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Abstract
BACKGROUND: During the milling of durum wheat to semolina, about 10–15% of total products produced is
residue flour, a lower value product than the semolina. This study investigated the potential for using the durum
residue flour as an additive in bread-making to improve its potential commercial value.
RESULTS: Incorporation of residue durum flour from 102 breeding lines into a low protein flour and standard
bakers’ flour at 20% incorporation improved the bake loaf volume with minimal change in Mixograph dough
mixing time and peak resistance in many of the lines tested. Loaf yellow b was always increased even with only a
10% incorporation. Baking flours can tolerate 20% incorporation with no deleterious affects on loaf volume and
bake score.
CONCLUSION: The results show a potential for using the lower value durum residue flour for baking bread of
acceptable quality with a slightly higher yellow colour. This would improve the profitability for the miller and
provide alternative ingredients to the baker for preparing specialty breads.
2008 Crown in the Right of the State of New South Wales and Society of Chemical Industry.
∗
Correspondence to: Dr Mike J Sissons, Tamworth Agricultural Institute, NSW Department of Primary Industries, 4 Marsden Park Road, Calala NSW
2340, Australia
E-mail: mike.sissons@dpi.nsw.gov.au
†
Present address: Food Science Australia, P.O. Box 52, North Ryde, NSW 1670, Australia
‡
Present address: Department of Grain Science and Industry, Kansas State University, Manhattan, KS 66506-2201, USA
(Received 28 August 2007; revised version received 28 November 2007; accepted 29 November 2007)
Published online 28 March 2008; DOI: 10.1002/jsfa.3197
2008 Crown in the Right of the State of New South Wales and Society of Chemical Industry. J Sci Food Agric 0022–5142/2008/$30.00
Effects of incorporating durum residue flour into wheat flour dough
caused a decrease in the mixing time (31 out of 102 peak resistance, although with this parameter, most of
samples), only 10 samples caused the mixing time the samples were not very different from the values
to decrease by more than 5% (Fig. 1). There were obtained for base wheat flour (data not shown).
more which increased the mixing time by at least 5%
(38 samples), and 20 which increased it by 10% or Effect on baking properties
more. The increase in mixing time appeared to be During the milling of durum grain using the Buhler
unrelated to protein content. On the other hand, none laboratory mill, three break flour fractions are
of the samples caused a significant increase in the peak produced. It is possible that there may be slight
resistance, but 21 samples caused a reduction of at compositional differences between these fractions and
least 5% (data not shown). when added to a bakers’ flour, have a different effect
With the low protein flour, almost all of the samples on loaf quality. This was tested by preparing an 80:20
showed an increase in mixing time. Most of these mixture of bakers’ flour and durum break fraction.
increased mixing time by at least 5% (Fig. 2). With There were no significant differences in loaf volume
peak resistance, most of the samples changed this (LV) and bake score (data not shown) between
parameter by less than 5%, but in contrast with the the three durum flour break fractions (Table 1).
standard bakers’ flour, peak resistance also increased Therefore, it was acceptable to pool the three break
by more than 5% with five of the durum flour samples fractions and this helped to provide sufficient sample
(data not shown). A smaller proportion of samples for baking.
showed a significantly lower peak resistance. Typical Loaf volume is one of the main characteristics of
Mixograph curves of wheat flour and wheat flour with bread quality although colour and textural properties
durum residue flour are shown in Fig. 3. are also important. When incorporated into the
The effects on the mixing time and peak resistance standard bakers’ flour, almost all of the durum residue
are independent of durum protein content (Fig. 4). flour samples produced an increase in LV (Fig. 5).
An increase in the mixing time is just as likely to Most of these increased the LV by more than 5%,
occur in a low protein durum flour as in a high some by more than 10%. Only six samples of durum
protein one. Similar observations were made with the residue flour decreased the LV by more than 5%. Full
loaf scoring was not carried out on the 35 g loaves, but
the crumb colour and texture were inspected visually
50 and judged to be acceptable. There was a trend for
Bakers’ flour
the change in LV to be affected by the protein content
40
of the durum flour, but the relationship was poor
(r = 0.25, P < 0.05); clearly other factors are also
Frequency
30
involved.
20 A more detailed analysis was performed to look at
the effects on LV and BS using 100 g pup loaves on
10 samples from set 3. This set contained a range of
durum with varying pasta quality (data not shown).
0 Each of a selected set of 10 durum residue flours
230-250 250-270 270-290 290-320 320-350
was incorporated into a standard bakers’ flour (11.9%
Mixing time range (sec)
protein) and a low protein flour (10.3%). There were
Figure 1. Distribution of mix time in bakers’ flour blends with different highly significant affects on LV and Minolta b∗ due
durum genotypes added at 20% incorporation. to sample (Table 2). For the standard bakers’ flour,
30
25
20
Frequency
15
10
Bakers’ flour
0
260-290 290-320 320-350 350-380 380-410 410-440 440-470 470-500
Mixing time ranges (sec)
Figure 2. Distribution of mix time in low protein wheat flour blends with different durum genotypes added at 20% incorporation.
1200 1200
(A) (C)
1000 1000
800 800
600 600
400 400
200 200
0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
Time (min) Time (min)
1200 1200
(B) (D)
1000 1000
800 800
600 600
400 400
200 200
0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7
Time (min) Time (min)
Figure 3. Mixograph curves of each control wheat flour with the same durum residue flour incorporated at 20%: (A) bakers’ flour, (B) bakers’ flour
plus durum flour, (C) low protein flour, and (D) low protein flour plus durum residue flour. The units on the Y axis are arbitrary units from the output
of the Mixograph.
600 60
Bakers’ flour
50
500 40
Frequency
30
400 20
10
300
0
140-160 160-180 180-200 200-220
LV range (cc)
200
8 12 16 20 Figure 5. Distribution of loaf volume in bakers’ flour blends with
different durum genotypes added at 20% incorporation.
Figure 4. Plot of mixing time (, in seconds) and peak resistance (,
in arbitrary units) against protein content of durum residue flours
incorporated into doughs with bakers’ flour. control, 27.6) to the control flour and only bread made
from 100% durum residue flour (Wollaroi) had a much
Table 1. Effects of the incorporation of 20% durum residue flour from
reduced LV and BS (18.9) compared to the control
each break on the volume of loaves prepared from a bakers’ flour baker flour, having an external appearance with rough
edges, a dark crust and coarse texture. The crumb
Sample Loaf volume (cm3 ) yellow colour of loaves made with durum residue flour
100% bread wheat flour 718 were all significantly higher than the standard bakers’
80% bread flour:20% durum first break 715 flour. This is due to the higher xanthophyl content
80% bread flour:20% durum second break 725 of durum endosperm compared to hexaploid wheat.
80% bread flour:20% durum third break 718 With the standard bakers’ flour, the 100% wheat flour
loaves had yellowness (Minolta b-value) of 18.9, while
the loaves with durum flour ranged from 20.8 to 23.0.
six of the ten durum residue incorporated flours The increase was relatively small, compared with the
had significantly greater LV compared to the 100% yellowness of a 100% durum loaf (33.0) but may still
standard bakers’ flour (Table 2). Only bread made be unacceptable to the baker. This would be one of
from 100% durum residue flour had significantly lower the main drawbacks in using durum residue flour for
LV. These results confirmed the 35 g trials in that bread baking although it would be possible to bleach
generally loaf volume was improved. All of the durum out the yellow pigment if acceptable on health and
incorporated flours had a similar BS (26.6–28.1 vs. safety grounds.
Table 4. Effect of durum residue flour incorporation at three different rates and from three cultivars into a high, standard and low protein bakers’
flour upon loaf quality
Sample HP SP LP HP SP LP
Protein percentages: HP = high protein baker’s flour with 13.8% protein; SP = standard bakers’ flour 11.9% protein; LP = low protein flour, 10.3%.
Y = Yallaroi residue flour; W = Wollaroi residue flour; K = Kamilaroi residue flour. Significance at ∗ = 5% and ∗∗∗ = 0.1%.
only lowered LV at the 20% rate while for Kamilaroi a tendency for a slight increase in mixing time
in the LP base, LV actually increased with increas- although some samples decreased this while others
ing durum flour addition. In no case was the LV of had no affect. Generally peak resistance was only
the durum incorporated flours higher than the control increased slightly. In another study using much higher
flour. In the HP base flour, two samples had equivalent incorporation rates (25, 50, 75%), Farinograph mixing
LV to the control and seven flours were significantly time and extensograph resistance were decreased in
lower in LV. For the SP base, five flours had equiva- flour blends.5 The improvement in our studies in
lent LV to the control and four flours were lower and LV was not obtained with a low protein base flour
for the LP base, three flours had equivalent LV to the substituted with 20% durum residue flour and again,
control while six flours had lower LV. The BS of the crust b was increased significantly. Thus it seems
durum incorporated flours ranged from 27.9 to 29.0 that the durum flour addition cannot overcome the
(cf. control flour, 28.9) showing that loaves of equiv- deficiency of the base flour. Durum wheat has naturally
alent appearance to the control flour were produced. higher levels of xanthophylls in the endosperm which
There were no differences between the 100% base account for a higher Minolta b-value in semolina
flour samples and those with added durum residue compared to wheat flour. The durum residue flour
flour for whiteness (L) and redness (a) values of the also has a yellow appearance because it is derived
crust (data not shown). The base flours had similar from the endosperm. Thus it is no surprise that
yellow colour. The addition of durum residue flour at addition of durum residue flour to a wheat base flour
any dose and source, significantly increased yellowness increased b, as observed. The improvement in LV is
(b) values of the loaves in all situations. As the dosage presumably due to the high gluten strength of the
of durum residue flour was increased, the b value durum residue flour. Indeed, Joesephdes et al.7 stated
increased, as to be expected and so levels below 10% that the durum genotype contributes to the effect of
incorporation would be needed to avoid this change. durum residue flour on bread quality when used in
The data shows that there can be a negative impact on combination and ascribed this to the gluten strength.
LV using some combinations of these durum residue Harris and Sibbitt15 found that when common wheat
flours while in other cases no reduction in LV was flour was substituted with durum flour below a 20%
obtained. However, in all situations, the yellow colour incorporation, there was no impact on loaf volume,
of the bread was significantly increased by the durum mixing requirements or crumb colour indicating this
flour addition even at a low 10% incorporation. dosage can be tolerated. Our results show there is a
difference in crumb colour. However, Boggini and
Pogna6 reported an increase in loaf volume of a
DISCUSSION 25% durum flour addition to flours with poor bread-
The analysis of many different durum genotypes (set 1) making quality. Similarly, Dekov et al.2 used durum
found that the substitution of 20% bread wheat flour residue flour in a soft wheat flour blend (15%) which
in a baking mixture with durum residue flour from improved bread-making quality. Our results show that
semolina milling in general, increased loaf volume loaf volume changes are dependent on the source of the
with no change in bake score but an increase in durum residue flour, there being differences between
crust and crumb yellowness. The effects on dough cultivars. Possible reasons are differences in protein
mixing as measured using the Mixograph showed content of the durum residue flours and differences in
the gluten strength and amount of insoluble glutenin Overall, there appears to be merit in studying further
which are linked to loaf volume.11 Results in Table 4 the use of durum residue flour as an additive in the
show that no improvements in LV and BS were production of the normal range of wheat breads to
obtained using the three durum varieties compared to improve the value of this by-product to the durum
the wheat flour control loaves but increases were noted miller. Providing loaf volume is not adversely affected,
with other sources (Tables 2 and 3). At the lowest the baker could reduce costs by decreasing the amount
incorporation rate used, all the breads had significantly of flour, since the durum residue is likely to be a
higher b-values compared to the control. Whether this cheaper ingredient. However, the additional yellow
increase in yellowness is unacceptable would depend colour might require a different market.
upon the market and there would always be the option
to bleach the flour if acceptable for health and safety.
Ozen3 reported the use of up to 5% durum residue ACKNOWLEDGEMENTS
flour in a baking formula had no deleterious effects This work was supported by a grant (DAN 238) from
on dough properties and bread quality. In our work, the Grains Research and Development Corporation.
there was no attempt to measure the effect of durum
residue flour on staling.
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