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Maximizing

the Life of
Tank Linings
by Mark B. Dromgool
KTA-Tator Australia

A protective lining forms a


barrier between the sub-
strate and the cargo of
the tank, with the aim of preventing sub-
strate corrosion, maintaining product puri-
ty, and decreasing erosion. It can also im-
prove the ease of decontaminating and
and vessels that hold aggressive chemicals.
These steps address important factors often
overlooked when specifying, applying, and
inspecting new or replacement linings. The
choice of lining type is obviously crucial
but is beyond the scope of this article.

cleaning the tank. In mild steel tanks, a lin-


ing allows a reactive or corrosive cargo to
Service Environment
be stored in a vessel that, if unprotected,
would be attacked by the cargo. The specifier must accurately and compre-
For a lining to be successful, it must hensively define the environment in which
do the following: the lining is expected to serve.
• insulate the cargo from the reactive sub-
strate, Tank Content
• prevent or minimize the permeation of First, the tank content must be described
any element of the cargo or another elec- fully, including the following aspects:
trolyte through the coating film to the sub- • liquid or solid nature, including what it
strate/lining interface, might be diluted with;
• resist corrosion products that may devel- • the concentration;
op from or on the substrate, • the temperature;
• form a full and continuous film with a • the fill level; and
high level of integrity and low levels of • the cyclic process that might be involved
moisture vapor transmission, and (which may include changes in fill level,
• display excellent adhesion and cohesion. concentration, and cycle time, as well as
Although the time to failure varies temperature).
widely, most tank linings fail. While failure Understanding the cyclic process to
cannot be avoided completely, premature which a tank is subject involves evaluating
failure can be minimized. This article will exactly what sequence of activity will occur
outline crucial steps for maximizing the life in the tank. (The plant operations staff can
of a protective lining in carbon steel tanks provide this information for a relining job,

62 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

while the design engineer should be con- the type of acid or alkali. Differing types of
sulted for lining of new process vessels.) acid or alkali can have a vastly different ef-
For instance, in a condensate/boiler fect on the durability of the lining. If the
feed tank, the vessel could be filled with tank is to contain an aggressive chemical,
cold water and have boiler treatment chem- then its solvency, its effect on the film due
icals added; it may then have elevated tem- to its hydroscopic nature, or other film ef-
perature condensate added into (or worse, fects should be determined. If there are
onto) the tank surface as the boiler water mixes of chemicals, their effects can be dif-
recycles. The tank may then reach an oper- ficult to determine. The cumulative effects
ating level of 115-125 F (46-52 C) with the of combinations can be unpredictable with-
boiler’s normal draw-off and condensate out accurate analysis of these conditions.
return. When the night or weekend boiler
load changes, tanks of this type have been Outage Demands
known to rise to 195-205 F (90-96 C). The Another aspect of service environment is
frequency and mode of adding boiler treat- the plant shutdown or outage demands on

When a tank is to be
relined, its history and
the performance of
linings in similar
environments can be
invaluable.
Photos courtesy
of the author.

ment chemical must also be considered. Is the coating. Is it necessary, for example, to
it, for instance, continuously added in a allow for a clean-out process that could in-
metering system, or is it shock-dosed every volve steam cleaning, high pressure water-
week (given a high dosage in a short time), jetting, or alkaline or acidic rinsing? It is
which will indicate an elevated peak in common practice in the petrochemical in-
chemical concentration? dustry to steam out tanks by filling them
When determining the contents of the partially with water and then running live
tank, one must often consider the pH and steam or condensate into the vessel until it

Copyright ©1996, Technology Publishing Company MARCH 1996 / 63


Making Linings Last

overflows. This type of service could de- propriate use of dissimilar metals. In one
stroy a lining that was designed to with- example with which the author was in-
stand many harsh chemicals but was not volved, a mild steel tank with an epoxy
designed for or capable of withstanding coating system was fitted with a large stain-
this combination of cleaning processes. less steel impeller. In less than 6 months,
In another instance, the concentration the tank was perforated with corrosion.
of a tank cargo may rise significantly during Small areas that were poorly coated or in-
the process sequence because of evapora- accessible in the mild steel tank shell were
tion of some of the water, which could in- forced to be very active anode sites be-
crease the aggressiveness of the cargo. cause of the large surface area of stainless
steel acting as a cathode. A similar failure
Temperature and Temperature Gradient occurred on an elevated temperature, boil-
The temperature and temperature gradient er feed water tank that had a large copper
across the tank structure, including the lin- coil as the inlet pipe and stainless steel
ing, must also be evaluated. Organic coat- items fitted to the tank along with galva-
ings have a coefficient of thermal expan- nized components. If possible, it is worth
sion significantly greater than most steel changing the construction materials in
substrates. The extent of this thermal ex- these conditions or insulating the electrical
pansion changes whether the tank is ther- connection between the dissimilar metals.
mally insulated or not. In certain instances,
the stress from the differing thermal expan- Tank History
sion rates is enough to exceed the bond Most of the considerations above are rele-
strength between the lining and the sub- vant if the tank is new or going into a new
strate or between individual layers in the process where there is no history. If the
lining. Thick films are particularly suscepti- tank is being relined or if a new tank was
ble to cracking from thermal expansion. constructed to replace an existing tank,
Failures often occur at a localized over- then a thorough investigation of the previ-
building of the lining. ous service environment of the tank or the
experience of other users of tanks in the
Effects of Dissimilar Materials same environment is very useful.
Another often overlooked effect is caused Assuming the present lining is to be
by dissimilar metals in the tank. It may be removed and replaced and the process is to
easy to assume that the tank is all carbon remain substantially unchanged, the exist-
steel. Further investigation, however, often ing lining and its manufacturer must be
reveals that flange bolts, float sensing fully and accurately identified. Additional
equipment, or other mechanical or electro- details such as its age, composition, and
mechanical devices are made of a dissimilar history, including whether the lining was
metal, such as copper or stainless steel, that recoated or repaired through its life, will
could markedly affect the ability of the lin- give a good indication of its effectiveness.
ing to survive. In some cases, the design or Obviously, its original and subsequent suit-
specification for these items may need to ability should be addressed. If, however,
be amended. Examples are stainless steel the lining has performed well for at least 10
bolts, stainless steel agitators, and copper- years, or failed because of mechanical dam-
or zinc-coated components for temperature age or a change in process, then the lining
sensing or fill height determination. and its application procedure may be con-
Gross failures of tank linings and en- sidered satisfactory. Full analysis of a failed
tire tanks have been caused by the inap- or deteriorated lining can be made by a

64 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

reputable coating consultant, a knowledge- these sources, insist on a written specifica-


able coating manufacturer, or a coating tion with a summary of the environment
testing laboratory. that the lining is to withstand. This can
It is a good idea to learn if there has have significant benefits if there is a failure.
been other satisfactory use in similar expo- Once the service environment and
sures by other users. Plants with similar candidate linings are determined, compara-
processes, similar chemistry, and similar tive exposure testing is worthwhile if time
tank lining services can be canvassed about allows. Relining plans should always be
the success of the lining types they have done enough in advance so that compati-
used. If the process has been undertaken in bility testing or side-by-side comparability
another environment, useful history can testing can be undertaken before the work
often be extrapolated for the planned pro- is scheduled. Assuming that the system op-
Linings must be able to
ject. If the planned service has not been tions can be narrowed down to a few can-
withstand conditions
undertaken before, it is valuable to select didate materials, it is important not to eval- during service outages
candidate lining materials and prepare a uate their merits on price alone. Other as well as during
number of test panels. Panels can be im- immersion service.
mersed, or partly immersed in the chemical
and, given sufficient time for the evaluation
and confirmation, important comparative
data about the various candidate options
can be gleaned.
If a coating has failed in a particular
service, it is a mistake to automatically re-
place it with the same material unless other
factors have caused the early breakdown. If
the only data available are from accelerated
immersion exposures, treat these test re-
sults cautiously. Such testing may give
some indication of performance and ex-
pected coating life, but there can be short-
comings in the extrapolation of short accel-
erated exposure times.

Service Environment and


Lining Recommendations
When seeking a confirmed recommenda-
tion from a coating manufacturer or coating
consultant, always ensure that they have all
the exposure data such as chemicals, pH
and concentration, temperature, pressure, important selection factors are the reputa-
and any cyclic nature of the operation. tion of the manufacturer, the performance
Even at the expense of some proprietary history of each lining, and the ability of the
information being forwarded to these peo- chosen system to be repaired and main-
ple, it is very important that they are fully tained. If one of the candidate materials,
aware of every factor that could have an once it has been in service, is extremely
implication for the lining’s service life. hard to repair or needs subsequent coats,
When seeking recommendations from another lining may be a better investment.

Copyright ©1996, Technology Publishing Company MARCH 1996 / 65


Making Linings Last

The ease and versatility of application radius of guillotined or gas-cut (flame-cut)


should also be considered. Linings that can edges must be satisfactory to ensure the ad-
be applied with conventional or airless hesion and integrity of the lining system to
spray equipment may have advantages be applied. The condition of the surface it-
compared to linings requiring specialist or self, whether new or being relined, must be
plural component application equipment. assessed, particularly for the presence of
Such equipment may be difficult to maneu- oil, grease, or soluble salts. All of these
ver or operate and, in unskilled hands, may items quickly attack tank linings.
not yield the desired film properties.
Condition of Existing Lining
For relining projects where the existing lin-
ing has not completely deteriorated, it is
Surface Preparation
worthwhile to evaluate the life expectancy
The highest level of surface preparation of the existing lining system until full re-
possible is strongly recommended in all moval is required. If there is only localized
tank lining work. The mechanical condition damage (blistering and minor pitting), the

A lining failure inside


a cement sludge tank
caused by poor site
preparation and poor
coating of the
field welds.

of the tank must be addressed as part of lining does not necessarily need to be fully
the evaluation of the tank for surface removed. It may be better to evaluate the
preparation. threat to the substrate’s integrity and, if the
substrate is not at risk, leave the existing
Mechanical Condition of the Tank lining in service for as long as possible.
The condition of the welds and the plate When the substrate’s integrity is at risk,
edges, the presence of weld spatter and the however, a full coating removal and re-
general continuity of the surface, and the placement should be planned.

66 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

In the author’s experience, spot repair cult to protect. A double blast sequence is
with localized blast on the deteriorated highly recommended for tank lining or re-
areas has sometimes caused massive failure lining projects. It allows the old lining to be
by blistering in areas adjacent to the repair fully removed for tank inspection, but it
areas, due to overblast damage. Previously also allows greater productivity per day
sound coating has suffered pinprick dam- once the second or final whip blast (Brush-
age from the abrasive stream impinging on Off Blast, SSPC-SP 7) is under way.
non-target surfaces. Even if microscopic at Typical production blasting rates for
first, this damage has opened a path removing an old lining inside a tank can be
through the old coating that allows the between a quarter and a third of the rate at
transmission of water vapor or electrolyte which a whip blast of a previously cleaned
to the substrate, causing blisters. In some surface can be completed. Therefore, larger
instances, where 50 percent to 80 percent areas can be lined after a single day’s re-
of a tank surface has been spot blasted or blast production. This means fewer joints in
spot and sweep blasted, the anniversary in- the lining, less contamination from dena-
spection showed massive damage on all tured coating or abrasive, and less chance
surfaces adjacent to the spot blast zones. of overblast damage while maintaining pro-
Spot blasting should be considered duction rates than if the first coat is applied
only if less than 10 percent of the tank sur- immediately after the first blast.
face requires repair. For damage above 10 A blast holding primer that is compat-
percent, it is preferable to delay recoating ible with the lining system should also be
until more of the residual value of the lin- considered. This primer generally allows
ing has been consumed, when a full blast faster lining of blasted surfaces with quick-
can then be planned. The incremental cost er drying. Holding the blast with a primer
of extending to a full blast is generally not also minimizes the chance of damaging a
excessive and can certainly be more attrac- slower drying, full thickness lining that has
tive when weighed against durability and been applied to an adjacent surface during
cost per year of service. the previous shift or day. The use of a blast
If spot blasting and repair are consid- holding primer also saves the multiple mix-
ered essential, then workers must fully and ing and wasting of high build material that
adequately mask the areas adjacent to the would be needed to coat the limited day’s
zone of repair so that there is no threat of production from a single blast process,
damage to sound areas. This can be done thereby reducing the potential for errors in
by taping insertion rubber, rubber sheeting, mix ratio. It can also allow for the use of a
tarpaulins, or heavy cardboard sheet more economical abrasive for the initial
around the repair zone to confine or re- blast, one that might not generate the re-
strict any threat of overblast damage. quired surface profile but could be
changed for the final blast when significant-
Sequence for Surface Preparation ly less abrasive is needed to achieve the
Pre-job planning should include developing profile specified. Before the second blast,
a sequence for surface preparation. Relin- the surface should be fully checked for sol-
ing projects may call for a blast/wash/blast uble salts and oil or grease. Detection kits
sequence to remove or lower the soluble for each are commercially available.
salt levels that may be underneath the film
or to allow the mechanical condition of the Climate Control
tank to be checked thoroughly, especially The specifier should consider humidity and
at welds, plate edges, and other areas diffi- climate control, ventilation, and air circula-

Copyright ©1996, Technology Publishing Company MARCH 1996 / 67


Making Linings Last

tion inside the tank during surface prepara- concentrate on the specified height. Be-
tion and coating application. Dehumidifica- yond a certain point, the profile height has
tion equipment will help to hold the blast. less of an effect on adhesion than does the
Ventilation removes dust to give the blast shape of the surface roughness generated.
and spray operator good visibility and to The most effective abrasive is one that pro-
avoid the possibility of contaminating the duces a uniform, jagged tooth with the
newly applied wet lining. Both dehumidifi- greatest increase in effective surface area
cation and ventilation equipment must be but with a height that is approximately 25
designed for the tank size, volume, and to 30 percent of the final dry film thickness
configuration, or they will be ineffective. (dft). The maximum profile height is 2.3 to
Heating the tank in cooler weather 3 mils (58 to 76 micrometers) for most coat-
will also help in most cases with the quality ings. Very few organic or inorganic coatings
of the tank lining. Care must be exercised, require a profile height above 4 mils (102
however, to ensure that the well estab- micrometers). The most common excep-
lished cold wall effect of high internal tem- tions are ultra high build materials and
peratures and a low substrate temperature thermal spray metallic coatings.
does not lead to blistering and damage. Substrates to be lined should never be
blasted with spherical abrasives such as
Abrasive Selection steel or chilled iron shot, or any other abra-
The type and size of abrasive are important sive that produces a similar peened shape.
to the work. The abrasive should produce Disbonding will result. Zinc silicate coat-
the profile shape and height required to ings, which have a metallurgical as well as
ensure acceptable lining adhesion to the a chemical bond to the steel surface, can
substrate. Abrasives should be chosen with readily detach from a shotblasted substrate.
characteristics that minimize shattering and,
more important, minimize embedment into Housekeeping
the substrate. Many of the heavy angular Another part of evaluating surface prepara-
grits, particularly chilled iron or steel grit, tion is determining the method of removal
can damage a lining if they are used as the of the spent abrasive and paint waste from
final abrasive. Minute pieces of these metal- the tank interior. Is it to be swept out or re-
lic abrasives can fracture and become em- moved by vacuuming? Before a lining is
bedded in the substrate. The abrasives and applied, the blast cleaned surface should
the tank substrate are often dissimilar met- be vacuumed as the final step. Sweeping
als. Embedded abrasives can therefore set or air blowing will not fully remove the
up a corrosion cell. They can also remain finely shattered abrasive from within the
as protrusions as well as embedments that profile shape. If not removed, the shattered
the lining cannot encapsulate and fully abrasive interferes with the lining’s adhe-
cover. A non-metallic abrasive that is low sion to the substrate and provides a site for
dusting and low fragmenting is preferred osmotic blistering.
for tank lining. It should be graded to pro-
vide even cleaning and to produce an even
profile shape and height.
There is much debate about profile
Coating Materials
requirements. The most crucial element is Getting the Material
the profile shape rather than the height. Before the project begins, the amount of
Because the profile height is a measurable coating required must be calculated and or-
item, too many specifiers and inspectors dered. The amount can be determined only

68 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

by accurately measuring or calculating the chemical resistance, many tank linings are
surface areas involved and allowing for all multi-component materials. Often, at least
contingencies. Having the lining on site be- one of the components is sensitive to mois-
fore surface preparation is complete will ture. If coating containers are left in the
also allow the contractor to check batch open and are allowed to heat and cool
numbers. Ideally, the lining materials need- through weather cycles, water can be intro-
ed for a project or a definable part of a duced into the coating even through the
project will come from the same batch. sealed lids as the unfilled space in the con-
When lining materials arrive on site, tainer expands and contracts with tempera-
the contractor or inspector should verify ture. Solvents, too, are very sensitive to Metallic
that the product specified matches the contamination with water, particularly be-
product received. For multi-pack products, cause the dished lids of the larger contain- abrasives
the sizes of all components should match. ers or drums can allow water to pond if ex-
That is, the part B component should be posed. Storage under a tarpaulin can be embedded
the correct size ratio for the part A. A num- nearly as bad as storing the materials in the
ber of tank lining failures have been caused open because lining materials can sweat
in a metal
by mixing the part A component for a one- under the tarp.
substrate
gallon (four-liter) kit with the part B for a
five-gallon (20-liter) kit or vice versa. For Mixing the Linings can set
linings that require solvent to be added, the Once the lining is ready to be mixed, the
solvent should be the one recommended material should be withdrawn from storage. up a
by the manufacturer, not a local substitu- If temperatures are outside the ideal range
tion. A more economical solvent may be noted above, withdrawal should be timed corrosion
used to clean out application equipment as so there will be no delay before mixing.
long as it is flushed out and there is no Once the blasted surface is nearly ready to cell if the
chance of it being mixed with the product be lined, the selected spray equipment
during application. should be assembled and tested. Testing metals
should be carried out using the solvent
Storage compatible with the lining. With airless
are
The lining material should be stored on site spray, filling and pressurizing the unit will dissimilar.
in a secure and weatherproof location. If assist in flushing the fluid lines and check-
the coating work is to be performed out- ing for system leaks.
side the normal conditions of temperature, The order of mixing components is
60 to 75 F (16 to 24 C), then the coating often overlooked. Once both components
should be stored in a controlled tempera- have been selected, the lower viscosity
ture environment. The ideal storage tem- (less thick) component should be stirred
perature for most protective coatings is be- first. This will often be the curing agent or
tween 68 and 75 F (20 and 24 C). In many catalyst for the lining. Even though it may
instances, a heated or cooled storage room appear homogeneous, it should always be
with temperature controls will be needed stirred or fully dispersed. The lower viscosi-
to maintain this range. The consistency of ty component should be stirred first be-
mixing, thinning, application effectiveness, cause it will be easier to clean the mixing
flow, cross-linking, and final cure depend equipment before use on the more viscous
on the lining temperature at the time of component. The second or heavier bodied
mixing. Lining containers should also be material is then stirred without any curing
stored in a place that will keep them free agent. Stirring the second component alone
from contact with water. Because of their ensures that all elements from within the

Copyright ©1996, Technology Publishing Company MARCH 1996 / 69


Making Linings Last

drum are fully blended and that it is at a and cure because temperatures and humid-
consistency adequate for spray application. ity levels change most then. Success de-
Breaking any lumps from the sides and set- pends upon satisfactory air temperatures,
tlement off the bottom of the container, substrate temperatures, and conditions of
preferably with a stick before complete relative humidity and dew point. These
power stirring, is the first step. conditions need to be maintained through-
Once the heavier component is fully out the application and initial curing. Con-
dispersed and while it is under agitation, densing moisture or dropping substrate
the part B component is added. (Often, temperature during cure is extremely detri-
more than 1 person is needed to mix the mental to the lining’s performance.
lining.) During the addition of the second
component, the product should be under Condition of the Equipment
agitation to prevent the chance of solvent Successful lining application also depends
shock (shocking the pigment out of the so- significantly on cleanliness of the equip-
lution by adding too much solvent), which ment, in particular, freedom from oil and
can happen if stirring is not performed uni- water in the compressed air supply and in
formly while the components are blended. the paint mixing and fluid lines. Generally
Some linings require an induction time speaking, the manufacturer’s recommenda-
after all components are fully dispersed. tion for application equipment is a good
The requirements for an induction time are place to start even though other equipment
normally given on the manufacturer’s prod- setups can be successful.
uct data sheet.
It is always sound practice to mix Selecting the Application Sequence
the full kit of the multi-component pack As with surface preparation, the sequence
rather than try to proportion it by eye. Even of coating application can have a signifi-
with considerable experience, it is very dif- cant impact on lining performance.
ficult to get an accurate ratio of a multi- The blast and prime process, as op-
pack coating without some method of posed to the blast and full coat or double
weighing or volumetrically measuring the blast sequence, has advantages for lining
constituent components. application as well as for surface prepara-
If the lining must be thinned for the tion. The need for extreme cleanliness be-
recommended application method, it tween coats and freedom from contamina-
should be performed after the induction tion during the intercoat interval can also
time. Otherwise, the lining could be over- dictate this coating sequence. Because of its
thinned because it heats up during induc- fast dry characteristics, a blast holding
tion and becomes less viscous. primer or a low viscosity first coat can pre-
vent dust contamination. Its tolerance for
early recoating with a high build lining can
improve the overall integrity of the lining.
Lining Application
The holding primer also allows welds and
Proper Application Conditions corners to be stripe coated before the first
If the lining is not applied under controlled high build coat. If the blast holding primer
climatic conditions, then application and is not used, then when the stripe coating is
subsequent drying and curing should be performed, the areas not coated might not
timed to occur when the conditions will be hold the blast long enough for the full coat
most suitable. Early morning or late after- to be applied. If the holding primer is not
noon are often not ideal for application used, then it is better to apply the stripe

70 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

coat after the first full build coat is applied es. Attention to welds, edges, and corners
and can be recoated. dictates that not only should they receive a
Stripe coating is critical. During the stripe coat, but they should also receive
conversion of a wet coating into a dry film, careful spray attention. They should be
the normal internal curing stresses inside a sprayed on both sides or on all exposed
lining have a tendency to pull the drying surfaces. It is not uncommon, when in-
coating away from edges and sharp cor- specting tank linings, to find uniform film
ners. Even with the careful rounding of thicknesses on plate surfaces while only 1
these edges in the mechanical preparation side of the welds is lined adequately.
of the tank, some thinning of the dry coat- A color contrast should exist between
ing will result. Stripe coating is designed to each lining in a system, including the
alleviate this low dft to help provide a uni- stripe coating, to help measure dfts.
form minimum dft on all areas of the tank. Unfortunately, many tank lining materials
Areas for stripe coating are edges, corners, are manufactured in only 2 colors, for in-
and welds, as well as the localized zones stance, white and buff. However, for the
where access with the spray equipment is
difficult, such as on the backs of angles or
on the reverse of stiffeners.
A quick-drying primer is preferred for
tank lining application. Once the primer is
cured enough to be relined without dam-
age, a stripe coat of the high build should
be applied, followed by a full spray appli-
cation of the same lining. Once the stripe
and full coats have dried, with the correct
recoat interval, the dft should be checked.
This approach allows a high probability of
achieving the required dft. If dfts on edges,
welds, and corners are still low, then the
intermediate film thickness readings will in-
dicate where attention is still required. A fish holding tank
inside a tuna fishing
Quality Assurance during vessel before relining.
Lining Operations The difficulty of access
caused by the ammonia
The applicators should be advised of the
refrigerant piping
target dfts per coat and the wet film thick- should be considered
nesses required to achieve the dfts. Over- when preparing a
building can be as detrimental as under- specification for relining.
building in tank lining applications,
especially because of solvent entrapment sake of the color contrast, it is often satis-
and insufficient cure. Both can lead to blis- factory to make a partial blend of the two
tering and coating detachment. An applica- colors and convert it with the correct ratio
tion sequence and the necessary equipment to give an intermediate shade that will be
help ensure that the largest possible area of different enough where the color contrast
the tank’s internal surface can be coated is required.
with good access and with an even spray Lighting and ventilation are again
pattern that will give reliable film thickness- major issues for coating application. It is

Copyright ©1996, Technology Publishing Company MARCH 1996 / 71


Making Linings Last

very difficult to apply a uniform coating Pre-Job Meeting


thickness if the applicator has minimal visi- A pre-job meeting that includes the client,
bility or if there are excessive spray mist the contractor, the inspector, and, possibly,
and solvent fumes inside the tank. the specifier is vital. All elements of the
Flameproof or explosion-proof light- work should be discussed, particularly the
ing is extremely important in any situation criteria for acceptance and the proposals
where solvent vapor is present. For ade- for the sequence of activities. Correctly
quate ventilation, the air movement should conducted, this meeting should clarify the
be sufficient to assure that the maximum demands of the project for all parties.
concentration of vapor does not exceed One procedure that the author has
10 percent of the lower explosive limit for adopted at the pre-job meeting for tank lin-
that vapor. ing work is preparing a written summary
Cleanliness at all stages of the final of key specification details for the supervi-
surface preparation and coating application sor. Often this document can be as simple
is very important. Cleanliness extends to as a one- or two-page summary of the
preventing perspiration drips in the tank climatic condition limits, the restrictions,
and preventing dirt or other foreign matter, the lining system, the interval between
including abrasive debris, from becoming coatings, the wet and dry film thicknesses,
embedded in the tank lining. Developing the solvent type, and any other relevant in-
a system for access and housekeeping formation such as the inspection accep-
ensures maximum cleanliness at all stages tance criteria and referenced standards.
of work. While the summary does not replace the
At all stages of the surface prepara- need for the supervisor to understand the
tion and lining application, the applicator, complete project specification, it is valuable
the supervisor, and the full crew must for quick reference.
assume responsibility for ensuring quality.
Quality is not as simple as achieving a On-Site Inspection
dft within the specified narrow range. Inspection has many stages. The first in-
Often, factors such as intercoat cleanliness, spection of the original condition should
observation of the climatic and substrate include a thorough visual check and rectifi-
conditions, and time for curing are not as cation, if needed, of all welds and steel-
obvious as dft when the coating system work conditions. Verifying the detection
is complete, but can be significantly more and removal of visible oil, grease, and
important in ensuring the integrity of dirt should receive priority at this same
the lining. time, too.
Once the first blast is performed, an
inspection can provide information about
the condition of steelwork and the height
Testing and Inspection and shape of the blast profile. Even though
Even though these items are last in the dis- the surface will be reblasted, checking the
cussion, they should be included in every profile at this time can help to determine if
stage of the process, from determining the the final surface will meet the specified cri-
need to line or reline to returning the ves- teria once the final blast is performed. Ad-
sel to service. Whether the inspection is ditionally, it can provide early indications
carried out by an independent third party of possible problems with achieving the
inspector or by the client’s own representa- specified profile on zones affected by heat,
tive, key points include the following. such as welds. On such zones, where met-

72 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company
Making Linings Last

allurgical differences create a harder sur- After the first coat, a full inspection
face, it is often difficult to achieve the pro- can give valuable guidance to the applica-
file specified. In this author’s view, many tor and the supervisor so that the balance
failures around tank welds may be caused of the application can rectify any non-con-
by this phenomenon. formance in the system so far. It is particu-
After the first blast, the inspector larly useful to detect and highlight areas
should also look for evidence of oil, grease, that are missed, or those that are high or
dirt, or soluble salt on the steel. These con- low in dft. Finding such areas at this point
taminants may have been introduced by can often save the application of an addi-
blasting or by the workers themselves. tional coat if the indications are that the
Many tank lining failures show evidence of present technique will not achieve the de-
a perfect hand print that was made on the sired final film.
blasted surface before application. Removal Methods of highlighting non-confor-
of these contaminants may require wash- mance should be considered. It is not a
Chalk marks highlight
ing, rinsing, steam cleaning, or solvent wip- sound idea to use wax crayons or felt tip non-conformance found
ing. If oil or grease is persistent, then swab- during inspection.
bing with a 1:1 mix of methanol and water
has proved to be very effective. Steam
cleaning between a double blast sequence
is recommended for removing soluble salts
from steel surfaces.
Inspection after the final blast should
include a visual confirmation that the blast,
vacuum or final clean, and profile meet the
specification. The blast cleanliness
achieved, it should be remembered, is the
condition evident at the time the lining is
applied, not the level when blasting was
completed.
Inspection should also include an ob-
servation of the lining mixing, visual confir-
mation of the components, and recording
of the batch numbers and quantities that
are prepared. At all stages, the climatic and
substrate conditions need to be measured
and recorded.
Once lining application has begun,
the inspection should include checking wet
film thicknesses; confirming that flow, lev-
eling, and atomization are appropriate; and pens. Chalk is generally superior, providing
assuring that the first coat is free of pin- the color does not interfere with the subse-
holes. If deficiencies in lining handling or quent lining. Bright colors have been
application cannot be corrected with spray known to show through the next wet coat.
technique, timely adjustments can be made The inspector should look for sweat-
to the application equipment; mixing, thin- ing on the first coat, particularly with
ning, or the temperature of the lining; or epoxies, which will always be detrimental
other variables. to adhesion of subsequent coats. The

Copyright ©1996, Technology Publishing Company MARCH 1996 / 73


Making Linings Last

1:1 mixture of methylated spirits in water is mum cure time is allowed, the cure is often
an effective remedy, and because of the compromised because of inspection, re-
miscibility and easy evaporation of the mix- work, or climatic changes that slow cure. If
ture, residual water is not a problem. the tank is filled before cure is complete,
The inspector should also note the disastrous failure may result.
need for recoating or repair. If deficiencies Continuity testing with high or low
are found in any coat, they should be recti- voltage equipment as appropriate for
fied before application continues, particu- the lining type and thickness should be
larly if there is a sequence of differing coat- carried out if specified. Continuity testing,
Mark B. Dromgool, ings in the lining system. (The argument however, can be performed only when
general manager and
principal of KTA-Tator that applicators will fix up the shortfall with the coating is cured and dft has been
Australia, has been in the additional finish coat should not be accept- checked completely. Continuity testing
protective coatings
industry for over ed.) Similarly, the inspector should observe must be performed in accordance with the
19 years. Ten years of his the stripe coat methods, discuss the op- standard specified. If touch-up is needed,
experience has included
the management of
tions, and ensure full compliance. the procedure must be authorized by the
several large grit blasting Checking the cure of each coat is im- lining manufacturer.
and application shops, portant. If accelerated or retarded curing is
a galvanizing operation,
and large field and site evident during the inspection of the first Recordkeeping
coating teams. coat, the problem is worth investigating. In One of the last stages of inspection is to
During this time period,
Dromgool gained one instance where a slowly curing first complete a full and final report, including
extensive experience in coat was ignored and a finish coat was ap- all achievements, non-conformances and
working on a variety of
structures, including plied, the lining failed. Investigation re- their rectification, full details of the lining
bridges, tanks, structural vealed that the mix ratio for the first coat used, batch numbers, and climatic and
steel, wastewater plants,
pulp and paper plants,
was incorrect. Even though the primer was other relevant data. This report will often
as well as chemical, coated with a finish having a correct mix be the only permanent record of all aspects
mining, and ratio, the tank lining failed because of the of the lining project. The report can be ex-
petrochemical facilties.
In 1993, Dromgool poor integrity and inadequate chemical tremely useful, whether the coating serves
formed Akarana structure of the primer. This failure resulted for many years or fails prematurely.
Coating Services,
a protective coatings in a rather expensive removal and replace-
engineering and ment procedure that could have been Anniversary Inspection
consulting firm. Two
years later he joined n avoided if the warning signs of slow cure Frequently, the last duty of the inspector is
KTA-Tator. had been heeded. If there is doubt about to perform the anniversary inspection ap-
Dromgool is a member
of SSPC and an
the integrity of any part of the system, it is proximately 12 months after the tank is put
Executive of the Blast better not to continue rather than risk the into service and just before the contractor’s
Cleaning & Coating consequences of a non-conforming lining. maintenance period expires.
Association of Australia.
He can be contacted at Once the system is applied, final
KTA-Tator Australia, checks will include a full dft check, a thor-
136 Lord Street,
Richmond,Victoria 3121, ough visual continuity check for missed or
Australia; thin areas, and verification of a touch-up
Conclusion
61/3/9428-9339;
fax: 61/3/9428/9131 procedure for any non-conforming zones. To maximize the life of a tank lining sys-
Once a satisfactory visual continuity check tem, take the time, plan the work, and stick
is completed, the lining must have enough to the plan. Compared to a poorly planned
time to cure before the tank is put into ser- project with a resulting lining life of only a
vice. Unfortunately, the outage time for the few years, a properly planned, well execut-
tank relining often includes only the mini- ed lining project can add as much as 12 or
mum time calculated without any al- 15 years to the achievable operating life of
lowance for lost time. When only the mini- the system. JPCL

74 / Journal of Protective Coatings & Linings Copyright ©1996, Technology Publishing Company

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