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  • LSV Test for Linear Sweep Voltammetry

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    JUAN PABLO GUERRERO JIMENEZ
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    This document contains the parameters and results for a linear sweep voltammetry test performed on an unknown electrode using a potentiostat. The test was run from -0.8V to 0.001V at a scan rate of 100 mV/s, recording current measurements at 46 data points. The document lists the test settings, equipment information, and a table of potential, time, current, and other data values measured during the voltammetry scan.

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    1CGE-4

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    This document contains the parameters and results for a linear sweep voltammetry test performed on an unknown electrode using a potentiostat. The test was run from -0.8V to 0.001V at a scan rate of 100 mV/s, recording current measurements at 46 data points. The document lists the test settings, equipment information, and a table of potential, time, current, and other data values measured during the voltammetry scan.

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    © All Rights Reserved
    Download as TXT, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    9 views29 pages

    LSV Test for Linear Sweep Voltammetry

    Uploaded by

    JUAN PABLO GUERRERO JIMENEZ
    This document contains the parameters and results for a linear sweep voltammetry test performed on an unknown electrode using a potentiostat. The test was run from -0.8V to 0.001V at a scan rate of 100 mV/s, recording current measurements at 46 data points. The document lists the test settings, equipment information, and a table of potential, time, current, and other data values measured during the voltammetry scan.

    Copyright:

    © All Rights Reserved
    Download as TXT, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 29

    EXPLAIN

    TAG LSV
    TITLE LABEL Linear Sweep Voltammetry Test &Identifier
    DATE LABEL 11/8/2018 Date
    TIME LABEL 16:41:52 Time
    NOTES NOTES 1 &Notes...

    PSTAT PSTAT REF600-18035 Potentiostat


    VINIT POTEN -8.00000E-001 F &Initial E (V)
    VFINAL POTEN 1.00000E-002 F &Final E (V)
    SCANRATE QUANT 9.99998E+001 &Scan Rate (mV/s)
    STEPSIZE QUANT 1.00000E+000 St&ep Size (mV)
    IMODE SELECTOR 0 I/E Range &Mode
    IRANGE QUANT 2.50000E+001 &Max Current (mA)
    AREA QUANT 1.96000E-001 Electrode &Area (cm^2)
    ELECTRODETYPE SELECTOR 0 Electrode Type
    STRIPPING TOGGLE F Used for Stripping
    POLARITY TOGGLE F Signal Polarity
    CONDIT TWOPARAM F 1.50000E+001 0.00000E+000 Conditionin&g
    Time(s) E(V)
    DELAY TWOPARAM F 3.00000E+001 0.00000E+000 Init. De&lay
    Time(s) Stab.(mV/s)
    EQDELAY QUANT 5.00000E+000 Equil. &Time (s)
    IRCOMP SELECTOR 0 IRCom&p
    PFCOR QUANT 2.50000E+001 PF Corr. (ohm)
    SAMPLINGMODE SELECTOR 0 Sampling &Mode
    EOC QUANT 0 Open Circuit (V)
    PSTATMODEL IQUANT 4 Pstat Model
    PSTATSECTION LABEL REF600-18035 Pstat Section
    PSTATSERIALNO LABEL 18035 Pstat Serial Number
    CTRLMODE IQUANT 1 Control Mode
    IESTAB IQUANT 2 I/E Stability
    CASPEED IQUANT 2 Control Amp Speed
    CONVENTION IQUANT 1 Current Convention
    ICHRANGE IQUANT 2 Ich Range
    ICHRANGEMODE TOGGLE F Ich Auto Range
    ICHOFFSETENABLE TOGGLE F Ich Offset Enable
    ICHOFFSET QUANT 0 Ich Offset (V)
    ICHFILTER IQUANT 2 Ich Filter
    VCHRANGE IQUANT 2 Vch Range
    VCHRANGEMODE TOGGLE T Vch Auto Range
    VCHOFFSETENABLE TOGGLE F Vch Offset Enable
    VCHOFFSET QUANT 0 Vch Offset (V)
    VCHFILTER IQUANT 2 Vch Filter
    ACHRANGE IQUANT 2 Ach Range
    ACHOFFSETENABLE TOGGLE F Ach Offset Enable
    ACHOFFSET QUANT 0 Ach Offset (V)
    ACHFILTER IQUANT 1 Ach Filter
    IERANGELOWERLIMIT IQUANT 1 I/E Range Lower Limit
    IERANGEMODE TOGGLE T I/E AutoRange
    IERANGE IQUANT 10 I/E Range
    POSFEEDENABLE TOGGLE F Positive Feedback IR Comp
    POSFEEDRESISTANCE QUANT 0 Positive Feedback Resistance (ohm)
    ACHSELECT IQUANT 0 Ach Select
    CABLEID IQUANT 14 Cable ID
    DCCALDATE LABEL 25/6/2018 DC Calibration Date
    ACCALDATE LABEL 25/6/2018 AC Calibration Date
    THERMOSELECT IQUANT 1 Thermo Select
    FRAMEWORKVERSION QUANT 5.68 Framework Version
    INSTRUMENTVERSION LABEL 2.50 Instrument Version
    CURVE TABLE 811
    Pt T Vf Im Vu Sig Ach IERange Over Cycle
    # s V vs. Ref. A V V V # bits #
    0 0.01 -7.99360E-001 -1.48111E-003 0.00000E+000 -8.00000E-
    001 5.66298E-004 10 ........... 0
    1 0.02 -7.98362E-001 -1.46525E-003 0.00000E+000 -7.99000E-
    001 5.66298E-004 9 ......s.... 0
    2 0.03 -7.97362E-001 -1.45485E-003 0.00000E+000 -7.98000E-
    001 6.66297E-004 9 ........... 0
    3 0.04 -7.96362E-001 -1.44505E-003 0.00000E+000 -7.97000E-
    001 6.66297E-004 9 ........... 0
    4 0.05 -7.95362E-001 -1.43445E-003 0.00000E+000 -7.96000E-
    001 6.66297E-004 9 ........... 0
    5 0.06 -7.94362E-001 -1.42465E-003 0.00000E+000 -7.95000E-
    001 6.66297E-004 9 ........... 0
    6 0.07 -7.93562E-001 -1.41485E-003 0.00000E+000 -7.94000E-
    001 5.66298E-004 9 ........... 0
    7 0.08 -7.92362E-001 -1.40505E-003 0.00000E+000 -7.93000E-
    001 7.66295E-004 9 ........... 0
    8 0.09 -7.91362E-001 -1.39505E-003 0.00000E+000 -7.92000E-
    001 6.66297E-004 9 ........... 0
    9 0.1 -7.90362E-001 -1.38545E-003 0.00000E+000 -7.91000E-
    001 6.66297E-004 9 ........... 0
    10 0.11 -7.89362E-001 -1.37565E-003 0.00000E+000 -7.90000E-
    001 6.66297E-004 9 ........... 0
    11 0.12 -7.88462E-001 -1.36625E-003 0.00000E+000 -7.89000E-
    001 5.66298E-004 9 ........... 0
    12 0.13 -7.87462E-001 -1.35625E-003 0.00000E+000 -7.88000E-
    001 6.66297E-004 9 ........... 0
    13 0.14 -7.86562E-001 -1.34665E-003 0.00000E+000 -7.87000E-
    001 6.66297E-004 9 ........... 0
    14 0.15 -7.85362E-001 -1.33745E-003 0.00000E+000 -7.86000E-
    001 6.66297E-004 9 ........... 0
    15 0.16 -7.84462E-001 -1.32785E-003 0.00000E+000 -7.85000E-
    001 4.66300E-004 9 ........... 0
    16 0.17 -7.83562E-001 -1.31825E-003 0.00000E+000 -7.84000E-
    001 7.66295E-004 9 ........... 0
    17 0.18 -7.82462E-001 -1.30905E-003 0.00000E+000 -7.83000E-
    001 6.66297E-004 9 ........... 0
    18 0.19 -7.81462E-001 -1.29964E-003 0.00000E+000 -7.82000E-
    001 6.66297E-004 9 ........... 0
    19 0.2 -7.80462E-001 -1.29064E-003 0.00000E+000 -7.81000E-
    001 6.66297E-004 9 ........... 0
    20 0.21 -7.79462E-001 -1.28104E-003 0.00000E+000 -7.80000E-
    001 5.66298E-004 9 ........... 0
    21 0.22 -7.78462E-001 -1.27184E-003 0.00000E+000 -7.79000E-
    001 5.66298E-004 9 ........... 0
    22 0.23 -7.77462E-001 -1.26264E-003 0.00000E+000 -7.78000E-
    001 6.66297E-004 9 ........... 0
    23 0.24 -7.76462E-001 -1.25344E-003 0.00000E+000 -7.77000E-
    001 6.66297E-004 9 ........... 0
    24 0.25 -7.75463E-001 -1.24424E-003 0.00000E+000 -7.76000E-
    001 6.66297E-004 9 ........... 0
    25 0.26 -7.74463E-001 -1.23504E-003 0.00000E+000 -7.75000E-
    001 6.66297E-004 9 ........... 0
    26 0.27 -7.73463E-001 -1.22564E-003 0.00000E+000 -7.74000E-
    001 7.66295E-004 9 ........... 0
    27 0.28 -7.72563E-001 -1.21664E-003 0.00000E+000 -7.73000E-
    001 7.66295E-004 9 ........... 0
    28 0.29 -7.71463E-001 -1.20744E-003 0.00000E+000 -7.72000E-
    001 6.66297E-004 9 ........... 0
    29 0.3 -7.70463E-001 -1.19844E-003 0.00000E+000 -7.71000E-
    001 5.66298E-004 9 ........... 0
    30 0.31 -7.69463E-001 -1.19004E-003 0.00000E+000 -7.70000E-
    001 6.66297E-004 9 ........... 0
    31 0.32 -7.68463E-001 -1.18084E-003 0.00000E+000 -7.69000E-
    001 6.66297E-004 9 ........... 0
    32 0.33 -7.67363E-001 -1.17204E-003 0.00000E+000 -7.68000E-
    001 7.66295E-004 9 ........... 0
    33 0.34 -7.66563E-001 -1.16284E-003 0.00000E+000 -7.67000E-
    001 6.66297E-004 9 ........... 0
    34 0.35 -7.65463E-001 -1.15424E-003 0.00000E+000 -7.66000E-
    001 7.66295E-004 9 ........... 0
    35 0.36 -7.64463E-001 -1.14524E-003 0.00000E+000 -7.65000E-
    001 7.66295E-004 9 ........... 0
    36 0.37 -7.63363E-001 -1.13644E-003 0.00000E+000 -7.64000E-
    001 7.66295E-004 9 ........... 0
    37 0.38 -7.62263E-001 -1.12784E-003 0.00000E+000 -7.63000E-
    001 5.66298E-004 9 ........... 0
    38 0.39 -7.61463E-001 -1.11904E-003 0.00000E+000 -7.62000E-
    001 6.66297E-004 9 ........... 0
    39 0.4 -7.60463E-001 -1.11044E-003 0.00000E+000 -7.61000E-
    001 5.66298E-004 9 ........... 0
    40 0.41 -7.59463E-001 -1.10164E-003 0.00000E+000 -7.60000E-
    001 6.66297E-004 9 ........... 0
    41 0.42 -7.58263E-001 -1.09264E-003 0.00000E+000 -7.59000E-
    001 7.66295E-004 9 ........... 0
    42 0.43 -7.57363E-001 -1.08464E-003 0.00000E+000 -7.58000E-
    001 5.66298E-004 9 ........... 0
    43 0.44 -7.56463E-001 -1.07584E-003 0.00000E+000 -7.57000E-
    001 5.66298E-004 9 ........... 0
    44 0.45 -7.55263E-001 -1.06724E-003 0.00000E+000 -7.56000E-
    001 6.66297E-004 9 ........... 0
    45 0.46 -7.54363E-001 -1.05864E-003 0.00000E+000 -7.55000E-
    001 5.66298E-004 9 ........... 0
    46 0.47 -7.53463E-001 -1.05024E-003 0.00000E+000 -7.54000E-
    001 6.66297E-004 9 ........... 0
    47 0.48 -7.52363E-001 -1.04164E-003 0.00000E+000 -7.53000E-
    001 6.66297E-004 9 ........... 0
    48 0.49 -7.51363E-001 -1.03283E-003 0.00000E+000 -7.52000E-
    001 4.66300E-004 9 ........... 0
    49 0.5 -7.50463E-001 -1.02463E-003 0.00000E+000 -7.51000E-
    001 5.66298E-004 9 ........... 0
    50 0.51 -7.49463E-001 -1.01623E-003 0.00000E+000 -7.50000E-
    001 5.66298E-004 9 ........... 0
    51 0.52 -7.48463E-001 -1.00783E-003 0.00000E+000 -7.49000E-
    001 7.66295E-004 9 ........... 0
    52 0.53 -7.47463E-001 -9.99834E-004 0.00000E+000 -7.48000E-
    001 7.66295E-004 9 ........... 0
    53 0.54 -7.46463E-001 -9.91033E-004 0.00000E+000 -7.47000E-
    001 7.66295E-004 9 ........... 0
    54 0.55 -7.45463E-001 -9.82833E-004 0.00000E+000 -7.46000E-
    001 5.66298E-004 9 ........... 0
    55 0.56 -7.44463E-001 -9.74833E-004 0.00000E+000 -7.45000E-
    001 7.66295E-004 9 ........... 0
    56 0.57 -7.43463E-001 -9.66032E-004 0.00000E+000 -7.44000E-
    001 6.66297E-004 9 ........... 0
    57 0.58 -7.42463E-001 -9.58232E-004 0.00000E+000 -7.43000E-
    001 6.66297E-004 9 ........... 0
    58 0.59 -7.41463E-001 -9.50032E-004 0.00000E+000 -7.42000E-
    001 6.66297E-004 9 ........... 0
    59 0.6 -7.40463E-001 -9.42032E-004 0.00000E+000 -7.41000E-
    001 7.66295E-004 9 ........... 0
    60 0.61 -7.39463E-001 -9.33431E-004 0.00000E+000 -7.40000E-
    001 6.66297E-004 9 ........... 0
    61 0.62 -7.38563E-001 -9.25431E-004 0.00000E+000 -7.39000E-
    001 6.66297E-004 9 ........... 0
    62 0.63 -7.37463E-001 -9.17431E-004 0.00000E+000 -7.38000E-
    001 7.66295E-004 9 ........... 0
    63 0.64 -7.36363E-001 -9.09630E-004 0.00000E+000 -7.37000E-
    001 5.66298E-004 9 ........... 0
    64 0.65 -7.35463E-001 -9.01630E-004 0.00000E+000 -7.36000E-
    001 7.66295E-004 9 ........... 0
    65 0.66 -7.34563E-001 -8.93430E-004 0.00000E+000 -7.35000E-
    001 4.66300E-004 9 ........... 0
    66 0.67 -7.33563E-001 -8.85229E-004 0.00000E+000 -7.34000E-
    001 7.66295E-004 9 ........... 0
    67 0.68 -7.32363E-001 -8.77629E-004 0.00000E+000 -7.33000E-
    001 6.66297E-004 9 ........... 0
    68 0.69 -7.31363E-001 -8.69429E-004 0.00000E+000 -7.32000E-
    001 6.66297E-004 9 ........... 0
    69 0.7 -7.30563E-001 -8.61829E-004 0.00000E+000 -7.31000E-
    001 7.66295E-004 9 ........... 0
    70 0.71 -7.29463E-001 -8.53628E-004 0.00000E+000 -7.30000E-
    001 5.66298E-004 9 ........... 0
    71 0.72 -7.28463E-001 -8.46028E-004 0.00000E+000 -7.29000E-
    001 6.66297E-004 9 ........... 0
    72 0.73 -7.27563E-001 -8.38228E-004 0.00000E+000 -7.28000E-
    001 6.66297E-004 9 ........... 0
    73 0.74 -7.26463E-001 -8.30227E-004 0.00000E+000 -7.27000E-
    001 6.66297E-004 9 ........... 0
    74 0.75 -7.25463E-001 -8.22427E-004 0.00000E+000 -7.26000E-
    001 5.66298E-004 9 ........... 0
    75 0.76 -7.24563E-001 -8.15027E-004 0.00000E+000 -7.25000E-
    001 5.66298E-004 9 ........... 0
    76 0.77 -7.23363E-001 -8.07227E-004 0.00000E+000 -7.24000E-
    001 6.66297E-004 9 ........... 0
    77 0.78 -7.22463E-001 -7.99426E-004 0.00000E+000 -7.23000E-
    001 6.66297E-004 9 ........... 0
    78 0.79 -7.21463E-001 -7.91826E-004 0.00000E+000 -7.22000E-
    001 5.66298E-004 9 ........... 0
    79 0.8 -7.20563E-001 -7.84226E-004 0.00000E+000 -7.21000E-
    001 6.66297E-004 9 ........... 0
    80 0.81 -7.19363E-001 -7.76825E-004 0.00000E+000 -7.20000E-
    001 6.66297E-004 9 ........... 0
    81 0.82 -7.18463E-001 -7.68825E-004 0.00000E+000 -7.19000E-
    001 6.66297E-004 9 ........... 0
    82 0.83 -7.17463E-001 -7.61625E-004 0.00000E+000 -7.18000E-
    001 7.66295E-004 9 ........... 0
    83 0.84 -7.16463E-001 -7.54025E-004 0.00000E+000 -7.17000E-
    001 4.66300E-004 9 ........... 0
    84 0.85 -7.15563E-001 -7.46424E-004 0.00000E+000 -7.16000E-
    001 5.66298E-004 9 ........... 0
    85 0.86 -7.14563E-001 -7.39224E-004 0.00000E+000 -7.15000E-
    001 6.66297E-004 9 ........... 0
    86 0.87 -7.13263E-001 -7.31824E-004 0.00000E+000 -7.14000E-
    001 6.66297E-004 9 ........... 0
    87 0.88 -7.12463E-001 -7.24423E-004 0.00000E+000 -7.13000E-
    001 5.66298E-004 9 ........... 0
    88 0.89 -7.11363E-001 -7.17023E-004 0.00000E+000 -7.12000E-
    001 5.66298E-004 9 ........... 0
    89 0.9 -7.10464E-001 -7.09823E-004 0.00000E+000 -7.11000E-
    001 7.66295E-004 9 ........... 0
    90 0.91 -7.09664E-001 -7.02623E-004 0.00000E+000 -7.10000E-
    001 7.66295E-004 9 ........... 0
    91 0.92 -7.08464E-001 -6.95422E-004 0.00000E+000 -7.09000E-
    001 4.66300E-004 9 ........... 0
    92 0.93 -7.07464E-001 -6.88022E-004 0.00000E+000 -7.08000E-
    001 4.66300E-004 9 ........... 0
    93 0.94 -7.06464E-001 -6.80822E-004 0.00000E+000 -7.07000E-
    001 6.66297E-004 9 ........... 0
    94 0.95 -7.05364E-001 -6.73422E-004 0.00000E+000 -7.06000E-
    001 6.66297E-004 9 ........... 0
    95 0.96 -7.04264E-001 -6.66421E-004 0.00000E+000 -7.05000E-
    001 6.66297E-004 9 ........... 0
    96 0.97 -7.03564E-001 -6.59621E-004 0.00000E+000 -7.04000E-
    001 6.66297E-004 9 ........... 0
    97 0.98 -7.02464E-001 -6.52421E-004 0.00000E+000 -7.03000E-
    001 5.66298E-004 9 ........... 0
    98 0.99 -7.01464E-001 -6.45420E-004 0.00000E+000 -7.02000E-
    001 8.66294E-004 9 ........... 0
    99 1 -7.00464E-001 -6.38220E-004 0.00000E+000 -7.01000E-
    001 5.66298E-004 9 ........... 0
    100 1.01 -6.99264E-001 -6.31220E-004 0.00000E+000 -7.00000E-
    001 6.66297E-004 9 ........... 0
    101 1.02 -6.98464E-001 -6.24220E-004 0.00000E+000 -6.99000E-
    001 5.66298E-004 9 ........... 0
    102 1.03 -6.97564E-001 -6.17419E-004 0.00000E+000 -6.98000E-
    001 7.66295E-004 9 ........... 0
    103 1.04 -6.96464E-001 -6.10619E-004 0.00000E+000 -6.97000E-
    001 5.66298E-004 9 ........... 0
    104 1.05 -6.95464E-001 -6.04219E-004 0.00000E+000 -6.96000E-
    001 6.66297E-004 9 ........... 0
    105 1.06 -6.94564E-001 -5.96819E-004 0.00000E+000 -6.95000E-
    001 6.66297E-004 9 ........... 0
    106 1.07 -6.93364E-001 -5.90018E-004 0.00000E+000 -6.94000E-
    001 5.66298E-004 9 ........... 0
    107 1.08 -6.92364E-001 -5.83818E-004 0.00000E+000 -6.93000E-
    001 6.66297E-004 9 ........... 0
    108 1.09 -6.91464E-001 -5.76818E-004 0.00000E+000 -6.92000E-
    001 5.66298E-004 9 ........... 0
    109 1.1 -6.90464E-001 -5.70018E-004 0.00000E+000 -6.91000E-
    001 6.66297E-004 9 ........... 0
    110 1.11 -6.89564E-001 -5.63817E-004 0.00000E+000 -6.90000E-
    001 6.66297E-004 9 ........... 0
    111 1.12 -6.88464E-001 -5.56817E-004 0.00000E+000 -6.89000E-
    001 6.66297E-004 9 ........... 0
    112 1.13 -6.87564E-001 -5.50417E-004 0.00000E+000 -6.88000E-
    001 5.66298E-004 9 ........... 0
    113 1.14 -6.86364E-001 -5.43817E-004 0.00000E+000 -6.87000E-
    001 6.66297E-004 9 ........... 0
    114 1.15 -6.85464E-001 -5.37216E-004 0.00000E+000 -6.86000E-
    001 8.66294E-004 9 ........... 0
    115 1.16 -6.84464E-001 -5.30816E-004 0.00000E+000 -6.85000E-
    001 6.66297E-004 9 ........... 0
    116 1.17 -6.83564E-001 -5.24416E-004 0.00000E+000 -6.84000E-
    001 6.66297E-004 9 ........... 0
    117 1.18 -6.82464E-001 -5.18016E-004 0.00000E+000 -6.83000E-
    001 7.66295E-004 9 ........... 0
    118 1.19 -6.81364E-001 -5.11815E-004 0.00000E+000 -6.82000E-
    001 4.66300E-004 9 ........... 0
    119 1.2 -6.80564E-001 -5.05615E-004 0.00000E+000 -6.81000E-
    001 6.66297E-004 9 ........... 0
    120 1.21 -6.79464E-001 -4.99215E-004 0.00000E+000 -6.80000E-
    001 5.66298E-004 9 ........... 0
    121 1.22 -6.78564E-001 -4.93215E-004 0.00000E+000 -6.79000E-
    001 6.66297E-004 9 ........... 0
    122 1.23 -6.77564E-001 -4.86815E-004 0.00000E+000 -6.78000E-
    001 6.66297E-004 9 ........... 0
    123 1.24 -6.76364E-001 -4.80814E-004 0.00000E+000 -6.77000E-
    001 5.66298E-004 9 ........... 0
    124 1.25 -6.75149E-001 -4.73216E-004 0.00000E+000 -6.76000E-
    001 6.66297E-004 8 ......s.... 0
    125 1.26 -6.74249E-001 -4.67336E-004 0.00000E+000 -6.75000E-
    001 6.66297E-004 8 ........... 0
    126 1.27 -6.73249E-001 -4.61356E-004 0.00000E+000 -6.74000E-
    001 6.66297E-004 8 ........... 0
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