AIM

AFIRNTU oEIAus REQuSED

CnEHICAL E0uATION-
TNDICAToR uED anoipalin
Exb FoT 0ourie to nt pier
O6STRVATioN TABLE
sellad fastirg Fe Rodry
22 32-1
4 43-1 339
23
3-1

CALOLAToNG
 PAGLNo.
ATE / 201

ACTIVITY - 3

AIM To aatermine the Btrengt and molu t

Soluhion
Or 9ivan Sodium, hydroxids CNa.0H)
OSin(H/20)OXalfc add s0luhon

APPARATUS CHEH ICA LS REQUIRED-

THEORY

CHEMCCAL EQUATION

CoOH (aal+ 2NaOH g)2 C0oNa (ag)+ 2H,oC0)

COOH Coo Na

,do n o t w r i k

DXOiC AddTn HhoFion Fiagk

ProcedUre NaoH in BuratFe>hange tmic in
proccdur

PRECAUTIONS :-(3-4)

RESULT
and Sren qh of aivon NaDH Soluhon is
HOlaJuy
H Ond X40 gIL
 AIM
-YTIVT34
AIM
APPARATUS CHEHICALS REQUIRED
APPP
foste Sample
HE
290p3242H3H020TA
IN RCSULT

ENt

OBSOsCpo
S.N

CP
 PAGENO
DATE 201

ACTIVITY-1
Do for porach aJum o wU as SO4
AIM:-

APPARA TUS AND CHENICALS REQUIRED

THEORY

PRDCE DURE

PRECAUT JONS
 PAGENo
DATE

SALT AN ALYSISS

PREPARATION OF ORIGINAL SOLUTION

dishilled wake
CP TaR a pinch OF salt dissolve it in
and shai mo Fest tube
(told Hot)

Group. No Group Ro en t Cahonb

O NH
dil. HCL Pb2
Grp. 1
GYp.2 dilHCQ+ Na, S Sol Cu2t
Grp. 3

Grp.4
Crp.
arp.6

ANALYSIS FOR Gr0 UP ZERO

ExperimanF Obsarvaion Tnferen c

O NaoH Test
Solid Salt t Evoluhon oF
Aa OH So ammonia
TNH, gas
 PAGENo
DATE 201

Dip one end of tha

g1ausb rod in dl HCe wnire NH4
Fumes Confimad
Bring iF ngar m
nouh of tha teF
fobd

2 Nasler's Roagant
TObt
bring ma uottom Brown NH4T
Olour Confimad
plu duppad in nuslar's
00gan hoor ths mouh
oF tho Osr Fub

ANALYS IS FOR GROUP ONE (Pb)

EXpERIHENT 08SERV ATION TNFE RENCE

Orlina) So of salt whffe Carp. 1 may

+ ai. HCL pYLupifor be prebonF

Tasrs for Pbt

onhr marory

OPOtaslom 10dida
TsF
 PAGENo
DATE 201

Origi nal Sol+ Yulow P-

KI 80 pYOupirate Con fimud

PoHasiom
Cnromake CRr04)

originad So+ YllOw PE

Lon hrmad
KCrO PreorpitaFe

ANALISIS FoR GROUP 2

Experi rmonr Observaho0n InFeren ce

Grp. 2 may
Oriainol son 8aR
d u l - HCR + Na,S pru pitake b presunt

bonhrmolory TesF for Cu

OPottosi um ta70 cyarnide

TF KLFeCCNJ,] )

bripinal Sol+ Chocolar2

brown ept onfirmo
K CFaCCN),
 PAGENo
DATE I 201

K Tot

Orgina sol+ UOhite Pot Cu2t

Lonhmd
RI Sol 1n orown so

ANALYS1S FOR GROUP TI

O 0.S t 4-5 drops

eb Lonc. HNO
Brou
PPE F may
a dd Solid ammonium
sen
prsenE
Chloride- boil -
to ol Coloured
under tap water PP
Getahnov A May b
add XCeSS OF LOnire Pebent
ammoniUm hydroxide
and Shake

L Group Reagen
NHC NHoH
Conc. HNO added
to uonvert F Fe

Conhmo.ory TSt For Fe

OPoHassium ferro-
anide Tes
 PAGEHo
DATE 201

KI Tost
Or ginal So+ UOhite PpE Cu
In orown So Lonfirm
KI Sol

ANALYSIS FOR GROUP TI

O 0.S t 4-5 drops

e onc. HNO
Paroudf Fer may
add Solid ammonium PP
an
Chloride- boil- (o ol Coloured
Under tap ater PP
add XCeSS OF
Getahnou A May ba
whife Pebent
ammonIUm hydroxide
Ond Shake

L Group RLagent-
NHACAt NHOH
Conc. HNO adde0
to onvert F F|

ConhrmaDry TLS For Fe

OPotassium ferro-
aide Tes
 PAGE No
DATE 1 201

O.S+PoH. ferro-Prussian 8ue Fe3 LonFirmed

Cyanide sol" Lolour PPE

(11) PoHacsiom Sul pho-

Cyanide Tes

Blood red Fe3t Lon Rmed

O.S+Pot. sulpho-
Cyanide Soln COlovr

Confirma rory Tést for AQ

O Lake Tes

O.S t2drops oF
Blue Litmus So Blut Ppt floaing A Bnfimed
amm o nium fn the OlourleSS
SO
hyaroxide drop-
wise bluc
ColoUr deveiDp

ANALYSIS FOR GROUP IV (Co, Ni Mn, Zn)

Na,S so in tia presence ef

LGroup RLagen
Solid ammoniom chloride and
ammonmum yaroyido
 PAGENo
DATE:1201

2t
O.5+ Solid NH,CA BlacR Co"NImay be
Presan
+NH40H + Na,S Coloure BUFF Pn may be
d

Son PP prsenE-

DUH zn may be
UWhite
putson
Con Hrmaory TesH Por Co

O Sodiom Nirare
TeS

O.S+ Amm. Hydro-| Yellou PPF Co Confirmed

xide+NaND Solid

Amm. thmiocyanae
Ether Tesh

O.S+Eher +
Bloe olour in Co
2t Lonfirmed
crystal eh amm.
nar 1ayer
thioyanaFe
Shale the tesSF

D'be, a llouo to
 PAGENo
DATE 201

Confirmatory Tesks fpr Ni

O Dimetmy Glyox ime

Tes

0.S+ NH0H Sol"+ Rose Rod pp N2 Lonfirmed

Peuw drops of dimahy
qly oxim

Sodiom Hydroxide
-Bx ater Tec

0.S+ Na OH Sol"+
NiLonhrmid
Apple Careen
Bromine warer Pp
Boil Cif reqd.)
 PAE M
DATE 21

ANION ANALVSIS

O Conc.H,sO4 Tes
Co ( coYbonate) CChloride)
s(sulphfdo) Bx (eromide)
So CSulphite) CToaide)

No, (Nirite) ND CNran)

CH Coo CAcetare)

COO Coxala+e)
CO0

Inde pan d ent Radicals

SOACSolphat@)

Po4 Cphosphae)

DilUH HSOa TesF Take a pinch 8 a l r . Add

1-2m e dul H,sO4 In it
obserue the change

0BSERVATTION INFERENCE

Ci Colourle ss odourleSS gas

Oith brisK eHervesun ce may bt presun

 PAGENo
DATE 201

tumb ind water

MIky
(donL in U-tubl)

i olourles gas 0ith Sm @l

uke hor h roten 2ggs S may be present
torns 2ad aceare paper
black

Colo0urle ss goas mu uke

har eh borning SOlph ur 80 may be presenu
urns acidihed potasafom
di'chro m ate papar grier

Civ) Reddugh - br0uon gas 9Tth

pungent Smuu turns NO AOy be

Ferroos SUlphar o black

NO gas VOved
co3, so NO are
CUoCen

CON FIRMATORY TESTS

O For Carbonar Co
 PAGE No
DATE: 1 201

EXPERIMENT 0BsERVATION INFERENCE

d)Lima Warer Ts

Pinch &ar+ dil.

S04, Ppass the gasbrisk Effervesconce COConfirmed
hrough uu Water

MgqS04 Test

Aqeous Sol" of SalFormah on of wnite o o hirmed

n
1 m o MasO4 Sol pre ipitare

D For Ss

) Sodiom Niro
Prosside Tost

Aqueovs so e Sal
+Feuo drops of Porple or violet SLonPirmed
Sodium niro procdde 0100raion
So

) Lead Acetae
TesF
 PAGE No
DATE 201

A 9. Sol" of &alt+
Bla CR ppt s2
s2 onfirmed
ead acetaFe So
 YhusChafte Wat ghtagt
Bnmuel Escamn 2022233

Chaeta Houks
2 Uds)
3
3 (Steugt Le
5
Ploe
deuu d Noluoi 5
5
6 Wad E

Reiatin
8 uawitim
3
Setido
1o Fludo
) T h u n a d