MICROBIOLOGICAL and CHEMICAL STANDARD for RAW PRODUCTS : S-LB-011
REVISED : # 07 ISSUED DATE : AUGUST 28, 2007 MICROBIOLOGICAL AND CHEMICAL STANDARD □ CUSTOMER STANDARD ☑ RAW PRODUCT ☑ TYC STANDARD □ COOKED PRODUCT □ VALUE ADDED PRODUCT A. ANTIBIOTIC CATEGORY ANTIBIOTIC SPECIFICATION METHOD FREQUENCY TEST BY RAW MATERIAL OXYTETRACYCLINE(ppm.) ND(Std.conc.minimum0.025) BIO-ASSAY EVERY PONDS INHOUSE LAB TETRACYCLINE GROUP(ppm.) ND (LOD=0.02) HPLC when RM positive* PRIVATE LAB OXOLINIC ACID (ppm.) ND (LOD=0.02) HPLC EVERY PONDS INHOUSE LAB CHLORAMPHENICOL (ppb.) ND (LOD=0.025) ELISA EVERY PONDS INHOUSE LAB MALACHITE GREEN(ppb) ND (LOD=0.05) LC-MSMS EVERY 3 MONTH DOF or PRIVATE LAB NITROFURANS (ppb.) ND(AOZ, AMOZ LOD=0.02, LC-MSMS SUPPLIER CONTROL to ASL DOF or PRIVATE LAB SEM ,AHD LOD=0.05) TEST EVERY 3 MONTH FINISHED PRODUCT TETRACYCLINE GROUP(ppm.) ND (LOD=0.02) HPLC DOF, PRIVATE OXOLINIC ACID (ppm.) ND (LOD=0.02) HPLC VERIFY EVERY DOF,INHOUSE LAB CHLORAMPHENICOL (ppb.) ND (LOD=0.025) ELISA TWO MONTH DOF,INHOUSE LAB NITROFURANS (ppb.) ND(AOZ, AMOZ LOD=0.02, LC-MSMS DOF,PRIVATE LAB SEM ,AHD LOD=0.05) REMARK : FREQUINCY : *Positive tested by BIO-ASSAY daily B. CHEMICAL CATEGORY ANTIBIOTIC SPECIFICATION METHOD FREQUENCY TEST BY RAW MATERIAL SULFITE (ppm.) < 10 MODIFIED MONIER WEEKLY INHOUSE LAB WILLIAMS METHOD PHOSPHATE (%) <0.5 MOLYBDENUM BLUE MONTHLY INHOUSE LAB FINISHED PRODUCT SULFITE (ppm.) <10 MODIFIED MONIER EVERY SHIPMENT INHOUSE LAB WILLIAMS METHOD PHOSPHATE (%) <0.5 MOLYBDENUM BLUE EVERY SHIPMENT INHOUSE LAB SALT CONTENT(%) <2 VOLUMETRIC METHOD EVERY SHIPMENT INHOUSE LAB MOISTURE (%) 75-84 MOISTURE BALANCE DEPEND ON CUSTOMER INHOUSE LAB REQUIREMENT C. MICROBIOLOGICAL CATEGORY MICROBIOLOGICAL SPECIFICATION METHOD FREQUENCY TEST BY RAW MATERIAL Aerobic Plate Count (CFU/g) < 1,000,000 BAM On line EVERY PONDS INHOUSE LAB Coliform (MPN/g) < 250 BAM On line INHOUSE LAB E. coli (MPN/g) <10 BAM On line INHOUSE LAB S. aureus (MPN/g) <100 BAM On line INHOUSE LAB Salmonella spp.(/25g) ND ISO 6579 INHOUSE LAB V. cholerae (/25 g) ND BAM On line INHOUSE LAB V. parahaemolyticus(MPN/ g) <3 BAM On line INHOUSE LAB FINISHED PRODUCT Aerobic Plate Count (CFU/g) <500,000 BAM On line DAILY : 4 PERIOD INHOUSE LAB Coliform (MPN/g) < 100 BAM On line RELEASE : 5 SAMPLE/ INHOUSE LAB E. coli (MPN/g) <10 BAM On line SHIPMENT INHOUSE LAB S. aureus (MPN/g) < 100 BAM On line INHOUSE LAB Salmonella spp.(/25g) ND ISO 6579 INHOUSE LAB V. cholerae (/25 g) ND BAM On line INHOUSE LAB V. parahaemolyticus(MPN/ g) <0.3 BAM On line INHOUSE LAB D. SANITATION DESCRIPTION SPECIFICATION FREQUENCY APC Coliform E. coli S.aureus Salmonella spp. V.cholerae V. parahaemolyticus CFU/100cm2 MPN/100cm2 MPN/100cm2 /100cm2 /100cm2 /100cm2 /100cm2 EQUIPMENT ONCE/WEEK 1. BEFORE WORK < 100 ND ND ND ND ND ND 2. AFTER CLEAN < 100 ND ND ND ND ND ND 3. DURING WORK < 5,000 < 10 ND ND ND ND ND PERSONNEL ONCE/WEEK 1. AFTER CLEAN < 100 ND ND ND ND ND ND 2. DURING WORK < 5,000 < 10 ND ND ND ND ND AIR TEST 50/15min NT NT NT NT NT NT ONCE / MONTH WATER & ICE < 100/ml ND(MPN/100ml)ND(MPN/100ml) ND/100ml ND/100ml ND/100ml ND/100ml ONCE/WEEK