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Keywords: Ohmic heating (OH) is a new heating method with high electrothermal conversion, simple equipment, high
Electrical conductivity accuracy of temperature control, and rapid heating. It is used in cooking rice. This study aimed to investigate the
Equivalent circuit effects of OH on the expansion behavior of rice grains, changes in the electrical conductivity (EC) of each
Ohmic heating
component, temperature, and quality at different heating rates (3 ◦ C/min, 6 ◦ C/min, and 9 ◦ C/min). The EC of
Rice
the rice grains was calculated using the equivalent circuit method. The results showed that the total volume of
the water–rice mixture did not change significantly during the heating stage of OH cooking of rice. The volume
and the proportion of rice in the water–rice mixed layer increased slowly before 62.5 ◦ C and then rapidly after
that. The EC of the water layer rice soaking water was lower than that of the water–rice mixed layer rice soaking
water. The regression models of the volume of the water–rice mixed layer, the proportion of rice in the mixed
layer, and the EC of each component were established. Besides, the internal temperature distribution was uneven
due to the difference in the EC of each part of the mixture, and the temperature gradually decreased from top to
bottom. Hence, the upper rice grains softened faster. This finding provided technical support to develop an
automatic rice cooking device with high efficiency using OH.
* Corresponding author.
E-mail address: xingshu-li@nwsuaf.edu.cn (X. Li).
https://doi.org/10.1016/j.ifset.2021.102757
Received 15 May 2021; Received in revised form 4 July 2021; Accepted 5 July 2021
Available online 8 July 2021
1466-8564/© 2021 Elsevier Ltd. All rights reserved.
X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
2008).
Fig. 1. Schematic diagram of ohmic heating experimental system for 2.2. OH experimental system for rice cooking
rice cooking.
The OH experimental system shown in Fig. 1 consisted of a control
half each. However, these hypotheses were contrary to the results of the system, an OH vessel, and a personal computer (ZX6-CP5S1, Hasee
preliminary experiment. In addition, the heating rate had a great in Group Co., Ltd., Shenzhen, China). The control system included MCU
fluence on the volume and EC of the water–rice mixture. Therefore, it (Micro Control Unit, STC12C5A60S2, Hongjing Technology Co., Ltd.,
was necessary to measure and infer the EC of each component of the OH Shenzhen, China), data acquisition module, and voltage regulator
cooking of rice more comprehensively and accurately. Most of the module. The data acquisition module collected voltage, current, and
existing OH rice cooking devices adopt constant-voltage heating. As the temperature data using voltage acquisition circuit (DL-PT202H1,
temperature increased, the EC of the water–rice mixture increased, and Xiangshang Electronics Co., Ltd., Nanjing, China), current acquisition
the heating rate inevitably became larger. However, the heating rate was circuit (DL-CT1010A, Xiangshang Electronics Co., Ltd.), and tempera
an important factor that affected the quality of rice (Ling Zhu et al., ture sensor circuit (WRCK-191, Wolan Instrument Co., Ltd., Shanghai,
2020), but it was difficult to obtain a constant heating rate for cooking China). A feedforward compensator was used to control the heating rate,
rice with constant voltage. while a PID (Proportion Integral Differential) controller was used to
Therefore, the objectives of this study were to (1) use a self- control the heat preservation temperature. PWM (pulse width modula
developed OH experimental system that can achieve a constant heat tion) signals were output with different duty cycles to adjust the output
ing rate to cook rice, and measure the EC of each component of the voltage, achieving the purposes of constant heating rate and heat pres
water–rice mixture during the rice cooking process at different heating ervation temperature.
rates; (2) calculate the EC of rice grains by the equivalent circuit The OH vessel structure and material height measurement are pre
method, which was an improved experimental method from Kanjana sented in Fig. 2. Three temperature sensors were located at the center of
pongkul (2017), and fit the EC regression model to provide electrical the water layer (recorded as the water layer temperature, shown in Fig. 2
characteristic reference for the computer simulation analysis of OH point A), the center of the water–rice mixed layer (recorded as the
cooking of rice; and (3) analyze the changes in rice quality and tem water–rice mixed layer temperature, shown in Fig. 2 point B), and the
perature during the cooking process and provide technical support for center of the water–rice mixture (recorded as the central temperature,
the development of OH experimental system. shown in Fig. 2 point C). The OH vessel was welded with a transparent
heat-resistant Plexiglass with a thickness of 5 mm to observe the
expansion of rice grains during the OH cooking process (Derde, Gomand,
2. Material and methods
Courtin, & Delcour, 2014). A pair of stainless steel plate electrodes with
a thickness of 1 mm were installed on both sides of the vessel. The in
2.1. Material and sample preparation
ternal dimensions of the vessel are 75 × 80 × 70 mm3. A transparent
ruler was pasted on one side of the vessel, and a camera was used to
Milled Japonica rice (Oryza sativa L.) was produced by Yihai Kerry
record the height change of the water–rice mixture during the cooking
Arawana Holdings Corporation (Jinlongyu, Panjin City, China) pur
process. The upper end of the vessel was covered with a foam board with
chased from a local market, and the average initial moisture content was
a rubber gasket during the test to keep it warm and prevent the evap
11.86 ± 0.16 g/100 g wet basis (w.b.). The gelatinization temperature of
oration of water during the cooking process. The surfaces were pasted
the rice was 72.9 ± 5.2 ◦ C, which determined by using the Chinese
with an insulation sponge with a thickness of 10 mm.
National Standard Method (GB/T 24852, 2010). The average length,
The height of the water–rice mixture was recorded with the tem
width, and thickness of the rice grains were 4.73 ± 0.32 mm, 2.81 ±
perature change during the cooking process with OH. The EC, σ (μS
0.24 mm, and 2.01 ± 0.16 mm, respectively. The packaged rice samples
cm− 1) of the water–rice mixture was calculated using Eq. (1) (Liu et al.,
in original sealed plastic bags were stored at 3 ± 1 ◦ C with 48% ± 0.5%
2017):
relative humidity in a refrigerator until testing (Liu & Wang, 2019). Tap
water was used in this study because it is generally used in cooking rice. i(T) L
σ= ⋅ (1)
Then, 30 L of tap water whose EC was 162.37 ± 8.41 μS/cm at 25 ◦ C was u(T) WH(T)
stored in a container for all tests.
Further, 100 g rice was soaked in 150 mL of tap water (water–rice where i(T) is the current (A) that flows through the sample at temper
ratio (mL/g) was 1.5:1) at room temperature (Zhu et al., 2020). The ature T, u(T) is the applied voltage (V) across the faces at temperature T,
water–rice mixture was cooked after soaking for 30 min (GB/T 15682, L is the length (cm) of the sample, W is the width (cm) of the electrode
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X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
Fig. 4. Central temperature change curves of water–rice mixtures when cook Fig. 5. Volume changes in water and rice in the water–rice mixtures during
ing rice by OH. ohmic cooking rice (square ■: 3 ◦ C/min; round ●: 6 ◦ C/min; triangle ▴: 9 ◦ C/
min; solid ■: total volume of water–rice mixtures; hollow □: total volume of
water–rice mixed layer).
1 1 1 1 1 1
= + = + + (8)
R(T) Rw (T) Rm (T) Rw (T) Rr (T) Rm− w (T)
temperature increase at the center of the water–rice mixtures was
1 H(T)⋅W 3.01 ◦ C/min, 6.07 ◦ C/min, and 9.17 ◦ C/min, and the R2 was >0.9995. In
= σ (T)⋅ (9) other words, the temperature changes in the water–rice mixtures met
R(T) L
the requirements of constant-rate heating of 3 ◦ C/min, 6 ◦ C/min, and
1 Sw (T) 9 ◦ C/min.
= σ w (T)⋅ (10)
Rw (T) L
4.1.2. Effect of the OH rate on the volumes of water–rice mixture and
1 Sr (T) water–rice mixed layer
= σr (T)⋅ (11)
Rr (T) L Fig. 5 shows the volume change in water and rice in the water–rice
mixtures during the OH cooking of rice. Before the central temperature
1 Sm− w (T) of the water–rice mixture rose to 40 ◦ C, the volume of the water–rice
= σ m− w (T)⋅ (12)
Rm− w (T) L mixed layer hardly changed. As the temperature continued to rise, the
volume of the water–rice mixed layer and the growth rate increased.
Using the aforementioned formula, all parameters except the EC of
However, the smaller the heating rate, the larger the volume of the
the rice grains could be obtained. Therefore, this method was used to
water–rice mixed layer when heated to a certain temperature. This was
calculate the relationship between the EC of rice grains and the cooking
because when the temperature was lower than 40 ◦ C, the rice grains
temperature during the OH process.
would absorb water slowly and the expansion of rice grains was not
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X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
4.1.3. Effect of the OH rate on the proportion of rice in the water–rice 4.3. Regression models of the volume of the water–rice mixed layer, the
mixed layer proportion of rice, and the EC of each component
Fig. 6 shows the change in the percentage of rice and CSA of water
and rice in the water–rice mixtures during the OH cooking of rice. The Eqs. 13–17 are the fitted multiple regression equations of the volume
results showed that the changing trend of the proportion of rice in the V (cm3) of the water–rice mixed layer, its proportion P (%) of rice, the EC
water–rice mixed layer was similar to the volume change in the water σ (μS/cm) of each component at the temperature T (25 ◦ C–95 C), and the
–rice mixed layer. heating rate v (3 ◦ C/min to 9 ◦ C/min). After comparison, it was
concluded that the regression model was the most suitable to use a
4.2. Change in the EC of each component during OH quadratic polynomial equation
Fig. 7 shows the EC of water–rice mixtures, rice soaking water, and V = 134.93 + 3.43v–0.87 T–0.09vT + 0.02v2 + 0.02 T 2 (14)
water–rice mixed layer at different heating rates.
P = 61.60 + 0.48v–0.30 T–0.03vT + 0.05v2 + 0.01 T 2 (15)
During the OH process of cooking rice, the EC of the water–rice
mixture (σ M) and the rice soaking water of each layer (σ w and σm-w)
σ r = 69.64 + 20.93v–8.34 T–0.67vT + 0.28v2 + 0.19 T 2 (16)
increased with the temperature at the same heating rate. The EC of the
water–rice mixture (σ M) was less than the EC of the rice soaking water
σ w = 127.33 + 6.67v–11.25 T–0.24vT + 0.78v2 + 0.04 T 2 (17)
(σ w and σ m-w)), and the EC of the water layer of rice soaking water (σw)
was less than that of the water–rice mixed layer (σ m-w). This was because
σ m− = − 107.33 + 6.02v + 24.58 T–0.50vT + 0.49v2 –0.05T 2 (18)
the EC became larger due to the increase in temperature (Zhu, Guo, Jia,
w
& Kang, 2015), and the expansion of the rice grains promoted the release Table 1 shows the analysis of variance of the regression equation and
of conductive substances inside them into the water (Kanjanapongkul, the reliability analysis of the regression equation. The quadratic term of
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X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
Table 1
Analysis of variance and reliability analysis of regression equation.
Volume of water–rice mixed Rice proportion of water–rice EC of rice (Eq. (15)) EC of rice soaking water in EC of rice soaking water in
layer (Eq. (13)) mixed layer (Eq. (14)) water layer (Eq. (16)) water–rice mixed layer (Eq. (17))
F P F P F P F P F P
v 26.94 <0.0001** 81.80 <0.0001** 39.37 <0.0001** 0.3702 0.5486 109.52 <0.0001**
t 702.61 <0.0001** 1459.12 <0.0001** 1441.77 <0.0001** 3022.79 <0.0001** 6940.69 <0.0001**
vt 35.79 <0.0001** 76.37 <0.0001** 33.76 <0.0001** 4.69 0.0405* 40.22 <0.0001**
v2 0.0079 0.9300 1.32 0.2617 0.0372 0.8487 0.3015 0.5880 0.2386 0.6296
t2 117.52 <0.0001** 264.54 <0.0001** 185.24 <0.0001** 10.16 0.0040** 22.23 <0.0001**
Model 171.48 <0.0001** 365.39 <0.0001** 331.27 <0.0001** 605.81 <0.0001** 1430.52 <0.0001**
R2 0.9728 0.9870 0.9857 0.9921 0.9967
Adjusted R2 0.9671 0.9843 0.9827 0.9905 0.9959
C.V./% 2.88 1.46 14.12 3.45 2.23
Adeq Precision 44.1020 64.1113 58.7628 75.1200 119.3141
Note: *Means significant difference (P < 0.05); **means extremely significant difference (P < 0.01).
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X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
Fig. 11. Changes in rice hardness at different parts with OH temperature at 3 ◦ C/min (a), 6 ◦ C/min (b), and 9 ◦ C/min (c).
4.5. Influence of OH on temperature distribution and rice quality grains would be when heated to the same temperature. The maximum
temperature difference and the temperature standard deviation of each
4.5.1. Temperature change part were small, that is, the temperature difference between the upper
Fig. 10 shows the temperature differences at different locations of the and lower parts was small, and the temperature distribution was uni
water–rice mixture. In the heating stage, the temperature of the water form. Therefore, the swelling of rice grains was similar and the hardness
layer was higher than the temperature at the center of the water–rice difference was small.
mixture. Also, the temperature of the water–rice mixed layer was the
lowest, that is, the temperature declined from top to bottom. In the OH 5. Conclusions
process with alternating current power supply, according to the Joule
law, the heat generated per unit time and unit volume inside the ma The OH rate had an impact on the expansion of rice grains and the
terial was. changes in the EC of each component, temperature, and quality. During
the heating stage of OH process of cooking rice, the total volume of the
q = σ(E)2 (19)
water–rice mixture did not change significantly. The volume and the
proportion of rice of the water–rice mixed layer increased slowly before
where q is the internal energy generation rate per volume (W/m3), σ is
62.5 ◦ C and then rapidly after that. The EC of the water layer rice
EC (S/m), and E is the electric field (V/m) (Jo & Park, 2019; Wang & Wu,
soaking water was lower than that of the water–rice mixed layer rice
1999). In this test, the water–rice mixture was in direct contact with the
soaking water. The EC of rice grains was derived using the parallel
electrode plate, and the voltage at different contact parts was the same,
equivalent circuit method. Further, the regression models of the volume
that is, the electric field strength was the same. Hence, it was observed
of the water–rice mixed layer, the proportion of rice in the mixed layer,
that the EC of the water layer was greater than the EC of the water–rice
and the EC of each component were established, which provided elec
mixed layer. The greater the EC, the more the heat produced. Therefore,
trical characteristics reference for future computer simulations. In
the water layer produced more heat compared with the water–rice
addition, the internal temperature distribution was uneven due to the
mixed layer, which made the temperature of the water layer higher. The
difference in the EC of each part of the mixture, and the temperature
water–rice mixed layer generated heat by itself when it was energized.
gradually decreased from top to bottom. Consequently, the upper rice
At the same time, under the effect of heat conduction, the heat was
grains softened faster. The faster the whole mixture was heated, the
transferred from the water layer to the water–rice mixed layer; also, the
harder the rice grains would be. Lower ohmic heating rate (such as 3 ◦ C/
lower part was in contact with the heating vessel, and part of the heat in
min ~ 6 ◦ C/min) can make the rice quality uniform and softer. There
the lower part was lost to the outside world. Therefore, the temperature
fore, OH can be considered to be an alternative method for cooking rice
of the upper part of the water–rice mixed layer was higher than the
to replace the traditional heating method.
temperature of the lower part.
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X. Ding et al. Innovative Food Science and Emerging Technologies 72 (2021) 102757
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