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Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically


Oscillating Dies

Article  in  IEEE Access · March 2018


DOI: 10.1109/ACCESS.2018.2811714

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Received January 15, 2018, accepted February 14, 2018, date of publication March 8, 2018, date of current version April 18, 2018.
Digital Object Identifier 10.1109/ACCESS.2018.2811714

Experimental Study on Fine Titanium Wire


Drawing with Two Ultrasonically Oscillating Dies
SHEN LIU , YUANCAI YANG, (Student Member, IEEE), TAO XIE, AND XIAOBIAO SHAN
School of Mechatronics Engineering, Harbin Institute of Technology, Harbin 150001, China
Corresponding author: Xiaobiao Shan (shanxiaobiao@hit.edu.cn)
This work was supported in part by the National Natural Science Foundation of China under Grant 51575130 and in part by the
Postdoctoral Scientific Research Staring Foundation of Heilongjiang Province under Grant LBH-Q12092.

ABSTRACT This paper investigates the influences of ultrasonic vibration on the two-pass titanium wire
drawing process through experiments conducted at different drawing speeds (99–480 mm/s) and under
various ultrasonic amplitudes (5.63–13.97 µm). Ultrasonic vibrators were designed, analyzed, and manufac-
tured to impose ultrasonic vibrations, along opposite directions, on the dies. Their dynamic characteristics
were predicted by finite element analysis and subsequently measured using specific instruments. The
interaction between the two vibrators, when driven by the same ultrasonic generator, resulted in the deviation
of coupled resonant frequency (50–60 Hz) and the decrease in maximum output amplitudes (about 4 µm).
A wire drawing equipment was developed to record the drawing forces under different experimental
conditions, and the surface morphologies of the drawn wires were then inspected with a scanning electron
microscope. Results show that increased ultrasonic amplitude contributes to greater drawing force reduction,
whereas higher drawing speed brings about the reverse effect. At the lowest drawing speed and with the
largest ultrasonic amplitude, the drawing force declined by over 50%. Both factors have influences on the
surface finish of the drawn wires. However, higher drawing velocity (480 mm/s) with the moderate ultrasonic
amplitude (9.69 µm) turned out to be most effective in removing the surface defects of the wire products.
This paper provides a low-cost, high-efficiency, and eco-friendly approach for the industrial production of
fine titanium wires at room temperature.

INDEX TERMS Metal forming, surface morphology, titanium wire, ultrasonic transducer.

I. INTRODUCTION at room temperature is further degraded by the strain hard-


Titanium and its alloys are distinguished by lightweight, high ening effect. Siegert and Möck [4] have presented that the
mechanical strength, good corrosion resistance, and excellent conventional cold wire drawing process requires large draw-
biocompatibility. These superior properties make titanium ing force, induces high contact and friction forces, leading
wires suitable for use in automobile, aerospace, military, and to increased energy consumption and rough surface finish,
biomedical industries. Cotton et al. [1] reported that, com- and therefore needs to be improved. Elevated temperature,
pared with steel springs, titanium springs have better corro- good lubrication condition, and suitable surface treatments,
sion resistance and can save up to 70% weight. Elias et al. [2] which contribute to reducing the flow stress and improv-
summarized the applications of titanium wires in medical ing the surface quality of the processed wires, are usually
and dental fields as joints and screws and emphasized the adopted during the titanium wire drawing process. Sever-
necessity of using titanium alloys as the material to make den- denko and Zhilkin [5] have reported that heat treatments,
tal plant devices. However, compared with traditional metal primarily annealing, are performed between passes to restore
wires, such as aluminum wires and steel wires, their usage is the plasticity of the drawn wires. Ishii et al. [6] patented
limited by two factors: the high cost of the raw material, and a method for beta-titanium wire production which involves
the complexity of the processing procedure, as Boyer [3] has cold drawing, heat treatment, solution treatment, and coat-
pointed out. Due to high mechanical resistance and high yield ing. Useful as these measures are, they are time-consuming,
stress to tensile strength (Y/T) ratio, titanium and its alloys polluting, and will remarkably increase the cost of the wire
are classified as less metallic materials, and their workability products.

2169-3536
2018 IEEE. Translations and content mining are permitted for academic research only.
16576 Personal use is also permitted, but republication/redistribution requires IEEE permission. VOLUME 6, 2018
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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

Ultrasonic-assisted drawing, which provides all the ben- process of titanium wire drawing. They found that, compared
efits of above-mentioned solutions, is a green technology with pure longitudinal vibration, the addition of torsional
about introducing ultrasonic vibrations to the wire draw- vibration could further decrease the drawing force by 23%,
ing process. Siegert and Möck [4] reported that ultra- however, causing slightly increased friction force, and worse
sonic vibration is beneficial for decreasing the drawing surface finish. Liu et al. [20] compared the cold dry drawing
force and improving the surface finish of the drawn wire. process of titanium wires under three circumstances: without
Gallego-Juarez and Graff [7] summarized the benefits of vibration, with large amplitude longitudinal vibration, and
ultrasonic vibrations in wire and tube drawing process: with longitudinal-torsional hybrid vibration. Considerable
increased drawing speed, prolonged die life, greater area improvement has been achieved with respect to the surface
reduction per pass, etc. Zhou et al. [8] studied the influence of finish of the drawn wires, with cracks and fragments almost
ultrasonic vibration on the forming process of aluminum and completely disappeared. However, a drawing force reduction
titanium, revealing that ultrasonic vibrations help to increase of only 5% was achieved, which has little commercial value
the plasticity and refine the grain size of titanium. Blaha and if force reduction is the sole criterion.
Langenecker first introduced power ultrasonics to the static Although inconsistencies, sometimes contradictions, exist
tensile test of monocrystalline zinc. They observed an abrupt among previous reports, generally, it is possible to reach the
decrease of 40% in drawing force when ultrasonic vibration following conclusions. First, regarding the feasibility, typical
of 800 kHz was imposed, and the drawing force bounced ultrasonic-related phenomena, basically acoustic softening,
back to its original value once the vibration was removed [9]. anti-friction, and enhanced surface finish were observed in
In their follow-up reports, Langenecker interpreted the phe- the wire drawing of both thick wires (rods, tubes) and fine
nomenon as a result of the activation and increased mobility wires, no matter for traditional metallic materials or for
of the lattice dislocations, which reduced the obstruction less deformable metals. Second, in terms of the efficiency,
at barriers during the metal deformation process [10], [11]. the influence of ultrasonic vibration seems less pronounced in
Eaves and his group reviewed the various hypotheses and fine wire drawing occasions, particularly for less deformable
experimental results about ultrasonic rod drawing and other materials. In addition, previous studies tended to focus on
metal forming processes, concluding that all these observa- the single-pass ultrasonic wire drawing rather than on multi-
tions could be explained by the superposition of an oscillatory pass wire drawing which is adopted in practical industrial
load on a steady state force [12], [13], which was later termed production. In this paper, we carried out an experimental
as stress superposition theory. They also proposed a multi-die study on the two-pass titanium wire drawing process with two
arrangement method in order to achieve greater area reduc- dies oscillating along opposite directions. The influences of
tion [14]. Until now, no consensus has been reached on the wire drawing speed and vibration amplitude of the dies on
mechanism of ultrasonic assisted metal forming processes, the drawing force and the surface finish of the processed wire
however, studies on relevant industrial applications have con- were studied. Ultrasonic vibrators were designed, analyzed,
tinued up to the present. Murakawa and Jin reported the tuned, and tested to impose ultrasonic vibrations on the dies.
experimental results of applying radial ultrasonic vibration, Due to unavoidable machining and assembly errors, discrep-
15 kHz, 4 µm, to the drawing of 85.8 mm stainless steel wire. ancies between the manufactured vibrators are unlikely to be
The operation realized the skin-pass ultrasonic wire drawing eliminated. Therefore, the coupling effects when they work
using the chlorine-free lubricants, and expanded the critical together were also investigated.
speed range of ultrasonic wire drawing by about 10 times,
to 55 m/min [15]. Susan et al. [16], [17] investigated the
effects of ultrasonic vibration during steel tube and wire
drawing process, both theoretically and experimentally. They
derived the mathematical equations to calculate the drawing
force according to the friction reversion mechanism. It was
found that ultrasonic vibration not only is responsible for the
decreased drawing force and friction force but also helps to
weaken the work hardening effect. For the drawing of fine
wires, Haiqun et al. [18] examined the possibility of intro-
FIGURE 1. Exploded diagram of the designed ultrasonic vibrator for wire
ducing longitudinal vibrations to the industrial production of drawing.
brass wire. The experimental results presented: a 17% rise in
drawing velocity from 980 mm/s, under conventional condi-
tions, to 1126 mm/s, with ultrasonic vibration; a 7% decrease II. ULTRASONIC VIBRATOR DESIGN
in drawing force at the lowest drawing speed of 676 mm/s In the wire drawing experiment, ultrasonic vibrations were
and with a driving voltage of 240 V; prolonged tension applied to the dies via the ultrasonic vibrators, the exploded
regulation period from 0.5 s to about 1.5 s; and improved view of which is displayed in Fig. 1. The system is com-
surface finish of drawn wires. Yang et al. [19] analyzed the prised of the ultrasonic transducer, the ultrasonic horn, and
influence of longitudinal-torsional composite vibration on the the wire drawing die. The ultrasonic transducer is employed

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

TABLE 1. Material parameters for the components of the vibrator.

FIGURE 2. 2D cross-section structure of the designed ultrasonic horn.

to convert electrical signals into mechanical movements in


the form of high-frequency longitudinal vibrations at the and 820 mm, respectively. Therefore, the length could be
output end. The output amplitude of the piezoelectric trans- calculated as 125.5 mm, and the amplification can be deter-
ducer is further amplified by the ultrasonic horn to meet the mined to be 3.61. More details about the calculations and
demands of subsequent titanium wire drawing experiments. design of ultrasonic horns could be found in the ultrasonics
As indicated in Fig. 1, the Langevin-type transducer mainly handbook. The 2D (two-dimensional) cross-section view of
consists of four components: the front mass which is made the designed stepped ultrasonic horn is illustrated in Fig. 2.
of 2A12 aluminum alloy, six pieces of PZT (lead zirconate The performance of the horn was further evaluated by FE
titanate) discs, the steel back mass, and the clamping bolt. (finite element) analysis in ANSYS R
, using APDL (ANSYS
Beryllium bronze sheets (not shown Fig. 1) are sandwiched Parametric Design Language) codes. Modal analysis results
between the PZT rings to serve as electrodes. These compo- show the horn resonates at the frequency of 19.929 kHz, with
nents are compressed tightly using the clamping bolt with a magnification ratio of 3.516, which is in good agreement
a preload of 20-30 MPa on the PZT discs. Higher acoustic with the calculated values.
impedance material, 2Cr13 stainless steel, was chosen for
the back mass to encourage mechanical wave propagation
towards the front mass. PZT-8 is the selected material for the
PZT rings, as it provides high mechanical quality factor, high
permittivity, and low dielectric losses, which is preferable
than other PZT materials for high power applications. The rel-
evant parameters about above materials are listed in Table 1.
Furthermore, to guarantee the performance of the transducer,
the contacting surfaces of the front and back masses with
the PZT rings or the electrodes should be ground to enhance
their flatness and roughness. The stepped half-wavelength FIGURE 3. FE model of the designed ultrasonic vibration system.

ultrasonic horn is also made of 2A12 aluminum alloy and


was connected to the transducer through threaded joints. The In order to study the dynamic performance of the ultra-
wire drawing die, 810 mm in diameter and 5.5 mm in height, sonic vibration system, an integrated FE model combining
is composed of a steel case and a diamond core and was the transducer, the horn, and the die was established in
attached to the thin end of the horn using the shrink-fitting ANSYS R
, as shown in Fig. 3. In the model, the PZT rings
technique. A shoulder was designed at the nodal position were meshed with the 3D (three-dimensional) 10-node cou-
where the ultrasonic amplitude reaches the minimum value so pled field element SOLID227, whereas the other components
that the vibrator could be installed on and dismounted from were meshed using the SOLID185 structural element. All of
the wire drawing experimental platform conveniently. the PZT rings were polarized along the thickness direction
The ultrasonic horn is an essential part of ultrasonic wire (Z direction), however, each adjacent two pieces of them were
drawing system as a consequence of the insufficient output installed along reverse directions, i.e., along or opposite to
amplitude of the ultrasonic transducer, which is normally the longitudinal vibration direction. The vibrator, as a whole,
4–5 µm, far below the minimum requirement of 10 µm. was constrained at the nodal position, as illustrated in Fig. 3.
Most frequently used ultrasonic horns can be classified as The piezoelectric strain matrix [d], the compliance coeffi-
stepped, exponential, conical, and catenoid, according to their cient matrix [s], and the permittivity matrix [ε S ] about the
longitudinal cross-section shapes. For an ultrasonic horn of PZT-8 [21] were defined by (1) to (3).
a specific type, the amplification factor is determined by  
the area ratio between the input and output surfaces. In the 0 0 −140
 0 0 −140 
current work, stepped ultrasonic was chosen because it can  
 0 0 350 
achieve the largest amplification factor, which is in proportion [d] =   × 10−12 m/V (1)
to the area ratio between the input and output surfaces. The  0 580 0  
 580 0 0 
ultrasonic horn was designed with an operating frequency
of 20 kHz, and the input and output diameters of 838 mm 0 0 0

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

FIGURE 4. Modal analysis result of the established FE model.

  FIGURE 5. Sensitivity analysis of the longitudinal resonant frequency


13.3 −4.26 −4.26 0 0 0 versus the lengths of the input and output sections.
 −4.26 13.3 −4.26 0 0 0 
 
 −4.26 −4.26 17.05 0 0 0 
[s] = 
 0

 0 0 41.16 0 0  
 0 0 0 0 41.16 0 
0 0 0 0 0 35.11
× 10−12 m2 /N (2)
 
h i 1800 0 0
εS =  0 1800 0  (3)
0 0 1500
Fig. 4 presents the contour of the deformed ultrasonic FIGURE 6. Transient response of ultrasonic vibrator (a) within 25 ms,
vibrator at its second order longitudinal resonant frequency. (b) from 24.2 ms to 24.6 ms.
It can be seen that the system resonated at 19.769 kHz, which
is quite close to the intended 20 kHz. And there was almost
no deformation at the nodal position, as had been expected. within 15 ms. Fig. 6(b) indicates the vibrator finally output a
Furthermore, the sensitivity of the resonant frequency to the stable sinusoidal vibration with an amplitude of 20.9 µm.
lengths of the input and output sections of the ultrasonic horn
was analyzed, the result of which is plotted in Fig. 5. It can
be found that the longitudinal resonant frequency of the ultra-
sonic vibration system shows an upward trend as the length of
the ultrasonic horn decreases, for both the input section and
the output section. However, the resonant frequency is more
sensitive to the length of the later than that of the former,
as illustrated in Fig. 5. This provides a convenient way to
regulate the resonant frequencies of the ultrasonic vibrators
in practice.
The time-varying output displacement of the vibrator at
FIGURE 7. Assembled prototypes of the ultrasonic vibration system.
the second resonant frequency was determined through tran-
sient analysis. During the simulation, an alternating voltage
of 19.769 kHz, 800 Vp-p was applied across the PZT rings, III. ULTRASONIC VIBRATORS TESTING
as illustrated in Fig. 3. The time duration was set as 25 ms, According to above simulation results, ultrasonic transducers
which equals to 500 vibration cycles. And the minimum and horns were manufactured, the assembly of which is dis-
recommended substep number was specified as 16 for each played in Fig. 7. The vibrators were fitted into the specially
vibration period. The dynamic response of the vibrator is designed holders through the shoulders machined at their
shown in Fig. 6. It can be seen that the amplitude of the nodal positions for subsequent tests, installation, and experi-
vibrator fluctuates remarkably at the beginning, however, sta- ments, because the shoulders themselves are too narrow to be
bilizes gradually as it reaches the steady value of about 20 µm clamped conveniently.

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

FIGURE 9. Vibration mode detection results: (a) mode shape of vibrator


A, (b) mode shape of vibrator B, (c) oscillating velocity of vibrator A at
different frequencies, (d) oscillating velocity of die B at different
FIGURE 8. Impedance measurement results: (a) impedance of vibrator A,
frequencies.
(b) phase angle of vibrator A, (c) impedance of vibrator B, (d) phase angle
of vibrator B.

the dies can effectively produce longitudinal vibrations.


The impedance testing equipment Agilent HP 4294A was In Fig. 9(c) and 9(d), we can see that the vibration veloc-
employed to measure the electrical impedance of the vibra- ity of the output surface was influenced by the frequency
tors, the results of which were plotted in Fig. 8. By comparing of the input chirp signals. The vibration velocities reached
Fig. 8(a) and Fig. 8(c), it can be seen that the impedance of their maximum values when the sweep frequency matched
the vibrators reaches their minimum values of 9.95  and with the resonant frequencies of the vibrators. As a result,
13.17  at the frequencies of 19.645 kHz and 19.656 kHz, the two vibrators resonated respectively at the frequency
respectively. That means the vibrators resonant at these fre- of 19.672 kHz and 19.664 kHz, with a negligible difference
quencies which are quite close to the targeted frequency of 8 Hz. On the other hand, if the frequency of the driving
of 20 kHz. The difference between the resonant frequencies voltage deviates from the resonant frequency, the vibration
of the two vibrators is merely 11 Hz, which is negligible. amplitude or velocity would drop significantly, considering
Also, from Fig. 8(b) and Fig. 8(d), we can find that the phase the narrow bandwidth of the ultrasonic vibrators. In Fig. 9(c)
angles of the vibrators are 5.8◦ and 3.4◦ , far below 10◦ . The and 9(d), when the frequency deviation exceeds 130 Hz,
power factors of the vibrators can be subsequently calculated the output amplitude and velocity are reduced by 50%, even
as 0.9948 and 0.9982, respectively, which means the vibrators though the driving voltage remains unchanged. The rela-
themselves can efficiently transfer electrical energy and there tionship between the frequency deviation and the oscillating
is no need to conduct the impedance matching procedure. amplitude (or velocity) reduction ratio is depicted in Fig.10.
What is more, as the phase angle difference between the Although the frequency difference between the vibrators
vibrators is only 2.4◦ , they almost vibrate at the same pace is rather insignificant, it is very difficult to be eliminated
when driven by the identical electrical signals. Similarly, entirely. When driven by alternating signals with the same
the vibrators would oscillate along opposite directions when ultrasonic generator, the two vibrators would interfere with
the driving signals have a phase difference of 180◦ . There- each other. For this reason, the coupled vibration mode
fore, the vibrators are qualified for the following two-pass of the vibrator when they work together was examined
wire drawing experiments. In general, as both the vibrators under the same sweep signal, the result of which is shown
have high mechanical quality factors, their frequency bands in Fig. 11. It could be seen that the output ends of the vibra-
(about 200 Hz) are relatively narrow, as shown in Fig. 8(b) tors arrived at their maximum displacement simultaneously.
and Fig. 8(d). Fortunately, the dynamic characteristics of the Fig. 11(b) shows, however, that the maximum value of their
vibrators are in good consistency. coupled oscillating velocity occurs at the coupled frequency
The mode shapes of the vibrators, as well as their oscil- of 19.727 kHz, which is 55 Hz and 63 Hz higher than the reso-
lating velocities at different frequencies, were measured nant frequencies of each vibrator. In other words, the coupling
using the Polytec PSV-400-M2 scanning laser vibrometer, effect between the vibrators whose dynamic performances are
the results of which are demonstrated in Fig. 9. During the in good agreement, would not exert remarkable influence on
test, chirp signals with a sweep frequency band of 18–20 kHz, their phase angle and coupled resonant frequency.
and a voltage of 10 Vp-p were applied to the vibra- The real-time output velocities of the ultrasonic vibra-
tors. From Fig. 9(a) and 9(b), it can be found that tors were measured by the Doppler Vibrometer using the

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

FIGURE 13. Velocity curves of (a) die A, (b) die B.

of 800 Vp-p , 19.672 kHz and 19.664 kHz in frequency were


applied to the piezoelectric transducers. The changing curves
of the vibration velocities of die A and die B with time are
plotted in Fig. 13.
It can be seen that the output velocities of the two vibrators
vary with time periodically in the form of sinusoidal curves,
the amplitudes of which are 2.457 m/s and 2.288 m/s, respec-
FIGURE 10. Variation of amplitude reduction ratio with frequency
deviation. tively. Based on this, the corresponding vibration amplitudes
of the individual vibrators, under the same driving voltage,
could be calculated as 19.88 µm and 18.51 µm, which are
quite close to the FE simulation result of 20.91 µm. Simi-
larly, the actual amplitudes of the vibrators working at their
resonant frequencies of 19.672 kHz and 19.664 kHz, as the
driving voltage increased from 100 Vp-p to 800 Vp-p , were
calculated, the results of which have been plotted in Fig. 14.
We can find that the changing curves of the vibrators are
alike. With the increment of the driving voltage, the output
amplitude rises almost linearly. However, the amplitude of
vibrator A is a little higher than that of vibrator B, when
FIGURE 11. Vibration mode detection results when the vibrators work
simultaneously: (a) coupled-mode shape, (b) the relationship between
excited by the same voltage. This can be attributed to the
oscillating velocity and frequency. relatively smaller impedance of vibrator A, as the energy
consumption of an ultrasonic vibrator is in reverse proportion
to its equivalent impedance.

FIGURE 14. Independent output amplitudes under different driving


voltages for (a) vibrator A, and (b) vibrator B.
FIGURE 12. Vibration measurement system with the Scanning Laser
Doppler Vibrometer. When die A and die B work simultaneously in the same
circuit, the interaction between them has to be taken into
account. In this condition, the vibrators are working at their
single-point velocity determination technique, the construc- coupled resonant frequency of 19.727 kHz, with the driving
tion of the testing equipment is shown in Fig. 12. During voltages ranging from 100 Vp-p to 800 Vp-p . The changing
the test, a point on the output surface of the vibrator was curves of their output amplitude with the increased driving
selected as the target point. Then, the position of the scanning voltages are shown in Fig. 15. The maximum output ampli-
head was adjusted so that the laser beam could focus on the tudes of the vibrators are 15.77 µm and 13.97 µm, much
point. Next, 100 kHz was assigned as the sampling frequency smaller than their corresponding values when working sep-
of the vibration testing instrument, and alternating voltages arately. Three reasons might be responsible for this. The first

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

FIGURE 15. Coupled output amplitudes under different driving voltages


for (a) vibrator A, (b) vibrator B.

is the frequency deviation between the coupled frequency and


their independent resonant frequencies. As shown in Fig. 10,
a 55 Hz to 60 Hz gap in frequency would cause about 17%
reduction in their output amplitudes. The second reason is the
impedance difference between the vibrators, which should
account for the inferior performance of vibrator B. The third FIGURE 17. The relationship between the wire drawing velocity and the
frequency of the modulator.
reason might be the inadequate output power of the ultrasonic
generator. The energy consumption will be reduced for each
vibrator when they work together compared with when they
work alone. However, it is still reasonable to use the vibrators of 19.727 kHz and remained unchanged. Their voltages, how-
for the subsequent wire drawing experiment, as their output ever, could be adjusted to regulate the oscillating amplitudes
amplitudes are quite close and higher than 10 µm, which of the dies. The vibrators were clamped by the specially
is sufficient for experimental purpose according to previous designed T-shaped steel frame, which, as a whole, were sub-
reports. sequently installed onto the Hiwin slide blocks. The slide
blocks can move smoothly along the slide guideways and
could be fixed at appropriate positions conveniently by the
lock bolts. The winding system is composed of an electromo-
tor, a reduction gearbox, a torque sensor, a coiler drum, and
the clutches between them. The wire drawing speed is deter-
mined by the output rotational velocity of the electromotor,
which is in turn regulated by the gearbox and the frequency
modulator. The relationship between the input frequency
of the modulator and the wire drawing velocity is plotted,
as shown in Fig. 17. It can be seen that the wire drawing
velocity increases linearly from 30 mm/s to 530 mm/s as the
FIGURE 16. Established experimental equipment for two-pass ultrasonic
input frequency changes from 10 Hz to 90 Hz. The two sides
wire drawing. of the torque sensor were respectively connected to the motor
and the coiler drum to measure the wire drawing force. The
torque values were acquired and shown in real time on the
IV. WIRE DRAWING AND INSPECTION EQUIPMENT screen of the digital display. During the experiment, the raw
The arrangement of the developed experimental equip- titanium wire, with a diameter of 0.4 mm, was pulled through
ment for double-die ultrasonic wire drawing is illustrated two oscillating dies, with a diameter reduction of 0.02 mm
in Fig. 16. The equipment is mainly composed of three for each pass. The material of the wire is commercially
systems: the wire feeding system to collect and provide the pure titanium (TA2), and graphite has been employed as the
raw wire; the ultrasonic vibration system to impose ultrasonic lubricant to reduce wire break-off ratio.
vibration on the dies; and the winding system which provides Although it is convenient for us to observe the changing
the drawing force and collects the drawn wire. Specifically, trend of the drawing force by reading the digital display, its
the ultrasonic vibration system or the vibrator consists of refresh rate is inadequate for the average drawing force calcu-
a piezoelectric transducer, an ultrasonic horn, and the wire lation. Therefore, a data acquisition system was established
drawing die, as aforementioned. The driving signals of the in LabVIEW R
, the block diagram of which is illustrated
vibrators, with a phase difference of 180◦ , are provided in Fig. 18. The system is made up of the torque sensor,
by the identical ultrasonic generator so that the two dies the NI 9215 data acquisition (DAQ) card, and the computer,
oscillate along the opposite directions. The frequencies of the as shown in Fig. 16. The output analog signal of the torque
driving signals were set as the coupled resonant frequency sensor is transferred to the NI 9215 module and converted into

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

FIGURE 18. Block diagram established in LabVIEW for wire drawing force
measurement.

the digital signal, which is subsequently transmitted to the FIGURE 20. Variation of drawing force with wire drawing velocity when
computer through LabVIEW 2016 interface. When subjected ultrasonic vibrations of different amplitudes were applied.

to the torque induced by the wire drawing force, the frequency


of the output signal generated by the sensor would change
correspondingly. This change will be detected by the program experiment, the frequency of the ultrasonic generator was
after Fourier transformation, and therefore, the torque or the set as the coupled frequency of the vibrators, 19.727 kHz,
drawing force could be calculated based on the relationship and remained unchanged. A phase difference of 180◦ existed
between the torque and the frequency deviation. The cal- between the driving signals of the vibrators so that the two
culated drawing force was displayed on the front panel of dies oscillated oppositely to each other. The output volt-
the program in real time and would be written to assigned age of the generator was adjusted to regulate the oscillating
local file path automatically. After the experiment, specimens amplitude of the dies which changes from 0 µm (without
of the drawn wire were submerged into a jar of acetone vibration) to around 15 µm. The minor difference between
solution, which was later put into an ultrasonic cleaner to the output amplitudes of the two vibrators, as have been
remove the dirt and stains adhering to the surface of the drawn analyzed in above sections, was ignored. Unless otherwise
wire. Then, Hitachi S4300 field-emission scanning electron stated, the amplitude mentioned below means the amplitude
microscope (FESEM) was employed to inspect the surface of die B or vibrator B. The input diameter of the raw wire was
morphologies of the drawn wire samples, and the appearance 0.4 mm, which was separately reduced by 0.02 mm when the
of the instrument is shown in Fig. 19. The image of the wire was pulled through die A and die B.
morphological features of the drawn wire specimen when Under traditional wire drawing conditions, where the
magnified to 25 times is presented in the monitor display, vibration amplitude is 0 µm, the value of the drawing force
as shown in the right subfigure. stabilizes at around 19 N with slight fluctuations, although
the drawing speed increased significantly from 100 mm/s
to 500 mm/s. Under ultrasonic wire drawing conditions,
however, the drawing force shows an upward trend with the
increment of the drawing velocity, especially when ultrasonic
amplitude exceeds 7 µm. In addition, although the drawing
force tends to be higher at increased drawing speed, it never
surpasses the original wire drawing force without ultrasonic
vibrations. Moreover, comparing those changing curves cor-
responding to different vibration amplitudes, the wire draw-
ing force is smaller when ultrasonic vibrations of larger
amplitude were superimposed. But exceptions may occur
when the ultrasonic amplitude was relatively lower, below
FIGURE 19. Appearance of the surface morphology inspection
7 µm for instance. At the drawing speed of 99mm/s and
instrument. 298 mm/s, the drawing forces tend to be lower than sur-
rounding data points. This might be caused by the inferior
performance of the motor or the gearbox, as the offsets about
V. RESULTS these points are almost the same. Therefore, the following
Fig. 20 shows the changing curves of wire drawing force conclusion could be drawn: first, ultrasonic vibration con-
along with the drawing velocity when ultrasonic vibrations tributes to reducing drawing force; second, increased draw-
of various amplitudes were applied to the dies. During the ing velocity weakens the drawing force decreasing effect;

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

TABLE 2. Influence of drawing velocity on drawing force reduction when We can arrive at similar conclusions that greater vibration
ultrasonic amplitude is 10.93 mm.
amplitude and lower drawing speed are beneficial for cutting
down the drawing force. Within the variation range given
in this work, the vibration amplitude seems to have a more
significant influence on the drawing force than the drawing
speed. To illustrate the influence of the vibration amplitude
more explicitly, the reduction rate of the drawing force at the
same drawing speed of 298 mm/s, but with different vibration
amplitudes, were calculated, as listed in Table 3.

TABLE 3. Influence of vibration amplitude on drawing force reduction at


the drawing speed of 298 MM/S.

third, larger ultrasonic amplitude boosts the drawing force


reduction phenomenon. To demonstrate the weakened force
reduction phenomenon under relative higher drawing veloc-
ity conditions more precisely, the drawing forces and the
relevant reduction rates at different drawing speeds, but with
the same ultrasonic amplitude of 10.93 µm, are summarized
in Table 2.

FIGURE 21. Variation of drawing force with ultrasonic amplitude at


different drawing velocities.

Fig. 21 presents the variation curves of wire drawing FIGURE 22. Surface morphologies of drawn wire specimens at the
force with the amplitude of the imposed ultrasonic vibration drawing speed of 99 mm/s.
at different drawing speeds. The experiment configuration
stayed unchanged as before. A remarkable decline in the To further investigate how the vibration amplitude and
wire drawing force could be easily observed as the ultrasonic wire drawing speed affect the surface finish of the processed
amplitude increases from about 5 µm to roughly 14 µm. titanium wires, specimens of the drawn wires produced at
In more detail, a very sharp decrease appears when the the speeds of 99 mm/s, 298 mm/s, 480 mm/s, and with the
ultrasonic amplitude is below 10 µm. However, this trend vibration amplitudes of 0 µm (without vibration), 5.63 µm,
is moderated when the ultrasonic amplitude is greater than 9.69 µm, and 13.97 µm were examined using the FESEM
10 µm. Wire drawing velocity also exerts some influence instrument, the results are shown in the following figures.
on these changing curves. For example, at the lowest draw- Fig. 22 presents the surface morphologies of the drawn wires
ing speed of 99 mm/s, the corresponding changing curve at the drawing speed of 99 mm/s with a magnification fac-
is relative irregular compared with curves at other drawing tor of 250. In the upper left subfigure, it is easy to find
speeds. Furthermore, the curves relating to higher drawing that galling, spalling, checking, with tiny chips and debris,
velocities are generally above those for lower drawing veloc- distribute evenly on most regions of the processed wire
ities, although they interweave with each other occasionally. surface when conventional drawing method was adopted.

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S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

In the other subfigures, with ultrasonic vibrations applied, Fig. 22(d) and 23(d). As for the samples drawn in moderate
the chips and debris were removed, making their surfaces vibration amplitude occasions, the surface quality has also
much cleaner. In addition, the vibration amplitude also affects been apparently improved.
the surface quality of the processed wires. When the applied
ultrasonic amplitude is insufficient, as shown in Fig. 22(b),
cracks and fragments still exist in the most areas of the
outer surface. However, these defections would disappear
with the increment of the vibration amplitude, as shown in the
third subfigure. But, when the amplitude surpasses a specific
value, to 13.97 µm for instance, flaws such as furrows and
fragments reappear, although this only occurs in very lim-
ited regions, as the lower right subfigure shows. Therefore,
it can be concluded that ultrasonic vibration is beneficial
for improving the surface finish of the drawn wire, but a
moderate vibration amplitude is more suitable at a relative
lower drawing speed.

FIGURE 24. Surface morphologies of drawn wire specimens at the


drawing speed of 480 mm/s.

Fig. 24 compares the surface finish of the titanium wire


samples drawn at the velocity of 480 mm/s, with different
vibration amplitudes of the dies. Still, all the samples show a
better surface finish than their counterparts in Fig. 22 and 23,
especially for those samples drawn with the assistance with
ultrasonic vibrations. For the sample drawn without ultra-
sonic vibration, there seems no change in its surface appear-
ance. However, the area with the surface defects has narrowed
down. In ultrasonic wire drawing conditions, the influence
of a higher drawing speed is much more impressive. All the
FIGURE 23. Surface morphologies of drawn wire specimens at the three samples, in spite of the difference in oscillating ampli-
drawing speed of 298 mm/s. tudes, have achieved a much better surface finish, especially
for the sample drawn with the largest vibration amplitude
Fig. 23 shows the surface appearance of the processed of 13.97 µm. Under this drawing speed, the surface mor-
wires drawn at the velocity of 298 mm/s when the dies phologies of the three ultrasonic drawing samples are alike,
oscillate with different amplitudes. Compared with Fig. 22, except several shallow furrows appear in Fig. 24(b) and an
the surface smoothness of these drawn wire samples has been unexpected debris shown in Fig. 24(c). That means ultrasonic
improved noticeably when the experiment was performed at vibration is still beneficial for enhancing the surface quality of
a relatively higher speed. More specifically, chips and debris the drawn wires at a relative higher drawing speed. However,
no longer adhere to the surface of the drawn wire even under its amplitude is no longer make a big difference in this aspect.
the traditional drawing conditions. Surface flaws of spalling In other words, when the oscillating amplitude reaches a
have been eliminated, although furrows and cracks along the specific value but the surface finish is still bad, increasing the
wire drawing direction appear instead. For ultrasonic wire drawing speed would be a better choice to tackle the problem.
drawing conditions, the surface quality improvement effect
is influenced by the amplitude of the imposed ultrasonic VI. CONCLUSION
vibration. When the dies oscillate with a smaller amplitude, In this paper, two-pass titanium wire drawing with the dies
for instance, 5.63 µm, a higher drawing speed can remarkably oscillating along opposite directions were studied experi-
improve the surface finish of the drawn wire, comparing mentally. The ultrasonic vibration system was designed and
Fig. 22(b) and 23(b). However, for the wires drawn with analyzed using an FE model established in ANSYS R
. The
a larger ultrasonic vibration amplitude, there is almost no influences of the lengths of ultrasonic horns on the res-
observable improvement in their surface quality, as shown in onant frequency, as well as the dynamic response of the

VOLUME 6, 2018 16585


S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

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of 13.97 µm, the drawing force could be decreased by pp. 645–655, Mar. 2016.
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the surface smoothness of the drawn wires, regardless
of at the lower, moderate, or higher drawing speeds.
But the optimal vibration amplitude is influenced by
SHEN LIU was born in Yongcheng, Henan, China,
the wire drawing velocity. When wire drawing was
in 1989. He received the B.S. degree from the
conducted at or below the moderate speed of 298 mm/s, School of Mechanical Engineering, Zhejiang Uni-
a medium vibration amplitude of 9.69 µm is the best. versity of Technology, in 2012, and the M.S.
However, in higher drawing speed (480 mm/s) occa- degree from the School of Mechatronics Engi-
neering, Harbin Institute of Technology, China,
sions, the vibration amplitude could change within a
in 2014, where he is currently pursuing the Ph.D.
wider range (5.63–13.97 µm) without inducing unac- degree. His research interests include energy har-
ceptable surface morphologies. vesting and ultrasonic-assistant wire drawing.

REFERENCES
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[2] C. N. Elias, J. H. C. Lima, R. Valiev, and M. A. Meyers, ‘‘Biomedical YUANCAI YANG was born in Zigong, Sichuan,
applications of titanium and its alloys,’’ JOM, vol. 60, no. 3, pp. 46–49, China, in 1993. He received the B.S. degree from
Mar. 2008. the School of Mechanical Engineering, Chongqing
[3] R. R. Boyer, ‘‘An overview on the use of titanium in the aerospace indus- University, in 2015, and the M.S. degree from
try,’’ Mater. Sci. Eng. A, vol. 213, nos. 1–2, pp. 103–114, Aug. 1996. the School of Mechatronics Engineering, Harbin
[4] K. Siegert and A. Möck, ‘‘Wire drawing with ultrasonically oscillat- Institute of Technology, China, in 2017, where
ing dies,’’ J. Mater. Process. Technol., vol. 60, nos. 1–4, pp. 657–660, he is currently pursuing the Ph.D. degree. His
Jun. 1996. research interests include self-sensing actuator and
[5] V. P. Severdenko and V. Z. Zhilkin, ‘‘Heat treatment in drawing of titanium ultrasonic-assistant wire drawing.
wire,’’ Met. Sci. Heat Treat. Met., vol. 1, no. 10, pp. 21–24, Oct. 1959.

16586 VOLUME 6, 2018


S. Liu et al.: Experimental Study on Fine Titanium Wire Drawing with Two Ultrasonically Oscillating Dies

TAO XIE was born in 1965. He received the XIAOBIAO SHAN was born in Fuzhou, Jiangxi,
B.S. degree from the Department of Precision China, in 1977. He received the B.S. degree from
Instrumentation, the M.S. degree from the School the School of Automotive Engineering, Harbin
of Astronautics, and the Ph.D. degree from the Institute of Technology, in 2001, the M.S. and
School of Mechatronics Engineering, Harbin Insti- Ph.D. degrees from the School of Mechatron-
tute of Technology, in 1987, 1990, and 2003, ics Engineering, Harbin Institute of Technology
respectively. Since 2003, he has been a Profes- in 2004 and 2008, respectively. He is currently an
sor with the School of Mechatronics Engineer- Associate Professor with the School of Mechatron-
ing, Harbin Institute of Technology. His research ics Engineering, Harbin Institute of Technology.
interests include ultrasonic-assisted wire drawing, His research interests include energy harvesting,
piezoelectric energy harvesting, smart structures, and dynamic simulation. ultrasonic-assisted wire drawing, nanogenerator, and dynamic simulation.

VOLUME 6, 2018 16587

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