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Article history: In this study, acoustic emission (AE) analysis method was applied to monitor the damage evolution
Received 11 August 2017 process of ultra high performance concrete (UHPC) under direct tensile test. Three types of UHPCs,
Received in revised form including high strain-hardening UHPC, low strain-hardening UHPC and strain-softening UHPC were
4 January 2018
investigated. Meanwhile, the crack width developments of UHPCs during the tensile test were measured.
Accepted 8 January 2018
Test results show that high strain-hardening UHPC exhibited high ductility by forming multiple
Available online 10 January 2018
microcracks invisible to naked eyes (typically below 0.05 mm) in the strain-hardening stage. The crack
width-strain curves indicate that increasing the ultimate tensile strain of UHPC can improve its crack
Keywords:
Ultra-high performance concrete
width control ability effectively. The AE analysis method could effectively detect the internal damages of
Strain-hardening the high strain-hardening UHPC at a strain of 600mε. At that time, the crack width was smaller than
Crack width control ability 0.01 mm that could not be detected by crack width measuring instrument in this study. For three types of
Acoustic emission UHPCs, damages were generated around the localized crack during the strain-softening stage. In a word,
Damage evolution mechanism the AE analysis method provides strong evidence to the multiple cracking behavior of UHPC during the
strain-hardening stage, and provides a clear explanation to the identical damage evolution mechanism
for three types of UHPCs during the strain-softening stage.
© 2018 Elsevier Ltd. All rights reserved.
https://doi.org/10.1016/j.cemconcomp.2018.01.007
0958-9465/© 2018 Elsevier Ltd. All rights reserved.
18 J.-Y. Wang, J.-Y. Guo / Cement and Concrete Composites 88 (2018) 17e28
3. Experimental program
3.3. Test method for crack width-strain curve
3.1. UHPC mixture and specimen preparation
As shown in Fig. 3 (b) and (c), during the UHPC direct tensile
test, the positions of the cracks generated at different tensile strain
The UHPC materials used in this study were commercial prod-
were firstly located by the Canon EOS 5DSR camera (50.6 MP) with
ucts named TENACAL® provided by Shanghai Royang Innovative
zoom lens (EF17-40 mm f/4 L USM). The camera's picture could be
Material Technologies Co., Ltd. TENACAL® consists of three com-
displayed on the computer screen in real time. After locating the
ponents, water, UHPC premixed powder and steel fibers.
crack, the width of the crack was immediately measured by the
Table 1 provides the mix proportion of the UHPC matrix. The
crack width measuring instrument with 0.01 mm resolution. In
maximum aggregate size of the UHPC matrix is 1.18 mm. The vol-
order to take the crack image more clearly and measure the crack
ume fractions of steel fibers in high strain-hardening UHPC, low
width more accurately, the loading rate of the tensile testing was
strain-hardening UHPC and strain-softening UHPC are 2.5%, 2.0%
set as 0.1 mm/min. The load for the start and end of the test were
and 1.5% respectively. A type of straight steel fibers with length of
0.5 kN and 20% of the peak stress, respectively. The whole test
13 mm and diameter of 0.2 mm and with brass coating were used,
program lasted about 1 h.
which properties are given in Table 2.
A laboratory mixer with 60-L capacity was used to prepare the
UHPC mixture. UHPC premixed powder was first dry-mixed for 3.4. Test method for localisation of AE sources
about 1 min. Water was then added gradually and mixed for
another 3 min. When the mixture showed suitable workability and The AE analysis system described in section 2 was applied to
viscosity for uniform distribution of fibers, the steel fibers were monitor the damage evolution process of the UHPCs. The setup of
dispersed carefully by hand into the mixture and mixed for another the direct tensile test with AE analysis system is given in Fig. 3. As
3 min. Finally, the UHPC mixtures were then placed in the molds shown in Fig. 3 (a) and (d), in order to cover the expected zone of
without vibration due to the self-compacting properties of the the process, 8 AE transducers were placed in a rectangular array
UHPC mixtures. The specimen dimension is shown in Fig. 2(a). just above the surface of double sides of the specimens. The AE
Since the width (50 mm) of the specimens is longer than three transducers were coupled to the surface of UHPC specimens with
times of the length of the fibers (13 mm), it could reduce the in- Vaseline locating at the positions shown in Fig. 3 (d).
fluence of the fiber orientation distribution. For each mixture, In this study, pencil lead test and localisation test of AE sources
specimens were prepared as follows: 1) nine specimens for direct were conducted. The pencil lead tests were conducted with UHPC
tensile test; 2) three 100 mm cubic specimens for 28-day specimens by following the ASTM E976-99 standard [27], which
compressive strength test according to Chinese standard GB/T used HB or 2B pencil lead with 0.5 mm diameter as a manual AE
31387e2015; 3) three 100 100 400 mm prisms for flexural source. During the test, the pencil lead elongation was set to be
strength test according to ASTM C1609; 4) three about 2.5 mm and the angle between the pencil lead and the UHPC
100 100 300 mm prisms for elastic modulus test according to specimen surface was about 30 . The pencil lead was broken within
Chinese standard GB/T 31387e2015. After casting, these specimens 30 mm to transducers employing approximately equal force at each
were covered with plastic sheets and stored at room temperature time to get almost the same AE sources. The purpose of pencil lead
for 24 h, then cured in the water at a temperature of 20 C until 28 test was to determine the AE wave propagation velocity through
days. The UHPC tensile specimen after curing is shown in Fig. 2(b). UHPC materials and the noise level of the test environment so as to
Table 1
Mix proportions of UHPC matrix.
733 kg/m3 220 kg/m3 220 kg/m3 982 kg/m3 147 kg/m3 3.67 kg/m3
20 J.-Y. Wang, J.-Y. Guo / Cement and Concrete Composites 88 (2018) 17e28
Table 2
Properties of steel fibers.
Fiber shape Tensile strength Elastic modulus Length/mm Diameter/mm Aspect ratio Density/kg$m3
/MPa /GPa
set the corresponding threshold and amplification. As shown in strength of the UHPCs, while the elastic modulus remains almost
Fig. 3 (d), the pencil lead was broken 3 times in each location, there the same.
had two different locations. Through the pencil lead test, the
threshold of the AE system was set as 35 dB. The stress level of AE
activities above this threshold are detected by transducers, and 4.2. Tensile properties of three types of UHPCs
recorded by the windows-based AE data operation program. Value
for gain of preamplifier was set as 40 dB, sampling frequency was Fig. 4 shows the axial tensile stress-strain curves of three types
set as 3 MHz and band characteristic was set as 20 kHze200 kHz. of UHPCs, each type of UHPCs contains three specimens. The stress-
The windows-based AE data operation program was carried out strain curves of high strain-hardening UHPC (Fig. 4(c)) start with a
in parallel with the UHPC direct tensile test as shown in Fig. 3 (e). steep initial ascending portion up to first cracking, followed by a
The coordinates (xae, yae and zae) and origin time tae of AE source strain-hardening branch where a considerable reduction in
monitored by this program can be plotted for description of the modulus of elongation, i.e. the ratio of stress to strain. The point
damage evolution process of the UHPC specimen under tensile where first cracking occurs is mainly influenced by the tensile
loading test. An example is given in Fig. 3 (e). strength of the matrix, which is called the elastic tensile strength
(fUte). The peak point at the end of the strain-hardening branch is
determined by the fiber bridging capacity, which is defined as the
4. Test results and discussion ultimate tensile strength (fUtu) [3,28]. Following the peak point,
there is generally a descending branch which is strain-softening
4.1. Compressive strength, flexural strength and elastic modulus of stage. Generally, the tensile behavior of high strain-hardening
three types of UHPCs UHPC can be divided into three stages, including strain based
elastic stage, strain based strain-hardening stage and strain based
The mechanical properties of three types of UHPCs are sum- strain-softening stage. The low strain-hardening UHPC (Fig. 4(b))
marized in Table 3, including 28-day compressive strength also has three stages based on the tensile behavior, while the strain-
(100 mm*100 mm*100 mm cubic specimen), flexural strength softening UHPC (Fig. 4(a)) exhibits strain softening immediately
(100 mm*100 mm*400 mm prismatic specimen) and elastic following the first cracking.
modulus (100 mm*100 mm*300 mm prismatic specimen). Table 3 Detailed information about the tensile properties including fUte,
shows that with an increase in fiber volume fraction from 1.5% to εUte, fUtu, εUtu is summarized in Table 4. According to the literature
2.5% results in an increase of compressive strength and flexural [13], the method of detecting the fUte is illustrated in Fig. 4. If the
J.-Y. Wang, J.-Y. Guo / Cement and Concrete Composites 88 (2018) 17e28 21
Table 3
Mechanical properties of three types of UHPCs.
there is no clear first peak point, two lines are drawn from both the
linear elastic and hardening stages, and the intersection point be-
tween the two lines is selected as fUte in this research.
The average elastic tensile strength fUte of high strain-hardening
UHPC, low strain-hardening UHPC and strain-softening UHPC are
10.4 MPa, 8.7 MPa and 7.7 MPa, respectively, and the corresponding
strain εUte are 0.024%, 0.023% and 0.021%, respectively. The average
ultimate tensile strength fUtu in high strain-hardening UHPC and
low strain-hardening UHPC is 12.6 MP and 9.4 MPa, respectively,
and the corresponding strain εUtu is 0.412% and 0.116%, respectively.
It can be concluded that elastic tensile strength, ultimate tensile
strength and their corresponding strains of high strain-hardening
UHPC are the highest. The ultimate tensile strain of high strain-
hardening UHPC is higher than the yield strain of steel bar (0.2%),
and achieves strain-hardening with high ductility under direct
tensile loading, which would contribute to the ultimate tensile
loading capacity of the reinforced ultra high performance concrete
(R-UHPC) structures.
tensile stress-strain curve shows a clear load drop right after first 4.3.2. High strain-hardening UHPC
cracking, as shown in Fig. 4(a), the first peak stress in tensile stress- As shown in Fig. 5 (c), high strain-hardening UHPC exhibits
strain curve is selected as fUte. However, as shown in Fig. 4 (b)-(c), if strain-hardening behavior after the first cracking, accompanying by
J.-Y. Wang, J.-Y. Guo / Cement and Concrete Composites 88 (2018) 17e28 23
Table 4
Tensile properties of three types of UHPCs.
Specimen types fUte fUte,average CoV εUte εUte,average CoV fUtu fUtu,average CoV εUtu εUtu,average CoV
(fUte) (εUte) (fUtu) (εUtu)
MPa MPa % % MPa MPa % %
Low strain-hardening UHPC 1 9.1 8.7 0.05 0.020 0.023 0.19 9.8 9.4 0.04 0.114 0.116 0.26
2 8.6 0.021 9.4 0.147
3 8.3 0.028 9.0 0.087
High strain-hardening UHPC 1 10.0 10.4 0.04 0.024 0.024 0.06 13.0 12.6 0.03 0.404 0.412 0.03
2 10.3 0.025 12.2 0.426
3 10.8 0.022 12.6 0.405
multiple microcracks indicated by the decreasing modulus of 4.4. Damage evolution mechanism of three types of UHPCs
elongation. During this stage, these microcracks were bridged and
controlled by steel fibers, but they were invisible to the naked eyes. Figs. 9e11 show the evolution of AE source locations during the
Photos of the high strain-hardening UHPC specimen at different direct tensile test, where the corresponding stress-strain curves of
strains in the tensile test are shown in Fig. 7. It shows that although three types of UHPCs are also illustrated. As shown in Figs. 9e11, six
the tensile strain reached 3500mε, the cracks of the specimen still points are chosen to describe different stages of the evolution of AE
could not be observed by the naked eyes (crack width smaller than source locations: Point A and C are chosen at 100mε and 600mε,
0.05 mm). which represent the elastic stage and strain-hardening stages
As shown in Fig. 5(c), in the high strain-hardening UHPC spec- (strain-hardening UHPCs) of stress-strain curves, respectively;
imen, the crack with crack width larger than 0.01 mm cannot be Point B, D, E are the points responding to the ultimate tensile
detected until the tensile strain reached 673mε, because the crack strength in the stress-strain curves of strain-softening UHPC, low
width measuring instrument has only a resolution of 0.01 mm. strain-hardening UHPC and high strain-hardening UHPC, respec-
Since 673mε exceeds the elastic tensile strain of high strain- tively; Point F is the point 4000mε later after the peak point of each
hardening UHPC (around 250mε), the high strain-hardening UHPC type of UHPCs, which represent the strain-softening stage of the
with strain range from 250mε to 673mε is supposed to be with stress-strain curves.
cracks. These cracks cannot be detected so that they all have crack
width below 0.01 mm. 4.4.1. Damage evolution process at different states
The ultimate tensile strain εUtu of high strain-hardening UHPC is It is shown that no AE sources were detected till the point A in
around 4260mε. To better describe the crack pattern, the distribu- three types of UHPCs, which indicates that the defects of UHPC
tion of the crack width is plotted in Fig. 8. The crack width ranges generated in the elastic stage cannot be detected by this AE analysis
from 0.01 mm to 0.05 mm, and average crack width is 0.03 mm, system. At the ultimate tensile strain of strain-softening UHPC
which will benefit the impermeability of the high strain-hardening (point B), 13 AE sources generated and almost all of them lay in a
UHPC with tensile strain below 4000mε. The results indicate that plane perpendicular to the direction of tension. By contrast, there
high strain-hardening UHPC achieves high ductility by forming was no AE sources in the low strain-hardening UHPC, and only 4 AE
multiple microcracks invisible to naked eyes (typically below sources were detected in high strain-hardening UHPC. The AE
0.05 mm) in the strain-hardening stage. sources in this stage might be motivated by the first UHPC matrix
cracking and fiber-matrix debonding.
4.3.3. Comparison of three types of UHPCs At point C, more AE sources at different height were detected in
As shown in Table 5, it is observed that when strain at point B strain-hardening UHPCs, indicating that multiple cracks occurred,
(strain at 2000mε), the crack width of high strain-hardening UHPC, while the new AE sources generated in the same plane for strain-
low strain-hardening UHPC and strain-softening UHPC were softening UHPC. It is interesting to see that although 53 AE sour-
0.02 mm, 0.1 mm and 0.5 mm, respectively. The results indicate ces were detected in high strain-hardening UHPC at point C, where
that strain-hardening behavior can improve the crack width control none of the detectable cracks with minimum width of 0.01 mm
ability of UHPC. In the other hand, when crack width reached were detected. This is a strong evidence to the fact that microcracks
0.05 mm (point A), the corresponding strain of high strain- with width smaller than 0.01 mm were generated in the high
hardening UHPC and low strain-hardening UHPC (0.431% and strain-hardening UHPC when it has a strain below 600mε.
0.093%, respectively) are very close to their ultimate tensile strain During the point D to point F, AE source locations of strain-
(0.426% and 0.115%, respectively). Meanwhile, the slope of crack softening UHPC show a tendency to concentrate around the thin
width-strain curves in the curves of two strain-hardening UHPCs plane at the same height, while that of strain-hardening UHPCs
become significantly steep at point A as shown in Fig. 5(b)-(c), show a wider distribution range. Especially for high strain-
which is a strong evidence to the crack localisation when UHPC hardening UHPC, the AE source locations distribute a widely-
reached the ultimate tensile strain and turns into strain-softening spread over the whole specimen.
stage. In other word, the crack width control ability of UHPC can To better represent the AE sources distribution, Fig. 12 shows the
be improved by increasing its ultimate tensile strain, which is distribution of the AE source locations till point E. The specimen is
meaningful for the durability or structural safety issues of UHPC in divided into ten equal parts along the height of 500 mm. In strain-
the serviceability limit state. softening UHPC, AE sources were detected in three parts, where
24 J.-Y. Wang, J.-Y. Guo / Cement and Concrete Composites 88 (2018) 17e28
wUt
εUt;soft ¼ (8)
lU
Where,
Table 5
Tensile properties of three types of UHPCs at point A and B illustrated in Fig. 5.
Specimen types fUte εUte fUtu εUtu A (w* ¼ 0.05 mm) B (ε* ¼ 0.02%)
/MPa /% /MPa /%
s/MPa ε/% s/MPa w/mm)
Fig. 7. Photos of the high strain-hardening UHPC specimen at different tensile strains.
5. Conclusion
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