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KOLEJ KEMAHIRAN TINGGI MARA SRI GADING

DIPLOMA IN CONSTRUCTION TECHNOLOGY


(BUILDING FORENSIC & MAINTENANCE)
TECHNICAL SCIENCE (DCC 1052)
REPORT OF ACID,BASE AND SALT

NAME I/C
MUHAMMAD TAUFIQ BIN SABLI 970420-01-6445
MUHAMMAD ASYRAF BIN ZAIN 971110-01-6719
KHAIRUL FAIZI BIN MD SUMARDI 970413-01-5559
SHAIKH AHMAD BAKHTIAR BIN SHAIKH ILYAS 970224-01-5403
MUHAMMAD DANIEL BIN ABD. HAMID 960305-14-6261

CLASS : DTF 1B
LECTURER: PUAN SALIHAH BINTI SOMBAR@ABD. HAMID

TABLE OF CONTENTS
CONTENTS PAGE
TABLE OF CONTENTS
INTRODUCTION
OBJECTIVES
PROCEDURE
APPARATUS
DISCUSSION
CONCLUSION
APPENDIX
INTRODUCTION

Acid-base titration is method in volumetric analysis used to


determine exactly the equivalence point. Equivalence point in a
titration is the point at which the reaction is stoichiometrically
complete. Consider the reaction :

HA(aq) + BOH(aq) ------> H2O(l) + BA(aq)


The equation in ionic form is :
H+(aq) + OH- (aq) ------> H2O(l)
At the equivalence point of a strong acid-strong base titration,the
acid concentration is equivalent to the base concentration or [H+] =
[OH-] where [H-] is the acid concentration and [OH-] is the base
concentration. The mole ratio of acid to base is 1:1 .
APPARATUS

Burette , 50 ml Conical flask 250 ml

pH meter Pipette
Beaker 100 Ml Acetic Acid

Hydrochloric acid Sodium Hydroxide

Phenolphthalein indicator
PROCEDURE

1. Pipette 20 ml of 0.1 m
HCI into a 250 mL
conical flask. Add 5
drops of
Phenolphthalein
indicator. Titrate the
acid with 0.1 M NaOH
from the burette until
the solution becomes
pink
2. Repeat procedure 1
to get an average
volume of NaOH
used. Record the
volume in Table 2 in
your lab report sheet.
Let the volume as x
mL
3. Pipette 20 mL of 0.1
M HCI solution into a
100 mL beaker. Using
a burette,add (x-3)
mL of 0.1 M NaOH
solution into the
beaker and record
the pH value
4. Repeat the addition
of 0.1 M NaOH Addition Volume of
solution to the NaOH
beaker as shown in added (mL)
Table 1. Record the
2 1.00
pH value for every
3 0.50
addition of NaOH and
complete the Tablen3 4 0.50
in your lab report 5 0.50
sheet. 6 0.20
7 0.20
8 0.20
9 0.20
10 0.20
11 0.50
12 0.50
13 0.50
14 1.0
OBJECTIVES

1. Student are able to perform a strong acid-strong base


2. Students are able to plot titration curves
3. Students are able to determine the critical level range
and pH at the equivalence point from the titration
curves
Addition Volume of Cumulative pH value
NaOH added Volume of
(mL) NaOH (mL)
1 - 16.5 1.37
2 1.00 17.5 1.74
3 0.50 18.0 1.89
4 0.50 18.5 2.26
5 0.50 19.0 4.81
6 0.20 19.2 10.18
7 0.20 19.4 10.83
8 0.20 19.6 11.15
9 0.20 19.8 11.40
10 0.20 20.0 11.60
11 0.50 20.5 11.61
12 0.50 21.0 12.08
13 0.50 21.5 12.26
4 1.00 22.5 12.24
DISCUSSION

Firstly our group adding 5 drops of Phenolphthalein indicator.


Then, titrate the acid with 0.1 M NaOH from the burette until
the solution becomes pink. We repeat the procedure for the
second time to get an average volume of NaOH used.
Thus, we record the volume in Table 2 in our lab report
sheet. Let the volume as x mL. Finally, we using a
burette, add (x-3) mL of 0.1 M NaOH solution into the
beaker and record the pH value.
APPENDIX
CONCLUSION

From our experiment, the critical range result is 11.04 pH,


while the equivalence point is 6.89 . Differentiate percentage
is 1.57%.
Finally, the
overall of this
result is
satisfied.

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