Date 4/o9/1

Expt. No...08
Page No. 32

Xperiment No-08
Aim enti6icaion unctional geoup 9 t3o iven 0xgonic
comgDund A' 8

detiication mpleA
raferiment Obiervation Onkne
Lm 7he given Compmund Bromhe ocder Gti ven Compourt
OQ fahen in CCa y bromine did no4 decobuKe Batuadd
ade a ) added dropsike

No obiervation ACoholic (-OH)

Dmmon'um ntrate Jn da aOup Oas
ctded to lal
of the abieni
given Compound

itmUs Tet Litmus fapee May cotedn

drop o he tur ed -CooH 7ouP
mpound va_put Orphenic genp
moist blue itmUs
aper

Cla tet; NO peculian Phenolic rop

Keno dmp drk colous Way abset
poundvw ere Obtained
ded in 5ml neutral Fels

Teacher's Signature:-
 Date14/281
Expt. No.08 Page No. 33

NoHCOs test
rolt
Brisk etfervecence -CoOH
uantity compaund a obtouned presen
a s added in Sm
NHCO 5 0 /

tstertet
Small antify6 comeand SOee uity -Coo srop
ml ethanol y 4-5dropr &meli Das Corki mes
conc H, S04a addes Obtane
armed

eacton
Sodiun Bicarbnate ten
CHCOOH aHCO3 CHsCooNa tCO H o
Re vexcere

ater tet
CsC0OH+C2tHsOH Cone S crh coo CaHs t
Ho
uity Sme

ddentiicotin
Cnperimecrt Obxervation nggrente
A drrop sADyganic
GiVentomp2un
Compound a tatcd enotoU iHus ape
rmoi&t bue tmw may tontain -o
pape Crneno) oC0OH
Teacher's Signature
 Date 14/29/1
Expt. No.. Page No.34

( negven comypound Bromine Aotn Gniven COmpound

A021 taken in l a ond dd not decolnurite Satzcdd
Dromhe Bon a j ad ded
to

drikey shapcd
A a chrops , cecic Cee cotouzed Phenofi -OH
do
anananium nitade Aolh precipitate obiermved roup pree-
abouJmi_a he Aufince

ArnaJ quantity the No obAervotion -cooHroup

oompound oa8 added in Csent
Bm a Sodium Bicarbonode

2-3 dvopA o compaund e k green col0uziPhenolic grO

Oas oddd to 5mi a Complex K0a iPreeat
oic chloride AoIn ob&eryed

m ethe coound Jo Dreciptae Mde hyde ard

OaA added to DNP ketonic eolp
easentOnd O a absend
Ahoked SeIl

oReactions invotredin idenicadisnK SCnple G

O Ferpi Chlomide Te

t3HC
+ Fe Cl
grc en comple
(DarE
Teacher's Signature :
 DateM/09/
ot. No.. OB
Page No. 35

Cocek Pemonium iteate

fo-
esult

hesircn Osori_compouinds.oehoving fnctinnal 9coup

-CoOH -OH (henoic)

Tecacher's Signature
 Date 21/c6/
Page No. 36
Expt. No.09.

Cxperimerl No-0
him Stntklcatien functional u p k a o o giren
Ongonic Compoundk&ampleAand B

pecimet Obserevation nherene

tmyA Tet dop compound itmu pape ture May be -C0

0plared on blve litmus Papee Ped Oa-OH(ererotd

moi

Jntadvrcdin 11 m 4 the Broine Apth did Cien amud

Ginen corpound SOL frleen in Cllan0 decolouzike &Aatuznted
and bomine Aotn Oal addd to
it in dcopoie manne Gith
houleing
darition Tet e given Colousless Avnoke He covpod
compound oa hecded in evotved
aiptodic
KS0Hc hath

errsic CNcaide Jet A foo Aopecilia dark phe-olic

dreopl the comPound u0aadded colou ua.0bserved
hrml e nestrel feric
U chlonideol abiend
Teacher's Signature:
 Date. 2/2/12
Expt. No..09 Page No. .34

2,4 DUP Tet ml s the precipitate COies

eompound utal add to mi esa obscryed CorDons
290NE_reagerd and thecontents gup.abent
eee&haked noell

Ce heOniuam NateTt red cotoz -OH CAtcorotic)

Acdoekafcemic amnoniumormadisn 9 p absert
toteOOdaea to arout n
e Stonce

Cacbyiamune leuto amal No ObnozioukOY oup

omou compoun m efcontupleaad Sme gert
HC ) adde nd to i fc observed
benabot 2m e 1OTh ale. ko
00 adadea and u0aramed
Sodiun iCouborcde l e t Amol Briilk ChfrevCs.cence oOH g a g

quandiycoapaund @al addas s Obkerved i& pxesent in

in 5m e NatHcO,Aoln Hhecompourd
tsterTey Jo asmall guondity
aubtance Lm a ethano euity dnei e npeued
HaS
D 4-5drops of conc Obtained Contains-COO
as added ard mea oup

Teacher'sSignature
 Date21/02/1a
Expt. No. Page No..38
Ronction nolv@ in3Meoigicatorn o Sorpe A

Sadiv ibonode Jeit

CHCa + NoHs CHsCo2Na CO
Rcoc Acd) canbnd SBn&t
Lerteevtsccoe
24Te
CHCOO CHOH 04 CH,Cooc,He ti,0

3detification Sampe 6
peiment Qbeevation
itau TA drop e Compad No change -COoH
Oaplaced on mOu bue Iitmu obierved -OHLpneecli
oper abient

2Unsouaadion Ted 4ivnDpmine dino+ Calven

Bnpie S6compoucd c teken in decol.ouhe compmund i&
Ccla rd bromine kol na addei Saturte
D droPi mounne aSithos
haki

Sgtio 1at H gien.copoundCaloude dmoke he conpaet

9heated in avOate bafh exolveg

Toocher's Signature
 Date 24/c3/n
Expt. No. 9 Page No,3

AFecol Chiozid Teat fCnaNe 2ecu lio phenolic,-OH

deops aCompound ndo dak colOUY gouparsent
adsed in Snl , neuto obAerye
Kic Clonde doln

5 2,9 DNP Tat-m conpound Jo ePi ere Oi

0 Cddcd to mearl Oblerved
B
Cocpony
2.4 DNP reagen group.obz.eat
and he contert&oece
KhGked e

6 Cacby Aamine let- o admallNo -H Scoup

amount 9 compound Jm
unplea1en
Amel oasen
cont Me ons oith
kcOroPS CKlOTD{OTm
as add ed hen obout 2n
ef to. ule koH as mired
yngarmea

Sadum bitonbonate Tef- No hbherve ceve 0OM 5e0up

A Lmal qa fy o Copou Dser.ed ahlen
dded in5mla NaHta,

8Sodium Metol TetPhot 2rm/a aferevecene Sith -OHCaleoholie)

fthe aubiidnte a-faken ad
foit fhe evoution roup iPreaer
Aacdium oeal Sa added Hydeogeo gal:

Toacher's Signature
 Date 24/os/
Expt. No..09 Page No. 40

Ceei amnNum Nitrate Teti e d colOuTed &ol -OH 9-

A eno dps ececic Qnmonium LA9aL obRerved
iteden0as addc to abour
Imla_ COb
Aubitance

Reactionk invoivea in idediflcation mple B

LSodiumMetalTet
CaHeOH+VaCs) HeOVa t ,g)
Ethanol Sodium adium
Etounocde

Cerci Ammoniugn Nitrae Tet

CrigoH + CNHA), Ce[No) CCHOH), Ce (NO,u 12N
Cerric Red Colou
Cotourie) Ammonum TCte

Resu t Jhegiven Aample A condains COOH fnctional

Carbozylic Aad e r e a &unpe B cortalns OH
gcoupie
nchional roup le HlCohol

Teacher'sSignature:-
 Date e&/o/n
Expt. No.10 Page No. 4

Üxperiment No-10
Dar 3aendijicatiso fundtionad gamp.a to gicen
oganiccompoundL ample A B

Sdcndii.catiena4 Sample
2perimed Obiprvotijon
Litr Test Pdrop e compaund nau o change cu -Coort
placeenmoiAt blue litmus Pape Observed -Ot Cphen)

2 Lnicduzndibn let ml 6 se BrDmine colou Cixen

Compound 00 taton in CCl4 did not decoloidecompourd
bxomine dtec na adaed ta it AAaturede)
in deopsise manner hoith hakiy

4onition Test The sivencompound Colbuxteydenake Shecomeourd

o heoted in cngader bath evDlved. 2alphadhc

1Feri CNoideTea1 AECnodecps No pecultar dak Phenolic

complesSaiaaaca in 5 coloux 9 s0bieve 2rap obiert
neutralforcic chlonidedon
2,4DNP Tt Imlef _compound 10a No pet ene cbkert Oie
added nar 3nd 24 PNP reaged cbonlgbp
absert

Teacher's Signature:
 Date Q5/19/
Expt. No.10 Page No. 42

ond condeo e e shake aell

6 acblambeTe 0 a mal ama o unpleuar -gop

o i c LOmpaundLm conc8me evolve abserd
HColsg octh 5 desoChimnanm
s add Jhen.Qbout 10 alc
KOH 0 md ard carm

Sadium 6icarbonde Teul Azmal O efevescente COOH raup

OLardifg compouncal_Gdet OEseve obtent
in5m uHCO, Aoin
8Sodiu. Metc lestAbout 2ml ttesence -OHColcoholic
efthesutbstomce n9ol token V a Sith evofutian y gcoupi
metod 9eL) odda to A
Hydoen30 prelend
Ceeic mmor/um itrote es Red coloured AoinOH 3noup
dnopA al, cerric Ammonium Oa Obiereved Canfirme
i ta o cdaes to
about
a i c conpound

PeAetio icsoted inthe dotifiCectien mple

YSodivm Meta Tet
CHOH +Na cs)
thone)
CaHs ONa H

Teocher's Signature :
ON OF CAFFFIAI
Date.05/10/
Page No. 43
Expt. No. 1o

2Cecei Pmmonivm Vitrate

CCH,OH), (elNoja 2nt4 NOs

CHsOH 1 ( N ) Ce (NO) Red Colourtey
Cplourless Yel low

dedilcalien e Snpte 6
oe
Tnperimen
Obiervedisa.
in coloux ooH-O
LHA le Adro0 a4campoundNo change
9 Paper Cpherole) abao
BaPlaLCed on noiAd blue litmus
pape

G e n coppund
2-Crkeduncdion e t ogive Osomine colouy did
Compaurd wa teben in CCl4
y nad decolourike iA Aazeded
bzaaune hoeder K9al Qdd d to
it in
dropuside manner

giion Tethe giten tonpourd olorle

Amoke Nhe Compou
s9Os heatei in aroter bath
CYDlyed &atiphodic

4-Feic woise et Ato

deps ef coplex sai addcd imSm o pecutiarr dart |Phenolic grop
netrol Rurric Chloride 0 colou aSa Obiervezabse

5Ceic Ammoniun nitoe tet |No chanse obierva Atcoholle

Afenodops o cerric arnmonjun gco2 ebier
Vitrcde90s added fo abat Jmd
organic camyaound
Tecicher's Signature
 Date 05/10/1
Expt. No..1 Page No. 44

Canhyl aine et .oimoJL amoun1 o ckange PMcgholic

oLogan compaund, Lml ef HCLalang obierved gcup abJert
5 dops o chlon/fom addd Jen
abt I07o ale kOH

72.4 Ne Ted rn ef compaund Heilou coloured C=0i

Se ad ded tonearly Bm 2,4 Dre pet
eageat Cund The tondentz n e obseed
ere corbony
hobed
roup prese

8 ToLenS Reaser le o the toliergFomation 9 Plgenydic

eager aJpout 1Od-ops o orzanic Aller mror
ompoundoas ad4ed in the tet telon the al Paceaent
the teat tube0@ heoded in tet fube so.a
aSctec bah. Oserved

9Fehlirgs Son +et 2m 03anic Red ept seePrexence a

compourd 9a odded to Im obAerved aldehydicge
Fenliy'g ol y Oa 0amei or fe i8 ConiRd

ReaCtior mvoledm 1detificntion mple 5

TOIlens Reae TCi
R-H+2 Les (nHs),J+30H"R-0 S
23ro)t4Hst 2,0
NFehlingls 3oln Te

--+24 50H R--0 +uot3tfo

Tecacher's Signature
C r H r r c N E PRON

Date 95/19h+
Page No. 45
Expt. No.

Reult
Lomple H CorstaiaOH (alcohotic groLp)
h e given
Contcins HO :e aldehydic
Sheeas Sample 6

Oetd

Teacher's Signature
 Date 12-/10f9
Expt. No.. Page No.46

xperiment No-
Pimddentficatian fuctianal geoup tS iven
axgani COmpounds Aampte A 6

dertiiation 2 Soepie A
tperinent Ckercdion

1Litmu TedA.deop e compound No charge Obed CoOH,

a placed o makt blue limus -DH
Paper not be Paeerd

2-Untatocdien eH Im 6 ven Eramine coloUx he copain

Lompaurd 9 a l taken in Ccla y
Cig not decofouxieiActurcded
Dxomine rOate OC) added it inn
rropuSise monner

atibn Tet Jhe given Compound Colouie Amoke

Hlegeuer
Sa hected in ausater bath evoled compovnt i4
aliphatic

Fereic Novide TetA fono drop Vo peculiar dak Phenali

the or3anic Compond 0a2 colouy 9@ obierved gcoup
added in Sm e utral e Cla 8ol ablent

Teacher's Signature:
 Date. 12/1e/1
Expt. No..4 PageNo...43

5 Cereeic ironium itrate Teat No change Atcahalic3rap

P o dnops. ofCornic ammoniu observed abset
nihode a.added toaboud
Im6craecompound
6Caby amdneet lo aAmall 9JOunpteasaunt dmell H 9oup
amount 00goriccompandJmevolved abAet
e conc HO alOns ith 5 deeops
ehchloxofoxmna1adde then
about 10T. g.ac KO K0a mines
and r m e d

2.4 DnuP Tet Lm ek compourdellor colnured

CHO0
s oddea to Bmd e 2,4 Drveppt ere obieeven CO-aroue
reRgerd Ong The conterds ere may beprejeat
ak.ed e j l

TollekTe4-Tothe Tollen No chage a

Adehydic
reasent about 1O droPs o obsenved 9op abtet
Orenic Compound nGu.adaca
Onathe tet tube hias heated
D 0der both

odofom Te4 Ho one m Yeloko ppt oere Gticen arganic

OnsoricCompoun in_atesttube obserxed after the Compaund ha
2 m of TNa so1 n204 daea To bol coolea don ketonic Co-)
the miatu NaOHA Sa unctiona
ogded in dropsize manner til 9cp
f 1pned pale yello aftervst Ch
t 9 o d , O a r mes

Teacher's Signature :
 TEALEAVES
Date12/10/1
Page No..48
Expt. No.
omple h
Reactio involved inidehicatiorn

odogoxm leat

RcoCHs + 3Na0H RcoCls 3 vaoH

RCOCla NaDH RCOONa CH1

ddenticatin
ObAetien
periment

Litru TetAdeop conpound sa Litmuk pape

etacea h moiked ed litrmus Pape tumed blue mag b
prelent

2Unsodcdion et m ) of the GirenBomne

colou Calxen
Com@ound 0 4 faken in CCla cundaa nat decoouxikecompand
bnmineAo a adned toit in
dropsike monner h9ith_ ating

nitian TeAt The zire Compound Colouke Amote Orzari

heateg in O0ater bath PVDlvedE compou
0a
isoliphad
Fereic ChiprrideTe Afe drops o o peculiar dasPnenalie
garlc compound9as aded in Bm
netral FeClg AoIn CoDun 0au oDAeedgup atlat

Toacher's Signature
 Date.19/19/
Expt. No..1.
Page No. 49

6 Coreic_Hmmonkin Nitrade Tent D Change

AfaO.dr0Ps ef.ceetc ammoniu PHcahcliccaup
ihecte BaL.odi.e Hoimi 9
Obierved Oaset
Cgaiccompaund

6 Sodivm Gicarbonade Teat A No efevescente

Snaullquontry 6 compaund
-Cootrovp
Obierre obsent
sOa.odaedin Sm ef NaHCOs
Soln

12.4 DNP Tet mi a lo pet obAerved Careony 9cop

compound nDal.added lo obsemt-CHO,-
m 12,4 De-caget
Cordects 4haked OeI

Carbylamlpe Te o9 8malVery Obnoniou

amounteOCms CorHCtAmell Og-amidePreient
along i thSdeop a ChlozogoamibobAeved
s0s odd od al kOH mined
en 1o
anda net

RERctieinvolved irn idotgicalien saple

R-WH, CHO 3KoH (olc.) NC+3kCLt 320
fmire Chlorofom Loryanide
Reu he gien Jample contain-Co-(keta) fincianal
gou shere a anple 1B (ontaind-H Auatianad o p

jeomuno 0up

Teacher's Signature:
 Date 2/1/
Expt. No..12
Page No..5D.

Pim
txperimamBNo2
Sdenti gicati
sfunctional gcoue tojieen
oxganic.compounis Sampe Aand 6.
daenticaisn Sanpe
peniment Obievation
Litmu Tet dmp ompound
Oa placeo onmot blue Litmuk pae
Change in coloun-CoOH-OH
phenalicgeoupabest
2Unsahuration e Lnls the jven Bromine colour did not tiue ompoir
compaund ataken in CCl4 od decolouzise Baturate
bxomineLo HO) Qdded to it in
dropAaike maher ithhaking.

Bgaitin letThe given tompaund Coloules Amoke eroly edOrgani

ugQl heated inauSater bath campoundi
Clprotic
4 leeric Chlonde Te A 4nO drops o peculiarr da-k Phenolic
ganig_compoundn 5m of colasa) obienved aaup able
nefra Felts hol

erri Pranmriun Nitrete TetA NO Charse obsenxeAlconalic

p dops Cerei uAmonium raup abse
Ninate b94 added to akoutJ
Tgeril compourd
Teacher's Signature:
 Date 2/1/
Page No.5
Expt. No.

NO e4fervescente COOH02p
6Sodiu Sicab>node Tet: A Amall
added Obuerved okokent
aanti omund koa
in5m 5.NatHcOs Aon

724 ONP Te mlg Compaund Nopphpblera Carbon

grap eCHO,)
a t added ta 3ml 2.4 DNe
abset
ere
neaent and The.onterntA
Ahated e11

To 04mal Very obncotious NH,Aminal

3ablanineTeit
3me 9 doryanido gnaup.is
nount DIgarit compound Jal
Observed Preent
CancHC aons uSih 5dra
ef_Chlonkaun h0as adde hen
alc KoH
toit about LO, {
aixed and arm ed

ction involved in ldentihicatian A nple H

+ CMCI3 3koH R-NC 3ECR t 3H,0

R-NH, Catc)
Armine Chioxofaxm JAocyanide

dentificatien omple 5
Sre nperiment ObAervadien ngenenre
blue calaux Change4Coof or -0H
1Litm Te Adrop the ompourd
toed
K0 plarea en mokt litmuk Paper phenolic)may-
be prelent

Teacher's Signature
 Date 92/11/7
Expt. No...2
Page No. 52.
2 Unsotadion Test mi
the Broe colox
Qu conmpound AS faken in
Ccla
Unsaturodion
did not detolounteeat preseat in The
byomine30 R.addez to.itin
dipike manne hth akint Cormpond

3 donitin leu he ghen Comraund lack Amote

OQ hent ed ina2ater bath. Gtirsn conpoucd
evol ed
i arramatlc
4 Sodium Bicarbonate Te A Smar No eferveicance=C0OHH oup
guanti9 Compoyncd Q Qdded in
Sm aHcossoln
obievet absect

5 2,4 PNP leat One m af Compau Noppt 2ene Carriaonyl arop

NOQAQdded to 3 of 2, 4 DNe Ob&ervea absent
reaset and Condet& ere haked
nelf

D (epri Prmmonium NHtr ate leH

E ACKO Grap a cereic Pmmonium
Cuceenpxtcipitcdephenolic grop
obkerve Pxexet
Nrate Oa added to abourt I
Oanic ComPDu

Cabyl amine 1e3 To g Amel NO obserxatisn

amOunt 9{ 0rgani Compaud Im absent
Lonc HCL along STh 5drapi
Chloplpsm 9a added Then toi
about 10 o cde koH wwa
mixed d Ahaked we

Teacher's Signaturo:
 Date //12
Expt. NO. --- - Page No. 53...

3 Ferrc Chlon'de Tet: Dark gc een Colouxed OF Coherdid)

A 4cn doPA af organic compound rpt C r e obAerved 9upidpreie
HG2 added i n 5 m G neutral Fecric
Chloide saln

Reactien ivolved in idenfiicotlon ( Sanpe

H-

+Fet
(O +3 HCl

DarK3een
Compiex

(Nr), CeCNo CeCNoa fo 2NHNO,

RouThe guen Japte AcandtainaN Lamnaap uSherea

HheAample B_cortaunsO (phenolid 9roup

Teacher's Signature
 Date 29/ 1/1
Expt. No..3 Page No.54

Cxpertment No.-13
Bim jo prepare o Sample B-napthol ani line dye
heoy tnilinereactk sath nitrous acidCNaNO+ COnc HO)
lat 23-216Ho fom
benzenediazooiuchlonde Ihe cesultir
benzene diazoniurnchlange Couple 2ith P-napthal ir altaline
medium10 fomred precittpcde phenyl- azoD=naphol LS napthol
Gniline dye

NaNo t H 273E-278E
Cconc) ONC1 aci2 H
Ariline Genzene
drazonom
Chlonde

213-278E ON=N-
Genzene +HO
diazonru
Chlonde
Snaphiho B-nont
online dye

Dpeoraik Requned 0250mi beaker

100m beaker
Meauiog cyliner
Eunne
heomete

Teacher's Signature :
 Date..09//17
Expt. No.. -- PageNo.55

Choial Kegixed Pniline CA 5m)

( NaNos (4gen)
-raphthalIgn)
) Con HC C1Om)
10/ NaoH saln (50ml

PDcedye

dn 250.m beaker 45 m Oniline and 1Om conc HCL 6 . o

0 aAmAEa0gether andplacedin ice bath.

dn 100 m beaker 4gm Na NO 0a dissolved in 20m s/ Ho

olacedin ice bath

NO)cooled NaND Aan O01 Cdded Blaty in dropusibe manner in

the 250 md beakerContcunirgariline cnd HCI Aain and then again
placed in ice bath

50m 10T, NaOH Aoln i token i n a becker and 1gm B-naphtho

i added toit

neppt a s n o diredb P r e s i n g t behoeen the fitterpapen.

ecation I N D E

iazotise cniline at O-5:

Adition f NaND80/ Jhould be done Alously

Teacher's Signature