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  • Scan 22 Jan 2023

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    Tukaram P S
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    1. This document summarizes salt analysis tests performed on an unknown salt sample. Physical properties of the salt such as color and solubility are recorded. 2. A series of acid and base tests were used to identify the cation and anion groups present in the salt. Observations such as gas evolution, precipitate color, and solubility are noted. 3. Confirmation tests using reagents like Nessler's reagent, potassium chromate, and sodium hydroxide further indicate the presence of ions like ammonium, lead, aluminum, zinc, and manganese. 4. Additional tests using ammonium oxalate and calcium sulfate suggest the salt contains calcium and sulfate ions. The document provides

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    1. This document summarizes salt analysis tests performed on an unknown salt sample. Physical properties of the salt such as color and solubility are recorded. 2. A series of acid and base tests were used to identify the cation and anion groups present in the salt. Observations such as gas evolution, precipitate color, and solubility are noted. 3. Confirmation tests using reagents like Nessler's reagent, potassium chromate, and sodium hydroxide further indicate the presence of ions like ammonium, lead, aluminum, zinc, and manganese. 4. Additional tests using ammonium oxalate and calcium sulfate suggest the salt contains calcium and sulfate ions. The document provides

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    © All Rights Reserved
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    10 views4 pages

    Scan 22 Jan 2023

    Uploaded by

    Tukaram P S
    1. This document summarizes salt analysis tests performed on an unknown salt sample. Physical properties of the salt such as color and solubility are recorded. 2. A series of acid and base tests were used to identify the cation and anion groups present in the salt. Observations such as gas evolution, precipitate color, and solubility are noted. 3. Confirmation tests using reagents like Nessler's reagent, potassium chromate, and sodium hydroxide further indicate the presence of ions like ammonium, lead, aluminum, zinc, and manganese. 4. Additional tests using ammonium oxalate and calcium sulfate suggest the salt contains calcium and sulfate ions. The document provides

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    © All Rights Reserved
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    of 4

    Camlin Page

    Date

    Satt Analyi
    Pheical appearence

    ColouY
    Physical state - Qmorphous/crystaine
    Solubility-CodHh
    hot H20o
    dl Hci

    Acid Radical

    Test Obs nteretence


    noup Coz may be present
    Sat+d HCt Brisk eterence

    *aroup2
    Solt + Conc HSO4 Whte tumes Cmaybe presenc
    Browntumes Br_moybe Present
    NOg maybe presert
    +CuA

    nroup3 Sa moaye present


    SatBaclh He ppt
    Contomatian Test

    Lime wate + qas Mlky COpresert


    COz +(CalcH)) CaCO3+ HO

    Sot+AgNogtil HNo ite ppt CI present


    Xcl+ Ag NOg AaCl2 + XNO3
    Comlin P3

    Salt + AqNO3 ale yello ppt


    xcl AgNO3 Br preset
    AgClh +XAo
    NOg
    TT1-Saturatedsat sol Broun YIq,
    TT2- fesO, Sol Centre of e NO3 present
    T:13-(1 + test tobe
    ZmI 2m

    4drops ot Conc Ho
    NOTE Prepare 1 testhbe o saks

    Basie Rodical

    Obs
    nroup O
    ntererencE
    Salt+ NaOH Pungent smellammciaNH aybe pesei

    aroup 1
    O.S+dil HCt Black ppt PE maype preset
    Carop2
    O.S+ HCl +HaS Black ppt PS maybe prest

    arop3
    O.S+ NH4Cl+ NH, OH White qelatinous Al present
    excess
    PPt
    nroup
    2 maybe presei
    OS+NHclHNH,OH WAte ppt
    +HaS M moybe prent
    Kk ppt
    Camiin Fage
    Oate

    saroupb
    O.StNHC+ NH,OH ite pt B&/c/Sa
    maybe present
    Cnroup 66
    arp 3t ammonium or White ppt M 2 moybe prese
    phosphate

    Lontirmation lest
    eNH
    Saltt Nesslers reagent Ornge-brawn ppt NH present

    Pb
    OSt pottassiym Yellouw pp P present
    chromade(kCra

    AL
    O.S+NaOH Sal hite ppt which A3 present
    cop s e dissolves when NaOH
    is odded
    Zn
    O.S+NaOH sol tte ppt,dssolves 2present
    uhen NaCHis added
    drop wise
    kMn
    O.S+NaOH 3ol Jhite p, toms braun M prcsent
    lon addung excess Naowl
    dop wse

    roup5
    Decantation ot he Soluton ppt needad
    Add hot facelic acid
    Dideinto thvee to identtfy
    Camlin
    Date
    Page

    Ba2 Yelw ppt


    TT1+K (ro,
    prese
    tlame test B
    NOTE:Apple qreen appears tor
    -

    tor Home test- Ca


    Brick ved oppears
    test-Sy
    Cimson red oppears tor lame

    Ca
    T.T2+ammonim JRte ppt Ca preset
    Oxalote(NH,CH Coor

    S 2*
    TT3+Calcium Jtte ppt S2+ presert

    suphate CaSO

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