SISTEMA DE GESTIÓN DE LA CALIDAD Código: I.PRD.47.

2
INSTRUCTIVO Versión: 01
Área: Producción
Raw Material Analysis for Animal Feeding Purposes
Página 1 de 4

Group Analysis Method/technique Result Limit of detection

Microbiological Salmonella ISO 6579:2002 Absence 0 in 25g
Microbiological Enterobacterias ISO 21528-22004 < 300 ufc/g 2ufc/g
Heavy metals Lead (Pb) AOAC 999.11 5ppm 0,01 ppm
Heavy metals Cadmium (Cd) AOAC 999.11 1ppm 0,01 ppm
Heavy metals Arsenic (As) AOAC 986.15 40ppm 0,01 ppm
Heavy metals Mercury (Hg) AOAC 986.15 0,2ppm 0,01 ppm
Dioxins Dioxins and furans XDS-CALUX Absence
Dioxins Dioxin-like PCB´s (dl- XDS-CALUX Absence
PCB´s)
Dioxins Sum of dioxina, furans and XDS-CALUX Absence
dl-PCB´s
Colorants Crystal violet LC/MS-MS; HLPC-FLUO; Absence 2ppb
HPLC-VIS; HPLC-UV
Colorants Leucocrystal violet LC/MS-MS; HLPC-FLUO; Absence 2ppb
HPLC-VIS; HPLC-UV
Colorants Malachite green LC/MS-MS; HLPC-FLUO; Absence 2ppb
HPLC-VIS; HPLC-UV
Colorants Bright green dye LC/MS-MS; HLPC-FLUO; Absence 2ppb
HPLC-VIS; HPLC-UV
Colorants Melanine LC/MS-MS; HLPC-FLUO; 2,5 ppb 6ppm
HPLC-VIS; HPLC-UV
Pesticides 4,4- LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
Dichlorobenzophenone HPLC-VIS; HPLC-UV
Pesticides Aldrin (SP) LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Cis Chlordae LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Trans Chlordane LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides DDD-pp + DDT-op LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Dichlobenil LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Diclobutrazol LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Heptachlor (SP) LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV

Propiedad de: AcuaNativa SpA

 SISTEMA DE GESTIÓN DE LA CALIDAD Código: I.PRD.47.2
INSTRUCTIVO Versión: 01
Área: Producción
Raw Material Analysis for Animal Feeding Purposes
Página 1 de 4

Pesticides Mirex LC/MS-MS; HLPC-FLUO; Absence 10µg/kg

HPLC-VIS; HPLC-UV
Pesticides o,p-DDD LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides o,p-DDE LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides p,p-DDE LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides p,p-DDT LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Pesticides Cypermethrin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Pesticides Deltamethrin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Pesticides Lufenuron LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Abamectin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Oxolinic acid LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Amoxicillin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Ciprofloxacin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Chlortetracycline LC/MS-MS; HLPC-FLUO; Absence 100µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Diflubenzuron LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Doxicycline LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Emamectin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Enrofloxacin LC/MS-MS; HLPC-FLUO; Absence 6ppb
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Erythromycin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Sparmycin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Florfenicol LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Propiedad de: AcuaNativa SpA
 SISTEMA DE GESTIÓN DE LA CALIDAD Código: I.PRD.47.2
INSTRUCTIVO Versión: 01
Área: Producción
Raw Material Analysis for Animal Feeding Purposes
Página 1 de 4

Antiotics/antiparasites Flumequine LC/MS-MS; HLPC-FLUO; Absence 6ppb

HPLC-VIS; HPLC-UV
Antiotics/antiparasites Ivermectin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Oxytetracycline LC/MS-MS; HLPC-FLUO; Absence 100µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Penicilin G LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Sarafloxacin LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Teflubenzuron LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Tetracycline LC/MS-MS; HLPC-FLUO; Absence 100µg/kg
HPLC-VIS; HPLC-UV
Antiotics/antiparasites Trimetoprim LC/MS-MS; HLPC-FLUO; Absence 20µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfachloropyridazine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfadiazine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfadimethoxine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfadoxin LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfamerazine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfamethazine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfamethoxazole LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfamethoxipiridazine LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfaquinoxaline LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Sulfamides Sulfatriazole LC/MS-MS; HLPC-FLUO; Absence 10µg/kg
HPLC-VIS; HPLC-UV
Hormones Dienestrol LC/MS-MS; HLPC-FLUO; Absence 2µg/kg
HPLC-VIS; HPLC-UV
Hormones Hexestrol LC/MS-MS; HLPC-FLUO; Absence 2µg/kg
HPLC-VIS; HPLC-UV
Propiedad de: AcuaNativa SpA
 SISTEMA DE GESTIÓN DE LA CALIDAD Código: I.PRD.47.2
INSTRUCTIVO Versión: 01
Área: Producción
Raw Material Analysis for Animal Feeding Purposes
Página 1 de 4

Nitrofurans AHD LC/MS-MS; HLPC-FLUO; Absence 1µg/kg

HPLC-VIS; HPLC-UV
Nitrofurans AMOZ LC/MS-MS; HLPC-FLUO; Absence 1µg/kg
HPLC-VIS; HPLC-UV
Nitrofurans AOZ LC/MS-MS; HLPC-FLUO; Absence 1µg/kg
HPLC-VIS; HPLC-UV
Nitrofurans SEM LC/MS-MS; HLPC-FLUO; Absence 1µg/kg
HPLC-VIS; HPLC-UV

Propiedad de: AcuaNativa SpA