Acid Rock Drainage Testing. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Concentrates and Metallurgical Samples. . . . . . . . . . . . . . . . . . . . . . . 43
ALS Mineralogy. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

Quality statement and accreditation . . . . . . . . . . . . . . . . . . . . . . . . 45


Terms & conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Global geochemistry locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

ALS reserves the right to alter listed prices at any time.


ALS operates
remote mine
site labs in the
most challenging
locations
Our experience includes all possible environments
ranging from the high Andes to the frozen Arctic;
from desert terrain to the equatorial tropics.

Lease or sale of mine site labs


› Containerised preparation facilities
› Customised analytical laboratories and methods

Core services in-lab or on-site


› Core sawing & sampling
› Core photography
› Hyperspectral mapping & interpretation
› CoreViewer™
Unrivalled
detection limits
Superior discrimination of anomaly versus background.
ALS's innovations in ICP-MS methodology continue to reduce detection limits for key
elements in our industry leading super trace methods.

ALS methods
Geochem Four-Acid and Aqua Regia Methods
ME-MS61L ™
Clear definition of anomalous trends via detection limits below upper crustal
ME-MS41L ™ abundance for Re, Te and Se and below regional background for key pathfinders
ME-MS41W ™ such as Tl, Sb, Te, Cd and As.

Improved detection limits Comparison of Se duplicate pairs with Previous Se DL = 0.1 ppm
previous and improved detection limits New Se DL = 0.003 ppm
PREVIOUS NEW IMPROVEMENT
ANALYTE 10
LDL PPM LDL PPM FACTOR
As 0.05 0.02 2.5
Bi 0.005 0.002 2.5 1
Se ppm duplicate

Re 0.002 0.0004 5
4-Acid
Se 0.2 0.006 33.33 0.1
Te 0.04 0.005 8
Tl 0.004 0.001 4
0.01
Bi 0.001 0.0005 2
Re 0.001 0.0002 5
Aqua 0.001
Se 0.1 0.003 33.33
Regia 0.0010 .010 .1 11 0
Te 0.01 0.003 3.33
Tl 0.002 0.001 2 Se ppm original

ALS method
ANALYTE LOWER LIMIT µg/L UPPER LIMIT µg/L
Au-PATH14L™ Au 0.0002 10

NEW Hydrogeochemistry method Ag 0.005 100


As 0.2 1000
Ultra low detection limits for Au and pathfinders Co 0.005 1000
in gold systems. Pd 0.005 100
Pt 0.01 100
Hydrogeochemistry is an effective tool for exploration where large
Sb 0.02 1000
regions of ground need to be evaluated using sparsely spaced samples.
Sample tracking at your fingertips
with the ALS Geochemistry App

Process Control Alert™ Overlimit Alert™


User-defined alert limits can be set up to Select analytes and receive SMS and/or
monitor grade control, mill processing and email alerts when a sample has triggered
environmental samples. If a routine analytical an overlimit assay to make rapid decisions.
control result falls outside of bounds, obtain View results graphically with overlimits
an alert and quickly address the situation. highlighted.

Secure access

Custom alerts

Geochemical results, workorder A dashboard of workorders Detailed tracking of individual


information and mine control data. with progress breakdown. workorders in the lab.

In-app access to the Geochemistry Lab locator with detailed Find the laboratory closest
Schedule of Services and Fees. contact information. to your location.

Ask your preferred ALS contact for Download


information on setting up your alerts the app
today
Cutting Edge Hyperspectral
Imaging & Processing
TerraCore is the only company in the industry with commercially available
LWIR spectral imaging as well as the standard VNIR & SWIR spectral range
to deliver the full spectrum required for rock characterization. Results are
delivered via CoreViewer™ and IntelliCore®.

CODE DESCRIPTION PRICE


Core cleaning, core box preparation, and labour may be
Various By Quotation
provided by ALS or TerraCore.

COREIM-10 VNIR-SWIR or SWIR hyperspectral imaging of core boxes $6.15 / foot


COREIM-11 and chip trays using TerraCore Core Imaging Systems. $20.00 / metre
COREIM-12 Pricing applies to in-lab services. $5.55 / chip sample
COREIM-10L
COREIM-11L LWIR and VNIR-SWIR hyperspectral imaging of core boxes $8.20 / foot
COREIM-12L and chip trays using TerraCore Core Imaging Systems. $27.00 / metre
Pricing applies to in-lab services. $7.80 / chip sample

*Minimum charge of $5500.00

Skeletonised core boxes have custom pricing. Please enquire.


*Chip trays must be black plastic. ALS can transfer samples to black trays for a fee.
Services include high resolution true colour RGB core photographs, mineral assemblage
maps and spectral parameters as image displays, numerical mineralogical parameters
and products averaged over 10cm intervals across the length of the core.

aiSIRIS™ by AusSpec brings a generational leap forward in AI interpretation


of TerraSpec® spectral data. Systematic collection of spectral data on dry,
coarse crushed rock and drill core can be easily integrated with existing
workflows with routine interpretation enabling delivery of large volumes
at fast turnaround times.

CODE DESCRIPTION DELIVERABLES PRICE PER SAMPLE


An economical package combining TerraSpec® 4 HR scanning and
aiSIRISTM expert spectral interpretation. Raw spectral files in ASD or ASCII format, and
300 samples
HYP-PKG The value of hyperspectral mineralogy in exploration and geometallurgy spreadsheet with mineral assemblages and $6.15
minimum*
increases substantially with larger sample volumes. Discounts are spectral parameters related to the project geology.
available for large submittals covering entire drilling campaigns.

Rapid and accurate interpretation of hyperspectral scans by the aiSIRIS™ Spreadsheet with mineral assemblages and spectral 300 samples
INTERP-11 $3.80
expert software. parameters related to the project geology. minimum*

Spectral scan using the TerraSpec® 4 HR spectrometer. Crushed reject or Raw spectral files in
TRSPEC-20 $4.15
RC chips are recommended as the optimal sample type. ASD or ASCII format.

*Discounts may apply for higher volumes of samples.

The original ASD files as well as the Access to the aiSIRIS™ App is More information about aiSIRIS™,
aiSIRIS™ output are reported on every included for quick spectral plots and TerraSpec® and TerraCore can be obtained
sample for one-to-one comparison. assessment against spatial data. from any ALS client services group.
Sample
Preparation
Sample preparation is designed to produce a
representative, homogenous sub-sample from
the original raw sample. Many variations on the
methods and packages in the following pages
are available, and sample preparation schemes
can be customised to suit any particular project
requirement. We have a wide range of expertise
available within ALS to help you with any questions
you might have.

Samples may be submitted to any of the locations


listed on the back pages of this schedule. We
can also offer advice on shipping to any of our
laboratories by ground, air cargo and air express.

Sample submission forms are available online


from www.alsglobal.com and on request.
Core Services CODE DESCRIPTION OF SERVICE PRICE
Our Core Services encompass LOG-COREBX Log in core box for processing. $2.25 /box
core handling and warehouse
management, core sawing and SAW-01 Automated high speed core sawing.
$10.10 /m
sampling, secure and comfortable SAW-01FT Cut sheet/details provided by client.
$3.15 /ft
logging facilities, and core
photography. They may be SAWM-01 $13.00 /m
Manual sawing for friable core.
bundled in any combination at SAWM-01FT Cut sheet/details provided by client.
$3.95 /ft
ALS facilities or on-site at your
project as needed. These prices Sampling core based on client instructions.
SAM-COR01 $4.15 /sample
reflect in-lab services; for custom Includes bagging sample for further preparation.
on-site quotes, please contact
minesitelab@alsglobal.com. Surcharge for friable core. Sampling core based on client instructions. Includes
SAM-COR01F $5.70 /sample
bagging sample for further preparation.
Our highly-trained core sawing
technicians use state of the art Daily rental of secure core logging facilities
LOG-COR10 $60.00 /day
computerised saws for precision with full spectrum lights and other amenities.
cutting of most rock types. Friable
PHO-WET High resolution core photography.
core may be sawn manually to
Delivery via secure file transfer or ALS CoreViewer™ (see below.) Core may be $4.45 /box
preserve material in the interval. PHO-DRY
photographed wet or dry based on client preference and requirements.

STO-COR10 Long-term storage of core boxes in ALS warehouses. $1.25 /box/month

6 | Sample Preparation Schedule of services & fees | 2020


CoreViewer ™
Photo archive, core logging support tool, and data integration
platform. Integration with major 3D modelling software.

Continuous
depth-registered
downhole
core image
strips

Fast & secure


connection

Search Graph down-


for specific hole geochemical,
intervals mineralogical,
or geophysical
data

CoreViewerTM is a fast and secure core photo archive, core Your core photos can be accessed in perpetuity using your
logging support tool, and data integration platform accessible secure WebtrieveTM login. For those companies using acQuire
over the web via computers and touch-screen tablets. GIM Suite, CoreViewerTM is available right inside the acQuire
Neo application, correlated with drill holes and all associated
Using core photos taken by ALS or provided by you over a
information in the database.
secure connection, we create continuous depth-registered
downhole core image strips. The box photos and core strips CoreViewerTM also integrates with major 3D modelling
are available to you through CoreViewerTM, where you can software, including Seequent Leapfrog Geo, Maptek Vulcan
search for specific intervals and graph any kind of downhole and Micromine for deep investigation and verification of
geochemical, mineralogical, or geophysical data for exploration, resource and geometallurgical models.
comparison against the images.

CODE PRC-PHOCLW & PRC-PHOCLD | PRICE $5.55/box


Sample CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
Submission Workorder/administration fee Single charge for each batch of
BAT-01 $30.35 / processed
Confidence and security in the applied per processing batch. samples processed.
batch
chain of custody for your samples
as they pass through our system Samples received with barcode
are paramount. Your samples are labels attached to sample bag.
LOG-21 Multi-part barcoded sample tags $0.70
given a barcode and logged into may be purchased from your Weigh raw sample and log into
our proprietary global laboratory local lab. global tracking system.
information management system
on receipt. We encourage clients LOG-22
Samples received without
$1.40
to barcode samples prior to barcode labels attached.

sending them to our laboratories.


Pulps received with barcode Weigh pulp and log into global
Our system will accommodate all LOG-23 tracking system. At least one out of $0.70
labels attached to sample bag.
major barcode formats. every 50 samples is selected
at random for routine QC tests (LOG-
Pulps received without barcode QC). The default specification is 85%
LOG-24 $1.40
Sample pick-up labels attached. passing 75 microns.

services Levy for disposal of all types of Required for relevant samples in
LEV-01 $0.75
May be arranged from any of laboratory waste. certain jurisdictions.

our locations. Please contact Required for relevant samples


Quarantine charge.
your nearest ALS office and imported into Australia.
QAR-01 AQIS-approved heat treatment $0.80
mention code PKP-21. and storage.
Additional charges apply for
samples over 500g.

8 | Sample Preparation Schedule of services & fees | 2020


Sample Storage CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
Materials submitted for analysis STO-REJ Monthly archive of coarse rejects. Longer term archiving of coarse
$0.80 > 45 days
are retained free of charge at our STO-BLK Monthly archive of pulps >250g. rejects and large pulps.
laboratories for a limited time,
Longer term storage of master
starting from the day we issue STO-PUL Monthly archive of pulps <250g. $0.35 > 90 days
pulps.
the final Certificate of Analysis.
Reasonable monthly charges will Monthly archive of screening reject Longer term storage of
STO-SCR $0.35 > 45 days
fractions. screening reject fractions.
apply to samples archived for
longer periods in our facilities. ALS Handling and retrieval of archived
RET-21 Stored samples. $68.35 / hour
samples.
sample storage facilities provide a
secure and organised environment DIS-21 Disposal of pulps and coarse fractions. Pulps and coarse fractions. $2.25
protected from the elements, and
all archive locations are included RTN-21 Return of samples to client. Returned samples. By Quotation
in the laboratory tracking system.

Specific Gravity CODE DESCRIPTION RANGE PRICE PER SAMPLE


& Bulk Density OA-GRA08 Specific Gravity on solid objects. Reported as a ratio. $13.65
Specific Gravity on pulps using
Specific gravity and bulk density OA-GRA08b Reported as a ratio. $13.65
pycnometer.
of ores are important parameters OA-GRA09 Bulk Density by water displacement. 0.01 – 20g/cm3 $13.65
that are often under-characterised Bulk Density after wax coating
OA-GRA09A 0.01 – 20g/cm3 $21.85
in the determination of grade and (wax removal not included).
tonnage of deposits.

Drill Core, Rocks CODE DESCRIPTION APPLICATION PRICE PER SAMPLE


and Chips Used as a preliminary step before fine
$3.10
Preparation
Coarse crushing of rock chip and drill crushing of larger sample sizes. No QC is
CRU-21 + $0.60 /kg
samples. performed for this method. If QC if required

Packages request CRU-21q for >70% passing 6mm.

Crush to 70% less than 2mm, riffle split


All packages include sample login $8.35
PREP-31* off 250g, pulverise split to better than
to the laboratory tracking system + $0.90 /kg
85% passing 75 microns.
and weighing. Excessively wet
Crusher/rotary splitter combo - Crush
samples may require additional to 70% less than 2mm, rotary split off
$8.35
drying for a surcharge. It is very PREP-31Y* + $0.90 /kg
250g, pulverise split to better than 85%
helpful to advise us of mineralised passing 75 microns.
Drill core, rock and chip samples.
samples that may require special Crush to 70% less than 2mm, riffle split
$9.60
equipment cleaning cycles. PREP-31B* off 1kg, pulverise split to better than
+ $0.90 /kg
85% passing 75 microns.

Crusher/rotary splitter combo - Crush


$9.60
PREP- to 70% less than 2mm, rotary split off
31BY* 1kg, pulverise split to better than 85% + $0.90 /kg
passing 75 microns.

Crush to 90% less than 2mm, riffle split


Drill core and rocks containing high-grade $15.10
PREP-31D* off 1kg, pulverise split to better than
or coarse gold and/or silver. + $2.10 /kg
85% passing 75 microns.

Crush to 70% less than 6mm, pulverise


$10.95
PREP-22* entire sample to better than 85% Drill core, rock and chip samples up to 3kg.
+ $0.30 /kg
passing 75 microns.

Crush to >70% less than 2mm, riffle


$12.25
PREP-32* split, pulverise 1.5kg to 85% passing Drill core, rock and chip samples.
+ $1.25 /kg
75 microns.
* Packages with common split size and particle fineness are listed. Please contact your local client services for alternatives.

Sample Preparation | 9
Soil & Sediment CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
Preparation PREP-41
Dry at <60°C/140°F, sieve sample to -180
Soil or sediment samples.
$1.80

Package micron (80 mesh). Retain both fractions. + $2.95 /kg

Drying temperature is kept low to


avoid the loss of mercury.

Miscellaneous CODE DESCRIPTION APPLICATION PRICE PER SAMPLE

Procedures CMP-21 Compositing of two or more samples. $2.35


May be done by volume/core length As requested.
These procedures may be used
CMP-22 (CMP-21) or by weight (CMP-22). $4.45
when specialised preparation or
sample compositing is required. Clean crushers with “barren” As required. The standard procedure
WSH-21 $2.65
material after every sample. uses compressed air cleaning between
An hourly labour charge may
Clean pulverisers with “barren” material samples and barren material between
apply to time-intensive projects. WSH-22
each batch.
$3.45
after every sample.
As required for samples received in
Transfer sample to drying tray or new
TRA-21 containers unsuitable for laboratory $1.40
sample bag.
storage, or requiring tray drying.

BAG-01 Bagging large pulps for storage. For large pulps/bulk masters. $1.40

Homogenise stored or composited


HOM-01 As required. $6.10
samples by light pulverizing.
Screening of samples to any number of
standard size fractions, as specified by Fraction sizing or custom screening as $6.85
SCR-51 /screen size
the client. Weight of undersize fraction requested.
reported for each screen size.

Portable XRF on CODE ANALYTES & LOWER LIMITS (PPM) PRICE PER SAMPLE
Prepared Pulps As 50 Fe 0.5% S 0.1%
Ca 0.5% Mn 100 Zn 50
ALS offers portable XRF analysis pXRF-30 $5.20
Cr 100 Ni 50
on pulps immediately after sample
Cu 50 Pb 50
preparation at the prep lab closest
Portable XRF scan of a non-mineralised pulverised sample.
to your project. Ranges: $3.90
Si 0.5%-47% Add-on to
pXRF-34
Ti 0.1%-60% multi-element
Zr 5ppm-5% analysis only
15g sample

Portable XRF
for Indicative Analysis
Portable XRF may be used to screen large volumes of
samples for intermediate to ore grade elements when
the standard lab test is relatively costly and time-
consuming. The pXRF method must be calibrated for
a specific sample suite on an individual project basis.
Submitting samples not represented in the calibration
suite creates a high risk of inaccurate results, including
false positives.
ALS offers custom calibration for pXRF on project-specific
sample suites, with our rigorous quality standards and
XRF expertise ensuring accurate, reliable results. The
pXRF instrument can be located in the prep lab nearest
your project, or on-site if the project is remote. Contact
your local client sevices team for more information.

10 | Sample Preparation Schedule of services & fees | 2020


Individual Drying
Sample CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
Preparation DRY-21
Drying of excessively wet samples in Default drying procedure for most rock $2.80

Procedures drying ovens. chip and drill samples. + $0.60 /kg


Drying of excessively wet samples in
Most soil and sediment samples that $2.95
The following procedures can DRY-22 drying ovens that are controlled to a
are analysed for volatile elements. + $0.65 /kg
be used either separately or maximum temperature of 60ºC.
combined in a package in $2.95
DRY-23 Air-drying of samples. Selective Leach procedures and others.
order to meet specific needs + $0.65 /kg
regarding sample size and
composition. Most of these Crushing
procedures are charged at a
rate that is based on sample CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
weight. Used as a preliminary step before fine
crushing of larger sample sizes. No
Multiple screen sizes and Coarse crushing of rock chip and drill $3.10
CRU-21 QC is performed for this method. If QC
screening methods are samples. + $0.60 /kg
if required request CRU-21q for >70%
available. Please contact passing 6 mm
your local client services Standard preparation procedure for
Fine crushing of rock chip and drill $3.10
group for options. CRU-31 samples where a representative split
samples to 70% passing 2mm. + $0.55 /kg
will be pulverised.

Fine crushing of rock chip and drill Option for when a finer crush is $3.45
CRU-36
samples to 85% passing 2mm. desired. + $1.15 /kg
Fine crushing of rock chip and drill Option for when a finer crush is $4.10
CRU-32
samples to 90% passing 2mm. desired. + $1.35 /kg
Note: Methods with common fineness requirements listed. Additional options available.

Splitting

CODE DESCRIPTION APPLICATION PRICE PER SAMPLE

$2.05
SPL-21* Split sample using a riffle splitter. Standard splitting procedure.
+ $0.40 /kg

$3.10
SPL-22* Split sample using a rotary splitter.
+ $1.05 /kg
Rotary splitting procedure.
Split sample using a Boyd crusher/rotary $2.05
SPL-22Y
splitter combination. + $0.40 /kg
Split a received pulp sample for
SPL-34 Pulp splitting procedure. $0.80
various analysis.
Note: For sample splitting and return or archive without analysis add suffix X to the codes above. Additional costs are incurred.

Pulverizing
A variety of different
CODE DESCRIPTION APPLICATION PRICE PER SAMPLE
pulverising bowls made
of diverse media are Pulverise a split or total sample up to Default procedure for samples that are
PUL-31* $4.90
250g to 85% passing 75 microns. finely crushed and split to 250g or less.
available on request. All ALS
equipment is standardised PUL-32*
Pulverise a 1,000g split to 85% passing
$6.95
as low Cr-steel, however, 75 microns. Large sample size to mitigate
substitution of bowls may Pulverise a 1,000g split to 90% passing nugget effect.
PUL-32a* $8.45
be required when specific 75 microns.
element contamination is Pulverise entire sample to 85% passing
PUL-21* Appropriate for samples up to 3kg. $11.25
a concern. Bowls available 75 microns.
include tungsten carbide, Pulverise up to 3kg to 85% passing 75
agate and zirconium. microns. For samples >3kg additional
PUL-23* $8.25
costs are incurred to split the sample prior
to pulverising and retaining the remainder.
Appropriate for RC drill chip
Pulverise up to 3kg to 85% passing samples not requiring crushing.
75 microns. For samples >3kg an
PUL-24* additional cost is incurred to split $8.25
Other options are the sample prior to pulverising. The
available for all stages remainder is discarded.
of sample preparation. Pulverise up to 100g concentrate Cost includes careful cleaning of the
Please contact ALS PUL-51* $20.50
sample to 85% passing 75 microns. pulverizing bowl after grinding.
with your specific
200g of sample pulverised to 85% less
requirements. PUL-34* Applicable for high grade material. $20.50
than 75 microns.
* Surcharges may apply to samples requiring excessively long pulverisation times.

Sample Preparation | 11
Precious
Metals
Analysis
The unique chemical properties of gold, silver,
and the platinum group elements pose challenges
in geochemical analysis. They often occur
heterogeneously in geological materials, at scales
ranging from micron-sized inclusions in minerals
to large nuggets. As a result, large analytical
charge weights are required to accurately represent
content in the overall sample. Solvent digestions
can also lose gold to adsorption on the original
sample when certain forms of carbon and sulphide
minerals are present, in a process called preg
robbing.
ALS has decades of expertise in reliable and
reproducible precious metals analysis by fire assay,
cyanide leach and aqua regia digestion at parts per
billion to percent levels.

Please submit at least three times nominal


sample weight for efficient service.
Gold by Fire Assay CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
An optimal fire assay flux recipe Trace Level
and rigorous quality control Au-ICP21 Au by fire assay and ICP-AES. $18.50
program easily handle problem 0.001-10 30g sample
Au-ICP22 50g sample $21.85
materials including chromite, Au
Au-AA23 Au by fire assay and AAS. $17.80
base metal sulphides and oxides,
0.005-10 30g sample
selenides, and tellurides. Au-AA24 50g sample $21.15

Choice of crushing fineness, Ore Grade


splitting technique and pulp Au-AA25 Au by fire assay and AAS. $18.50
size can all affect the analytical 0.01-100 30g sample
Au-AA26 50g sample $21.85
outcome of fire assay gold
Au
methods. Discuss with your Au-GRA21 Au by fire assay and gravimetric finish. $23.10
0.05-1000 30g sample
local ALS laboratory for more Au-GRA22 $27.95
50g sample
information.

Metallic Screening CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
When samples contain coarse 1kg pulp screened to 100 microns.
gold, the metallic screening Other screen sizes available. Duplicate
Au-SCR21 Au $61.60
30g assay on screen undersize. Assay of
procedure is recommended for entire oversize fraction.
accurate results. 1kg pulp screened to 100 microns.
Other screen sizes available. Duplicate
Au-SCR24 Au $68.30
50g assay on screen undersize. Assay of
0.05-100,000 entire oversize fraction.
(0.01-1000 mg) 1-2kg pulp screened to 100 microns.
Duplicate 50g assay on screen
Au-SCR24B Au $92.95
undersize. Assay of entire oversize
fraction.
2-3kg pulp screened to 100 microns.
Duplicate 50g assay on screen
Au-SCR24C Au $117.35
undersize. Assay of entire oversize
fraction.

* Options available for various sample weights, screen sizes and undersize assays.

Silver CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE


Trace level and low-grade silver Trace Level
samples may be analysed by acid Ag by aqua regia digestion and AAS.
Ag-AA45 0.2-100 $6.85
digestion for maximum sensitivity 0.5g sample
Ag
and precision. Multi-element Ag by HF-HNO3-HClO4 digestion,
Ag-AA61 0.5-100 $9.55
HCl leach and AAS. 0.25g sample
packages including Ag are listed in
the Targeted Exploration section. Ore Grade
Ag-OG46 Ag by aqua regia digestion, ICP-AES
Because silver can suffer from 1-1,500 $12.25
(Ag-AA46) or AAS finish. 0.5g sample
nugget effect, occasional duplicate Ag by HF-HNO3-HClO4 digestion with
Ag-OG62
analysis may help detect sampling 1-1,500 HCl leach, ICP-AES or AAS finish. $15.00
(Ag-AA62) Ag
error at these low levels. At 0.4g sample
higher grades, fire assay with Ag-GRA21 Ag by fire assay and gravimetric finish. $24.50
larger nominal weights may be 5-10,000 30g sample
Ag-GRA22 50g sample $29.30
preferable.
Au and Ag by fire assay and
ME-GRA21 $30.10
Au 0.05-1,000 gravimetric finish.
Ag 5-10,000 30g sample
ME-GRA22 $34.80
50g sample

Precious Metals Analysis | 13


Platinum Group CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Elements Trace Level
Pt 0.0001-1 Super trace Pt, Pd and Au by fire assay and
Platinum, palladium, rhodium
PGM-MS23L Pd 0.0002-1 ICP-MS finish. $24.75
and gold may be determined by Au 0.001-1 30g nominal sample weight
standard lead oxide collection Pt 0.0005-1 Pt, Pd and Au by fire assay and ICP-MS finish.
PGM-MS23 $21.55
fire assay and ICP-MS or ICP-AES Pd 0.001-1 30g nominal sample weight
finish. For the full list of platinum PGM-MS24 Au 0.001-1 50g nominal sample weight $24.75

group elements, nickel sulphide Rh by fire assay, gold collection and ICP-MS.
Rh-MS25 Rh 0.001-1 $25.35
30g nominal sample weight
collection fire assay must be used
Pt, Pd 0.002-15
for a quantitative analysis.
Au, Rh 0.002-5 Au, Pt, Pd, Ir, Os, Rh, Ru by nickel sulphide
PGM-MS25NS Ir 0.001-5 collection fire assay and ICP-MS finish. $170.75
Os 0.002-1 30g nominal sample weight.
Ru 0.003-5
PGM-ICP23 Pt 0.005-10 Pt, Pd and Au by fire assay and ICP-AES finish. $20.50
Pd 0.001-10 30g nominal sample weight
PGM-ICP24 Au 0.001-10 50g nominal sample weight $23.60

Ore Grade
Pt 0.01-100
Pt, Pd and Au by fire assay and ICP-AES finish.
PGM-ICP27 Pd 0.01-100 $22.15
30g nominal sample weight
Au 0.01-100

Gold Cyanidation CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Au-AA13 Au 0.03-50 $10.95
In mining and exploration Au, Ag, Cu by cyanide leach with AAS finish.
Ag-AA13 Ag 0.03-350
30g sample + $5.45 /element
applications, cyanide leach tests Cu-AA13 Cu 0.1-2,000
are used to establish the potential Au by cyanide leach with AAS finish.
cyanide extraction efficiency for Au-AA14 Au 0.01-200 12hr Leach. $34.15
gold and silver. Up to 1kg sample
Au by accelerated cyanide leach using
High concentrations of some
LeachWELL Assay Tabs™ with AAS finish.
sulphides, particularly chalcopyrite, Au-AA15a $39.75 (500g)
4hr Leach.
Au-AA15b $42.75 (1kg)
can negatively impact gold Au 0.01-300 500g sample request Au-AA15a
Au-AA15c $44.25 (2kg)
extraction. For samples that are For 1kg request Au-AA15b
Au-AA15d $48.75 (3kg)
expected to contain high copper For 2kg request Au-AA15c
For 3kg request Au-AA15d
sulphide concentration please
contact ALS for suggestions. Au Preg Rob Leach with Gold Spike.
Au-AA31
Au 0.03-500 Au Preg Rob Leach without Gold Spike. $12.25 each
Au-AA31a
10g sample per method
Note: Cyanide disposal fees apply in some countries.

Process Samples CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Au in cyanide liquor by extraction with
Includes gold in cyanide liquors or Au-AA16 Au 0.001-2,500mg/L
AAS finish.
$24.55
captured on activated carbon.
Au on carbon by ashing, aqua regia
Au-AA44 Au 1-10,000 $43.70
Minimum sample weight digestion and AAS. Duplicate analysis.
required varies, contact your
local lab.

Precious Metals CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
in Concentrates Concentrates

and Bullion Au-CON01


Ag-CON01
Au
Ag
0.07-999,985
0.7-995,000
Au and Ag by fire assay and gravimetric finish. $94.70 each

High precision analysis and Pt-CON01


umpire assay of precious metals Pd-CON01 Pt, Pd, Rh 0.07-1,000,000 Pt, Pd and Rh by fire assay and AAS finish. $99.15 each
in concentrates and bullion are Rh-CON01

performed by the most senior fire Bullion


assay technicians and checked Au-GRA24 Au 0.01-1,000 fineness Routine bullion assays by fire assay with
$144.60 each
by certified assayers to ensure Ag-GRA24 Ag 0.01-1,000 fineness gravimetric finish.
accuracy. Au-UMP20 Au 0.07-1,000,000 Umpire assay for bullion samples by fire
$227.15 each
Ag-UMP20 Ag 0.7-1,000,000 assay with gravimetric finish.
Minimum sample weight Pt-UMP20
Umpire assay for bullion samples by fire
required varies, contact your Pd-UMP20 Pt, Pd, Rh 0.07-1,000,000 $213.00 each
assay with gravimetric finish.
local lab. Rh-UMP20

14 | Precious Metals Analysis Schedule of services & fees | 2020


Super Trace CODE ANALYTE RANGE DESCRIPTION PRICE PER SAMPLE
Gold in Soils & Au-CN43™ Au by cyanide extraction with ICP-MS finish. $22.90
Au 0.02ppb-1ppm 25g sample
Sediments Au-CN44™ 50g sample $25.55

ALS offers the lowest detection Au-ST43™ Au by aqua regia extraction with ICP-MS finish. $19.10
limits in the industry for gold Au 0.1ppb-0.1ppm 25g sample
Au-ST44™ 50g sample $21.25
in soils and sediments by both
cyanide and aqua regia digestion,
using our innovative super trace
analytical methodology.
Full multi-element geochemical CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
suites may be read from the Au 0.0001-1 Cu 0.01-10000 Nb 0.002-500 Ta 0.005-500
same digest solution as our Ag 0.001-100 Fe 0.001-50 % Ni 0.04-10000 Te 0.01-500
aqua regia and ICP-MS super Al 0.01-25 % Ga 0.004-10000 P 0.001-1 % Th 0.002-10000
trace gold method. This package As 0.01-10000 Ge 0.005-500 Pb 0.005-10000 Ti 0.001-10 %
mirrors our ME-MS41L™ method, B 10-10000 Hf 0.002-500 Pd 0.001-100 Tl 0.002-10000
with slight adjustments made to AuME-ST43™ Ba 0.5-10000 Hg 0.004-10000 Pt 0.001-100 U 0.005-2500 $39.00
accommodate the larger nominal 25g sample
Be 0.01-1000 In 0.005-500 Rb 0.005-10000 V 0.1-10000
sample weight necessary for Bi 0.001-10000 K 0.01-10 % Re 0.001-50 W 0.001-10000
AuME-ST44™
representative gold analysis. Ca 0.01-25 % La 0.002-10000 S 0.01-10 % Y 0.003-500 $41.30
50g sample
Cd 0.001-1000 Li 0.1-10000 Sb 0.005-10000 Zn 0.1-10000
Ce 0.003-500 Mg 0.01-25 % Sc 0.005-10000 Zr 0.01-500
Co 0.001-10000 Mn 0.1-50000 Se 0.1-1000
Cr 0.01-10000 Mo 0.01-10000 Sn 0.01-500
Cs 0.005-500 Na 0.001-10 % Sr 0.01-10000

Bulk Leach CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Extractable Gold Au-CN12*
BLEG – ICP-MS finish.
Au 0.0001-10 BLEG – extraction AA finish. $41.00
Au-AA12**
BLEG is used where cyanide Up to 1kg sample
leaching from a stream sediment BLEG – ICP-MS finish.
Au-CN11*
sample may detect gold Au 0.001-10 BLEG – extraction AA finish. $27.40
Au-AA11
anomalies that would otherwise Up to 1kg sample

go unnoticed. * Silver and copper may also be reported by these methods for an additional fee.
** Silver, Copper, Lead and Zinc may also be reported for an additional fee.
Prices for cyanide leaching of
samples over 1kg by quotation.

Precious Metals Analysis | 15


Low Level Gold in CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Soils & Sediments Trace Level

Our trace level methods by Au-TL43 Au by aqua regia extraction with ICP-MS finish. $16.70
aqua regia digestion and ICP-MS Au 0.001-1 25g sample
finish are excellent for regolith, Au-TL44 50g sample $18.60
where gold anomalies indicating
Intermediate Grade
mineralisation below surface
are well-characterised. Aqua Au-OG43 Au by aqua regia extraction with ICP-MS finish. $15.95
Au 0.01-100 25g sample
regia dissolves native gold as Au-OG44 $17.85
50g sample
well as gold bound in sulphide
minerals; however, depending on
the composition of the soil, gold CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
determined by this method may Au 0.001-1 Co 0.1-10000 La 0.2-10000 Re 0.001-50 Tl 0.02-10000
or may not match recovery from Ag 0.01-100 Cr 1-10000 Li 0.1-10000 S 0.01-10% U 0.05-10000
fire assay methods. Al 0.01-25% Cs 0.05-500 Mg 0.01-25% Sb 0.05-10000 V 1-10000
As with our super trace methods, As 0.1-10000 Cu 0.2-10000 Mn 5-50000 Sc 0.1-10000 W 0.05-10000
AuME-TL43™
multi-element packages can be 25g sample B 10-10000 Fe 0.01-50% Mo 0.05-10000 Se 0.2-1000 Y 0.05-500 $27.50
read from the same digestion Ba 10-10000 Ga 0.05-10000 Na 0.01-10% Sn 0.2-500 Zn 2-10000
AuME-TL44™ Be 0.05-1000 Ge 0.05-500 Nb 0.05-500 Sr 0.2-10000 Zr 0.5-500 $29.85
solution as trace level gold for a
50g sample
complete exploration tool. Bi 0.01-10000 Hf 0.02-500 Ni 0.2-10000 Ta 0.01-500
Ca 0.01-25% Hg 0.01-10000 P 10-10000 Te 0.01-500
Cd 0.01-1000 In 0.005-500 Pb 0.2-10000 Th 0.2-10000
Ce 0.02-500 K 0.01-10% Rb 0.1-10000 Ti 0.005-10%

16 | Precious Metals Analysis Schedule of services & fees | 2020


Generative
Exploration
Every method listed in the following four
pages involves some aspect of our innovative
methodology for super trace analysis on the ICP-
MS. Detection limits have been pushed orders
of magnitude below average crustal abundance
for the majority of elements, enabling excellent
precision at geochemical background levels and
clearly defined geochemical anomalies. Digestion
methods appropriate for any sample medium are
available - soils, sediments, regolith, vegetation,
water, rocks, and drill core. ALS remains committed
to solving long-standing analytical challenges in
exploration geochemistry by making use of new
instrumentation and fresh ideas from our team of
expert analytical chemists and geochemists.

Please submit at least three to four times the


nominal sample weight for efficient service.
Four Acid Super CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Trace Analysis Ag 0.002-100 Cu 0.02-10,000 Na 0.001%-10% Sr 0.02-10,000
Al 0.01%-50% Fe 0.002%-50% Nb 0.005-500 Ta 0.01-500
This super trace package is suitable
As 0.02-10,000 Ga 0.05-10,000 Ni 0.08-10,000 Te 0.005-500
for regional drilling, trenching and
Ba 1-10,000 Ge 0.05-500 P 0.001%-1% Th 0.004-10,000
hand samples in unmineralised
Be 0.02-1,000 Hf 0.004-500 Pb 0.01-10,000 Ti 0.001%-10%
rocks, and can also be used ME-MS61L™
Bi 0.002-10,000 In 0.005-500 Rb 0.02-10,000 Tl 0.002-10,000
effectively in areas of thick regolith 0.25g $39.20
Ca 0.01%-50% K 0.01%-10% Re 0.0004-50 U 0.01-10,000
for bedrock mapping. ALS has sample
Cd 0.005-1,000 La 0.005-10,000 S 0.01%-10% V 0.1-10,000
lowered the detection limits on
Ce 0.01-500 Li 0.2-10,000 Sb 0.02-10,000 W 0.008-10,000
key pathfinder elements such
Co 0.005-10,000 Mg 0.01%-50% Sc 0.01-10,000 Y 0.01-500
as As, Sb, Se and Tl to near or
Cr 0.3-10,000 Mn 0.2-100,000 Se 0.006-1000 Zn 0.2-10,000
below average crustal abundance,
revealing anomalous patterns at Cs 0.01-500 Mo 0.02-10,000 Sn 0.02-500 Zr 0.1-500

levels previously unattainable due Dy 0.005-1000 Ho 0.002-1000 Sm 0.004-1000

to technical limitations. Er 0.004-1000 Lu 0.002-1000 Tb 0.002-1000


MS61L-REE™ $6.60 Add-on only
Eu 0.004-1000 Nd 0.005-1000 Tm 0.002-1000
The rare earth elements and
Gd 0.005-1000 Pr 0.004-1000 Yb 0.004-1000
lead isotopes are available
²⁰⁴Pb 0.01-10000 ²⁰⁶Pb 0.01-10000 ²⁰⁷Pb 0.01-10000
as add-ons to expand the MS61L-PbIS™ $10.40 Add-on only
²⁰⁸Pb 0.01-10000
utility of the method in
greenfields exploration.

Portable XRF for CODE DESCRIPTION PRICE PER SAMPLE


Lithogeochemistry Portable XRF scan of a non-mineralised pulverised sample.
Ranges:
Add on to
The crucial lithogeochemical Si 0.5%-47%
pXRF-34 $3.90 multi-element
elements - silicon, titanium, and Ti 0.1%-60%
analysis only
zirconium - may be added to any Zr 5ppm-5%
15g sample
ALS four acid method for a more
complete element suite.

18 | Generative Exploration Schedule of services & fees | 2020


Aqua Regia CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
for Soils and Ag 0.001-100 Co 0.001-10,000 La 0.002-10,000 Pt 0.002-25 Th 0.002-10,000

Sediments Al
As
0.01%-25%
0.01-10,000
Cr
Cs
0.01-10,000 Li 0.1-10,000 Rb 0.005-10,000
0.005-500 Mg 0.01%-25% Re 0.0002-50
Ti 0.001%-10%
Tl  0.001-10,000
Aqua regia digestion with Au 0.0002-25 Cu 0.01-10,000 Mn 0.1-50,000 S 0.01%-10% U  0.005-10,000
super trace ICP-MS analysis B 10-10,000 Fe 0.001%-50% Mo 0.01-10,000 Sb 0.005-10,000 V  0.1-10,000
ME-MS41L™*
provides extremely low Ba 0.5-10,000 Ga 0.004-10,000 Na 0.001%-10% Sc 0.005-10,000 W  0.001-10,000 $32.10
0.5g sample
detection limits useful for Be 0.01-1000 Ge 0.005-500 Nb 0.002-500 Se 0.003-1000 Y  0.003-500
regional and deep cover Bi 0.0005-10,000 Hf 0.002-500 Ni 0.04-10,000 Sn 0.01-500 Zn 0.1-10,000
exploration. Ca 0.01%-25% Hg 0.004-10,000 P 0.001%-1% Sr 0.01-10,000 Zr 0.01-500

The rare earth elements and Cd 0.001-1000 In 0.005-500 Pb 0.005-10,000 Ta 0.005-500

lead isotope concentrations Ce 0.003-500 K 0.01%-10% Pd 0.001-25 Te 0.003-500

add new dimensions to Dy 0.002-1000 Ho 0.001-1000 Sm 0.002-1000


super trace data. REEs Er 0.002-1000 Lu 0.001-1000 Tb 0.001-1000 $6.60
MS41L-REE™
may be useful pathfinders Eu 0.002-1000 Nd 0.002-1000 Tm 0.001-1000 Add-on only
despite reflecting only the Gd 0.002-1000 Pr 0.002-1000 Yb 0.002-1000
labile component, while Pb ²⁰⁴Pb 0.005-10000 ²⁰⁶Pb 0.005-10000 ²⁰⁷Pb 0.005-10000 $10.40
MS41L-PbIS™
isotopic signatures can be ²⁰⁸Pb 0.005-10000 Add-on only
used in fingerprinting and * Gold determinations by this method are semi-quantitative due to the small sample weight used.
hydrothermal fluid history. For Au with multi-element using a 25g or 50g charge please use AuME-ST43™ or AuME-ST44™.

Selenium in Soils CODE ANALYTE & RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
Se at this level holds Se-MS46 Se 0.003-100
Aqua regia digestion and ICP-MS analysis.
$19.10
information for exploration 25g sample

vectoring as well as
environmental baselines.

Clay Separation CODE DESCRIPTION PRICE PER SAMPLE


The clay fraction in soils acts as a SCR-CLAY
Separation of the -10 micron fraction from soils.
$22.50
trap for elements migrating to the Minimum 300g of sieved soil required.

surface from depth, and may be


used to enhance subtle anomalies.

Generative Exploration | 19
Halogen Analysis CODE DESCRIPTION PRICE PER SAMPLE
Fluorine, chlorine, bromine and Vegetation sample is ashed at 475°C for 24 hours. Pre- and post-ashing weights
iodine hold significant promise in are reported. Average ash yields are 2-4% for species commonly used in
VEG-ASH01 $7.25
exploration surveys.
exploration, since many metals Minimum sample weight required 100g.
are transported through the Sample pre-treatment for super trace halogens analysis. Required for soils and
crust as halide complexes in un-ashed vegetation.
HAL-PREP01 $12.25
hydrothermal fluids. Minimum sample weight required varies, contact your local lab to discuss
your project.
Soil, vegetation or water may be
analysed by this method.
CODE ANALYTES & DETECTION LIMITS (ppm) DESCRIPTION PRICE PER SAMPLE
F 0.05 Cl 0.1 De-ionised water leach with ICP-
ME-HAL01™ $36.40
Br 0.02 I 0.002 MS & ion chromatograph analysis.

Ionic Leach™ CODE ANALYTES & DETECTION LIMITS (ppb) PRICE PER SAMPLE
Ionic Leach is designed to
TM Ag 0.1 Eu 0.1 Nb 0.1 Tb 0.1

enhance the most subtle labile As 0.5 Fe 0.1ppm Nd 0.1 Te 0.5

geochemical anomalies for a Au 0.02 Ga 0.5 Ni 1 Th 0.02

wide range of commodities. Ba 10 Gd 0.1 Pb 0.1 Ti 5


Be 0.2 Ge 0.1 Pd 0.05 Tl 0.05
It is a static sodium cyanide
Bi 0.3 Hf 0.05 Pr 0.1 Tm 0.1
leach using the chelating agents
Br 0.05ppm Hg 0.1 Pt 0.1 U 0.05
ammonium chloride, citric acid
Ca 0.2ppm Ho 0.1 Rb 0.1 V 0.2
and EDTA with the leachant ME-MS23™ $43.20
Cd 0.2 I 0.01ppm Re 0.01 W 0.1
buffered at an alkaline pH of 8.5.
Ce 0.1 In 0.1 Sb 0.5 Y 0.1
Nominal sample weight is 50g Co 0.3 La 0.1 Sc 1 Yb 0.1
(wet weight, no screening). Cr 1 Li 0.2 Se 2 Zn 10
Prepared vegetation samples Cs 0.1 Lu 0.1 Sm 0.1 Zr 0.1
may be leached at a Cu 1 Mg 0.01ppm Sn 0.2
5g sample size. Dy 0.1 Mn 0.01ppm Sr 1
Er 0.1 Mo 0.5 Ta 0.05
MS23-PbIS™ 204
Pb 0.01 206
Pb 0.01 207
Pb 0.01 208
Pb 0.02 $10.40 Add-on only

Other Selective Leaches


In addition to Ionic Leach™, ALS offers a variety
of standard partial leaches targeting particular
soil fractions. They can be done individually or
in sequence to best suit project needs.

Minimum sample size is 5g for each leach or


for any combination in sequence.

Please enquire for more details.

20 | Generative Exploration Schedule of services & fees | 2020


Hydrogeochemistry CODE DESCRIPTION PRICE PER SAMPLE

Water that has interacted with WAT-PREP02 Filter water samples to <0.45um and acidify with nitric acid before analysis. $5.60
rock will take on trace elements
WAT-PREP03 Filter water samples to <0.45um before analysis. $3.70
which are then transported with
the water, producing a larger WAT-PREP04 Acidify water samples with nitric acid before analysis. $1.90
footprint diagnostic of that rock.
Where collection of traditional
CODE ANALYTES & DETECTION LIMITS (µg/L) PRICE PER SAMPLE
media such as soils is difficult or
Au 0.002 Cu 0.1 Ni 0.2 Ta 0.01
impossible such as in swamps, in
Ag 0.005 Fe 0.003mg/L P 0.005mg/L Te 0.01
areas with significant transported
Al 3 Ga 0.05 Pb 0.05 Th 0.005
cover, and areas where invasive
As 0.05 Hf 0.005 Pd 0.005 Ti 0.2
sampling is not possible,
B 3 Hg 0.05 Pt 0.005 Tl 0.002
hydrogeochemistry provides
Ba 0.05 In 0.01 Rb 0.01 U 0.002
a direct detection tool on the
Be 0.005 K 0.01mg/L Re 0.002 V 0.05
same scale as stream sediment ME-MS14L™ $59.25
Bi 0.01 La 0.005 S 0.2mg/L W 0.01
sampling.
Ca 0.02mg/L Li 0.1 Sb 0.01 Y 0.005
Add on packages for anions by Cd 0.005 Mg 0.005mg/L Sc 0.01 Zn 0.5
ion chromatography, REE and Pb Ce 0.005 Mn 0.05 Se 0.05 Zr 0.02
isotopic ratios are also available. Co 0.005 Mo 0.05 Si 0.03mg/L
ALS offers multiple reliable and Cr 0.5 Na 0.01mg/L Sn 0.05
cost-effective water analysis Cs 0.005 Nb 0.005 Sr 0.05
packages to suit your exploration Dy 0.005 Gd 0.005 Nd 0.005 Tb 0.005
program. MS14L-REE™ Er 0.005 Ho 0.005 Pr 0.005 Tm 0.005 $17.50 Add-on only
Eu 0.005 Lu 0.005 Sm 0.005 Yb 0.005
Trace elements and metals
Br 0.05mg/L NO3 0.005mg/L pH 0.1 units Conductivity 2µS/cm
analyses require at least 50mL
MS14L-ANPH™ Cl 0.5mg/L SO4 0.5mg/L TDS 3mg/L Alkalinity 1mg/L $50.45 Add-on only
of water. Au requires a minimum
F 0.02mg/L
of 100mL of water. Anions and
physical parameters require a
minimum of 150mL of water.
Please contact ALS for information
on sampling methodology and
preservation if needed. Sampling
kits may be purchased at some
locations, please enquire.

Super Trace Au CODE ANALYTES & DETECTION LIMITS (µg/L) PRICE PER SAMPLE

and Pathfinders Au-PATH14L™ As


Ag 0.005-10
0.2-1000
Co
Pd
0.005-1000
0.005-100
Pt
Sb
0.01-100
0.02-1000
Tl
W
0.005-1000
0.02-1000 $44.40
Our new super trace gold and Au 0.0002-10
pathfinder package offers industry
leading detection limits for
exploration of many gold bearing
ore systems.

Generative Exploration | 21
Biogeochemistry CODE DESCRIPTION PRICE PER SAMPLE

Plants selectively absorb trace Milling of dry plant tissue to 100% passing 1mm. Produces a homogenous and
elements from soil, bedrock and VEG-MILL01 $7.25
representative pulp that can be subsampled for analysis.
water at depth and incorporate
them into their tissue. Analyses Vegetation sample is ashed at 475°C for 24 hours. Pre- and post-ashing weights
of plant tissues can therefore be VEG-ASH01 are reported. Average ash yields are 2-4% for species commonly used in $7.25
used as a large-scale geochemical exploration surveys. Minimum recommended sample weight is 100g.
sampling device in areas where
the rocks of interest are covered CODE ANALYTES & DETECTION LIMITS (ppm) PRICE PER SAMPLE
by transported cover and non- Ag 0.001 Cu 0.01 Nb 0.002 Ta 0.001
prospective lithologies. Careful Al 0.01% Fe 1 Ni 0.04 Te 0.02
selection of plant species, tissue As 0.01 Ga 0.004 P 0.001% Th 0.002
type and growth age are important Au 0.0002 Ge 0.005 Pb 0.01 Ti 0.001%
factors to be considered as the B 1 Hf 0.002 Pd 0.001 Tl 0.002
geochemical response will vary with ME-VEG41™ Ba 0.1 Hg 0.001 Pt 0.001 U 0.005
these factors. unashed
Be 0.01 In 0.005 Rb 0.01 V 0.05
1g sample $22.50
ALS provides multiple digestion Bi 0.001 K 0.01% Re 0.001 W 0.01
and preparation methods for Ca 0.01% La 0.002 S 0.01% Y 0.003
explorers using this sample media. Cd 0.001 Li 0.1 Sb 0.01 Zn 0.1
Preparation methods can include the Ce 0.003 Mg 0.001% Sc 0.01 Zr 0.02
separation of the tissue of interest Co 0.002 Mn 0.1 Se 0.005
from other plant parts, milling and Cr 0.01 Mo 0.01 Sn 0.01
ashing. Cs 0.005 Na 0.001% Sr 0.02
Ag 0.00005 Cu 0.0005 Nb 0.0001 Ta 0.00005
Ashing results in the concentration
Al 0.000005 Fe 0.05 Ni 0.002 Te 0.001
of many elements of interest to
As 0.0005 Ga 0.02% P 0.000001 Th 0.0001
explorers and when calculated back
Au 0.00001 Ge 0.00025 Pb 0.0005 Ti 0.000001
to the original sample weight has
B 0.05 Hf 0.0001 Pd 0.00005 Tl 0.0001
the effect of dropping detection ME-VEG41a™
Ba 0.005 Hg 0.00005 Pt 0.00005 U 0.00025
limits of many elements by an order ashed
0.25g Be 0.0005 In 0.00025 Rb 0.0005 V 0.0025
of magnitude. Please contact your $22.50
sample Bi 0.00005 K 0.000005 Re 0.00005 W 0.0005
local lab to discuss your specific
Ca 0.000005 La 0.01% S 0.000001 Y 0.00015
project goals.
Cd 0.00005 Li 0.005 Sb 0.0005 Zn 0.005
Ce 0.00015 Mg 0.000001 Sc 0.0005 Zr 0.001
Co 0.0001 Mn 0.005 Se 0.00025
Cr 0.0005 Mo 0.0005 Sn 0.0005
Cs 0.00025 Na 5E-07 Sr 0.001
Dy 0.002 Gd 0.002 Nd 0.001 Tb 0.001
VEG41-REE™
Er 0.002 Ho 0.001 Pr 0.002 Tm 0.001 $6.60 Add-on only
VEG41a-REE™
Eu 0.002 Lu 0.001 Sm 0.003 Yb 0.003

22 | Generative Exploration Schedule of services & fees | 2020


Targeted
Exploration
No single method covers all types of geological
materials for all geochemically-relevant elements
at all concentrations. Sample type, commodity of
interest, geochemical pathfinders and expected
concentration of target elements should all be
considered when selecting appropriate methods for
your project.

Broadly, aqua regia readily dissolves many sulphide,


oxide and carbonate minerals, as well as retaining
mercury, a particularly volatile element. Four acid
digestions quantitatively dissolve nearly all minerals,
but it may sometimes be necessary to use even
stronger techniques such as fusions in order to fully
digest barite, rare earth oxides, and tin, tungsten,
niobium and tantalum minerals.

The choice between various instrument finishes


should be informed by the expected concentrations of
the elements of interest in the sample.

Please submit at least four times


the nominal sample weight for
efficient service.
Aqua Regia With CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
ICP-MS Finish Ag 0.01-100 Cs 0.05-500 Mo 0.05-10,000 Sr 0.2-10,000
Al 0.01-25% Cu 0.2-10,000 Na 0.01%-10% Ta 0.01-500
Method selection can be key to
As 0.1-10,000 Fe 0.01%-50% Nb 0.05-500 Te 0.01-500
achieving exploration success.
Au* 0.02-25 Ga 0.05-10,000 Ni 0.2-10,000 Th 0.2-10,000
Sample type, target commodity,
B 10-10,000 Ge 0.05-500 P 10-10,000 Ti 0.005%-10%
and pathfinder elements should
all be considered when selecting ME-MS41™ Ba 10-10,000 Hf 0.02-500 Pb 0.2-10,000 Tl 0.02-10,000

the most appropriate method for 0.5g Be 0.05-1,000 Hg 0.01-10,000 Rb 0.1-10,000 U 0.05-10,000 $25.65
sample Bi 0.01-10,000 In 0.005-500 Re 0.001-50 V 1-10,000
your project.
Ca 0.01%-25% K 0.01%-10% S 0.01%-10% W 0.05-10,000
Aqua regia is an excellent
Cd 0.01-1,000 La 0.2-10,000 Sb 0.05-10,000 Y 0.05-500
exploration tool for various deposit
Ce 0.02-500 Li 0.1-10,000 Sc 0.1-10,000 Zn 2-10,000
types that involve gold, silver and
Co 0.1-10,000 Mg 0.01%-25% Se 0.2-1,000 Zr 0.5-500
base metals hosted in sulphide
Cr 1-10,000 Mn 5-50,000 Sn 0.2-500
and carbonate minerals.
* Gold determinations by this method are semi-quantitative due to the small sample weight used.
For Au with multi-element using a 25g or 50g charge please use AuME-TL43™ or AuME-TL44™.

Single Elements CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
by Aqua Regia ME-MS42™ Ag 0.01-25 Hg 0.005-25 Se 0.2-250 U 0.05-250 $13.65
0.5g As 0.1-250 Re 0.001-250 Te 0.01-250 + $1.40 /element
When analytical results for one
sample Bi 0.01-250 Sb 0.05-250 Tl 0.02-250
or only a few elements with low
detection limits are required. More + Add element symbol as prefix to method code.

elements are available on request.

Four Acid CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Digestion With Ag 0.01-100 Cu 0.2-10,000 Na 0.01%-10% Sr 0.2-10,000

ICP-MS Finish Al
As
0.01%-50%
0.2-10,000 Ga
Fe 0.01%-50% Nb
0.05-10,000 Ni
0.1-500
0.2-10,000
Ta
Te
0.05-100
0.05-500
Four acid digestion quantitatively ME-MS61™ Ba 10-10,000 Ge 0.05-500 P 10-10,000 Th 0.01-10,000
0.25g
dissolves nearly all minerals Be 0.05-1,000 Hf 0.1-500 Pb 0.5-10,000 Ti 0.005%-10%
sample $30.75
in the majority of geological Bi 0.01-10,000 In 0.005-500 Rb 0.1-10,000 Tl 0.02-10,000
materials. However, barite, rare Ca 0.01%-50% K 0.01%-10% Re 0.002-50 U 0.1-10,000
earth oxides, columbite-tantalite, *ME-MS61m™ Cd 0.02-1,000 La 0.5-10,000 S 0.01%-10% V 1-10,000 $42.20
and titanium, tin and tungsten 0.75g
sample Ce 0.01-500 Li 0.2-10,000 Sb 0.05-10,000 W 0.1-10,000
minerals may not be fully Co 0.1-10,000 Mg 0.01%-50% Sc 0.1-10,000 Y 0.1-500
digested. Cr 1-10,000 Mn 5-100,000 Se 1-1,000 Zn 2-10,000
Despite the potentially Cs 0.05-500 Mo 0.05-10,000 Sn 0.2-500 Zr 0.5-500
incomplete digestion of REEs, Dy 0.05-1,000 Gd 0.05-1,000 Nd 0.1-1,000 Tb 0.01-1,000
$38.45
the leachable portion of these ME-MS61r™ Er 0.03-1,000 Ho 0.01-1,000 Pr 0.03-1,000 Tm 0.01-1,000
Full suite
elements may hold important Eu 0.03-1,000 Lu 0.01-1,000 Sm 0.03-1,000 Yb 0.03-1,000
exploration vectoring information * Note: To include Hg by a separate method in the suite of elements above, please request ME-MS61m™ instead of ME-MS61™.
and can be chosen as an add-on.

24 | Targeted Exploration Schedule of services & fees | 2020


Single Elements CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
by Four Acid Ag 0.01-100 Ga 0.05-500 Se 1-500 Tl 0.02-500
ME-MS62™ As 0.2-500 Mo 0.05-500 Sn 0.2-500 U 0.1-500 $16.45
When analytical results for one
0.25g sample Bi 0.01-500 Re 0.002-100 Te 0.05-500 W 0.1-500 + $1.40 / element
or only a few elements with low
Cd 0.02-500 Sb 0.05-500 Th 0.01-500
detection limits are required. More
+ Add element symbol as prefix to method code.
elements are available on request.

Aqua Regia With CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
ICP-AES Finish Ag 0.2-100 Co 1-10,000 Mn 5-50,000 Sr 1-10,000
Al 0.01%-25% Cr 1-10,000 Mo 1-10,000 Th 20-10,000 $12.35 full package
These methods are economical
ME-ICP41 As 2-10,000 Cu 1-10,000 Na 0.01%-10% Ti 0.01%-10% or $6.05
tools for first pass exploration
0.5g B 10-10,000 Fe 0.01%-50% Ni 1-10,000 Tl 10-10,000 + $0.80 /element
geochemistry. Data reported from sample Ba 10-10,000 Ga 10-10,000 P 10-10,000 U 10-10,000
an aqua regia digestion should
*ME-ICP41m Be 0.5-1,000 Hg 1-10,000 Pb 2-10,000 V 1-10,000 $19.10
be considered as representing 1g sample Bi 2-10,000 K 0.01%-10% S 0.01%-10% W 10-10,000
only the leachable portion of the
Ca 0.01%-25% La 10-10,000 Sb 2-10,000 Zn 2-10,000
particular analyte.
Cd 0.5-1,000 Mg 0.01%-25% Sc 1-10,000
*To include Hg to a lower detection limit of 0.005ppm by a separate method, please request package ME-ICP41m.

Portable XRF for CODE ANALYTES & RANGES PRICE PER SAMPLE
Lithogeochemistry Portable XRF scan of a non-mineralised pulverised sample.
Ranges:
Add-on to
The crucial lithogeochemical Si 0.5%-47%
pXRF-34 $3.90 multi-element
elements - silicon, titanium and Ti 0.1%-60%
analysis only.
zirconium - may be added to any Zr 5ppm-5%
15g sample
ALS four acid method for a more
complete element suite.

Targeted Exploration | 25
Four Acid CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Digestion With Ag 0.5-100 Cr 1-10,000 Na 0.01%-10% Ti 0.01%-10%

ICP-AES Finish ME-ICP61


0.25g
Al
As
0.01%-50% Cu
5-10,000 Fe
1-10,000
0.01%-50%
Ni
P
1-10,000
10-10,000
Tl
U
10-10,000 $16.45 full package
10-10,000 or $8.75
Four acid digestions are able sample Ba 10-10,000 Ga 10-10,000 Pb 2-10,000 V 1-10,000 + $0.80 /element
to dissolve most minerals, but Be 0.5-1,000 K 0.01%-10% S 0.01%-10% W 10-10,000
although the term “near-total” *ME-ICP61m Bi 2-10,000 La 10-10,000 Sb 5-10,000 Zn 2-10,000 $27.90
is used, not all elements are 0.75g Ca 0.01%-50% Mg 0.01%-50% Sc 1-10,000
quantitatively extracted in some sample
Cd 0.5-1,000 Mn 5-100,000 Sr 1-10,000
sample matrices. Co 1-10,000 Mo 1-10,000 Th 20-10,000
* To include Hg in the suite of elements above, please request method ME-ICP61m

Resistive Elements CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
By Fusion ME-MS85™ Ce 0.1-10,000 Rb 0.2-10,000 Ta 0.1-2,500 W 1-10,000 $18.30
0.1g La 0.1-10,000 Sn 1-10,000 Th 0.05-1,000 Y 0.1-10,000 + $1.40 /element
The lithium borate fusion & ICP-MS
sample
finish allows analysis of the most Nb 0.2-2,500 Sr 0.1-10,000 U 0.05-1,000 Zr 2-10,000
resistive elements at trace levels. Note: For high-grade range request ME-MS85h
Additional elements are available
on request.

Intermediate CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE


Level Aqua Regia Ag 1-200 Cr 5-50,000 Mo 5-50,000 Th 100-50,000
Al 0.05%-50% Cu 5-50,000 Na 0.05%-50% Ti 0.05%-50%
These packages can be used
As 10-100,000 Fe 0.05%-50% Ni 5-50,000 Tl 50-50,000
as an economical alternative
Ba 50-50,000 Ga 50-50,000 P 50-50,000 U 50-50,000 $20.50 full package
to analysing low grade ore ME-ICP41a
Be 5-500 Hg 5-50,000 Pb 10-50,000 V 5-50,000 or $12.25
or samples with known 0.4g sample
Bi 10-50,000 K 0.05%-50% S 0.05%-10% W 50-50,000 + $2.65 /element
mineralization. Data reported from
Ca 0.05%-50% La 50-50,000 Sb 10-50,000 Zn 10-50,000
an aqua regia digestion should
Cd 5-2,500 Mg 0.05%-50% Sc 5-50,000
be considered as representing
only the leachable portion of the Co 5-50,000 Mn 25-50,000 Sr 5-50,000

particular analyte.

26 | Targeted Exploration Schedule of services & fees | 2020


Intermediate CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Level Four Acid Ag 1-200 Cr 10-100,000 Na 0.05%-30% Ti 0.05%-30%

Digestion Al
As
0.05%-30%
50-100,000
Cu
Fe
10-100,000
0.05%-50%
Ni
P
10-100,000
50-100,000
Tl
U
50-50,000
50-50,000
These packages can be used Ba 50-50,000 Ga 50-50,000 Pb 20-100,000 V 10-100,000 $23.25 full package
as an economical alternative ME-ICP61a
Be 10-10,000 K 0.1%-30% S 0.05%-10% W 50-50,000 or $15.05
0.4g sample
to analysing low grade ore Bi 20-50,000 La 50-50,000 Sb 50-50,000 Zn 20-100,000 + $2.65 /element
or samples with known Ca 0.05%-50% Mg 0.05%-50% Sc 10-50,000
mineralization. Four acid Cd 10-10,000 Mn 10-100,000 Sr 10-100,000
digestions are able to dissolve Co 10-50,000 Mo 10-50,000 Th 50-50,000
most minerals, but not all
elements are quantitatively
extracted in some samples.

Halogens CODE ANALYTES & RANGES (ppm) DESCRIPTION PRICE PER SAMPLE
Elemental analysis of the halide Cl-IC881 Cl 50-20,000 KOH fusion and ion chromatography. 0.2g sample $22.90
minerals containing chlorine and Cl-ELE81a Cl 50-20,000
Specific to Cl in phosphates only.
$20.50
fluorine generally require fusions KOH fusion and ion selective electrode. 1g sample

that will retain the elements Cl-XRF20 Cl 0.001%-6% Lithium borate fusion and XRF. 0.7g sample $20.50

in solution, as well as specific Cl-VOL66 Cl 0.01-65% Nitric acid digestion and titration. 1g sample $34.55
instrumentation for analysis. KOH fusion and ion selective
F-ELE81a F 20-20,000 $20.50
electrode. 0.2g sample
Na2O2 fusion, citric acid leach and
F-ELE82 F 0.01-100% $30.35
ion selective electrode. 0.1g sample
F-IC881 F 20-20,000 KOH fusion and ion chromatography. 0.2g sample $22.90
Cl 50-20,000 KOH fusion and ion chromatography.
ME-IC881 $31.55
F 20-20,000 0.2g sample

Mercury CODE ANALYTE & RANGES (ppm) DESCRIPTION PRICE PER SAMPLE
Aqua regia quantitatively Trace level Hg by aqua regia and ICP-MS.
Hg-MS42 Hg 0.005-100 $11.45
dissolves Hg and uses a digestion 0.5g sample

temperature low enough to avoid High grade Hg by aqua regia and ICP-AES.
Hg-ICP42 Hg 1-100,000 $10.90
0.5g sample
fuming off this volatile element.
Hg in ores by acid digestion and ICP-AES.
Hg-CON01 Hg 1-10,000 $82.00
2g sample

Loss On Ignition CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
LOI measures the content of OA-GRA10 Gravimetric procedure after drying at 105°C. $16.45
a sample lost as gases when 2 hours (normal samples).
H2O (Moisture) 0.01-100 $17.25
subjected to high temperatures, 24 hours (hygroscopic samples).
OA-GRA11 QAQC samples inserted
often including water and CO2. 5g sample
for monitoring
Many more temperatures and H 2O + Combustion furnace and infrared
ignition times are available, please OA-IR06 (Water of 0.01-100 spectrometry. $16.45
enquire. Crystallization) 1g sample
Loss on ignition at 500°C.
OA-GRA05xf LOI @ 500°C 0.01-100 $13.65
1g sample.
Loss on ignition at 1000°C.
OA-GRA05 LOI @ 1000°C 0.01-100 $13.25
1g sample.

Targeted Exploration | 27
Conductivity, CODE ANALYTES & RANGES DESCRIPTION PRICE PER SAMPLE
pH and Acid OA-GRA04 Acid Insoluble 0.01%-100%
Acid insoluble content.
$16.45
1g sample.
Insolubles OA-ELE03 pH 0.1-14
pH on 1:10 sample to water ratio.
$10.95
5g sample
These methods provide crucial
Specific conductivity on 1:10 sample
information for mineral processing
OA-ELE04 Conductivity 1-100,000μS/cm to water ratio. $13.65
and environmental assessment 5g sample
studies. Soil pH on 1:1 sample to water ratio.
OA-ELE05 Soil pH 0.1-14 $13.65
20g sample
Soil pH and
Add on to Soil pH. $5.20 add-on to
OA-ELE05AP soil acid 0.1-14
Addition of HCl and pH re-measured. soil pH only
neutralization
Soil Soil conductivity on 1:1 sample to water ratio.
OA-ELE06 1-100,000μS/cm $9.60
Conductivity 20g sample
OA-ELE07 Paste pH 0.1-14 Paste pH on 10g sample saturated with water. $8.25
Paste pH
Add on to Paste pH. $5.20 add-on to
OA-ELE07AP and soil acid 0.1-14
Addition of HCl to paste and pH re-measured. Paste pH only
neutralisation

Stable Isotopes CODE ANALYTE DESCRIPTION PRICE PER SAMPLE


Many important parameters Offered in partnership with the Mineral Deposit Research
C and O in Unit (MDRU) at the University of British Columbia. Carbon
of mineralizing fluids may be Carbonate Minerals
LS-ISTP01 and oxygen isotopic composition is determined specifically $37.85
determined from stable isotope on carbonate minerals in whole-rock pulps using laser
ratios. The isotopic alteration spectroscopy. 0.5g sample
halo may extend beyond visible O-ISTP01 Specific to clays and silicate minerals. Determination using
O and H in Silicate
mineralogy changes, creating a a complex gas collection procedure and IRMS. Sample must $118.95 each
H-ISTP01 Minerals
larger deposit footprint for easier be supplied as a single-mineral separate. TAT is 30 days.
exploration vectoring. Specific to sulphide and sulphate minerals. Determination
S-ISTP01 Sulphur using TC/EA and IRMS. Sample must be supplied as a $59.50
single-mineral separate. TAT is 30 days.
Specific to minerals containing carbon and/or oxygen.
CO-ISTP01 Carbon and Oxygen Determination using acid digestion and IRMS. Sample must $45.40
be supplied as a single-mineral separate. TAT is 30 days.

28 | Targeted Exploration Schedule of services & fees | 2020


Pb Isotope Ratios CODE ANALYTE DESCRIPTION PRICE PER SAMPLE
For Exploration PbIS-RAT41 Six isotope ratios
Pb isotope ratios by acid digestion and ICP-MS analysis.
$36.70
Total Pb content of the sample is required in advance. May
This fast, low-cost analysis including 204Pb, be run on whole rock pulps. 0.5g sample
206
Pb, 207Pb, and
of Pb isotope ratios in pulps PbIS-RAT61 208
Pb isotopes For Aqua Regia Digestion request PbIS-RAT41 $40.15
allows fingerprinting of different For Four Acid Digestion request PbIS-RAT61
lithologies and hydrothermal fluid NOTE: Samples must contain >2ppm Pb for analysis to be viable
flow pathways, providing a new
vector to ore deposits.

Radiogenic CODE ANALYTE DESCRIPTION PRICE PER SAMPLE


Isotopes May be done on whole rock pulps or on specific Pb-bearing
minerals. Measurement by acid digestion
Pb-ISTP01 Pb/Pb $281.20
These methods provide insight and HR-ICP-MS. Samples may require Hg separation at an
into provenance and character additional cost. TAT is 30 days.
of hydrothermal fluids and Performed on whole rock pulps. Measurement by column
rock genesis, helping unravel Nd-ISTP01 Sm/Nd separation and HR-ICP-MS. Total Sm and Nd content is $589.40
required in advance. TAT is 30 days.
geological history for a more
sophisticated understanding of
your ore body.

Geochronology CODE ANALYTE DESCRIPTION PRICE PER SAMPLE


These methods may be used to Done on targeted minerals. Rock and drill core should be
date the ages of specific minerals, submitted intact or crushed only, as sample prep is included
Ar-ISTP01 Ar/Ar in the price. Measurement by irradiation and step heating $2,678.00
hydrothermal alteration events, in a mass spectrometer. Price includes sample preparation.
and emplacement of volcanic- Turnaround time approximately 8 months.
plutonic units. Age constraints on Specific to molybdenite. Rock or drill core must be received
important events can help refine whole as steel jaw crushing will contaminate the sample
the deposit model and identify with Re. Age can only be determined for rocks of >0.5
Re-ISTP01 Re/Os $1,879.75
Ma, and the molybdenite separate must contain >100ppm
alteration that did not contribute
Re. Price includes mineral separation, solvent extraction,
to mineralization. column separation and TIMS analysis. TAT is 70 days.
Sample sizes required for most U-Pb dating by LA-ICP-MS of igneous rocks using zircon and
monazite. Age of the sample is reported. Analysis includes
isotopic analysis methods vary $825.00 /20 grains*
a standard set of 30 elements, including REE. Price includes
depending on mineralogy and preparation of up to 1kg of sample.
U-ISTP02
purpose; please contact client U/Pb
U-ISTP03 U-Pb dating of detrital grains by LA-ICP-MS. Age probability
services for more information. distribution in the sample is reported. Analysis includes a
$1,090.00 /60 grains*
standard set of 30 elements, including REE. Preparation of
2kg of sample included in price.
* larger numbers of grains can be analyed at an increased cost.

Mineral Chemistry CODE ANALYTE DESCRIPTION PRICE PER SAMPLE


ALS has partnered with CODES Quantitative analyses of in situ minerals. Advantage of
Laser ablation
Analytical Laboratories, at the LA-MIN mineral analyses small spot size (15-80 micron). Trace and major element $33.00 /analysis
University of Tasmania, to provide compositions are reported.
state of the art mineral analyses
for exploration, mining and Mineral mounts Preparation of 25 mm round mounts for in-situ mineral
MIN-MOUNT analyses in rock samples (no crushing, mineral separation $45.50 /mount
metallurgical applications.
and grain mounting).

CL imaging of grains for isotopic dating using SEM. Cost


SEM-IMG Grain imaging dependent on number of grains or amount of time taken for $122.00 /30 grains
mineral relationship imaging.
$91.00 per section/
Preparation of thin sections for both reflected light
PREP-THINP Thin section Reflected light, SEM
microscopy and SEM analysis, and for transmitted light
PREP-THINS preparation $45.50 per section/
microscopy only.
transmitted light

Targeted Exploration | 29
Whole Rock
Analysis &
Litho­
geochemistry
Analyses related to lithogeochemistry, alteration minerals,
and trace element mobility are important tools for
understanding ore-forming geological environments.
Managing and interpreting large datasets generated
by lithogeochemical techniques, while traditionally
challenging, have been greatly simplified by powerful
software tools now available to geologists and
geochemists.

No single analytical method is able to encompass the full


range of elements required for effective lithogeochemical
investigation. ALS offers many analytical packages
designed to provide comprehensive information for these
studies using the most appropriate methods for every
element; essentially, complete rock characterization.

Please submit at least four times the nominal


sample weight for efficient service.
Whole Rock CODE ANALYTES AND RANGES (%) DESCRIPTION PRICE PER SAMPLE
Analysis ME-XRF26*
Al2O3 0.01-100 Fe2O3 0.01-100 Na2O 0.01-10 SrO 0.01-1.5

Both x-ray fluorescence (XRF) and BaO 0.01-66 K 2O 0.01-15 P2O5 0.01-46 TiO2 0.01-30 Fused disc XRF,
OA-GRA05x LOI by furnace $34.15
ICP-AES instrument finishes can ME-GRA05 CaO 0.01-60 MgO 0.01-50 SO3 0.01-34 LOI 0.01-100 or TGA
be used effectively for the major 2g sample
Cr2O3 0.01-10 MnO 0.01-39 SiO2 0.01-100
rock-forming elements following * For non-mineralised samples with moderate sulphide content, please request ME-XRF06.
a fusion. These methods are not For mineralised and/or high sulphide content >4%, please request ME-XRF15c. Performed on dried sample therefore expected to
suitable for samples with base or report slightly higher than ME-ICP06.
precious metals mineralization.
CODE ANALYTES AND RANGES (%) DESCRIPTION PRICE PER SAMPLE
Specific commodities such as
Al2O3 0.01-100 Fe2O3 0.01-100 Na2O 0.01-100 TiO2 0.01-100
iron ore, bauxite, and base metal ME-ICP06* Fused bead, acid
sulphides should be analysed OA-GRA05
BaO 0.01-100 K 2O 0.01-100 P2O5 0.01-100 LOI 0.01-100 digestion and
$34.15
with packages designed for those ME-GRA05 CaO 0.01-100 MgO 0.01-100 SiO2 0.01-100 ICP-AES. LOI by
sample types. Please see the Ores 2g sample furnace or TGA
Cr2O3 0.002-100 MnO 0.01-100 SrO 0.01-100
& Commodities section for more
*For mineralised and/or high sulphide content >4%, please request ME-XRF15c.
whole rock analysis options.
Both the ME-XRF26 and ME-ICP06 packages include LOI by furnace or TGA.

Trace Elements by CODE ANALYTES AND RANGES (ppm) DESCRIPTION PRICE PER SAMPLE
Li Borate Fusion Ba 0.5-10,000 Hf 0.1-10,000 Sn 1-10,000 Y 0.1-10,000
Ce 0.1-10,000 Ho 0.01-1,000 Sr 0.1-10,000 Yb 0.03-1,000
A lithium borate fusion prior to acid
Cr 10-10,000 La 0.1-10,000 Ta 0.1-2,500 Zr 2-10,000
dissolution and ICP-MS analysis
Cs 0.01-10,000 Lu 0.01-1,000 Tb 0.01-1,000 Fused bead, acid
provides the most quantitative ME-MS81™
Dy 0.05-1,000 Nb 0.1-2,500 Th 0.05-1,000 digestion $34.25
analytical approach for a broad suite 2g sample
Er 0.03-1,000 Nd 0.1-10,000 Tm 0.01-1,000 and ICP-MS
of trace elements. Options for adding
Eu 0.02-1,000 Pr 0.02-1,000 U 0.05-1,000
the whole rock elements from an
Ga 0.1-1,000 Rb 0.2-10,000 V 5-10,000
ICP-AES analysis on the same fusion,
Gd 0.05-1,000 Sm 0.03-1,000 W 1-10,000
or base metals from a separate four
Combination of Rare Earth & Trace Elements from method ME-MS81™ plus whole rock
acid digestion, are available. ME-MS81d™ $47.15
package by method ME-ICP06.
Ag 0.5-100 Co 1-10,000 Mo 1-10,000 Sc 1-10,000 Four acid
ME-4ACD81 $8.20
As 5-10,000 Cu 1-10,000 Ni 1-10,000 TI 10-10,000 digestion and
0.25g sample Add-on only
Cd 0.5-1,000 Li 10-10,000 Pb 2-10,000 Zn 2-10,000 ICP-AES

Whole Rock Analysis & Litho­geochemistry | 31


Complete CODE ANALYTES AND RANGES (ppm) PRICE PER SAMPLE
Characterization SiO2 0.01-100% MgO 0.01-100% TiO2 0.01-100% BaO 0.01-100%

Packages ME-ICP06
Al2O3 0.01-100% Na2O 0.01-100% MnO 0.01-100% LOI 0.01-100%
Fe2O3 0.01-100% K 2O 0.01-100% P2O5 0.01-100%
By combining a number of
methods into one cost effective CaO 0.01-100% Cr2O3 0.002-100% SrO 0.01-100%

package, a complete sample ME-IR08 C 0.01-50% S 0.01-50%


characterization is obtained. Ba 0.5-10,000 Gd 0.05-1,000 Sm 0.03-1,000 W 1-10,000
These packages combine Ce 0.1-10,000 Hf 0.2-10,000 Sn 1-10,000 Y 0.1-10,000
whole rock analysis, trace
Cr 10-10,000 Ho 0.01-10,000 Sr 0.1-10,000 Yb 0.03-1,000 Sold only as complete
elements by fusion, aqua regia
Cs 0.01-10,000 La 0.1-10,000 Ta 0.1-2,500 Zr 2-10,000 packages.
digestion for the volatile trace
elements, carbon and sulphur by ME-MS81™ Dy 0.05-1,000 Lu 0.01-1,000 Tb 0.01-1,000 CCP-PKG01 $82.75
combustion analysis, and several Er 0.03-1,000 Nb 0.2-2,500 Th 0.05-1,000
detection limit options for the CCP-PKG03 $93.60
Eu 0.03-1,000 Nd 0.1-10,000 Tm 0.01-1,000 Includes ME-XRF26
base metals.
Ga 0.1-1,000 Pr 0.03-1,000 U 0.05-1,000 instead of ME-ICP06
Other method combinations
Ge 5-1,000 Rb 0.2-10,000 V 5-10,000
are available for complete
As 0.1-250 In 0.005-250 Se 0.2-250
characterization. Please enquire
with your local client services ME-MS42™* Bi 0.01-250 Re 0.001-250 Te 0.01-250
team for more information. Hg 0.005-25 Sb 0.05-250 Tl 0.2-250

These packages are suitable only Ag 0.5-100 Cu 1-10,000 Ni 1-10,000 Zn 2-10,000


for unmineralised samples. To ME-4ACD81 Cd 0.5-1,000 Li 10-10,000 Pb 2-10,000
add gold analysis, please see the Co 1-10,000 Mo 1-10,000 Sc 1-10,000
Precious Metals section.
Ag 0.01-100 Cu 0.2-10,000 Ni 0.2-10,000 Zn 2-10,000
CCP-PKG05 $96.45
Minimum sample size is 10g. ME-MS61™ Cd 0.02-1,000 Li 0.2-10,000 Pb 0.5-10,000 Includes ME-MS61™
instead of ME-4ACD81
Co 0.1-10,000 Mo 0.05-10,000 Sc 0.1-10,000
Ag 0.002-100 Cu 0.02-10,000 Ni 0.08-10,000 Zn 0.2-10,000 CCP-PKG06 $109.15
Includes ME-MS61L™
ME-MS61L™ Cd 0.005-1,000 Li 0.2-10,000 Pb 0.01-10,000
with super trace
Co 0.005-10,000 Mo 0.02-10,000 Sc 0.01-10,000 detection limits.

*Other customisable options such as super trace detection limits ME-MS42L™ available for substitution of ME-MS42™

32 | Whole Rock Analysis & Litho­geochemistry Schedule of services & fees | 2020


Specific
Ores &
Commodities
Procedures for the evaluation of ores and high grade
materials are optimised for accuracy, precision and recovery
of the target element. No single digestion or analytical
method is suitable for all cases, and ALS provides a wide
variety of procedures so the most appropriate method can
be selected. Choices include acid digestions with ICP-AES
finish; fusion and XRF determination for resistive elements
and bulk commodities; specialised solvent digestions for
uncommon ores; and classical volumetric methods for very
high grade base metals.

Please submit at least four times


the nominal sample weight for
efficient service.
Copper Mineral CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Selective Leaches Cu-AA04 Cu 0.01-10
Citric acid leach and AAS finish.
$13.65
0.25g sample
These methods may be run Sulphuric acid leach and AAS finish.
Cu-AA05 Cu 0.001-10 $13.65
alone or in sequence to 1g sample
semi-quantitatively identify Sulphuric acid/Na sulfite leach and AAS finish.
Cu-AA07n Cu 0.001-100 $13.65
potential recovery by various 1g sample
ore processing methods. 0.001-100 Sulphuric acid/ferric sulphate leach and AAS
Cu-AA08q Cu $14.65
ALS can also provide finish. 1g sample
Cyanide leach and AAS finish.
custom methods based on Cu-AA17 Cu 0.001-10 $19.85
2g sample
metallurgical requirements.
Sequential leach for oxide, sulphide and
Cu-PKG06LI Cu Various residual Cu. Various options available. $41.00
1g sample

Total Copper CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Aqua regia is an effective Aqua regia digestion and ICP finish.
Cu-ICP41 Trace Cu 1-10,000 ppm $6.85
solvent for copper oxides 0.5g sample
and sulphides, but Cu-ICP61 Trace Cu 1-10,000 ppm
Four acid digestion and ICP finish.
$9.55
copper occurring with 0.25g sample

other commodities like Cu-OG46 Cu Assay 0.001-50


Aqua regia digestion and ICP finish.
$12.25
molybdenum can be 0.4g sample

analysed by four acid Four acid digestion and ICP finish.


Cu-OG62 Cu Assay 0.001-50 $15.00
0.4g sample
digestion for consistency
across data sets. Screen 1kg sample to 100 microns, duplicate
assay on 0.25g of undersize fraction and
Cu-SCR21 Native Cu 0.01-100 $126.95
assay of entire oversize fraction by four acid
digestion and AAS finish.
Cu-VOL61 HNO3-HCl-HF-H2SO4 acid digestion followed by $47.85
Cu
0.01-100 titration. Cu-CON02 done in duplicate.
Cu-CON02 Concentrate $82.00
2g sample

Iron Ore Analysis CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Lithium borate fusion and XRF Al2O3 0.01-100 K 2O 0.001-6.3 Sn 0.001-1.5
finish is the industry method As 0.001-1.5 MgO 0.01-40 Sr 0.001-1.5
of choice for the analysis ME-XRF21u Ba 0.001-10 Mn 0.001-25 TiO2 0.01-30 $45.20
(unnormalised)
of oxide iron ores. Single CaO 0.01-40 Na2O 0.005-8 V 0.001-5 LOI determination
or multi-temperature LOI is ME-XRF21n Cl 0.001-6 Ni 0.001-8 Zn 0.001-1.5 Fused disc XRF. must be done as
(normalised)
available, customisable as Co 0.001-5 P 0.001-10 Zr 0.001-1 part of procedure.
required. 0.7g sample Cr203 0.001-10 Pb 0.001-2 Total 0.01-110
Cu 0.001-1.5 S 0.001-5
Fe 0.01-75 SiO2 0.01-100

Furnace or
OA-GRA05x Loss on Ignition $6.05
Thermogravimetric
ME-GRA05 1g sample + $3.60 / temperature
Analyser (TGA)

Davis Tube CODE DESCRIPTION PRICE PER SAMPLE


Recovery DTR_PREP Multi-stage sieving and pulverizing. $60.25
DTR_REC Wash time and mass recovery. By Quotation
ALS recommends discussion
WT_DTR Weight of DTR fractions. By Quotation
to determine optimum
DTR_FeRec DTR iron recovery. By Quotation
protocol for your particular
XRF analysis on various DTR fractions (head, concentrate, tailing).
ore type. Grind curve ME-XRF21h/c/t
0.7g sample each
$45.20 each
confirmation tests, laser OA-GRA05xh/xc/xt Loss on Ignition reported required as part of the ME-XRF21h/c/t methods. $9.65 each
sizing, cyclosizing and wet Ferrous iron by titration (FeO; 0.01-100%).
screening are also available. Fe-VOL05 $24.20
1g sample
MAG-SUS Magnetic susceptibility. $13.60
*Note: These methods are not suitable for samples with base or precious metals mineralisation.

34 | Specific Ores & Commodities Schedule of services & fees | 2020


Trace Level CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Lithium Ag 5-12,500 Er 0.02-25,000 Mo 2-25,000 Ta 0.04-25,000

Exploration As
B*
4-25,000
8-25,000
Eu
Fe
0.03-25,000 Nb
0.05%-25% Nd
0.8-25,000
0.07-25,000
Tb
Te
0.01-25,000
0.5-25,000
Lithium hosted in pegmatites Ba 2-25,000 Ga 0.5-25,000 Ni 10-25,000 Th 0.1-25,000
and jadarite can occur with ME-MS89L™ Be 0.4-25,000 Gd 0.03-25,000 Pb 0.5-25,000 Ti 0.005%-25% $41.10
economic grades of rare 0.2g sample Bi 0.1-25,000 Ge 0.5-25,000 Pr 0.03-25,000 Tl 0.02-25,000 *$5.55
earths and other trace metals Ca 0.1%-25% Ho 0.01-25,000 Rb 0.5-25,000 Tm 0.01-25,000 Add-on only
*B-MS89L
such as boron and cesium. Cd 0.8-25,000 In 0.3-25,000 Re 0.01-25,000 U 0.2-25,000
A sodium peroxide fusion Ce 0.2-25,000 K 0.05%-25% Sb 0.3-25,000 V 1-25,000
is required for complete Co 0.5-25,000 La 0.08-25,000 Se 3-25,000 W 0.3-25,000
recovery in these deposits. Cs 0.1-25,000 Li 2-25,000 Sm 0.04-25,000 Y 0.2-25,000
Cu 20-25,000 Lu 0.05-25,000 Sn 3-25,000 Yb 0.02-25,000
Dy 0.03-25,000 Mn 10-25,000 Sr 20-25,000 Zn 10-25,000
*B-MS89L - Glassless digestion and analysis to eliminate boron from labware

Intermediate and CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Ore Grade Lithium Al2O3 0.02%-100% Cu 0.01%-50% MnO 0.01%-50% TiO2 0.02%-83%
As 0.01%-10% Fe2O3 0.01%-100% Ni 0.005%-30% Zn 0.01%-60%
More elements may be ME-ICP89
CaO 0.01%-70% K 2O 0.01%-60% Pb 0.01%-30% $40.95
added to these methods, 0.2g sample
Co 0.005%-30% Li 0.001%-10% S 0.01%-60%
and they may be packaged
Cr2O3 0.01%-88% MgO 0.01%-50% SiO2 0.2%-100%
with ICP-MS finishes for
This package combines ME-ICP89 with ICP-MS determination of Nb, Ta, Sn, W, U
associated pegmatite-hosted MS91-PKG $55.35
and Th for an extended pegmatite exploration suite. 0.2g sample
commodities at trace levels.
Assay grade lithium and/or boron by Na2O2 fusion and
$19.90 one element
Li 0.001%-10% ICP-AES. Our highest precision method for Li and B resource
ME-ICP82b
B 0.02%-50% determination in known deposits.
$23.20 both elements
0.2g sample

Lithium In CODE ANALYTES & RANGES DESCRIPTION PRICE PER SAMPLE


Sedimentary Li-ICP41 Li 10ppm-1%
Aqua regia and ICP-AES finish. Multi-element
$6.85
package also available. 0.5g sample
Deposits Li-ICP61 Li 10ppm-1%
Four acid and ICP-AES finish. Multi-element
$9.55
package also available. 0.25g sample
In many cases, aqua regia
Ore grade Li by specialised four-acid digestion
provides better recovery of
Li-OG63 Li 0.005%-10% and ICP-AES finish. Best suited to Li-bearing $13.45
Li than four acid digestions silicate sediments. 0.4g sample
due to complex chemical Roasting samples prior to analysis may increase
reactions. Roasting samples RST-21 Dry roasting pre-treatment Li recovery due to excess water content $8.25
prior to four acid digestions, promoting insoluble salt formation.
particularly hectorite, may
mitigate this effect.

Lithium Brines CODE ANALYTES & RANGES (mg/L) PRICE PER SAMPLE
ALS analyses brine samples Includes a suite of 35 elements relevant to brine exploration
as received. If the samples ME-MS14b™ Li 0.01-10 in addition to Li. $27.40
Requires 50mL brine.
require acidification or
Ag 1-100 Cd 0.5-100 Mg 5-10,000 Sb 5-1,000
filtration in the lab, please
Al 100-10,000 Co 2-1,000 Mn 1-1,000 Sr 2-1,000
indicate this prominently on ME-ICP15
As 10-1,000 Cr 2-1,000 Mo 1-1,000 Ti 100-1,000
the sample submittal form.
Requires B 5-10,000 Cu 1-1,000 Na 100-150,000 V 1-1,000 $39.60
100mL Ba 10-1,000 Fe 100-10,000 Ni 2-1,000 Zn 1-1,000
brine
Be 0.1-100 K 500-150,000 P 100-1,000
Ca 50-10,000 Li 10-3,000 Pb 5-1,000
pH, Conductivity, Physical parameters and alkalinity of lithium brines.
Li-BrPKG $21.50
TDS, Alkalinity Requires 100mL brine.

Specific Ores & Commodities | 35


Uranium CODE ANALYTE PRICE PER SAMPLE
ALS is qualified and experienced An exploration package targeted at unconformity-hosted uranium deposits where
in handling NORM samples in the ore is in the basin sedimentary rocks. 1g sample
every area with active uranium
Includes full 62 element suite from ME-MS41L™. Includes REEs and Pb isotope
exploration and mining, with UEXP-PKG01 concentrations. $58.25
added lab certification in certain 204
Pb, 206Pb, 207Pb, 208Pb – 0.005-250ppm
jurisdictions. We are known
internationally for leading the Also includes ultra-trace boron by fusion from B-MS82L.
B – 5-10,000ppm
industry in lowest detection limits
and innovative solutions. Full 48 element suite from ME-MS61™, optimised for U with specific CRMs for
ME-MS61u™ superior quality control. $46.20
0.25g sample

Ore grade U assay (0.01%-15%).


U-XRF10* $20.50
2g sample

Ore grade U assay (0.01%- 51%). Fusion with oxidising flux.


U-XRF15b $36.10
0.5g sample
*For samples with >4% sulphide choose method U-XRF15b.

Ore Grade Rare CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Earth Elements Ce* 3-50,000 Ho 0.05-5,000 Rb 1-50,000 Tm 0.05-5,000
Dy* 0.3-5,000 La* 3-50,000 Sm* 0.2-5,000 U 0.3-5,000
Many REEs occur in minerals
ME-MS81h™ Er 0.2-5,000 Lu 0.05-5,000 Sn 5-50,000 W 5-50,000
resistant to acid digestion, so $54.25
0.1g sample Eu 0.2-5,000 Nb 1-5,000 Ta 0.5-5,000 Y 3-50,000
fusion is the preferred method of
Gd* 0.3-5000 Nd* 0.5-50,000 Tb* 0.05-5,000 Yb 0.2-5,000
decomposition. ALS offers ICP-MS/
Hf 1-50,000 Pr* 0.2-5,000 Th 0.3-5,000 Zr 10-50,000
ICP-AES and XRF determinations.
*These elements may be determined up to 30% by ME-OGREE.
These methods are most
appropriate for known ores;
CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
see the Whole Rock Analysis &
CeO2 0.01-50 Ho2O2 0.01-10 Sm2O3 0.01-10
Lithogeochemistry section for
Dy2O3 0.01-10 La2O3 0.01-50 Tb4O7 0.01-10
trace level methods. ME-XRF30
Er2O3 0.01-10 Lu2O3 0.01-10 Tm2O3 0.01-10 $36.10
0.7g sample
Eu2O3 0.01-10 Nd2O3 0.01-10 Y 0.01-10
Gd2O3 0.01-10 Pr6O11 0.01-10 Yb2O3 0.01-10
OA-GRA05x Furnace or Thermogravimetric Analyser (TGA) $6.05
Loss on Ignition
ME-GRA05 1g sample + $3.60 / temperature

Uncommon Metals CODE ANALYTE RANGE (ppm) DESCRIPTION PRICE PER SAMPLE
These elements have many high- Be-ICP81 Be 0.01%-100%
Sodium peroxide fusion and ICP-AES finish.
$19.90
tech applications in electronics, 0.2g sample

engineering and pharmaceuticals. NaOH fusion and ICP-MS finish for super trace B.
B-MS82L B 5-10,000 $22.30
0.5g sample
They require specialised
B 0.02%-100% Na2O2 fusion and ICP-AES finish. B and/or Li may $19.90 one element
digestions and instrument ME-ICP82b
Li 0.001%-10% be reported. 0.2g sample $23.20 both elements
methods for precise and accurate
HNO3-HF digestion with orthophosphoric acid
measurement. Ge-MS66 Ge 1-500
leach and ICP-MS finish. 0.5g sample
$34.15

Potash CODE ANALYTES & RANGES (%) PRICE PER SAMPLE


This package is designed for potash Al2O3 0.01-100 Fe2O3 0.01-100 P2O5 0.01-46
exploration to report total chemical BaO 0.01-66 K 2O 0.01-65 SO3 0.01-71
composition of samples as well as ME-XRF26k CaO 0.01-60 MgO 0.01-50 SiO2 0.05-100
$66.65
the proportion of analytes that can Cl 0.01-65 MnO 0.01-39 SrO 0.01-1.5 ME-POTPKG
be leached with water. ME-XRF26k Cr2O3 0.01-10 Na2O 0.01-55 TiO2 0.01-30 Sold only as a
is a fusion-XRF method that reports complete package
OA-GRA05x LOI 0.01-100 Fe2O3 0.01-100 P2O5 0.01-46
total content where ME-ICP03k is Ca 0.01 - 25 K 0.01 - 55 Na 0.01 - 42
ME-ICP03k
a water-leach method that reports Fe 0.01 - 50 Mg 0.01 - 25 S 0.01 - 30
soluble elements. OA-GRA04k OA-GRA04k Water Insoluble 0.5-100
provides the percentage of residue
insoluble in water using
a gravimetric method.

36 | Specific Ores & Commodities Schedule of services & fees | 2020


Bauxite Analysis CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
XRF is the industry-standard Al2O3 0.01-100 MgO 0.01-40 SrO 0.01-1.5
analytical method for bauxite ME-XRF13u BaO 0.01-10 MnO 0.01-31 TiO2 0.01-30 $45.20
(unnormalised)
analysis. Results are reported CaO 0.01-40 Na2O 0.01-5.3 V 2O5 0.01-8 Fused disc XRF. LOI determination
on a dry weight (110°C) basis by Cr203 0.01-10 P2O5 0.01-23 Zn 0.01-1.6 0.7g sample. must be done as
ME-XRF13n
default. Additional characterization (normalised) Fe2O3 0.01-100 SiO2 0.05-100 ZrO2 0.01-1.5 part of procedure.
methods such as organic carbon, K 20 0.001-6.3 SO3 0.01-12.5 Total 0.01-110
reactive silica and available Furnace or
alumina comply fully with CETEM OA-GRA05x Loss on Ignition. Thermo- $6.05
ME-GRA05 1g sample gravimetric +$3.60 /temperature
performance criteria. Multi-screen
Analyser (TGA).
sizing to determine the optimum
Total Organic Carbon (Non Carbonate Carbon), 0.02%-100%. TOC by
screen size for recovery and C-IR17
0.1g sample Combustion.
$34.15
subsequent wet beneficiation are Reactive Silica and Available Alumina, 0.1-100%. ME-LICP01 Microwave
also available. standard digestion temperature 145°C, ME-LICP02 standard digestion digestion,
ME-LICP01
temperature 235°C. Alternative temperatures, caustic strength and chemical $41.25 each
ME-LICP02
sample/caustic weight ratio may be requested by the client. separation and
1g sample ICP-AES analysis.
Fourier Transform
*Si-NIR07 Kaolinitic Silica, 0.4%-100%. 2g sample $5.10
infrared (FT-NIR).
*Si-NIR07 requires calibration to be set up with multiple samples from the same deposit that have been analysed by an
alternative technique for Kaolinitic Silica to set up a chemometric algorithm.

Nickel Laterite CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
The elements listed are reported ME-XRF12u* Al2O3 0.01-100 Fe2O3 0.01-100 Ni 0.005-7.8 Zn 0.001-1.6
(unnormalised)
by default, but others are CaO 0.01-40 K 2O 0.01-6.3 P2O5 0.005-23 Total 0.01-110 $45.20
available if they are significant ME-XRF12n*
Co 0.001-7 MgO 0.01-50 Pb 0.005-1.8 Fused disc XRF. LOI determination
in your deposit. Loss on Ignition (normalised) Cr2O3 0.005-10 MnO 0.005-30 SiO2 0.05-100 must be done as
0.7g sample part of procedure.
(LOI) is an important component Cu 0.001-1.6 Na2O 0.01-5.3 TiO2 0.01-30
of the total analysis. Furnace or
$6.05
OA-GRA05x Loss on Ignition
Thermogravimetric
ME-GRA05 1g sample +$3.60 /temperature
Analyser (TGA)
*Scandium may be added for an additional cost.

Phosphates CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
The elements listed are reported Al2O3 0.01-100 K 2O 0.01-10 Na2O 0.01-11 TiO2 0.01-30 $45.20
ME-XRF24*
by default, but others are 0.7g CaO 0.01-60 MgO 0.01-50 P2O5 0.01-50 Total 0.01-110 Fused disc XRF.
LOI determination
available if they are significant must be done as
sample
Fe2O3 0.01-100 MnO2 0.01-48 SiO2 0.01-100 part of procedure.
in your deposit. Loss on Ignition
(LOI) is an important component Furnace or
OA-GRA05x Loss on Ignition $6.05
Thermogravimetric
of the total analysis. ME-GRA05 1g sample +$3.60 /temperature
Analyser (TGA).
*Fluorine may be added for an additional cost.

Chromite and CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Manganese Ores ME-XRF26s
Al2O3 0.01-100 Fe2O3 0.01-100 Na2O 0.01-10 TiO2 0.01-30 $45.20
BaO 0.01-66 K 2O 0.01-15 P2O5 0.01-46 Total 0.01-110 LOI determination
The elements listed are reported 0.7g Fused disc XRF. must be done as
sample CaO 0.01-60 MgO 0.01-50 SO3 0.01-34
by default, but others are part of procedure.
Cr2O3 0.01-60 MnO 0.01-80 SiO2 0.05-100
available if they are significant
Furnace or
in your deposit. Loss on Ignition OA-GRA05x Loss on Ignition $6.05
Thermogravimetric
(LOI) is an important component ME-GRA05 1g sample +$3.60 /temperature
Analyser (TGA).
of the total analysis.

Specific Ores & Commodities | 37


Aqua Regia CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Overlimit Methods Ag 1-1,500ppm Co 0.0005-30 Mn 0.01-60 Pb 0.001-20 $9.60
(+)-OG46
As 0.001-60 Cu 0.001-50 Mo 0.001-10 S 0.01-10 +$2.65 /element
Aqua regia is a powerful 0.4g sample
solvent for sulphides, silver Cd 0.001-10 Fe 0.01-100 Ni 0.001-30 Zn 0.001-30
and base metals. This
method may be triggered
automatically on multi-
element geochemistry
packages.

Four Acid Overlimit CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Methods Ag 1-1,500ppm Co 0.0005-30 Mg 0.01-50 Pb 0.001-20
(+)-OG62 As 0.001-30 Cr 0.002-30 Mn 0.01-60 S 0.01-50 $12.35
Four acid digestion breaks
0.4g sample Bi 0.001-30 Cu 0.001-50 Mo 0.001-10 Zn 0.001-30 +$2.65 /element
down most silicates and
Cd 0.001-10 Fe 0.01-100 Ni 0.001-30
all but the most resistive
minerals. This method may
be triggered automatically on
multi-element geochemistry
packages.

Titration Methods CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Certain ore deposits naturally Cu-VOL61 Cu 0.01-100 Cu by Titration. 0.5g sample $47.85
have extremely high (>30%) Zn-VOL50 Zn 0.01-100 Zn by Titration. 1g sample $27.40
base metal content over
Pb-VOL70 Pb 0.01-100 Pb by Titration. 1g sample $41.00
short intervals. Specialised
Fe-VOL51 Fe 0.01-100 Total Fe in Concentrates by titration. 1g sample $48.85
digestions and classical
chemistry methods are Fe-VOL05 FeO 0.01-100 Ferrous Iron (FeO) by titration. 1g sample $24.20
required to analyse these
samples.

XRF For Resistive CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Minerals (+)-XRF10
Ba 0.009-45 Sn 0.01-60 W 0.01-50
Nb 0.01-10 Ta 0.01-50 Zr 0.01-50 $16.45
Some resistive minerals, 2g sample
Sb 0.01-50 Th 0.01-15 + $4.05 /element
particularly those containing
+ Add element symbol as prefix to method code. NOTE: This method is suitable for elements reporting over-range by ME-MS81
Sn, W, Nb or Ta, require a
fusion for complete recovery.
This method is only suitable
for samples with <4%
sulphides.

38 | Specific Ores & Commodities Schedule of services & fees | 2020


Sodium Peroxide CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Fusion & ICP-AES Al 0.01-50 Cr 0.01-30 Mg 0.01-30 S 0.01-60 $42.20 full package

Na2O2 fusions are used ME-ICP81 As 0.01-10 Cu 0.002-30 Mn 0.01-50 Si 0.1-50 or $13.65
0.2g sample Ca 0.05-50 Fe 0.05-70 Ni 0.002-30 Ti 0.01-30 + $2.65 /element
for sulphides, arsenides,
chromite, rutile, ilmenite Co 0.002-30 K 0.1-30 Pb 0.01-30 Zn 0.002-30
and titanite. This selection is
designed for nickel sulphides,
but elements are also
available individually.

Oxidizing Fusion & CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
XRF Finish Al₂O₃ 0.01-100 Fe 0.01-75 P₂O₅ 0.01-25 Th 0.002-5
As 0.01-10 HfO₂ 0.01-10 Pb 0.005-20 TiO₂ 0.01-30
Samples are analysed by XRF
BaO 0.01-66 K₂O 0.01-6.3 Rb 0.005-5 U 0.001-5
following a lithium borate
Bi 0.01-5 La₂O₃ 0.01-50 S 0.01-20 V 0.01-5.6
fusion with the addition of ME-XRF15b*
CaO 0.01-40 MgO 0.01-40 Sb 0.005-20 W 0.001-15.9 $36.10
strong oxidizing agents to 0.5g sample
CeO₂ 0.01-50 Mn 0.01-30 SiO₂ 0.01-100 Zn 0.005-20 + $3.80 /element
decompose sulphide-rich
ores. Co 0.01-7 Mo 0.005-2 Sn 0.005-20 Zr 0.01-20
Cr 0.01-10 Nb 0.005-20 Sr 0.01-5
Other elements are available Cu 0.005-20 Ni 0.005-20 Ta 0.002-16.4
to report on request. LOI may
OA-GRA05x Furnace or Thermogravimetric Analyser (TGA). $6.05
be optionally added to this Loss on Ignition**
ME-GRA05 1g sample + $3.60 /element
method, but it is not used to
normalise results. *Na is not reportable due to the oxidising flux used in sample preparation. **LOI is required as part of the ME-XRF15b method.

Base Metal CODE ANALYTES & RANGES (%) PRICE PER SAMPLE
Concentrates By Al2O3 0.01-100 MgO 0.01-40 Sn 0.01-79

XRF As
Ba
0.01-10
0.01-50
Mn
Mo
0.01-30
0.01-60 TiO2
Ta 0.01-41
0.01-50
Samples are analysed by XRF Bi 0.01-5 Nb 0.01-35 V 0.01-5.6
following a lithium borate ME-XRF15c* CaO 0.01-40 Ni 0.01-50 WO3 0.01-100 $46.55
fusion with the addition 0.25g sample Co 0.01-7 P 0.01-10 Zn 0.01-50 + $3.80 /element
of strong oxidizing agents Cr 0.01-10 Pb 0.01-32 Zr 0.01-20
to decompose sulphide Cu 0.01-50 S 0.01-40 Total 0.01-110
concentrates. Fe 0.01-75 Sb 0.01-80
Other elements are available K 2O 0.01-6.3 SiO2 0.01-100
to report on request. LOI may OA-GRA05x Furnace or Thermogravimetric Analyser (TGA). $6.05
Loss on Ignition**
be optionally added to this ME-GRA05 1g sample + $3.60 /element
method, but it is not used to *Na is not reportable due to the oxidising flux used in sample preparation. **LOI is required as part of the ME-XRF15c method.
normalise results.

Intermediate CODE ANALYTES & RANGES (%) PRICE PER SAMPLE


Level Oxidising Ag 1-1500ppm Co 0.001-20 Mn 0.005-50 S 0.05-50

Digestion ME-ICPORE
As
Bi
0.005-30
0.005-30
Cu
Fe
0.001-40
0.01-100
Mo
Ni
0.001-10
0.001-30
Sb
Tl
0.005-100
0.005-1 $27.65
A strong oxidising digestion Ca 0.01-50 Hg 8-10000ppm P 0.01-20 Zn 0.002-100
utilising HNO3, KClO3 and Cd 0.001-10 Mg 0.01-50 Pb 0.005-30
HBr with aqua regia is
applicable to basemetal ores
and particularly suitable for
massive sulphides.

Specific Ores & Commodities | 39


Carbon,
Sulphur, ARD &
Concentrates
The following pages describe methods useful in resource
estimation, process metallurgy, and characterization and
umpire services for bulk concentrates. The wide variety
of sulphur and carbon minerals and compounds present
in many deposits can complicate the determination of
acid drainage potential or oxygenation requirements for
ore processing. Likewise, target element deportment may
not be revealed by geochemical analysis and assays only;
process mineralogy is often required to fully characterise
the location of key economic and penalty elements,
with implications for mineral processing design and
environmental remediation.

Please submit at least four times the


nominal sample weight for efficient service.
Sulphur Methods CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Accurate sulphur speciation can S-IR08 S (Total) 0.01%-50%
Total sulphur by induction furnace/IR
$16.45
be crucial to early identification 0.1g sample

of recovery and environmental Solvent leach, gravimetric finish.


S-GRA07 S (Elemental) 0.01%-100% $36.85
3g sample
issues on many projects.
HCl (15%) leach of sulphates, gravimetric
Variations on the most common finish. Note: little to no dissolution of
speciation methods can be S-GRA06a S (Sulphate) 0.01%-50% $30.10
barite/celestite.
implemented to suit your project’s 1g sample
specific mineralogy; please HCl (25%) leach of sulphates, Leco furnace.
contact client services in your Note: little to no dissolution of barite/
S-IR06a S (Sulphide) 0.01%-50% $21.85
celestite.
region for more information.
0.1g sample
NaCO3 leach of sulphates, gravimetric finish.
S-GRA06 S (Sulphate) 0.01%-40% $34.15
1g sample
NaCO3 leach of sulphates, induction furnace/IR.
S-IR07 S (Sulphide) 0.01%-50% $34.15
0.1g sample

Sulphur and CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Carbon Packages ME-IR08
C (Total) and
S (Total)
0.01%-50% Total carbon and sulphur by induction furnace/
0.01%-50% IR. 0.1g sample
$22.85
These elements are often Organic carbon and sulphide sulphur by HCI
C (Organic) and 0.01%-50%
determined together, so ALS ME-IR06a (25%) leach of carbonates and sulphates, $30.55
S (Sulphide)* 0.01%-50%
provides several economic induction furnace/IR. 0.1g sample
packages for convenience. *Sulphide sulphur may be overstated if BaSO4 or SrSO4 are present.

Carbon Methods CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
Carbon has important Total carbon by induction furnace/IR.
C-IR07 C (Total) 0.01%-50% $16.45
metallurgical and environmental 0.1g sample
implications for many types of HCl (25%) leach of carbonates, induction
C-IR06a C (Organic) 0.01%-50% furnace/IR. Other acid strengths available. $21.85
mineral deposits. Carbonates may
0.1g sample
consume acid, impacting leach
HClO4 digestion and CO2 coulometer.
process design and mine waste C-GAS05 CO2 (Carbonate) 0.2%-50% $23.10
0.1g sample
remediation, while preg robbing HCl (50%) leach of carbonates, roasting to
by organic carbon can interfere C-IR18 C (Graphite) 0.02%-50% remove organic carbon, induction furnace/IR. $35.55
with the cyanidation of gold and 0.1g sample
silver ores. C (Non- Dilute acid digestion followed by combustion furnace.
C-IR17 0.02%-100% $34.15
Carbonate) 0.1g sample
Requires
C-CAL15 C (Carbonate) 0.02%-100% Carbonate carbon by difference.
C-IR07, C-IR17

Carbon, Sulphur, ARD & Concentrates | 41


Acid-Base PARAMETERS ABA-PKG01(M/S) ABA-PKG04(M/S) ABA-PKG05(M/S/B) ABA-PKG06E*
Accounting
Net Neutralization Potential (NNP) √ √ √
Acid-base accounting
Maximum Potential Acidity (MPA) √ √ √
(ABA), also called static
Neutralization Potential (NP) & Fizz √ √ √
testing, calculates a net
neutralization potential Ratio (NP : MPA) √ √ √
(NNP) representing the Neutralization Potential (EN 15875 NP) √
ability of a body of rock Acid Potential (EN 15875 AP) √
to produce acid rock
Maximum Acid Potential (EN 15875 AP Max) √**
drainage or to neutralise
free acid. Neutralization Potential Ratio (EN 15875 NPR) √
Net Neutralization Potential (EN 15875 NNP) √
The choice of package will
depend on the method Paste pH √ √ √

of determining the Sulphate by ICP √


neutralizing potential that HCl-leachable Sulphate √ √
is required by law in your
Total Sulphate (Carbonate Leach) √
region, this information
Sulphide (calculated) √ √ √
can be obtained from your
local regulatory agency. Sulphide (analysed) √** √** √**
Total Sulphur √ √ √ √
Minimum sample size
for all ABA packages Inorganic Carbon (CO2) √ √
is 100g. Inorganic Carbon (calculated) √

Sulphide is determined Organic Carbon √


by calculation in these Total Carbon √
packages. If you Sobek Method √ √ √
would prefer sulphide
Modified Sobek (M) Option √ √ √
determined by analysis,
Siderite Correction (S) Option √ √ √
add A to the package
code. (additional cost.) MEND Method (B) Option √
EN 15875 Method Option √
* meets EU regulations. ** optional parameter. See client services for pricing.

Net Acid CODE DESCRIPTION PRICE PER SAMPLE


Generation OA-VOL11
Net Acid Generation. Hydrogen peroxide is used to rapidly oxidise sulphides.
By Quotation
NAG is reported in kg H2SO4 /tonne at pH 4.5 and pH 7.0. 2.5g sample
NAG provides a quantitative
estimation of the acid that can be
generated by mine waste.

42 | Carbon, Sulphur, ARD & Concentrates Schedule of services & fees | 2020


Humidity Cells & CODE DESCRIPTION PRICE PER SAMPLE
Metal Leaching OA-HCTSET Humidity cell set-up and maintenance fees.
Tests to quantify metal leaching By Quotation
Periodic analysis of humidity cell leachate.
from mine waste under meteoric OA-HCT01 Many instrument finishes, particle sizes and sample weights are available;
conditions can range from simple please enquire.
shake flask analysis to long term
column leaches. Many analytical
options are possible on the
leaches; prices will vary based on
analytical package requested.

Various Elements CODE ANALYTES & RANGES (%) DESCRIPTION PRICE PER SAMPLE
in Concentrates Zn Mo
Appropriate digestion and titration
All control assays are overseen (+)-CON02 Cu Co 0.01%-100% or gravimetric finish. $82.00 /element
4g sample
by experienced certified assayers Pb Ni
and analysed in duplicate at Four acid digestion and AAS finish.
As-CON01 As 0.01%-15% $82.00
a minimum to assure quality. 1g sample
Umpire assays are also available – HCl digestion and ICP-AES finish.
Hg-CON01 Hg 1-10,000ppm $82.00
please enquire. 1g sample
KOH fusion and ion selective
Precious metals in concentrates
F-CON01 F 20-20,000ppm electrode. $99.15
and bullion are found in the 0.2g sample
Precious Metals section.
+ Add element symbol as prefix to method code. More elements are available. Please enquire.

High-Grade Multi- CODE ANALYTES & RANGES (ppm) PRICE PER SAMPLE
Element Analysis Ag 0.1-1,000 Fe 0.02%-100% Ni 2-100,000 Th 2-5,000
Al 0.02%-100% Ga 0.5-5,000 P 100-100,000 Ti 0.01%-100%
This is a four acid multi-element
As 2-100,000 Ge 0.5-5,000 Pb 5-100,000 Tl 0.2-5,000
procedure specifically designed for
Ba 50-100,000 Hf 1-5,000 Rb 1-5,000 U 1-10,000
major, minor and trace elements
Be 0.5-10,000 In 0.05-2,500 Re 0.02-500 V 5-100,000
in high-grade samples and
Bi 0.1-100,000 K 0.02%-100% S 0.05%-10% W 1-100,000
concentrates. Extra care is taken ME-MS61c™
Ca 0.05%-100% La 5-5,000 Sb 0.5-10,000 Y 1-5,000 $273.25
with senior staff reviewing the 0.4g sample
Cd 0.2-5,000 Li 2-5,000 Sc 1-10,000 Zn 20-100,000
results in detail.
Ce 0.1-5,000 Mg 0.02%-100% Se 10-10,000 Zr 5-5,000
Aqua regia/ICP-MS and oxidizing Co 1-100,000 Mn 10-100,000 Sn 2-5,000
fusion/XRF options are also Cr 10-100,000 Mo 0.5-100,000 Sr 2-100,000
available. Cs 0.5-5,000 Na 0.02%-100% Ta 0.5-1,000
Cu 2-100,000 Nb 1-5,000 Te 0.5-5,000

Industrial Minerals CODE ORE/PRODUCT ANALYTES DESCRIPTION PRICE PER SAMPLE


Industrial minerals commonly ME-XRF26*
Cementitious Al2O3, CaO, Fe2O3, K 2O, LOI, MgO, MnO, Fusion, XRF
$24.50
have highly refractory components Materials Na2O, SiO2, SO3, TiO2 0.7g sample

requiring aggressive digestions. Chromite and Al2O3, BaO, CaO, Cr2o3 Fe2O3, K 2O, MgO, Fusion, XRF
ME-XRF26s* $45.20
Manganese Ore MnO, Na2O, P2O5, SO3, SiO2, TiO2 0.33g sample
These methods are designed
Limestone, Dolomite, Fusion, ICP-AES
to completely dissolve the ME-ICP86
Magnesite, Magnesia
CaO, MgO, Al2O3, Fe2O3, SiO2, LOI
0.1g sample
$48.20
analytical sub-sample, leaving no
* LOI determination must be performed as part of this procedure and incurs additional cost.
inhomogenous residual material
behind.

Carbon, Sulphur, ARD & Concentrates | 43


ALS Mineralogy CODE ANALYSIS RANGE OF SERVICE
ALS Mineralogy has a market BMA
QEMSCAN Bulk Mineral Mineral composition, elemental deportment and assay reconciliation.
leading position in the Analysis

range and capabilities of QEMSCAN Bulk Mineral Mineral composition, estimate of the liberation, elemental deportment and
BMAL
Analysis with Liberation assay reconciliation.
our automated mineralogy
MLA Bulk Mineral and XBSE analysis with additional X-Ray mapping of similar-appearing gangue or
equipment, which includes MIN-GXMAP Textural Analysis with minerals of interest to improve grain segmentation (for texturally complex or
the Mineral Liberation X-Ray Mapping finely intergrown samples)
Analyser (MLA), QEMSCAN®, MLA Sparse phases - Au, Data for requested minerals only - does not include bulk mineralogy data
X-ray Diffraction, TIMA and Ag, PGE, U minerals etc. - Mineral List and relative abundances, elemental distributions, particle
HyLogger™. MIN-SPL present at ppm to ppt size and grain size distributions, mineral liberation, locking and association
levels or losses of minerals data, particle image line ups, - includes high resolution photomicrographs of
Quantitative mineralogical data of interest to tails typical minerals of interest.
are an essential component in Mineral List and abundances (to <0.5 Wt%), elemental distributions, particle
a range of applications such as MLA Bulk Mineral and size and grain size distributions, mineral liberation, locking and association
MIN-XBSE
Textural Analysis data, grade recovery curves, particle image line ups, assay reconciliation -
processing mineralogy, plant
includes spread sheet reporting - additional reporting options available.
surveys, ore characterization,
MLA Bulk Mineral Analysis Mineral List and abundances (to ~0.5-1 Wt%), elemental distributions,
precious metal and trace MIN-XMOD
by X-Ray Point Counting chemical assay reconciliation - includes basic spreadsheet reporting.
mineral characterization, and QEMSCAN Particle Mineral Mineral composition, abundance, liberation, locking, association, elemental
PMA
geometallurgy analyses. Analysis deportment and assay reconciliation. Typically includes 4-5 size fractions.
QEMSCAN Trace Mineral Trace mineral characterisation includes liberation, locking, association and
Access to state-of-the art TMS
Search size. Cost is dependent on grade and desired number of grains for analysis.
technology and a highly
Fully quantitative XRD, including the quantification of the amorphous material
trained technical team ensures XRDQ Quantitative XRD
present.
that your requirements are met Mineral abundance, normalised over the crystalline content, excluding the
with high-quality data fit for XRDSQ Semi-quantitative XRD
quantification of amorphous material.
your purpose.
All prices are by quotation. Please contact ALS for more information.
Contact us to determine
methods and pricing specific
for your project.
Additional reporting options are also available on request.
Mineralogical data available from our range of technologies include:

• Mineral species, compositions, and abundances • Annotated high-resolution maps and mineral
• Elemental deportment line-ups
• Mineral grain and particle size distribution • SEM backscatter images
• Grain size and grain texture data • SEM particle maps
• Mineral liberation including association and locking • Cathodoluminescence imaging
• Mineral grade and element grade recovery curves • Mineral x-ray and wavelength spectra summary
• Colour-coded particle maps and minerals line-ups • XRD analyses of all crystalline materials

Copper sulphides Micas


Pyrite Chlorite
Iron oxides Titanium minerals
Feldspars Apatite
Carbonates Other minerals
Quartz

Americas Australia
Kamloops Perth Brisbane
2957 Bowers Place, 6 MacAdam Place, Balcatta 32 Shand St, Stafford
Kamloops BC V1S 1W5 Western Australia 6021 Queensland 4053
T +1 250 828 6157 T +61 8 9344 2416 T +61 7 3243 7152
F +1 250 828 6159 F +61 8 9345 4688 F +61 7 3243 7218
metallurgy.kamloops@alsglobal.com metallurgy@alsglobal.com mineralogy@alsglobal.com

44 | Carbon, Sulphur, ARD & Concentrates Schedule of services & fees | 2020


Quality
Management
Systems
ISO/IEC 17025:2017 ISO/IEC 17025:2017 ISO/IEC 17025:2017 ISO/IEC 17025:2017
Providing exceptional quality Accredited Methods Accredited Methods Accredited Methods Accredited Methods
assays to our clients is one of the in North America* in Romania* in Turkey* in Laos*

cornerstones of ALS’s business


model. We achieve this via a
global quality program that has
been strategically designed to
integrate quality requirements
into every process from sample
preparation through analysis. It
is an integral part of day-to-day ISO/IEC 17025:2017 Accredited Methods and ISO ISO/IEC 17025:2017 ISO/IEC 17025:2017 Accredited
9001:2015 Registration in Peru* Accredited Methods Methods and ISO 9001:2015
activities, involves all levels of in Ireland Registration in Australia*
ALS staff, and is monitored at
top management levels. The
global quality program includes
inter-laboratory test programs
and regularly scheduled internal
audits that meets all requirements ISO/IEC 17025:2017 Accredited Methods in Zambia* ISO/IEC 17025:2017 Accredited
of ISO/IEC 17025:2017 and ISO Methods in South Africa and Ghana*
9001:2015.
All ALS Geochemistry hub and
many multi-purpose laboratories
are accredited to ISO/IEC
17025:2017 for specific analytical
procedures.
ISO/IEC 17025:2017 Accredited Methods and ISO 9001:2015 Registration in China*
* Please contact us for details
regarding ISO/IEC 17025:2017
accreditation and scopes of
accreditation; or ISO 9001:2015
certification at individual labs.

ISO 9001:2015 ISO 9001:2015 ISO/IEC 17025:2017


Registration in Spain* Registration in Accredited Methods in
Chile* Mongolia*

ISO/IEC 17025:2017 ISO/IEC 17025:2017


Accredited Methods in Accredited Methods in Russia*
Kazakhstan*

Open Lab™ Initiative


The Open Lab™ Initiative is about enabling complete confidence in the accuracy of data produced by ALS
through transparency in the laboratory process.
Through the Open Lab™ Initiative, we provide access to all of your results in perpetuity and the ability to track
sample status in real time through Webtrieve™, our on-line interface to laboratory data. Webtrieve™ also
displays complete chain of custody audit trails, important QC data, and standard reference material control
charts relevant to your samples. Please ask your local laboratory to have a Webtrieve™ account set up for you.

| 45
Selected Terms & Conditions
1. Terms and Conditions d) All fees due and payable after the Due Date (Outstanding 5. Termination
Amount) will be subject to the payment of interest at a
Complete Terms and conditions of service are included a) ALS may suspend or terminate its obligations under this
rate of 1.5% per month of the Outstanding Amount from
with each service quotation provided to clients. The Agreement if (a) monies payable to ALS by the client are
the Due Date up to and including the date of payment,
following lists some of the key terms and conditions that outstanding 60 days or more (unless otherwise agreed)
unless ALS and the Client otherwise agree in writing.
will be applicable to every quotation for work. after the date of invoice, (b) other substantial breach by
e) The Client will indemnify ALS for any fees incurred by ALS the Client of their obligations under the Agreement, which
2. Provision of Services to recover the Outstanding Amount, including any solicitor breach is not remedied within 30 days of written notice
fees, or collection agency fees. from ALS requiring the breach to be remedied, (c) by
a) The Client acknowledges that it is the Client’s sole giving the Client 60 days written notice of ALS’s intention
responsibility to make its own assessment of the to terminate.
4. Limitation of Liability
suitability for any purpose of the Services, detection limits
and confidence intervals inherent in ALS’s standard testing a) To the full extent permitted by law, ALS excludes all b) The Client may terminate its obligations under this
methodology, the ALS Report and its contents. warranties, terms, conditions or undertakings (Terms), Agreement in the event of a substantial breach by ALS of
whether expressed or implied, in relation to the Services, its obligations under the Agreement, which breach has not
b) If the Client requires the Services to be performed by been remedied within 30 days of written notice from the
the ALS Report, or its contents. Where any legislation
specific test method, or requires detection limits and/ Client to ALS requiring the breach to be remedied.
implies any Terms in this Agreement that cannot be
or confidence intervals different to those inherent in
modified or excluded then, such Terms shall deem to be
ALS’s standard testing methodology, then the Client must c) If ALS, acting reasonably, suspects that the Client is
included. However, to the full extent permitted by law,
instruct ALS of such a variation prior to ALS performing the insolvent or is having difficulties paying its debts as and
ALS’s liability to the Client for any breach of any Terms that
Services. when they become due, or the Client is insolvent, ALS
cannot be excluded by law is limited at ALS’s option to the
may give written notice to the Client of ALS’s intention to
c) ALS may transfer samples within its laboratory network re-performance of the Services or the refund of the fee for
immediately suspend or terminate is obligations under this
to maximise efficiencies and improve turnaround of the the Services.
Agreement.
samples. No additional cost will be charged to the client
b) Notwithstanding any other provision in this Agreement,
for this service optimisation measure. d) In the event of termination, ALS is entitled to be paid for
the cumulative liability of ALS under this Agreement to the
all work performed before the date of termination and for
Client and any third party is limited for any claim for loss
3. Fees and Payment any unavoidable commitments entered into by ALS before
or damage whatsoever, whether arising in tort or contract
the date of termination.
a) ALS reserves the right to review prices at any time if or any other cause of action, to the value of the Services
significant changes to ALS’s costs are incurred that are provided by ALS to the Client.
6. Confidential Information
beyond ALS’s control. Such changes may include, but c) Notwithstanding any other provision in this Agreement,
are not limited to, changes in legislative requirements, a) Neither ALS nor the Client will disclose Confidential
the cumulative liability of ALS under this Agreement to the
Client variations to sample numbers, analytes requested, Information of the other party to any third party without
Client and any third party is limited for any claim for loss
turnaround required, or reporting requirements. the prior written consent of the other party, unless
or damage whatsoever, whether arising in tort or contract
required by law or the rules of a relevant stock exchange.
b) Payment terms, subject to approved credit, are payment or any other cause of action, to the value of the Services
in full, 30 days from the date of invoice (Due Date), unless provided by ALS to the Client. b) ALS and the Client will only use Confidential Information
otherwise agreed in writing prior to the placement of an of the other party for the purpose of the supply of the
d) The Client acknowledges that during the performance of
order or submission of samples. Services.
the Services, any samples supplied by, or on behalf of,
c) All prices quoted by ALS are exclusive of GST (or other the Client or parts thereof may be altered, lost, damaged
or destroyed. ALS will not be liable whatsoever to the Please refer to the ALS Website for full Terms and
value added tax if relevant) unless stated otherwise.
Client or any third party for any samples so altered, lost, Conditions
damaged or destroyed.

46 | Schedule of services & fees | 2020


Global Locations
71 commercial laboratories • >20 on-site laboratories

Sweden
Malå
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Our integrated network of Our services are available through


71 laboratories around the world any one of the many general service
ensures consistent quality and laboratories listed on these pages.
dependable client service wherever we We also provide custom services for
might meet you. on-site laboratory and sample preparation
facilities, as well as mobile laboratories
and sample preparation installations.

Visit our website for complete location details at


alsglobal.com/locations

Global Locations | 47
ARGENTINA CANADA CHINA
Mendoza ClientServicesECAN@alsglobal.com Guangzhou
+54 261 431 9880 ClientServicesWCAN@alsglobal.com +86 20 3687 5966
alsgeo.mendoza@alsglobal.com Kamloops alsgeo.guangzhou@alsglobal.com
+1 250 573 5700
AUSTRALIA alsgeo.kamloops@alsglobal.com COLOMBIA
Adelaide Lebel-sur-Quévillon Medellin
+61 8 8359 0890 +1 819 753 7293 +57 4 306 9122
alsgeo.adelaide@alsglobal.com alsgeo.lebel@alsglobal .com alsgeo.medellin@alsglobal.com
Brisbane Moncton
+61 7 3243 7222 +1 506 855 4269 ECUADOR
alsgeo.brisbane@alsglobal.com alsgeo.moncton@alsglobal.com Quito
Burnie Rouyn-Noranda +59 32 247 6475
+61 3 6431 6333 +1 819 797 2810 alsgeo.quito@alsglobal.com.ec
alsgeo.burnie@alsglobal.com alsgeo.rouyn-noranda@alsglobal.com
Kalgoorlie Sudbury ETHIOPIA
+61 8 9021 1457 +1 705 560 7225 Addis Ababa
alsgeo.kalgoorlie@alsglobal.com alsgeo.sudbury@alsglobal.com +251 9454 36 909
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+61 7 4740 1700 +1 250 635 3309
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+61 8 9347 3222 +1 705 360 1987 +358 50 570 7141
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+61 7 4796 0600 +1 819 825 0178 GHANA
alsgeo.townsville@alsglobal.com alsgeo.valdor@alsglobal.com Kumasi
Vancouver +233 54 444 4440
BOLIVIA +1 604 984 0221 alsgeo.kumasi@alsglobal.com
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+56 51 267 2783
CAMBODIA alsgeo.laserena@alsglobal.com
Phnom Penh Santiago
+855 99 434 534 +56 2 2654 6100
alsgeo.phnompenh@alsglobal.com alsgeo.santiago@alsglobal.com

48 | Global Locations Schedule of services & fees | 2020


LAOS PERU SWEDEN
Pakse Arequipa Malå
+856 20 2271 1091 +51 54 46 3649 +46 911 65 800
alsgeo.pakse@alsglobal.com alsgeo.arequipa@alsglobal.com alsgeo.mala@alsglobal.com
Vientiane Lima Piteå
+856 21 31 3438 +51 1 574 5700 +46 911 65 800
alsgeo.vientiane@alsglobal.com alsgeo.lima@alsglobal.com alsgeo.piteab@alsglobal.com
Cajamarca
LIBERIA +51 947 737 799 TURKEY
Monrovia alsgeo.cajamarca@alsglobal.com Izmir
+233 244 314509 +90 232 281 71 10
alsgeo.monrovia@alsglobal.com ROMANIA alsgeo.izmir@alsglobal.com
Rosia Montana
MALI +40 258 780 395 USA
Bamako alsgeo.rosiamontana@alsglobal.com ClientServicesUSA@alsglobal.com
+223 223 6949 Elko
alsgeo.bamako@alsglobal.com RUSSIA +1 775 738 2054
Chita alsgeo.elko@alsglobal.com
MAURITANIA +7 3022 368038 Fairbanks
Nouakchott alsgeo.chita@alsglobal.com +1 907 452 2188
+222 45290034 Moscow alsgeo.fairbanks@alsglobal.com
alsgeo.nouakchott@alsglobal.com +7 495 419 0474 Reno
alsgeo.moscow@alsglobal.com +1 775 356 5395
MEXICO alsgeo.reno@alsglobal.com
ClientServicesMEX@alsglobal.com SAUDI ARABIA Tucson
Chihuahua Jeddah +1 520 747 3218
+52 614 417 9728 +966 12 6361199 alsgeo.tucson@alsglobal.com
alsgeo.chihuahua@alsglobal.com alsgeo.jeddah@alsarabia.com
Guadalajara ZAMBIA
+52 33 3619 7438 SERBIA Ndola
alsgeo.guadalajara@alsglobal.com Bor +26 0 979 376284
Hermosillo +381 648243340 alsgeo.ndola@alsglobal.com
+52 662 218 4403 alsgeo.bor@alsglobal.com
alsgeo.hermosillo@alsglobal.com
Zacatecas SOUTH AFRICA
+52 492 768 1474 ClientServicesAfrica@alsglobal.com
alsgeo.zacatecas@alsglobal.com Johannesburg
+27 11 608 0555
MONGOLIA alsgeo.johannesburg@alsglobal.com
Ulaanbaatar
+976 11 343882 SPAIN
alsgeo.ulaanbaatar@alsglobal.com Seville
+34 9555 13 035
MYANMAR alsgeo.seville@alsglobal.com
Mandalay
+95 9 447367745 SUDAN
alsgeo.mandalay@alsglobal.com Atbara
+24 9900 598 990
NAMIBIA alsgeo.atbara@alsglobal.com
Okahandja
+264 644 06498
alsgeo.okahandja@alsglobal.com

Global Locations | 49
Reactive nonmetal Alkaline earth metal Lanthanide Metalloid Noble gas
Alkali metal Transition metal Actinide Post-transition metal Unknown chemical properties
PERIODIC TABLE OF ELEMENTS
1.008 4.0026
[1.0078, 1.0082]
More than two digestion methods are
METHOD OPTIONS FOR THE DECOMPOSITION available for most elements and outcome
HYDROGEN OF GEOLOGICAL MATERIALS is dependent on geological type. HELIUM

6.94 9.0122 10.81 12.011 14.007 15.999 18.998 20.180


[6.938, 6.997] [10.806, 10.821] [12.009, 12.012] [14.006, 14.008] [15.999, 16.000]
Atomic number Lithium borate fusion
Atomic weight Sodium peroxide fusion

LITHIUM BERYLLIUM Element symbol Fire assay (lead or nickel sulfide collection methods) BORON CARBON NITROGEN OXYGEN FLUORINE NEON
Isotopic analysis available Aqua regia
22.990 24.305 26.982 28.085 30.974 32.06 35.45 39.95
[24.304, 24.307] [28.084, 28.086] [32.059, 32.076] [35.446, 35.457] [39.792, 39.963]

Primary option Four acid


Secondary option Other (combustion, specialty)
SODIUM MAGNESIUM ALUMINIUM SILICON PHOSPHORUS SULFUR CHLORINE ARGON

39.098 40.078(4) 44.956 47.867 50.942 51.996 54.938 55.845(2) 58.933 58.693 63.546(3) 65.38(2) 69.723 72.630(8) 74.922 78.971(8) 79.904 83.798(2)
[79.901, 79.907]

POTASSIUM CALCIUM SCANDIUM TITANIUM VANADIUM CHROMIUM MANGANESE IRON COBALT NICKEL COPPER ZINC GALLIUM GERMANIUM ARSENIC SELENIUM BROMINE KRYPTON

85.468 87.62 88.906 91.224(2) 92.906 95.95 101.07(2) 102.91 106.42 107.87 112.41 114.82 118.71 121.76 127.60(3) 126.90 131.29

RUBIDIUM STRONTIUM YTTRIUM ZIRCONIUM NIOBIUM MOLYBDENUM TECHNETIUM RUTHENIUM RHODIUM PALLADIUM SILVER CADMIUM INDIUM TIN ANTIMONY TELLURIUM IODINE XENON

132.91 137.33 178.49(2) 180.95 183.84 186.21 190.23(3) 192.22 195.08 196.97 200.59 204.38 207.20 208.98
[204.38, 204.39]

57-71
lanthanoids
CAESIUM BARIUM HAFNIUM TANTALUM TUNGSTEN RHENIUM OSMIUM IRIDIUM PLATINUM GOLD MERCURY THALLIUM LEAD BISMUTH POLONIUM ASTATINE RADON

138.91 140.12 140.91 144.24 150.36(2) 151.96 157.25(3) 158.93 162.50 164.93 167.26 168.93 173.05 174.97

89-103
actinoids
FRANCIUM RADIUM
LANTHANUM CERIUM PRASEODYMIUM NEODYMIUM PROMETHIUM SAMARIUM EUROPIUM GADOLINIUM TERBIUM DYSPROSIUM HOLMIUM ERBIUM THULIUM YTTERBIUM LUTETIUM

ACTINIUM THORIUM PROTACTINIUM URANIUM NEPTUNIUM PLUTONIUM AMERICIUM CURIUM BERKELIUM CALIFORNIUM EINSTEINIUM FERMIUM MENDELEVIUM NOBELIUM LAWRENCIUM

ppb 1 100 10,000 1x10-7 34285.7


CONVERSION ppm = g/ton = µg/g 0.001 0.1 10 10,000 34.2857 carat 1 ton (avdp.) 1 oz (troy) 1
Troy oz/ton (short) 0.00003 0.00292 0.29167 291.67 1 mg/g 41.666 kg 907.18474 g 31.1035
FACTORS: % 1x10-7 0.00001 0.001 1 0.0034

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