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Metall. Res. Technol.

Vol, No (2017)
© EDP Sciences, 2017 Metallurgical Research
DOI: 10.1051/metal/2017024 &
Technology
Available online at:
www.metallurgical-research.org

REGULAR ARTICLE

Potential of horizontal direct chill cast EN AW 6082 rods


as forging stock in the manufacture of light weight
suspension components
Yucel Birol1,*, Emre Gokcil2, and Seracettin Akdi2
1
Metallurgical and Materials Engineering Department, Dokuz Eylul University, Izmir, Turkey
2
R&D Centre, AYD Steering and Suspension Parts, Selcuklu, Konya, Turkey

Received: 6 January 2017 / Accepted: 20 March 2017

Abstract. Commercial EN AW 6082 rods cast at less than 50 mm in diameter via horizontal casting appear to
be adequate candidate as forging stock for the manufacture of small size automotive suspension components.
Cast forging stock relies entirely on the forging deformation to develop the fibering known to be very beneficial
for superior dynamic and impact properties. Hence, the forging die design is critical to ensure the sufficient
amount and suitable orientation of fibering across the section of the component. Forgings produced from cast
stock, submitted to an artificial ageing cycle directly after the forging step offer superior fatigue and impact
energy values with respect to their counterparts processed with a solution heat treatment (SHT). The superior
fatigue and impact energy values of the former are attributed to the particle characteristics; i.e. the spacing of
void forming particles in these forgings is relatively smaller than in forgings processed with a separate SHT. The
coalescence of voids at these particles eventually occurs at smaller loads and deteriorates toughness.
Keywords: aluminium alloys / hardness measurement / mechanical characterization / light microscopy /
thermomechanical processing / age hardening

1 Introduction of long parts like control arms, cast forging stock has also
received attention [6–13]. Casting-forging route is regarded
Unlike castings, aluminium forgings are always porosity suitable only for large section forgings since the DC cast
free thus taking advantage of well established heat billets are seldom produced at less than 150 mm diameter.
treatment processes to improve mechanical properties in Lack of commercial cast forging stock in small diameters
heat treatable aluminium alloys [1]. When forged and heat makes an intermediate extrusion process inevitable for
treated, common aluminium alloys exhibit a far superior relatively small forging components.
strength to weight ratio than many grades of steel. The Horizontal direct chill (HDC) casting units are techni-
distinct advantage of forged aluminium components stands cally capable of producing smaller diameter aluminium alloy
out when the forging is designed to provide optimum grain rods either for extrusion stock or as foundry alloy ingot. Such
structure to suit the application improving both static and rods at suitable diameters (d < 50 mm) are thus commercial-
cyclic properties [2]. Optimum mechanical properties are ly available. Their much smaller size renders an extrusion
obtained in the fibre direction. step to reduce their diameter to forging stock unnecessary.
One of the most popular applications of aluminium The present work was undertaken to investigate the
forgings is the automotive suspension components [3]. The potential of HDC EN AW 6082 rods at less than 50 mm in
material of choice for this application is often the age- diameter for the manufacture of EN AW 6082 alloy
hardening EN AW 6082 alloy because of its excellent suspension components. Recently, it has been shown that
combination of mechanical properties and corrosion resis- a forging process cycle without a solution heat treatment
tance [4,5]. The EN AW 6082 forging stock is typically (SHT) offers a more uniform structure across the section of
produced with the extrusion of direct chill (DC) cast billets to the EN AW 6082 alloy forgings with substantial benefits in
reduce its diameter to forging stock dimensions. While mechanical properties [14]. It is of great interest to find out if
extruded bar is the standard forging stock in the manufacture the processing of cast forging stock without a separate SHT
offers the same benefits as for extruded forging stock. Hence,
the forging campaigns conducted on an industrial scale in the
* e-mail: yucel.birol@deu.edu.tr present investigation were planned with and wihout a SHT.
2 Y. Birol et al.: Metall. Res. Technol. Vol, No (2017)

2 Experimental which is capable of operating at 100 Hz with a maximum


load of 15 kN. The fatigue test samples were prepared
Commercial EN AW 6082 alloy rods produced with the according to ASTM-E466 and cycled at a stress amplitude
HDC casting process with a diameter of 42 mm were used of 175 MPa, at a frequency of 30 Hz with a minimum to
for industrial scale forging experiments. The chemical maximum stress ratio of 1. The fatigue test results were
composition of these rods were measured with a commer- reported as the average number of cycles to fracture from 5
cial optical emission spectroscopy unit and are listed in different fatigue tests of the same group. The location of
Table 1. The as-cast rods were first submitted to a samples machined from the forgings for the tensile, fatigue
homogenization treatment to eliminate the interdendritic and impact tests is described in detail in [14].
segregation. This was an 8-h treatment at a temperature of
570 °C followed by furnace cooling. Half of the homogenized 3 Results and discussion
bars were preheated to approximately 520 °C and were
forged on a 1600 ton forging press into suspension parts
before they were immediately quenched in water. The The macrostructure across the transverse section of the
forged components were subsequently solutionized at HDC cast rod is shown in Figure 2a. The section is free from
530 °C for 4 h and quenched in water before they were flaws, porosity and shrinkage. The grain structure is
artificially aged at 180 °C for 8 h (Group 1, Fig. 1a). The uniform across the section and the average grain diameter
second group of suspension components were processed in a is estimated to be 99.5 ± 7.1 mm (Fig. 2b). These features
similar manner. However, several revisions were imple- are typical of vertical direct chill (VDC) casting and show
mented in the preheating, forging and post-forging no unanticipated differences in the HDC cast counterpart.
operations to ensure sufficient Mg and Si solute levels It is worth noting, however, that the present cast stock
before the artificial ageing treatment. The round bars were reveals a substantial level of interdendritic segregation,
preheated to 560 °C, a higher temperature with respect to quite untypical of VDC cast billets (Fig. 3). These
that employed in Group 1 and were forged into the same segregation patterns cannot be accounted for by gravity
suspension components with the same forging parameters. effects since they appear to be quite symmetrical with
These forgings were quenched in water right after the respect to the casting axis. Considering that the HDC cast
forging operation and were directly artificially aged at rods are cast at much smaller diameters than the VDC cast
180 °C for 8 h (Group 2, Fig. 1b). billets, the marked segregation in the former is rather
unexpected and needs to be eliminated before any hot
Samples sectioned from the as-received horizontally working operation. It is also inferred from the extent of
cast and homogenized rods and samples from the precipitation across the section of the cast rods that the
artificially aged forgings were prepared with standard cooling rate following solidification has been rather slow.
metallographic techniques: ground with SiC paper, This is consistent with the hardness of the horizontally cast
polished with 3 mm diamond paste and finished with rod, 60 ± 0.8 HB, which is considerably higher than the soft
colloidal silica. Their microstructures were examined after temper value.
etching with a 0.5% HF solution using a Nikon MA200 A homogenization cycle was employed to eliminate the
model optical microscope to identify the particle features. segregation of the cast stock. Typical microstructures near
The grain structures across different sections of the the edge and at the center of the homogenized rods are
forgings were checked after etching in a solution of %32 shown in Figure 4a and b, respectively. The microstruc-
HCl, %32 HNO3, %32 H2O and %4 HF. Sections from the tural features of the section are generally similar. The
forging stock, forged and heat treated components were homogenized rod is characterized with coarse Fe-based
also anodised in Barker’s solution, 5 mL HBF4 (48%) in intermetallic particles, intermediate size dispersoids and a
200 mL water, and then examined with an optical very fine dispersion of Mg-Si precipitates. The precipitate
microscope under polarized light. X-ray diffraction free zones mark the grain boundary network. The coarse
(XRD) patterns were recorded with a Rigaku D/Max compound particles and intermediate size dispersoids
2200/PC Diffractometer equipped with CuKa radiation to (Fig. 4) were identified by XRD analysis to be cubic
assist in the identification of the intermetallic particles. ac-Al12(Fe,Mn,Cr)3Si particles and a fine dispersion of
Hardness of the forgings was measured with a Brinell Mg2Si precipitates (Fig. 5). Mn and Cr is responsible for the
Hardness Tester under a load of 250 kgf using 5 mm predominance of the cubic phase over the monoclinic
diameter steel ball with a dwell time of 10 s. The tensile b-Al5FeSi variety and the homogenization anneal certainly
tests were performed using a screw driven ZWICK/ must have helped with the b-Al5FeSi ! ac-Al12(Fe,Mn,
ROELL Z250 tensile testing machine in air at room Cr)3Si transformation [15]. Hardness of the homogenized
temperature. The cross-head speed was 1 mm/min. The material was measured to be 60.1 ± 1 HB, implying a slow
strain was measured with an extensometer attached to the cool down following homogenization retaining a fraction of
sample and with a measuring length of 36 mm. The 0.2% Mg and Si in solution.
proof stress was reported as the yield stress. Samples Microstructures of the Group 1 forgings near the edge
processed with and without a SHT were tested for their and at the centre of the section of the suspension
toughness by using a 300 J pendulum impact testing component are shown in Figure 6a, c and b, d, respectively.
machine (DMC 6705CE, UK) in the Charpy mode at an In the latter group, the precipitate-free boundaries
impact velocity of 5.24 m/s. Fatigue tests were conducted delineate equiaxed dendritic grains near the edge of the
on a MTS Landmark desktop model fatigue testing unit section (Fig. 6a and c). The microstructure at the centre of
Y. Birol et al.: Metall. Res. Technol. Vol, No (2017) 3

casng homogenizaon preheang soluonizing a)Group 1


forging

temperature
700 °C
570 °C quenching
530 °C
520 °C

ageing 180 °C

me
casng homogenizaon Preheang-forging
temperature

700 °C quenching
b) Group 2
570 °C
560 °C

ageing 180 °C

me
Fig. 1. The forging cycles employed (a) with and (b) without a separate solution heat treatment.

Table 1. Chemical composition of the EN AW 6082 alloy forging stock (wt.%).

Si Fe Mn Mg Cu Cr Ti Zn Al
1.18 0.224 0.7476 0.707 0.065 0.142 0.038 0.01 96.79

the section, on the other hand, is markedly different. A very the cast stock have apparently not been deformed to an
dense dispersion of particles is the predominant feature appreciable extent during the forging process. The friction
with no evidence of precipitate-free zones (Fig. 6b and d). in the contact zone between the forging die and the work
The particles seem to be aligned at still higher resolutions piece leads to a sticking that avoids the free plastic flow of
(Fig. 6d) due to the plastic flow associated with hot forging. the surface grains.
Surprisingly, the forgings that have been submitted to a The shape factor of the grains were estimated and were
SHT, reveal almost identical features (Fig. 7). It should be plotted on a semi-logarithmic scale as a function of depth
noted, however, that the number density of the particles is from the surface (Fig. 10). It is inferred from Figure 10 that
markedly higher in Group 1 forgings. the surface region that covers approximately 20% of the
The transverse section of the forgings from Group 1 and mid-section has not been affected by the forging deforma-
Group 2 look very similar at overview magnifications tion. From this point on, grains are gradually replaced with
(Fig. 8). There is no evidence for coarse surface grains that pancake shaped grains while traversing towards the centre.
form particularly during the SHT of forgings produced Finally, the grains at the centre of the section are fully
from extruded stock [7]. Such peripheral coarse surface fibrous. The shape factor increases to approximately 20
grains are known to degrade the surface quality and reduce near the centre. These features are almost identical in
the impact toughness of the high strength extrusions and Group 1 and Group 2 forgings in spite of a high temperature
forgings [16,17]. Micrographs taken from the same sections, SHT after forging in the former. The SHT that has a
from the edge to the centre, after anodising are shown in marked effect on the section grain structures in the forging
Figure 9b and c, respectively. The section grain structure of of suspension components from extruded stock does not
the cast rod is also included to evidence the extent and appear to have any effect in the case of cast forging stock. It
distribution of fibering upon forging operation (Fig. 9a). has been shown earlier that SHT is the single most critical
They are consistent with the metallographic analysis of step of the entire thermomechanical processing of extruded
transverse sections. It is evident from Figure 9b and c that forging stock with a very negative impact on the grain
the grains at the edge of the section are predominantly structure [6,7]. The only step that can introduce deforma-
equiaxed in both groups of forgings. The surface grains of tion to the strain-free cast forging stock and form the
4 Y. Birol et al.: Metall. Res. Technol. Vol, No (2017)

a b a

1cm 500μm

Fig. 2. (a) Section photo and the (b) grain structure of the
horizontally cast EN AW 6082 rod.

20μm
a
b
!

200µm 20μm
b Fig. 4. Microstructure of homogenized EN AW rod near the edge
(a) and at the centre (b) of the section.

Al(111) Al(200
Intensity (a.u.)

: αc-Al12(Fe,Mn,Cr)3Si
: β-Mg2Si

100µm 30 35 40 45 50 55 60
2θ (degrees)
Fig. 3. Dendritic segregation of the horizontally cast EN AW
6082 rod (a, b). Fig. 5. X-ray diffraction spectrum of the homogenized material.

fibrous grains in the entire processing cycle is the forging stock. The hardness profiles across the section of forgings
step. It is then fair to conclude from the similarity of the (Fig. 11) are uniform across the section and a hardness drop
structural features of Group 1 and 2 forgings that the near the edge that would signal such a softening process is
subsequent SHT fails to renew the grain structure due to not evident. In summary, the section structure of
the high levels of Mn and Cr in the present alloy. There is suspension components forged from HDC cast rods with
no evidence to claim that recrystallization has taken place and without a subsequent SHT is claimed to be adequate
during the entire forging cycle. The cast forging stock, with no coarse surface grains and with substantial degree of
having additionally been homogenized, is entirely free of fibering that is known to be very advantageous in terms of
any retained deformation, unlike the extruded forging dynamic and impact properties. The fibering of the grains
Y. Birol et al.: Metall. Res. Technol. Vol, No (2017) 5

a b

100µm 100µm

c d

20µm 20µm
Fig. 6. Microstructure of the Group 1 suspension component near the edge (a, c) and at the centre (b, d) of the transverse section.

and its alignment with the loading of the component can be impact fracture energy of Group 2 samples is striking. Both
improved further by further optimization of the forging die the number of cycles to fracture and the impact energy
design. This work is underway at AYD tool shop. values of Group 2 forgings, processed without a SHT, are
The mechanical properties of the forgings produced nearly twice as those of Group 1 forgings. Such improve-
with (Group 1) and without a SHT (Group 2) prior to ments in dynamic and impact properties in spite of
artificial ageing are listed in Table 2. The tensile properties comparable hardness and tensile properties is consistent
are essentially similar. This is not surprising considering with a previous report [14,18]. It is fair to conclude that the
the nearly identical microstructural features of the two benefits of a forging process without a separate SHT [14],
groups (Figs. 6 and 7). It is worth noting, however, that the has been confirmed also for the cast forging stock in the
tensile properties are relatively superior with respect to the present work.
suspension components produced from extruded stock It has been reported that forgings of the same alloy, in the
using the same processing cycles employed in the present same temper, with comparable hardness and tensile proper-
work [14]. Hardness of the Group 1 and 2 suspension ties can show markedly different fracture behaviour, depend-
components were measured to be 117 ± 1 and 116 ± 4 HB, ing on the intermetallic particle characteristics [18–24]. An
respectively, and suggest that the elimination of the SHT in increase in the spacing of intermetallic particles delays void
the processing cycle does not degrade the age hardening nucleation to higher loads and improves toughness while
potential of the present alloy owing to the fine tuning the smaller inter-particle spacing accelerates fracture through
preheating and the post hot forging operations. the formation of coarse voids [25]. The spacing of particles is
In contrast to tensile properties, there are marked relatively smaller in Group 1 forgings than in Group 2. This is
differences in the fatigue lives and the Charpy impact confirmed with the image analysis of section micrographs
energy values of the two groups. The improvement in the that evidence the difference between the particle character-
number of cycles to fracture under cyclic loading and the istics (Fig. 12). The total number of particles in unit area of
6 Y. Birol et al.: Metall. Res. Technol. Vol, No (2017)

a b

100µm 100µm

c d

20µm 20µm
Fig. 7. Microstructure of the Group 2 suspension component near the edge (a, c) and at the centre (b, d) of the transverse section.

a b

1mm

Fig. 8. Overview of the section of (a) Group 1 and (b) Group 2 suspension component.
Y. Birol et al.: Metall. Res. Technol. Vol, No (2017) 7

500μm

500μm

500μm

Fig. 9. Grain structures across the section of (a) cast rod, (b) Group 1 and (c) Group 2 suspension components.

130

2,0 120
Group 1
110
log (grain shape factor)

Group 2
hardness (HB)

1,5
100

90
1,0
80

0,5 70
Group 1
edge centre 60 Group 2
0,0 50
0,0 0,2 0,4 0,6 0,8 1,0 1 2 3 4 5 6 7
fraction mid-section depth from surface (mm)
Fig. 10. Change in the shape factor of grains across the section of Fig. 11. Change in hardness across the section of (a) Group 1 and
suspension components with depth from the edge of the section. (b) Group 2 suspension components.

Table 2. Mechanical properties of suspension components produced from horizontally cast EN AW rods with and
without a SHT.

Group Process s Y (MPa) s UTS (MPa) A50 (%) Hardness (HB) Cycles to fracture (Nf) Impact energy (J)
Group 1 w/SHT 329 356 10.9 117 ± 1 125,269 ± 97,570 9±1
Group 2 w/o SHT 340 372 10.1 116 ± 4 300,736 ± 206,025 17 ± 3
8 Y. Birol et al.: Metall. Res. Technol. Vol, No (2017)

a) GROUP 1 b) GROUP 2

Fig. 12. Image analysis results of (a) Group 1 and (b) Group 2 suspension components.

Group 1 forgings is markedly higher leading to a smaller inter- References


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Cite this article as: Yucel Birol, Emre Gokcil, Seracettin Akdi, Potential of horizontal direct chill cast EN AW 6082 rods as
forging stock in the manufacture of light weight suspension components, Metall. Res. Technol. Vol, No (2017)

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