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1. Pipeline Right of Way Department, NNPC/PPMC Gombe Area Office, Gombe State,
Nigeria.
State, Nigeria.
hamisdgumel@yahoo.com
alikundiri@yahoo.com
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Abstract
This paper presents an experimental study of the effect of Volumetric Shrinkage Strain
(VSS) of Rice husk ash treated Black Cotton soil (BCS). Eighty (80) samples were
prepared using two compactive efforts of Standard Proctor (SP) and Modified Proctor
(MP) at 2 and 4% dry and wet of optimum moisture contents (OMC). The samples were
extruded from the compaction moulds and allowed to air dry in the laboratory for a
period of 28days. Results showed that the soil was classified as A-7-5(18) according to
classification system and MH (Silt of high plasticity) in accordance with Unified Soil
Classification System (USCS). Also, the higher compactive effort the lower values of
VSS due to the closer packing of soil fabric. Similarly, VSS decreases with higher RHA
contents up to an optimal value of 10% content, and increases with higher moulding
water content for specimens compacted on the wet side of the optimum. The addition of
RHA led to decrease in the plasticity index from 24 to as low as 3% with subsequent
improvement in the index properties of the soil with increase in MDD from 1.41 to 1.53
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1. Introduction
The “black cotton soil” is one of the problematic soils that has great tendency for Shrink-swell
behabiour due to moisture variation. Clays generally exhibit undesired change in engineering
properties such as low shear strengths, plastic, compressible and have low resilient modulus
when in contact with moisture (Osinubi and Kundiri, 2007; Moses and Afolayan, 2013; Kundiri
et al., 2016). Cohesive soils can creep over time under constant load, especially when the shear
stress approaches its shear strength, thus making them prone to sliding (). For these reasons,
lightly loaded structures such as foundations, pavements, canal beds and linings and residential
buildings founded on them are severely prone to menace of damage (Chen, 1988).
Desiccation cracks are common phenomenon which occur due to volume changes
resulting from cyclic swell-shrink moisture variations in cohesive soils, and can create pathways
for percolation of fluids (Rayhani et al., 2007; Allaire et al., 2009; Taha and Taha, 2012). The
“self –healing” Phenomenon weakens the strength of clay soils, resulting to shrinkage and
subsequent reduction in crack dimensions during the wetting process in a barrier system
In general, the natural stability of black cotton soil can be improved by means of various
agro and industrial admixtures such as lime, fly ash, rice husk ash, cement, silica fumes etc. to
improve the properties of the soil for most geotechnical applications (Kodikara et al., 2000;
Rice husk ash (RHA) is one of the major Agricultural wastes found abundantly. The
burning of rice husk generates about 20-23% of its weight as ash. The RHA is defined as a
pozzolanic material (ASTM C 168, ASTM 1997) due to its high amorphous silica content
(Mehta, 1986; Della et al., 2002). The objective of this paper is to examine the effect of Rice
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Husk Ash on Moisture – Density relationship as well as the Volumetric Shrinkage Strain of
2.1 Materials
2.1.1 Black-cotton soil: The soil sample used for this study was obtained from Baure village
(latitude 100 16’N and longitude110 21’E) in Yamaltu-Deba Local Government Area of Gombe
state, using the method of disturbed sampling and collected at depth between 0.5m to 1.0m. The
materials were preserved in polythene bags to avert moisture loss, transported to the Soil
2.1.2 Rice Husk Ash: Rice husks were obtained from rice mill in Yelwa area of Bauchi, and
burnt using controlled furnace of Abubakar Tafawa Balewa University Bauchi to produce the
2.1.3 Water: Portable drinking water was used in absence of distilled water for the purpose of
3. Methods
Laboratory tests were conducted for the determination of the index properties of the natural soil
and soil – RHA mixtures samples in accordance with BS 1377 (1990). The two compactive
efforts of Standard Proctor (SP) and Modified Proctor (MP) were carried out as specified by
Head (1992). These samples were classified as A-7-5(18) according to the Association of
(AASHTO, 1986), and MH according to the Unified Soil Classification System (USCS) (ASTM,
D2487, 1998). Compaction tests were carried out to determine the Optimum Moisture Content
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(OMC) and Maximum Dry Density (MDD) on air-dried soil samples passing through 4.75mm
sieve size.
Volumetric Shrinkage Strain (VSS) test was conducted on Eighty (80) prepared samples
in accordance with BS 1377 (1990) on the RHA treated Black Cotton Soil (BCS). The specimens
were prepared by mixing the soil with 0, 5, 10, and 15% RHA at four different moisture contents
of 2 and 4% on dry and wet sides of the optimum moisture contents using the two compactive
efforts of SP and MP. The specimens were carefully extruded from the compaction moulds and
allowed to dry on the laboratory table at ambient temperature for 28 days. The circumferential
diameter and height of the specimens were measured in triplicate to compute the volumetric
shrinkage strains.
The results of the oxide and elemental composition were obtained using X-ray fluorescence
(XRF) for both the black cotton soil (BCS) and Rice Husk Ash (RHA) as presented in Tables 1
and 2 respectively.
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Table 1: Oxide Composition of Black Cotton Soil
CaO 0.53
SiO2 31.05
Al2O3 18.21
Fe2O3 4.74
MnO 0.38
TiO2 2.34
LOI < 50
CaO 1.58
SiO2 67.3
Al2O3 4.96
Fe2O3 0.95
MgO 0.53
LOI < 20
The main oxides of the BCS sample and the RHA is Silicon dioxide (SiO2) and
Aluminium (III) Oxide with 31.05 and with 18.021% respectively. The cations are exchangeable
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with another group of different cations having the same total charge in the RHA, thus stabilizing
and improving the properties of the BCS, as observed by (Rathan et al., 2016; Alhassan and
Alhaji, 2017)
Preliminary tests were conducted for determination of index properties and classification
of the soil. The Engineering properties of both the natural and treated soil samples are
summarized in Table 3.
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Table 3: Engineering Properties of Soil.
0 5 10 15
Liquid Limit, % 62 62 62 65
Plastic Limit, % 38 45 57 59
Plasticity Index, % 24 17 8 3
% Sand (0.06-2mm) 15 15 15 15
Group Index 18 15 12 12
USCS Classification MH MH MH MH
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* Nigerian Building and Road Research Institute
Physical inspection showed that the soil is dark grey in color and has an activity value of
2.35 which indicated that the soil is an active Montmorillonite. The activity decreases from 2.35
to 0.29 with increase of 5 to 15% in RHA content. This shows that the plasticity and index and
swell potential decreases from 24 to 3% and medium to low respectively. The specific gravity of
the soil was observed to be 2.62 which also indicated the prevalence of montmorillonite minerals
(Das, 2005). The liquid limit maintained a constant value of 62% up to 10% RHA blend, but
further increase up to 15% RHA increased the liquid limit to 65%. This could be due to the effect
of reduction in the diffused double layer as well as due to incomplete dilution of clay content to
the of the mix. The subsequent increase in the liquid limit could be attributed to the increase in
RHA which introduced more pozzolanic substances from the ash. This requires more amount of
water for the completion of hydration process (Rahman, 1986; Osula, 1991; Akinyele et al.,
2015).
The Optimum Moisture Content (OMC) values obtained were 28.8 and 24.6% with
corresponding Maximum Dry Density (MDD) of 1.52 and 1.53Mg/m 3 for SP and MP
The Maximum Dry Density (MDD) obtained are 1.52 and 1.53Mg/m 3 for SP and MP
28.8 and 24.6% for Standard Proctor and Modified Proctor compactive efforts respectively. The
MDD increased with increase in RHA content, as the OMC reduced. This could be attributed to
the RHA occupying the void within the soil matrix and also the flocculation of the soil particle
due to ions exchange. These results are no doubt in agreement with earlier studies by Eberemu,
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2011; Kundiri and Kundiri,2002; Osinubi and Stephen, 2007; Oriola and Moses, 2010; Kundiri
et al., 2016. The trends of the moisture – density relationships are presented in figure 5 and 6.
The MP compactive effort gave the highest values of MDD of 1.53Mg/m3 which corresponds to
OMC values of 22.3%. It could be observed that there was an increase in MDD and decrease in
OMC with higher compactive effort. This in agreement with established works (Blotz et al.,
Figure 1: Moisture – Density relationship for natural and treated soils using SP compactive
effort.
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Figure 2: Moisture – Density relationship for natural and treated soils using MP compactive
effort.
The shrinkage is mainly as a result of loss of moisture due to evaporation, as the surface
dehydrates drying proceeds from the surface and it goes deeper downwards until it affects the
entire specimen (Khire et al., 1997; Tang et al., 2010; Eberemu, 2011). The cracking is not likely
to occur in compacted soil liners with volumetric shrinkage strain (VSS) of less than 4% upon
drying (Daniel and Wu, 1993; Osinubi and Kundiri, 2007). The specimens compacted at higher
molding water contents shrank more resulting in high VSS, which conformed to similar findings
by researchers such as Daniel and Wu, 1993; Albrecht and Benson, 2001; Osinubi and Eberemu,
2010. In general, decrease in the VSS was observed with increasing RHA contents for both
compaction energies up to 10%; and subsequently there was slight increase in VSS with addition
of 15% RHA. This could be attributed to the pozzolanic input of the RHA treatment which
The variations of VSS with moulding water content relative to the optimum using the SP
and MP compactive efforts for both natural and treated soils are shown in Figures 3 and 4.
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Figure 3: Variation of VSS with RHA treatments relative to optimum for SP compactive
effort.
Figure 12: Variation of VSS with RHA treatments relative to optimum for MP compactive effort.
It could also be deduced that BCS compacted at higher compactive effort showed lower
VSS values due to the closer packing of soil fabric, as in agreement with earlier findings by
(Daniel and Wu, 1993; Albrecht and Benson, 2001; Tang et al., 2011; Kundiri et al., 2016).
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Generally, the VSS decreased with higher compaction energy and RHA content for specimens
compacted on the wet side of the optimum and thus contain much water as against the specimens
compacted on the dry side of the optimum which had less water. This also agreed with earlier
researches by (Osinubi et al., 2010; Eberemu et al., 2011). Improvement in VSS of the samples
with increase in RHA contents and compactive efforts are shown in Plates 1 - 3.
Plate 1: Samples showing dessications (VSS) for natural (untreated) soil at different moisture
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Plate 2: Samples showing improvement in VSS for RHA treated samples using SP compactive
Plate 3: Samples showing improvement in VSS for RHA treated samples using MP compactive
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5 CONCLUSION
(1) The soil was classified as A-7-5(18) and MH according to AASHTO and USCS
classification systems.
(2) The addition of RHA resulted to decrease in the plasticity index from 24% to as low as
3%, and swell potential from medium to low degree according to NBRRI classification.
(3) Addition of RHA from 0 to 10% resulted to increase in MDD from 1.41 to 1.52 Mg/m 3
(4) The VSS decreases with increase in RHA content to a minimum of 4 and 4.1% for SP
(5) In conclusion, higher compaction energy and increase in RHA contents improves swell-
shrink potentials of BCS by improving the plasticity with subsequent reduction in the
VSS.
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