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  • Bacth 2 Log 1b

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    Heni fidyayuningrum
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    The document contains the results of an ICP-OES practical laboratory for Logistics class 1B Batch 2. It includes calibration standard readings and concentration values for calcium, magnesium, and zinc. Sample readings and concentration calculations for 12 unknown samples are also presented, along with calibration curves and correlation coefficients for each element.

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    The document contains the results of an ICP-OES practical laboratory for Logistics class 1B Batch 2. It includes calibration standard readings and concentration values for calcium, magnesium, and zinc. Sample readings and concentration calculations for 12 unknown samples are also presented, along with calibration curves and correlation coefficients for each element.

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    Download as XLSX, PDF, TXT or read online from Scribd
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    18 views5 pages

    Bacth 2 Log 1b

    Uploaded by

    Heni fidyayuningrum
    The document contains the results of an ICP-OES practical laboratory for Logistics class 1B Batch 2. It includes calibration standard readings and concentration values for calcium, magnesium, and zinc. Sample readings and concentration calculations for 12 unknown samples are also presented, along with calibration curves and correlation coefficients for each element.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 5

    DATA HASIL PRAKTIKUM ICP-OES

    KELAS LOGISTIK 1B BATCH 2

    Conc. in Calib Units


    Ca 317.933 Mg 285.213 Zn 206.200
    Sample Id Acquisition Time Dataset File Method File
    (µg/g) (µg/g) (µg/g)

    1 blanko 3/19/2022 11:21:11 AM batch 2 log 1b batch 2 log 1b 0.000 0.000 0.000
    2 calib std 1 3/19/2022 11:23:32 AM batch 2 log 1b batch 2 log 1b 0.000 0.000 0.000
    3 Calib Std 2 3/19/2022 11:28:17 AM batch 2 log 1b batch 2 log 1b 0.020 0.020 0.020
    4 calib std 3 3/19/2022 11:32:22 AM batch 2 log 1b batch 2 log 1b 0.050 0.050 0.050
    5 Calib Std 4 3/19/2022 11:36:45 AM batch 2 log 1b batch 2 log 1b 0.100 0.100 0.100
    6 calib std 5 3/19/2022 11:40:26 AM batch 2 log 1b batch 2 log 1b 0.200 0.200 0.200
    7 Calib Std 6 3/19/2022 11:43:46 AM batch 2 log 1b batch 2 log 1b 0.500 0.500 0.500

    Ca 317.933 Mg 285.213 Zn 206.200


    Sample Id Acquisition Time Dataset File Method File
    (µg/g) (µg/g) (µg/g)

    8 yamalube 3/19/2022 11:49:03 AM batch 2 log 1b batch 2 log 1b 7.461 0.030 4.167
    9 top 1 3/19/2022 11:55:33 AM batch 2 log 1b batch 2 log 1b 5.805 0.014 3.375
    10 castrol 3/19/2022 11:58:39 AM batch 2 log 1b batch 2 log 1b 1.616 4.958 5.472
    11 meditran 3/19/2022 12:02:23 PM batch 2 log 1b batch 2 log 1b 11.692 0.026 3.657
    12 sample x 3/19/2022 12:06:20 PM batch 2 log 1b batch 2 log 1b 4.212 2.181 4.597

    Sample Id Acquisition Time Dataset File Method File Ca 317.933 Mg 285.213 Zn 206.200

    13 yamalube 3/19/2022 11:49:03 AM batch 2 log 1b batch 2 log 1b 0.8% 0.7% 1.0%
    14 top 1 3/19/2022 11:55:33 AM batch 2 log 1b batch 2 log 1b 1.9% 7.2% 0.8%
    15 castrol 3/19/2022 11:58:39 AM batch 2 log 1b batch 2 log 1b 6.2% 4.2% 0.5%
    16 meditran 3/19/2022 12:02:23 PM batch 2 log 1b batch 2 log 1b 1.0% 37.9% 82.7%
    17 sample x 3/19/2022 12:06:20 PM batch 2 log 1b batch 2 log 1b 2.3% 3.4% 0.4%

    Corrected Intensities
    Ca 317.933 Mg 285.213 Zn 206.200
    Sample Id Acquisition Time Dataset File Method File
    (cps) (cps) (cps)

    1 blanko 3/19/2022 11:21:11 AM batch 2 log 1b batch 2 log 1b 19679.4 8223.0 1029.0
    2 calib std 1 3/19/2022 11:23:32 AM batch 2 log 1b batch 2 log 1b -570.8 245.9 32.7
    3 Calib Std 2 3/19/2022 11:28:17 AM batch 2 log 1b batch 2 log 1b 58458.7 37774.0 3368.6
    4 calib std 3 3/19/2022 11:32:22 AM batch 2 log 1b batch 2 log 1b 55957.7 62189.4 6012.6
    5 Calib Std 4 3/19/2022 11:36:45 AM batch 2 log 1b batch 2 log 1b 106935.2 151077.9 16997.7
    6 calib std 5 3/19/2022 11:40:26 AM batch 2 log 1b batch 2 log 1b 148461.3 243541.1 33508.6
    7 Calib Std 6 3/19/2022 11:43:46 AM batch 2 log 1b batch 2 log 1b 248764.6 550574.6 69163.9

    Ca 317.933 Mg 285.213 Zn 206.200


    Sample Id Acquisition Time Dataset File Method File
    (cps) (cps) (cps)

    8 yamalube 3/19/2022 11:49:03 AM batch 2 log 1b batch 2 log 1b 3551152.2 45862.5 585263.5
    9 top 1 3/19/2022 11:55:33 AM batch 2 log 1b batch 2 log 1b 2769364.9 29055.8 474224.7
    10 castrol 3/19/2022 11:58:39 AM batch 2 log 1b batch 2 log 1b 792402.0 5435953.0 768286.6
    11 meditran 3/19/2022 12:02:23 PM batch 2 log 1b batch 2 log 1b 5548008.6 42075.4 513767.2
    12 sample x 3/19/2022 12:06:20 PM batch 2 log 1b batch 2 log 1b 2017332.4 2398836.0 645569.5

    Sample Id Acquisition Time Dataset File Method File Ca 317.933 Mg 285.213 Zn 206.200

    13 yamalube 3/19/2022 11:49:03 AM batch 2 log 1b batch 2 log 1b 0.8% 0.5% 1.0%
    14 top 1 3/19/2022 11:55:33 AM batch 2 log 1b batch 2 log 1b 1.8% 3.9% 0.8%
    15 castrol 3/19/2022 11:58:39 AM batch 2 log 1b batch 2 log 1b 6.0% 4.1% 0.5%
    16 meditran 3/19/2022 12:02:23 PM batch 2 log 1b batch 2 log 1b 1.0% 25.8% 82.5%
    17 sample x 3/19/2022 12:06:20 PM batch 2 log 1b batch 2 log 1b 2.3% 3.4% 0.4%
    Calibration Curves in Calibration Units
    Cor. Coef:
    Ca 317.933 Equ: Linear Calculated Intercept 0.957257
    Sample Id Corrected Intensity Entered Conc. Calculated Cal Unit Conc. % Residual Error
    blanko 0.0 0.000 -0.063 N/A
    calib std 1 -570.8 0.000 -0.064 N/A
    Calib Std 2 58458.7 0.020 0.061 205.43
    calib std 3 55957.7 0.050 0.056 11.57
    Calib Std 4 106935.2 0.100 0.164 63.80
    calib std 5 148461.3 0.200 0.252 25.89
    Calib Std 6 248764.6 0.500 0.464 -7.14

    Cor. Coef:
    Mg 285.213 Equ: Linear Calculated Intercept 0.996970
    Sample Id Corrected Intensity Entered Conc. Calculated Cal Unit Conc. % Residual Error
    blanko 0.0 0.000 -0.012 N/A
    calib std 1 245.9 0.000 -0.012 N/A
    Calib Std 2 37774.0 0.020 0.022 11.42
    calib std 3 62189.4 0.050 0.045 -10.79
    Calib Std 4 151077.9 0.100 0.126 25.87
    calib std 5 243541.1 0.200 0.210 5.20
    Calib Std 6 550574.6 0.500 0.491 -1.78

    Cor. Coef:
    Zn 206.200 Equ: Linear Calculated Intercept 0.995623
    Sample Id Corrected Intensity Entered Conc. Calculated Cal Unit Conc. % Residual Error
    blanko 0.0 0.000 -0.007 N/A
    calib std 1 32.7 0.000 -0.007 N/A
    Calib Std 2 3368.6 0.020 0.017 -16.07
    calib std 3 6012.6 0.050 0.036 -28.71
    Calib Std 4 16997.7 0.100 0.114 13.99
    calib std 5 33508.6 0.200 0.232 15.88
    Calib Std 6 69163.9 0.500 0.486 -2.79

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