UALUTATINE INOR GANIC ANALYSI1

SYSTEMATIC ANALYSIS OF A SIMPLE SALT ZnS04

I.PRELIMIN ARY TBSTS

SYO EPERMENT OBSERVATIoN INFERENCE
1 oloun ard Apptahand
Whute ptuilkina Aicne of ",Fe",Fe
hlounand
aaAane of the olud Nand naya
Aiven ak is noted.
salte
2.Dry Raudng Tet
Talke a pindh of salk Salk tuans yelle Mayb 2n*

a dny et tuhe andwhun hot and wute

whent a

3Soulauty Test
ha soubliby e thu
Seesanui eted ia
i)Distiled Watex Soluble Mayoe chloriu, ulpeudt,
bSomida,Nitrate,ete
and asnu of otÜA
LailonatES

4Fan olour Text

No Aescna 0t_C a -
1OA0 pindh ct sal
n a wdrch glass Miz Chanacteais uBa
wihDemc.RCI. Take
paste na oak6 Dd
avd so t te fiama

5 A Tet
Carean olouaed Prescnuof Zuc
t a mitbure af Sal
luaon,cornu t00 and
ioloaltnitate. tt ik
Bunenn
ant n a
 6.Auton wit olilite
Hudhehlerie aud
A Shall amound ot No
he ealt u addid chakacteltta (0and
to diuuke kuhechlonic

7Adtien wit onc.H, SOa

Take a pindh ef sat No
n &dny test uie and dhauteskdi BT

$Action wn Mn02 and

Lonc Ha S0
uven slt ndd No
Ma and n. HaS04 chaiacena r,I
anA urin.

9:Lapeh Toning Test

0rikuluy Wtn thu No
Lalk it upe Chasadestisy
tumina and nK,30

o.Ation wi Na OR
Kat tu Salk iti NaOH Na gak
Aescnc ct NH
Nolved

Hiak tu Salk wikeHuyR No Posunu of_ acetate

aluohol and oneH, SDa chasackeehta
Poun thu ywAxAure Ma

I2.Tok for 0nalate

No chana Aanna of oxalaje
uith dil.H504 and KMno ved
 Chemyl Ngicls Tet
saktuhated witi No Alesxna
chahackenistiuk doloida
a a etcpoudtaseugs. NalH
ulien takin in aneteA
ESttult. Nou add
auie acud ard ad aulot,.

SYSTEMA IC ANALY9s OF ACID RADICAL

Sodium Conlonate Extad Tet

Repaiadi on fNa, eatract

Etil.a mall amount o Salk wih anydbous Na, 2 and
distiludWakeh. Beil, acl and ilteh he fiitta|e calud Sodiurn
Anlmate ntrat. t dindud iota five portions

Sno ExPERMENT OBSERVATLON INFERENCE

1.Sives Nitate Test
6 ths firck* portiton of No

Hh entat add dil-HNO2 phipekike

And AaN03_SElukit formad

2 Banium Chlside Test

Nuhalize hi tondL Iite perAptake ixt Presn of So
akien siH odil HCLand hdL in conu HCi Rniomed
ada Batl outien.

3.kadAetote Teak
NouAn tu hird hlhite peidpitate Prenu ot SO4
Sukain Antnonium
aCtAc aud and
wt aukate and Na O
add ad autate. IMAxtwre em

4brpush Rina Test No browun ring Aosene of NO

Neutralie ta fourt konmed
 orion t dal.M4

.and ndd fly yid

04tietion and ad
.Fe
AnL ,S4 d y o
f t
.odarg u

5 Ammorniun Moldake Test

NCuhoi t h ttion No
t LorHNO and adp A Api t u
Ammaium modae nd omid
Wwm.

L SYSTEMATIC ANALySIS OF BASIC RADIAL

Prepasation 0f cloas slt 90lutien

cisan salt olution u hepard b diaclvul t ae
sat in distiud ohes
1)or instulee oranates other on glube Atnororium
LANeOnake tha glen saki te lbedisolved inute niiL au
1Eor Sulpnide uss t dilute ritdic ad and diiute
ud dnloric acdd miature ayd filtes:
GROVP
Sno NO EXPERIMEN1 OesERVATLN INFERENCE
Tthu A puion add NopeAupitnte
P2

2 To t uua lutien 0dd No perutnhe Arkuntu 0f ea

diu and pis S ermud

To Io tu cdoah Solution add No eAupitake Absuce 4

NHaC) and NH4 OH 4
formaa A,Fe2,Et
h das alt calutiorn DlcA White Pren pt N op
add Ni4cl NH4DH and
pas hs PUALAPtLLte_ 2nt
 . Confirmatory Tewts For Aud Rodical
Cornmotony Test r Sulhote Aud Radical so2)
ExPERMENT oSERYATLO INFERENCE
99luionadd White perupitake Preschu bf 0
BaAa solutien

A Anutl to aloove W percpkato Prescnu ot_SO

peraptadte unuiundisaved icmad

V.Contärmatory Tes For Baic Radical

Gornkjirmatonu Rt Ar Ze Baxic Radicad (zn):

ExPERIMENT C8SERVATLON TNFERENCE
1 To bhe olaahSalt olukion eloate perapette
add NaDH_in dhopk to exOs Golul h exes_o oanmed

NuOH

2 Totu l salk tution Buih vite

add etarium esocuanide perigitate Lonimed

VRESUL1
ahgiven Sintpl saltortaing
)Aud radkcal_(anion) Suliphoke
Bai Yadical Ccatin) Zinc

b ta oven iwpl Sali Zinc Sulhake (Zns0)