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Expt. No.:.
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SALT ANALYSIS
Analyis Salt- 01
|AlM: lo dutuamine the_RuoAOnce al_otidand baaic uadivalk
n ven_sat sampla

Physion Exanination
Coloux- Colounlos
Nakuu-staluine
Deluausence Not deliauisant (Aksence_of C, NOg.CHa(0
Ddoun Haing _punguat smell and Ammoncal cmell
LfxARNLA NH)
Soluhiluty Solublein wadtx
Donaity uss denae
IDENIIFIATION OF ACID RADICAL
xpoxAimoMt OhaosvatOn Inteunce
ke a euw grams OE Redduah Broum vapouw Br may_be
SalLt.& haatik guntly a l obtauined preAmt
then Chong
2.Take a ww qnamsdf No chasacteistHc Absonce of (03
Salk_amdLadd chamg s0, S, NO
ew ml dul H2S0y

3 Tako a kw grams Radduah brAUn vapou B may be

ofsalt and jew |utn pungnnt_smelupreasut
PreARMt

m oLonc H2SO4
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Confirmatoy eat
ExpaAimMt Obgeavahiom InkeLm
Take a u mi of A ight yellow pptobtained Preaona
aq Soln:Salt add whidh upaakialy d
k ml of AqND3Saluble in NHOH umkirmud.
Sol.

2. Hoat a small quuntity Evolukien of yellouish

of salt wh solid brouum vapoLn of brormine Preaanc
nrmid
Br
MnO2 amd HaSouwuhith tuma staach _p1pAs
pllow
IOENTIFICATION OF ASLC RADICAL
xpoumeut Obievaion Injuuco2
Coloun of saltL olouxlis Abconca of Fe2*,
noted FeNi2 Mnon
2.Smel of salt vv Hawing_ungmt NH ion may be
nAtid Sml preAmt.

3 Flame eat
Take a uW oAams No chaaacttxisHc Absenca Of Cu
of salt and make thona ba2tS
paatawth_uonc._
HC and indroduce
tinto nM-
luminous pata
Hame

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Confiumatoty teat
LXpeAmemt Ohusvabienn Innce
Tuke a u grams fColoueleu gao uuth PreaenC a NH
Salt add Na0 Rungunt moll i ien
Sbtained
.Take a kw mlof Broum ppt o Preunu dNH
Saud saln andadd Obtainud gn u_tonrmd

reng&nt.

RESULT:
Tho given salt centuina 8a00 acid Aadical and
N a baaic Aadital

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SALT ANALYSIS
Analyuin Salt-0202
Aim To
To Cyutamahcally analye the given salt amd
i d u ithe anusn and the CaHon_prenemtin

Phyaital _ExaminakHom
Loloua ptouwleas
AppAnAance (ustalline
Smell-Vineg smell
IAMom Analusis
EXRmemt 0bsextah IneinA
TD theSalt added_No
No_tharatkexisHiC_
Dil HCou reathiom Qnigna are absout
2. o the_Salt_addedReddish broun PreARMMe
Ln.H2SOu_ VapOL exolves nikadu aN03).
Con-firmatouy teut
o salt addod Roddipn bxown PHOAAMMO
Conc Ha SOy t u npOLN Abtained ND Lonkmed
tunima
d.Tosalt added conc fnuty odoun of
HaSOy and heat hen add DAAdukcdid N03 i wnimad
ethyl adcohol k_pouz
to 250ml H20 beaku

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LCakion Aulysi
ExpOhimet
Heak apinch_of salt | No ObAunvatie
charocleristic roation| NHyi v dbsut
wHh Con NaOH

2 0 he Salt sotn hde precipitat.

laddad dil HU Obtained
Ph [goupli
hAmt
Con&irnnars tat
To Salk soln_added Yellouw ppt iu obtained PreunO_ _Pb2+
KISolukien 10n LonOUned
.loSalt 6oln. added Yellou ppt_is dbtained Preaenca Ph2t
Ka u0y Soln Lon_w Lonrmad|

RESOLT: The givn salt y laad nitrath

Cnho Ph2+
Anion NOg

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SALL ANALYSIS -03

AIm: To Systematically vanalyHe the qiwen salt saln- ond
identiht the anin md cabom presemt in ik
Physiua, Exammunahiom
Calsus lalsunlokA
AppeaxamL- (uyatalluine
Smoll No khaaLkenetic Amll
ANION ANA LYSIS
Cxpunmont bLAAvati@n
:To the salt_add dil. No chaxacouiakic Absence(t CO3
H2S0y_ Machon NO ,S So3
2.To the salt add Nothaxackenistic Absene of HaL00,
Cnc H2SO4_ Aoacion r,bx1, No
8 To salt.salo. add lhite ppt. shtainnd PLAeno A
Ball Saln 2
SO4-
Confir mateu leat
expLAimaut ObAtAvakiom Inhun
ToTothe obove ppt pt_in insoluble Proaumca 0t SO
add dil HU mHrmid
2. To tho Salk Soln uwhib gpt abtainel ProAdMa d SOu
nirrmud
Sh.
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CATION ANALYSIS
xpaAimeamt Obaeavaho6m
:Heat a pndh ot salt NO Chaaclckisho nenima
with conc NaOn reathom 8-bsAved
Absmue of NM
To the salt saun
add No Chaaackeu stH qoup
dil M Absene o GPL_
o the above saln reatkiom obsaved Caiona.
No characesishic
add dil Hu H2S reachon 6bseredL Abtena o u
4To the above Soln.hit
add soud NMyU | ppt gelatinA AL3t Lgaop
Land NHuOH sala. Amud _podsmt
Confirmators seat ->
ExpumaMt_ ObAeavadom_
To the ppt _o discalved Blue lake ia Preasmco AL3+
exces blue litmuaA AmAd o mrÝned
Soln and NAy0M

RESULT
The qiven salt_u
aaluminium suphat LAlzsou)
it h Cai0n>_AS* and Anum So2

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SALT ANA LYSIS -04

AIm:To teat the preaunce
the qiven balt. oacid amd bai hadital in

Phuyaical Examinakion
Ndture
ColDulesu
Coloux Custalline
Deliquesence: poliquo scant
Odo Odounlask
Solubility in wate: Sotuble in _uakti.
TDENTIFICATION OF AUD RADICAL
expeLUMeAut 0bsewakOm
ake a kew qnam ofreeniah Yellow em mayhe
salt andhuat it 04obtained
nty andl then
Shongy
Take a wum gHamsl No chaaacknishic Absence d D
aSalt md addChange So 2, NO
H250y
3 Take a w gramsnAe uhito ume hesenco o
salt_amdl add AsR_ablained 16m_
w ml Cent
H2S0q
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LConfirmatouy taak
JTakea ew ml ot aq. Whib ppt i
Soln. add jeuw ml btauined ProAerceo
AgNOa sdln. Tom congrmed
2 Tothe_above saln
add MnO2 Greenuah yellow Prosumne U
ga 0bBained 1enOmHmLd.

IDENTIFICATION OF BASIC RADICAL

XpOimeMt 0basavati0m
Take Small_amount of- No chaaceisHic Intunc
Salt and add Na0HL Absence a NHu
2 To above soln. add_dil Nochang
whit ppt_is
HCE 0btained
Absence I" ?P_
3. To above saln._pass No uhih Catien
paku Absente a T gp
H2SgaAL obtaingd
4 Boil Äs and add No wit ppt Cabisn
NiHyOM ad NAyU.0btaunud Absence o ugp
5 Pass _2S gas to the |Dirty uuhite ppt Cahm
Prosencoaf
above s.alh. odained Oup Cutim
CONFIRMATORY TEST-
Cxpnimont 0bauryahion
Oissolve the ppt in ppt olissolves Proaur
dil HCI and divido
it inh_2 pauta: Lmr u d

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o) To 1stpant add
Na 0H abtainedL
bTo 2n_past add Bush whu
KA lFe CcND6 Pp ia obained

RESULT:
The given _salt sampl Cmtains aaAcd hadcal
he
Qnd zn 2t aA bauic hadital

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