ESTIMATION ob _fPOTASSUUM _ FRERMANGANATECKMAD«)//NSINen | ——bommuic RACID (ci H9 04) Page No. |-—+ i : |_ + Becuee IA Potassium perman, (Kinds) reacts writ | i i H, . 7 | temperature. Ton 1 BC 04 = 10 Co, + De" i Mn Ds + 50,0, + loh* > &Mn** + 1000, + &H,0 | | -28nD4 + len* + (0e" Han iphe § 2HLD | |__| Procepuee = |b wes : | dissolved fae fn_-250 ml , Woatéy anc _prepated | |_M) 50 Solution 9 —Oxalle acid. wing 220m | standard volumetric. fade. | iy The _burrette _‘is_unaahed. — ust wale and | vinseoh _usitte _KMaOx @nd___ filled __up__t_Zev0_mnaak pipelte__In_ washed — _usith _wsaler aac Hae bin The _ vivaed voit oxalic _ add _and. _§0_ mL | Same» _ Pipetbect__out into a dean conical ffaak. |Gdutin tater in te! Potassium permanganas 1 purelte (Ritrenk) | _ Pe) “Soutin tasen in Fa mL Q Standard _ Pipelle (Titand) 3 Uhe “en gork _ Gdded iL H S04 (Acidic medinny 4 Indicate Selig Indicate | (Krina,) | 5 End pink Appearance 2 Perrranok pole pink Uteur. 6 Temperatiare °C - Tec 11 Molecular mare & ibe g mol" CALUMATION PART FoR tue Etanpeep _m/50 OxALIC AUD Sorution : PREPARATION OF 1 Mol = Oxalic add contains AM Oralic aud contains = Be AM Ondic atid Cmtained in 250 mo +WELMtING PROCEDURE Weight a weighi ng bottle Weight — a Used hottte + Oxahie Acid Weight Q Oratic aud rotid Volume § the Oxatic acid Aol bien peepaved Molavity 4 = Oxalic acid dotu tion Volume G Oxalic add ctution | taken fpr each titration TABULAR GoLuMN : Standard Oxolic acid Ve KMnOq | ] ie | | S.no | Volume 2 Oxatie Initial Yeeding Final vending, | Vatu Indicator | add taken — [the buvete Hoe burvele te King, in ome | (KMadg) in mi. (KMn04,) in aL soln. Uarduened ee | | fo me | | Sele | 1 | | | | Sndiots|| i&_] | | (lente) | | 1 | | | Ld | | CONMRDANT VALUE : || DETERMINATION OF MOLARITY DF _KMnO4 SOLUTION: 1] | Volumetric formula: i [Vi Min = Va Many Not : 4 indicates KMn0, and A indicates Oxalic audValueVy + Volume Kin Oy Pie Molavi ty § KMn0y m + No. @ electrons gained by KMnd, Vy = Votume. & Oxalic aad M, = Molar BR Oxalic add Ny = DM. % eectroma lose by Oxalic add M, = Me Xn, : foe i ail] | Aropunt Q Kindy present in one lie § the given Solutio | = Motarity of KMn, x Movecucar Mass of kMnd,