Si NP3 N

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

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Sample: SiNP3N | Sample:
Operator: NHA | Operator:
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.S | File:
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ Measured | Sample Mass:
Cold Free Spa32.3094 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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Summary Report | Isotherm Tabular Report
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| Relative Press
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Surface Area | 0.010688695
| 0.107216454
Single point s 225.4762 m²/g | 0.212697862
| 0.296486624
BET Surface A228.8553 m²/g | 0.406271523
| 0.498046433
t-Plot Micropo 3.9161 m²/g | 0.60548947
| 0.707751304
t-Plot External 224.9392 m²/g | 0.794603769
| 0.903093679
BJH Adsorption | 0.988631078
between 1.700188.624 m²/g | 0.903887458
| 0.800605533
BJH Desorption | 0.704112083
between 1.700228.9683 m²/g | 0.60912845
| 0.497704355
D-H Adsorption | 0.393449844
between 1.700205.174 m²/g | 0.301794755
| 0.204932323
D-H Desorption | 0.110237132
between 1.700231.4631 m²/g | 0.010112774
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Pore Volume |
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Single point ad |
less than 170. 0.359144 cm³/g |
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t-Plot micropo 0.001658 cm³/g |
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BJH Adsorption |
between 1.7000.325442 cm³/g |
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BJH Desorption |
between 1.7000.338185 cm³/g |
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Pore Size |
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Adsorption ave6.27722 nm |
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BJH Adsorption
6.9014 nm |
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BJH Desorption
5.9080 nm |
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D-H Adsorption6.4883 nm |
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D-H Desorption5.8895 nm |
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Freundlich |
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Qm·C: 23.2534 ± 0.6803 cm³/g STP |
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m: 4.8495 ± 0.3566 |
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Temkin |
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q·alpha/Qm: 0.052782 ± 0.009169 kJ/mol·(cm³/g STP) |
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A: 1.9040 ± 1.5786 mmHg |
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DFT Pore Size |
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Volume in Por < 1.483 nm : 0.02098 cm³/ |
Total Volume i<= 108.566 nm : 0.27061 cm³/ |
Area in Pores > 108.566 nm : 24.613 m²/g |
Total Area in >= 1.483 nm : 108.036 m²/g |
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DFT Surface Energy |
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Total Area : 426.143 m²/g |
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Nanoparticle Size: |
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Average Partic26.2174 nm |
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Horvath-Kawazoe |
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Maximum pore0.359144 cm³/g |
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Median pore wi7.7153 nm |
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MP-Method |
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Cumulative sur |
0.74525 nm and
129.6198 m²/g |
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Cumulative po |
0.74525 nm and
0.164100 cm³/g |
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Average pore h1.26601 nm |
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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SiNP3N | Sample: SiNP3N
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.S | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2927 g Warm Free Sp11.1935 cm³ Measured | Sample Mass:0.2927 g
32.3094 cm³ Equilibration In5 s | Cold Free Spa32.3094 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
No | Automatic DegNo
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otherm Tabular Report | Isotherm Linear Plot
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Absolute Pres Quantity AdsoElapsed Time S( aturation Pr |
760 | SiNP3N - Adsorption
8.123408318 36.28838566 00:42 | Relative PressQuantity Adso
81.4845047 55.36015678 00:48 | 0.010688695 36.28838566
161.6503754 65.80209914 00:52 | 0.107216454 55.36015678
225.329834 73.62407577 00:56 | 0.212697862 65.80209914
308.7663574 84.91082142 01:03 | 0.296486624 73.62407577
378.5152893 96.08583999 01:08 | 0.406271523 84.91082142
460.1719971 112.2580179 01:17 | 0.498046433 96.08583999
537.8909912 131.2188895 01:28 | 0.60548947 112.2580179
603.8988647 147.7759088 01:35 | 0.707751304 131.2188895
686.3511963 181.8617453 01:54 | 0.794603769 147.7759088
751.3596191 232.1851007 02:04 | 0.903093679 181.8617453
686.9544678 218.8045172 02:16 | 0.988631078 232.1851007
608.4602051 154.4717006 02:41 |
535.1251831 144.4491984 02:47 |
462.9376221 134.0329187 02:55 |
378.2553101 109.1028187 03:07 |
299.0218811 83.63742768 03:15 |
229.3640137 74.17961728 03:21 |
155.7485657 65.10257434 03:27 |
83.78022003 55.69995757 03:36 |
7.685708523 35.74986524 04:02 |
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Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
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| Sample: SiNP3N
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.1935 cm³ M| Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ M
Equilibration In5 s | Cold Free Spa32.3094 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
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| Isotherm Log Plot
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SiNP3N - Desorption | SiNP3N - Adsorption SiNP3N - Desorption
Relative PressQuantity Adso| Relative PressQuantity AdsoRelative PressQuantity Adso
0.988631078 232.1851007 | 0.010688695 36.28838566 0.988631078 232.1851007
0.903887458 218.8045172 | 0.107216454 55.36015678 0.903887458 218.8045172
0.800605533 154.4717006 | 0.212697862 65.80209914 0.800605533 154.4717006
0.704112083 144.4491984 | 0.296486624 73.62407577 0.704112083 144.4491984
0.60912845 134.0329187 | 0.406271523 84.91082142 0.60912845 134.0329187
0.497704355 109.1028187 | 0.498046433 96.08583999 0.497704355 109.1028187
0.393449844 83.63742768 | 0.60548947 112.2580179 0.393449844 83.63742768
0.301794755 74.17961728 | 0.707751304 131.2188895 0.301794755 74.17961728
0.204932323 65.10257434 | 0.794603769 147.7759088 0.204932323 65.10257434
0.110237132 55.69995757 | 0.903093679 181.8617453 0.110237132 55.69995757
0.010112774 35.74986524 | 0.988631078 232.1851007 0.010112774 35.74986524
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| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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| Sample: SiNP3N | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
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| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ M| Sample Mass:
| Cold Free Spa32.3094 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
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| Isotherm Linear Absolute Plot | Isotherm Log Absolute Plot
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| SiNP3N - Adsorption SiNP3N - Desorption | SiNP3N - Adsorption
| Absolute Pres Quantity AdsoAbsolute Pres Quantity Adso| Absolute Pres
| 8.123408318 36.28838566 751.3596191 232.1851007 | 8.123408318
| 81.4845047 55.36015678 686.9544678 218.8045172 | 81.4845047
| 161.6503754 65.80209914 608.4602051 154.4717006 | 161.6503754
| 225.329834 73.62407577 535.1251831 144.4491984 | 225.329834
| 308.7663574 84.91082142 462.9376221 134.0329187 | 308.7663574
| 378.5152893 96.08583999 378.2553101 109.1028187 | 378.5152893
| 460.1719971 112.2580179 299.0218811 83.63742768 | 460.1719971
| 537.8909912 131.2188895 229.3640137 74.17961728 | 537.8909912
| 603.8988647 147.7759088 155.7485657 65.10257434 | 603.8988647
| 686.3511963 181.8617453 83.78022003 55.69995757 | 686.3511963
| 751.3596191 232.1851007 7.685708523 35.74986524 | 751.3596191
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
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NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2927 g Warm Free Sp11.1935 cm³ M| Sample Mass:0.2927 g Warm Free Sp
32.3094 cm³ Equilibration In5 s | Cold Free Spa32.3094 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
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otherm Log Absolute Plot | Isotherm Pressure Composition
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NP3N - Adsorption SiNP3N - Desorption | SiNP3N - Adsorption SiNP3N - Desorption
Quantity AdsoAbsolute Pres Quantity Adso| Weight % N2 Absolute Pres Weight % N2
36.28838566 751.3596191 232.1851007 | 0.323799623 8.123408318 2.071777147
55.36015678 686.9544678 218.8045172 | 0.493976174 81.4845047 1.952382806
65.80209914 608.4602051 154.4717006 | 0.587149153 161.6503754 1.378343995
73.62407577 535.1251831 144.4491984 | 0.656944296 225.329834 1.28891366
84.91082142 462.9376221 134.0329187 | 0.757655417 308.7663574 1.195969668
96.08583999 378.2553101 109.1028187 | 0.857369602 378.5152893 0.973519514
112.2580179 299.0218811 83.63742768 | 1.001673214 460.1719971 0.746292982
131.2188895 229.3640137 74.17961728 | 1.170860213 537.8909912 0.661901368
147.7759088 155.7485657 65.10257434 | 1.318597747 603.8988647 0.580907325
181.8617453 83.78022003 55.69995757 | 1.622744123 686.3511963 0.497008201
232.1851007 7.685708523 35.74986524 | 2.071777147 751.3596191 0.31899443
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Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
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| Sample: SiNP3N |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
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N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.1935 cm³ M| Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ M|
5s | Cold Free Spa32.3094 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
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| BET Surface Area Report |
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| BET Surface A228.8553 ± 1.7871 m²/g |
NP3N - Desorption | Slope: 0.018912 ± 0.000146 g/cm³ STP |
Absolute Pres | Y-Intercept: 0.000109 ± 0.000028 g/cm³ STP |
751.3596191 | C: 174.064792 |
686.9544678 | Qm: 52.5718 cm³/g STP |
608.4602051 | Correlation Coe
0.9999405 |
535.1251831 | Molecular Cros0.1620 nm² |
462.9376221 | |
378.2553101 | |
299.0218811 | |
229.3640137 | |
155.7485657 | Relative PressQuantity Adso1/[Q(Po/P - 1)] |
83.78022003 | 0.010688695 36.28838566 0.000297731 |
7.685708523 | 0.107216454 55.36015678 0.002169292 |
| 0.212697862 65.80209914 0.00410565 |
| 0.296486624 73.62407577 0.005724175 |
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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Sample: SiNP3N | Sample: SiNP3N
Operator: NHA | Operator: NHA
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ M| Sample Mass:0.2927 g
Cold Free Spa32.3094 cm³ Equilibration In5 s | Cold Free Spa32.3094 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
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BET Surface Area Plot | BET Isotherm Plot
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SiNP3N Not Fitted | SiNP3N
Relative Press1/[Q(Po/P - 1)]Relative Press1/[Q(Po/P - 1)]| Relative PressQuantity Adso
0.010688695 0.000297731 | 0.010688695 36.28838566
0.107216454 0.002169292 | 0.107216454 55.36015678
0.212697862 0.00410565 | 0.212697862 65.80209914
0.296486624 0.005724175 | 0.296486624 73.62407577
| 0.406271523 84.91082142
| 0.498046433 96.08583999
| 0.60548947 112.2580179
| 0.707751304 131.2188895
| 0.794603769 147.7759088
| 0.903093679 181.8617453
| 0.988631078 232.1851007
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| Sample: SiNP3N
| Operator: NHA
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| Automatic DegNo
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| Langmuir Reports
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| Primary Data
SiNP3N - BET Equation |
Relative PressQuantity Adso|
0.010688695 34.69246861 |
0.107216454 56.19687705 |
0.212697862 65.38417067 |
0.296486624 73.72247582 |
0.406271523 87.80791093 |
0.498046433 104.1313881 |
0.60548947 132.7612495 |
0.707751304 179.4613465 |
0.794603769 255.5733791 |
0.903093679 542.1666385 |
0.988631078 4623.858711 |
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| Freundlich Tabular Report | Freundlich Plot
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| Qm·C: 23.2534 ± 0.6803 cm³/g STP |
| m: 4.8495 ± 0.3566 | SiNP3N
| Correlation Coe
0.994637 | log(P)
| | 0.909738283
| | 1.91107503
| | 2.208576717
| | 2.352818697
| Absolute Pres Quantity Adsolog(P) log(Q) |
| 8.123408318 36.28838566 0.909738283 1.559767648 |
| 81.4845047 55.36015678 1.91107503 1.743197311 |
| 161.6503754 65.80209914 2.208576717 1.818239748 |
| 225.329834 73.62407577 2.352818697 1.867019856 |
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NHA | Operator: NHA
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reundlich Plot | Temkin Tabular Report
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| q·alpha/Qm: 0.052782 ± 0.009169 kJ/mol·(cm³/g STP)
| A: 1.9040 ± 1.5786 1/mmHg
log(Q) | Correlation Coe
0.957593
1.559767648 |
1.743197311 |
1.818239748 |
1.867019856 |
| Absolute Pres Quantity Adsoln(P)
| 8.123408318 36.28838566 2.09474981
| 81.4845047 55.36015678 4.400412876
| 161.6503754 65.80209914 5.085435826
| 225.329834 73.62407577 5.417565258
| 308.7663574 84.91082142 5.732584866
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| Sample: SiNP3N |
| Operator: NHA |
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| Automatic DegNo |
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| Temkin Plot |
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9169 kJ/mol·(cm³/g STP) | |
| SiNP3N |
| ln(P) Quantity Adsorbed (cm³/g STP) |
| 2.09474981 36.28838566 |
| 4.400412876 55.36015678 |
| 5.085435826 65.80209914 |
| 5.417565258 73.62407577 |
| 5.732584866 84.91082142 |
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t-Plot Report | t-Plot
| Harkins and Jura
Micropore Vol 0.001658 cm³/g |
Micropore Area3.9161 m²/g | SiNP3N
External Surfa224.9392 m²/g | Thickness (nmQuantity Adso
Slope: 145.422288 ± 0.089368 cm³/g·nm STP | 0.373334867 55.36015678
Y-Intercept: 1.071725 ± 0.039511 cm³/g STP | 0.445075473 65.80209914
Correlation Coe 1.000000 | 0.498933508 73.62407577
Surface Area C1.000 |
Density Conver0.0015468 |
Total Surface 228.8553 m²/g |
Thickness Ran0.35000 nm to 0.50000 nm |
Thickness Equa Harkins and Jura |
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Thickness Curve |
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t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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t-Plot Report - Data |
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Relative PressStatistical Thi Quantity AdsoFitted |
0.010688695 0.26414568 36.28838566 |
0.107216454 0.373334867 55.36015678 * |
0.212697862 0.445075473 65.80209914 * |
0.296486624 0.498933508 73.62407577 * |
0.406271523 0.573615127 84.91082142 |
0.498046433 0.644566671 96.08583999 |
0.60548947 0.745247381 112.2580179 |
0.707751304 0.8716842 131.2188895 |
0.794603769 1.022352532 147.7759088 |
0.903093679 1.3369617 181.8617453 |
0.988631078 1.894817489 232.1851007 |
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| Sample: SiNP3N
| Operator: NHA
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| Automatic DegNo
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| Alpha-S Method
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| 4029- At least two fitted data points are needed for Alpha
Not Fitted |
Thickness (nmQuantity Adso|
0.26414568 36.28838566 |
0.573615127 84.91082142 |
0.644566671 96.08583999 |
0.745247381 112.2580179 |
0.8716842 131.2188895 |
1.022352532 147.7759088 |
1.3369617 181.8617453 |
1.894817489 232.1851007 |
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| f-Ratio Method | BJH Adsorption Pore Distribution Repor
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| Primary Data |
| A reference file has not been chosen. |
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| Diameter Rang
| Adsorbate Prop
| Density Conver
| Fraction of Po
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| Pore Diameter
| 170.4 - 21.3
| 21.3 - 10.2
| 10.2 - 7.2
| 7.2 - 5.2
| 5.2 - 3.9
| 3.9 - 3.2
| 3.2 - 2.5
| 2.5 - 2.0
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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SiNP3N | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.SMP | File:
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1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2927 g Warm Free Sp11.1935 cm³ Measured | Sample Mass:
32.3094 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
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JH Adsorption Pore Distribution Report | BJH Desorption Pore Distribution Repo
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Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
0.00 | Fraction of Po
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Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
23.18771495 0.098539744 0.098539744 16.99861233 16.99861233 | 170.4 - 21.4
12.09398972 0.068078454 0.166618199 22.51645846 39.5150708 | 21.4 - 10.5
8.11742703 0.032057049 0.198675248 15.79665538 55.31172618 | 10.5 - 7.1
5.835628929 0.040088806 0.238764195 27.47875013 82.79047631 | 7.1 - 5.2
4.365565397 0.0338883 0.272652495 31.05054826 113.8410246 | 5.2 - 3.9
3.455691409 0.021730055 0.29438255 25.15277301 138.9937976 | 3.9 - 3.1
2.720942326 0.019717438 0.314099989 28.98619096 167.9799885 | 3.1 - 2.5
2.197682576 0.011342134 0.325442123 20.6438074 188.6237959 | 2.5 - 2.0
|
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SiNP3N | Sample:
NHA | Operator:
| Submitter:
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No | Automatic Deg
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JH Desorption Pore Distribution Report | Dollimore-Heal Adsorption Pore Distribu
|
Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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| Diameter Rang
1.7000 nm to 300.0000 nm | Adsorbate Prop
0.95300 nm | Density Conver
0.0015468 |
0.00 |
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| Pore Diameter
| 170.5 - 21.4
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| 21.4 - 10.3
23.3678755 0.026119135 0.026119135 4.470947235 4.470947235 | 10.3 - 7.3
12.43219636 0.138403665 0.1645228 44.53072043 49.00166766 | 7.3 - 5.3
8.061531117 0.01311505 0.17763785 6.507473489 55.50914115 | 5.3 - 4.0
5.84411243 0.017869452 0.195507301 12.2307378 67.73987895 | 4.0 - 3.3
4.355424802 0.060657916 0.256165217 55.70792157 123.4478005 | 3.3 - 2.6
3.365799557 0.064020754 0.320185971 76.08385765 199.5316582 | 2.6 - 2.1
2.701476014 0.010537937 0.330723908 15.60322848 215.1348867 | 2.1 - 1.6
2.157471831 0.007461293 0.338185201 13.83340074 228.9682874 |
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SiNP3N | Sample:
NHA | Operator:
| Submitter:
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No | Automatic Deg
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|
ollimore-Heal Adsorption Pore Distribution Report | Dollimore-Heal Desorption Pore Distribu
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
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|
1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
|
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|
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
95.92902614 0.081391333 0.081391333 3.393814624 3.393814624 | 170.5 - 21.5
15.85403037 0.065119574 0.146510907 16.42978415 19.82359878 | 21.5 - 10.6
8.796130943 0.034189916 0.180700823 15.54770662 35.37130539 | 10.6 - 7.2
6.273429042 0.041535782 0.222236605 26.48362299 61.85492838 | 7.2 - 5.3
4.656453887 0.035651697 0.257888303 30.62562042 92.4805488 | 5.3 - 4.0
3.643375147 0.023975417 0.281863719 26.32220479 118.8027536 | 4.0 - 3.2
2.91445137 0.021972374 0.303836094 30.15644645 148.9592 | 3.2 - 2.6
2.343564963 0.01369083 0.317526923 23.36752793 172.326728 | 2.6 - 2.1
1.860888273 0.015281166 0.33280809 32.84703694 205.1737649 | 2.1 - 1.6
|
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SiNP3N | Sample:
NHA | Operator:
| Submitter:
|
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No | Automatic Deg
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|
|
ollimore-Heal Desorption Pore Distribution Report | Horvath-Kawazoe Report
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
| Maximum Pore
1.7000 nm to 300.0000 nm | at Relative Pr
0.95300 nm | Median Pore W
0.0015468 | Relative Press
|
| Diameter of Ad
| Diameter of Ad
| Diameter of S
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Diameter of Sa
96.01358616 0.021644978 0.021644978 0.901746451 0.901746451 | Interaction Pa
16.09155837 0.125199991 0.146844968 31.12190574 32.0236522 |
8.903332889 0.015785024 0.162629992 7.091737015 39.11538921 | Density Conver
6.254502151 0.019834386 0.182464378 12.68486932 51.80025854 |
4.681661374 0.060595881 0.243060258 51.7729719 103.5732304 |
3.596200568 0.065078944 0.308139203 72.38633462 175.959565 |
2.883975834 0.01344218 0.321581383 18.64395613 194.6035212 |
2.339181698 0.010412419 0.331993802 17.80523393 212.4087551 | Absolute Pres
1.849079651 0.008808255 0.340802057 19.05435569 231.4631108 | 8.123408318
| 81.4845047
| 161.6503754
| 225.329834
| 308.7663574
| 378.5152893
| 460.1719971
| 537.8909912
| 603.8988647
| 686.3511963
| 751.3596191
|
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|
|
SiNP3N | Sample:
NHA | Operator:
| Submitter:
|
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No | Automatic Deg
|
|
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|
|
orvath-Kawazoe Report |
|
Slit Pore Geometry (Original H-K) |
|
|
|
|
0.359144 cm³/g |
0.988631078 |
7.7153 nm |
1.069e-002 to 9.886e-001 | Volume in Por
| Total Volume i
0.3000 nm | Area in Pores
0.2574 nm | Total Area in
0.3040 nm |
0.2609 nm |
3.49e-043 erg·cm^4 | Pore Size Table
|
0.0015468 | Pore Width (n
| 1.483289338
| 1.590515054
| 1.715611708
| 1.8585793
Relative PressQuantity AdsoPore Width (n Cumulative PoDifferential P | 2.001546978
0.010688695 36.28838566 1.034615 0.056130875 0.05425291 | 2.16238568
0.107216454 55.36015678 1.828413695 0.085631091 0.037163346 | 2.341095234
0.212697862 65.80209914 2.512918491 0.101782687 0.023596031 | 2.519804789
0.296486624 73.62407577 3.118555967 0.11388172 0.019977353 | 2.734256221
0.406271523 84.91082142 4.111097197 0.131340059 0.017589534 | 2.948707652
0.498046433 96.08583999 5.214871496 0.148625577 0.015660374 | 3.181030107
0.60548947 112.2580179 7.14647652 0.173640702 0.012950435 | 3.431223586
0.707751304 131.2188895 10.20117189 0.202969378 0.009601179 | 3.699287918
0.794603769 147.7759088 15.2436544 0.228579776 0.005078926 | 4.003093956
0.903093679 181.8617453 33.90083968 0.281303748 0.002825934 | 4.324771359
0.988631078 232.1851007 276.7552014 0.359143914 0.000320522 | 4.664319445
| 5.039609578
| 5.432770394
| 5.879544281
| 6.344189191
| 6.844575808
| 7.398575836
| 7.98831723
| 8.631671354
| 9.310767526
| 10.06134779
| 10.86554079
| 11.72334651
| 12.65263702
| 13.67128093
| 14.76140894
| 15.94089173
| 17.20973066
| 18.58579369
| 20.06908354
| 21.65959748
| 23.39307962
| 25.25166062
| 27.27107913
| 29.45133516
| 31.79242869
| 34.33010654
| 37.06436055
| 40.03094025
| 43.22984018
| 46.67893786
| 50.39609442
| 54.4170594
| 58.75969939
| 63.44189191
| 68.49937012
| 73.96788359
| 79.86529889
| 86.24523218
| 93.12554458
| 100.5598686
| 108.5660545
|
|
|
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.S | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2927 g Warm Free Sp11.1935 cm³ Measured | Sample Mass:0.2927 g
32.3094 cm³ Equilibration In5 s | Cold Free Spa32.3094 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
|
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Porosity Distribution by Original Density Functional Theor | Porosity Distribution by Original Density
Model: N2 @ 77K on Carbon, Slit Pores | Model: N2 @ 77K on Carbon, Slit Pores
Method: Non-negative Regularization: 0.00000 | Method: Non-negative Regularization:
Standard Deviation of Fit: 0.66885 cm³/g STP |
|
|
|
| Standard Deviation of Fit: 0.66885 cm³/
< 1.483 nm : 0.02098 cm³/ |
<= 108.566 nm : 0.27061 cm³/ |
> 108.566 nm : 24.613 m²/g | Isotherm Table
>= 1.483 nm : 108.036 m²/g | Relative Pressure
| (P/Po) Experimental
| 0.01178367 36.55863017
ore Size Table | 0.01451552 37.23204232
| 0.017706521 38.01652783
Cumulative VoIncremental VoCumulative AreIncremental Ar| 0.02139844 38.92017233
0.021628488 0.000647701 0.873331293 0.873331293 | 0.02563123 39.94917819
0.024493999 0.002865511 4.47657995 3.603248656 | 0.03044224 41.10702623
0.027419278 0.002925279 7.886767728 3.410187778 | 0.035865448 42.39346537
0.031217325 0.003798047 11.97381122 4.087043489 | 0.041930798 43.80333491
0.03334835 0.002131025 14.10318899 2.129377777 | 0.048663601 45.32521714
0.03334835 0 14.10318899 0| 0.056084011 46.93993519
0.034774428 0.001426078 15.3214892 1.218300202 | 0.064206667 48.6189555
0.038302511 0.003528083 18.121772 2.800282802 | 0.073040441 50.32273127
0.043617672 0.005315161 22.00960175 3.887829756 | 0.082588248 51.99905513
0.048603456 0.004985783 25.39127519 3.38167344 | 0.092847057 53.58152985
0.054004118 0.005400662 28.78681796 3.395542763 | 0.103808001 54.98823388
0.06075159 0.006747472 32.71980107 3.932983114 | 0.115456402 56.21626623
0.066724709 0.005973119 35.94913575 3.229334676 | 0.127772301 57.48272454
0.074253624 0.007528914 39.71068342 3.76154767 | 0.140730694 58.79844849
0.082921856 0.008668232 43.71932645 4.008643031 | 0.154301897 60.15815926
0.09251869 0.009596834 47.83432523 4.114998783 | 0.168452203 61.55629421
0.103238431 0.01071974 52.08852002 4.254194786 | 0.183144197 62.98708579
0.114762776 0.011524345 56.3310499 4.242529885 | 0.198337302 64.44465985
0.125651541 0.010888765 60.03499865 3.703948745 | 0.213988706 65.92317913
0.135367576 0.009716035 63.09796994 3.062971297 | 0.230053101 67.42149698
0.144248584 0.008881008 65.69301978 2.59504984 | 0.246484801 68.94454322
0.150836432 0.006587848 67.47386201 1.780842222 | 0.263235897 70.49770919
0.156965472 0.00612904 69.00836289 1.534500881 | 0.280259013 72.08755144
0.163859134 0.006893662 70.60565782 1.597294936 | 0.297506303 73.72157009
0.169906196 0.006047062 71.9045973 1.298939482 | 0.314930797 75.41515588
0.174371578 0.004465382 72.79222822 0.887630913 | 0.332486212 77.16940846
0.179076337 0.00470476 73.65822463 0.86599641 | 0.35012731 78.97366083
0.184359112 0.005282775 74.55946476 0.901240135 | 0.367810607 80.81680374
0.190406032 0.00604692 75.51530023 0.955835469 | 0.385494202 82.68745502
0.197234858 0.006828826 76.5143033 0.999003071 | 0.40313831 84.57419867
0.204733517 0.007498659 77.53028476 1.015981455 | 0.420704991 86.50271625
0.212721086 0.007987569 78.53243313 1.002148371 | 0.4381589 88.52670989
0.220818875 0.008097789 79.47350408 0.941070952 | 0.455466807 90.62619405
0.228140956 0.007322081 80.26142645 0.78792237 | 0.472598106 92.77981727
0.234587909 0.006446952 80.90390246 0.642476013 | 0.489524394 94.96692644
0.240301509 0.0057136 81.43148382 0.527581357 | 0.506219923 97.16913913
0.245410804 0.005109295 81.86830493 0.436821105 | 0.522661209 99.38987667
0.249976696 0.004565892 82.22993592 0.361630991 | 0.5388273 101.6479864
0.254007717 0.004031022 82.52556203 0.295626115 | 0.5546996 103.9602561
0.256690179 0.002682462 82.70772435 0.182162319 | 0.570261598 106.3408917
0.25901521 0.002325032 82.85398758 0.146263225 | 0.585499227 108.8015537
0.261676596 0.002661386 83.00903434 0.155046766 | 0.60040009 111.351279
0.263902049 0.002225452 83.12912019 0.120085754 | 0.614954293 113.9702416
0.265816832 0.001914783 83.22478534 0.095665154 | 0.629153311 116.5658691
0.267093789 0.001276957 83.28386289 0.059077551 | 0.642990828 119.1206929
0.268194203 0.001100415 83.33101111 0.047148224 | 0.656461716 121.6256478
0.269400947 0.001206744 83.3789015 0.047890386 | 0.669562697 124.0730172
0.270210813 0.000809865 83.40866663 0.029765131 | 0.682291925 126.4563141
0.270610236 0.000399423 83.42226177 0.01359514 | 0.694648683 128.7701727
0.270610236 0 83.42226177 0| 0.706633508 131.0103117
0.270610236 0 83.42226177 0| 0.71824801 133.1843274
0.270610236 0 83.42226177 0| 0.729494929 135.3048147
0.270610236 0 83.42226177 0| 0.740377605 137.3691481
0.270610236 0 83.42226177 0| 0.750900388 139.3752064
0.270610236 0 83.42226177 0| 0.761068285 141.3213919
0.270610236 0 83.42226177 0| 0.770887017 143.2066072
0.270610236 0 83.42226177 0| 0.780362606 145.0301414
| 0.789501607 146.7916823
| 0.798311174 148.487875
| 0.806798697 150.1089948
| 0.814971626 151.6944565
| 0.822837889 153.2832619
| 0.830405474 154.9057233
| 0.837682605 156.5847078
| 0.844677329 158.3366343
| 0.851397991 160.1725686
| 0.857852995 162.099062
| 0.864050388 164.1188047
| 0.869998574 166.2315369
| 0.875705481 168.4343846
| 0.881179392 170.7226902
| 0.886428118 173.0901566
| 0.891459525 175.5294517
| 0.896281302 178.0324503
| 0.9009009 180.5904787
| 0.90532577 183.1749289
| 0.909563184 185.6678836
| 0.913620114 188.0546567
| 0.917503417 190.3392807
| 0.921219707 192.5256482
| 0.924775481 194.6175812
| 0.928177178 196.6188672
| 0.931430817 198.5330476
| 0.934542298 200.3635943
| 0.937517405 202.1139085
| 0.940361619 203.7872166
| 0.943080306 205.3866743
| 0.945678592 206.9152975
| 0.948161721 208.3761721
| 0.950534225 209.771963
| 0.95280093 211.1055107
| 0.954966187 212.3793751
| 0.957034409 213.5961511
| 0.959009588 214.7581881
| 0.960896015 215.8680109
| 0.962697208 216.9276885
| 0.964416981 217.9394651
| 0.96605891 218.9054447
| 0.967626274 219.827556
| 0.969122529 220.7078328
| 0.970550597 221.5479935
| 0.971913695 222.3499316
| 0.973214507 223.1152251
| 0.974455774 223.845487
| 0.975640416 224.5424357
| 0.976770699 225.2074036
| 0.977849126 225.8418636
| 0.978878021 226.4471832
| 0.979859591 227.02466
| 0.980795979 227.5755563
| 0.981689274 228.1010994
| 0.982541502 228.6024817
| 0.98335427 229.0806498
| 0.984129488 229.536726
| 0.984869003 229.9717973
| 0.985574186 230.3866703
| 0.986246824 230.7823968
| 0.986888289 231.1597836
| 0.987500012 231.5196721
| 0.988083303 231.8628339
|
|
|
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
| Sample: SiNP3N
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.S | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
Warm Free Sp11.1935 cm³ Measured | Sample Mass:0.2927 g Warm Free Sp
Equilibration In5 s | Cold Free Spa32.3094 cm³ Equilibration In
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
| Automatic DegNo
|
|
|
|
|
|
|
| Cumulative Surface Area vs. Pore Width
|
orosity Distribution by Original Density Functional Theor |
odel: N2 @ 77K on Carbon, Slit Pores | Cumulative Surface Area
ethod: Non-negative Regularization: 0.00000 | Pore Width (n Cumulative Surface Area (m²/g)
| 1.483289338 0.873331293
| 1.590515054 4.47657995
| 1.715611708 7.886767728
| 1.8585793 11.97381122
tandard Deviation of Fit: 0.66885 cm³/g STP | 2.001546978 14.10318899
| 2.16238568 14.10318899
| 2.341095234 15.3214892
| 2.519804789 18.121772
| 2.734256221 22.00960175
Fitted Quantit Absolute ResidRelative Resid| 2.948707652 25.39127519
36.50663292 0.05199725 0.001422298 | 3.181030107 28.78681796
37.26342277 -0.03138045 -0.00084283 | 3.431223586 32.71980107
38.18022848 -0.16370065 -0.00430604 | 3.699287918 35.94913575
38.94347158 -0.02329926 -0.00059864 | 4.003093956 39.71068342
39.73834952 0.210828665 0.005277422 | 4.324771359 43.71932645
41.3071795 -0.20015327 -0.00486908 | 4.664319445 47.83432523
42.20441948 0.189045895 0.004459317 | 5.039609578 52.08852002
44.03454734 -0.23121243 -0.00527842 | 5.432770394 56.3310499
45.08352489 0.241692249 0.005332401 | 5.879544281 60.03499865
47.33017516 -0.39023997 -0.0083136 | 6.344189191 63.09796994
48.58741928 0.031536222 0.00064864 | 6.844575808 65.69301978
49.95202829 0.370702978 0.007366511 | 7.398575836 67.47386201
52.01765983 -0.01860471 -0.00035779 | 7.98831723 69.00836289
53.48443271 0.09709714 0.001812138 | 8.631671354 70.60565782
54.92338892 0.064844962 0.001179252 | 9.310767526 71.9045973
56.29352666 -0.07726044 -0.00137434 | 10.06134779 72.79222822
57.57756407 -0.09483953 -0.00164988 | 10.86554079 73.65822463
58.77634785 0.022100644 0.000375871 | 11.72334651 74.55946476
60.32843477 -0.17027551 -0.00283046 | 12.65263702 75.51530023
61.3849663 0.171327911 0.002783272 | 13.67128093 76.5143033
63.4943114 -0.50722561 -0.00805285 | 14.76140894 77.53028476
64.45628666 -0.01162681 -0.00018042 | 15.94089173 78.53243313
65.39262297 0.530556157 0.008048097 | 17.20973066 79.47350408
68.04673831 -0.62524133 -0.00927362 | 18.58579369 80.26142645
68.95076534 -0.00622212 -9.02482E-05 | 20.06908354 80.90390246
69.85856753 0.639141659 0.009066134 | 21.65959748 81.43148382
72.44136909 -0.35381765 -0.00490817 | 23.39307962 81.86830493
73.36923875 0.352331334 0.004779216 | 25.25166062 82.22993592
76.19204833 -0.77689246 -0.01030154 | 27.27107913 82.52556203
77.16771341 0.00169505 2.19653E-05 | 29.45133516 82.70772435
78.1852362 0.788424633 0.009983387 | 31.79242869 82.85398758
81.61316548 -0.79636174 -0.00985391 | 34.33010654 83.00903434
82.68 0.007441683 8.99977E-05 | 37.06436055 83.12912019
83.77200404 0.802194631 0.009485099 | 40.03094025 83.22478534
86.98628631 -0.48357006 -0.00559023 | 43.22984018 83.28386289
88.04729956 0.479410327 0.005415431 | 46.67893786 83.33101111
91.82377066 -1.19757661 -0.01321446 | 50.39609442 83.3789015
92.79704412 -0.01722685 -0.00018567 | 54.4170594 83.40866663
93.73708314 1.229843296 0.012950227 | 58.75969939 83.42226177
97.85702878 -0.68788964 -0.0070793 | 63.44189191 83.42226177
98.70764193 0.682234741 0.006864228 | 68.49937012 83.42226177
103.1972107 -1.54922428 -0.01524107 | 73.96788359 83.42226177
103.9816896 -0.02143351 -0.00020617 | 79.86529889 83.42226177
104.7580234 1.582868369 0.014884851 | 86.24523218 83.42226177
109.7074885 -0.90593481 -0.00832649 | 93.12554458 83.42226177
110.4517169 0.89956213 0.008078597 | 100.5598686 83.42226177
115.8129101 -1.84266847 -0.01616798 | 108.5660545 83.42226177
116.5423104 0.023558738 0.000202107 |
117.2875315 1.8331614 0.01538911 |
122.4826588 -0.8570109 -0.0070463 |
123.2240386 0.848978595 0.006842572 |
128.0204876 -1.56417353 -0.01236928 |
128.7438161 0.026356654 0.00020468 |
129.4630995 1.547212249 0.011809851 |
133.9177127 -0.73338527 -0.00550654 |
134.5818104 0.723004268 0.005343522 |
138.071202 -0.70205389 -0.00511071 |
138.682835 0.692371395 0.00496768 |
141.9830165 -0.66162461 -0.0046817 |
142.5542528 0.65235447 0.004555338 |
146.2239874 -1.19384605 -0.00823171 |
146.7695937 0.022088581 0.000150476 |
147.3164425 1.171432493 0.007889078 |
150.6327565 -0.52376175 -0.00348921 |
151.1797912 0.514665385 0.003392776 |
153.8182222 -0.53496035 -0.00349001 |
154.3787159 0.527007441 0.003402117 |
157.1797646 -0.59505678 -0.00380022 |
157.7483306 0.588303659 0.003715525 |
160.8613655 -0.68879692 -0.00430034 |
161.4161266 0.682935436 0.004213075 |
164.9167658 -0.79796109 -0.00486209 |
165.4388617 0.792675219 0.004768501 |
169.3368679 -0.90248334 -0.00535807 |
169.8248813 0.897808869 0.005258873 |
174.0796249 -0.98946832 -0.00571649 |
174.5442191 0.985232593 0.005612919 |
179.0850824 -1.05263214 -0.00591259 |
179.5416291 1.048849594 0.00580789 |
184.1917438 -1.01681486 -0.00555106 |
184.6546498 1.01323383 0.005457238 |
188.9606346 -0.90597797 -0.00481763 |
189.4368215 0.90245926 0.004741319 |
193.3331351 -0.8074869 -0.00419418 |
193.8135648 0.804016401 0.004131263 |
197.3459876 -0.72712042 -0.00369812 |
197.8094799 0.723567768 0.003644571 |
201.0216699 -0.65807564 -0.00328441 |
201.4593433 0.654565244 0.003238596 |
204.3784071 -0.59119057 -0.00290102 |
204.7989436 0.587730717 0.002861582 |
207.4372018 -0.52190423 -0.00252231 |
207.8575822 0.518589875 0.00248872 |
209.7758028 -0.00383977 -1.83044E-05 |
211.5177058 -0.41219505 -0.00195255 |
211.97 0.409326922 0.001927338 |
213.9404162 -0.34426511 -0.00161176 |
214.4166379 0.341550142 0.001590394 |
216.1620071 -0.29399624 -0.00136193 |
216.6362909 0.291397512 0.001343293 |
218.1973088 -0.25784375 -0.0011831 |
218.65 0.25538422 0.001166642 |
219.8301179 -0.00256193 -1.16543E-05 |
220.9085442 -0.20071139 -0.0009094 |
221.3494087 0.198584856 0.000896351 |
222.5022753 -0.15234376 -0.00068515 |
222.9648823 0.150342799 0.000673835 |
223.942778 -0.09729097 -0.00043463 |
224.447031 0.095404707 0.000424885 |
225.2033005 0.0041031 1.82192E-05 |
225.7308088 0.111054816 0.000491737 |
226.2538888 0.193294443 0.000853596 |
226.7658899 0.258770087 0.001139833 |
227.2666029 0.30895337 0.001357586 |
227.7614083 0.339691096 0.001489213 |
228.2566825 0.345799128 0.001512666 |
228.7621227 0.318527099 0.001390458 |
229.288009 0.248717022 0.001083561 |
229.8396465 0.132150865 0.000574639 |
230.4184087 -0.0317384 -0.00013776 |
231.0145153 -0.23211844 -0.00100579 |
231.5894789 -0.42969533 -0.00185887 |
232.1999252 -0.68025305 -0.00293821 |
232.771839 -0.90900511 -0.00392044 |
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| Sample: SiNP3N |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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| Incremental Surface Area vs. Pore Width |
| |
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| Incremental Surface Area |
ace Area (m²/g) | Pore Width (n Incremental Surface Area (m²/g) |
| 1.483289338 0.873331293 |
| 1.590515054 3.603248656 |
| 1.715611708 3.410187778 |
| 1.8585793 4.087043489 |
| 2.001546978 2.129377777 |
| 2.16238568 0 |
| 2.341095234 1.218300202 |
| 2.519804789 2.800282802 |
| 2.734256221 3.887829756 |
| 2.948707652 3.38167344 |
| 3.181030107 3.395542763 |
| 3.431223586 3.932983114 |
| 3.699287918 3.229334676 |
| 4.003093956 3.76154767 |
| 4.324771359 4.008643031 |
| 4.664319445 4.114998783 |
| 5.039609578 4.254194786 |
| 5.432770394 4.242529885 |
| 5.879544281 3.703948745 |
| 6.344189191 3.062971297 |
| 6.844575808 2.59504984 |
| 7.398575836 1.780842222 |
| 7.98831723 1.534500881 |
| 8.631671354 1.597294936 |
| 9.310767526 1.298939482 |
| 10.06134779 0.887630913 |
| 10.86554079 0.86599641 |
| 11.72334651 0.901240135 |
| 12.65263702 0.955835469 |
| 13.67128093 0.999003071 |
| 14.76140894 1.015981455 |
| 15.94089173 1.002148371 |
| 17.20973066 0.941070952 |
| 18.58579369 0.78792237 |
| 20.06908354 0.642476013 |
| 21.65959748 0.527581357 |
| 23.39307962 0.436821105 |
| 25.25166062 0.361630991 |
| 27.27107913 0.295626115 |
| 29.45133516 0.182162319 |
| 31.79242869 0.146263225 |
| 34.33010654 0.155046766 |
| 37.06436055 0.120085754 |
| 40.03094025 0.095665154 |
| 43.22984018 0.059077551 |
| 46.67893786 0.047148224 |
| 50.39609442 0.047890386 |
| 54.4170594 0.029765131 |
| 58.75969939 0.01359514 |
| 63.44189191 0 |
| 68.49937012 0 |
| 73.96788359 0 |
| 79.86529889 0 |
| 86.24523218 0 |
| 93.12554458 0 |
| 100.5598686 0 |
| 108.5660545 0 |
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Differential Surface Area vs. Pore Width | Cumulative Pore Volume vs. Pore Width
|
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Differential Surface Area | Cumulative Pore Volume
Pore Width (n Differential Surface Area (m²/g) | Pore Width (n Cumulative Pore Volume (cm³/g)
1.483289338 28.81149106 | 1.483289338 0.021628488
1.590515054 114.0392591 | 1.590515054 0.024493999
1.715611708 100.8285276 | 1.715611708 0.027419278
1.8585793 122.0982724 | 1.8585793 0.031217325
2.001546978 64.76991766 | 2.001546978 0.03334835
2.16238568 0 | 2.16238568 0.03334835
2.341095234 36.67715214 | 2.341095234 0.034774428
2.519804789 83.06963776 | 2.519804789 0.038302511
2.734256221 113.9043439 | 2.734256221 0.043617672
2.948707652 102.8981279 | 2.948707652 0.048603456
3.181030107 103.1808559 | 3.181030107 0.054004118
3.431223586 119.9988358 | 3.431223586 0.06075159
3.699287918 96.47470425 | 3.699287918 0.066724709
4.003093956 110.8864813 | 4.003093956 0.074253624
4.324771359 120.7558946 | 4.324771359 0.082921856
4.664319445 123.8827969 | 4.664319445 0.09251869
5.039609578 128.4613605 | 5.039609578 0.103238431
5.432770394 126.7433725 | 5.432770394 0.114762776
5.879544281 109.9832566 | 5.879544281 0.125651541
6.344189191 92.81327269 | 6.344189191 0.135367576
6.844575808 77.72867913 | 6.844575808 0.144248584
7.398575836 53.07331215 | 7.398575836 0.150836432
7.98831723 45.84241943 | 7.98831723 0.156965472
8.631671354 48.01715357 | 8.631671354 0.163859134
9.310767526 39.02989165 | 9.310767526 0.169906196
10.06134779 26.47042387 | 10.06134779 0.174371578
10.86554079 26.08602055 | 10.86554079 0.179076337
11.72334651 27.25674241 | 11.72334651 0.184359112
12.65263702 28.63600204 | 12.65263702 0.190406032
13.67128093 29.84470132 | 13.67128093 0.197234858
14.76140894 30.46265672 | 14.76140894 0.204733517
15.94089173 30.07365596 | 15.94089173 0.212721086
17.20973066 28.2313523 | 17.20973066 0.220818875
18.58579369 23.60693468 | 18.58579369 0.228140956
20.06908354 19.33152018 | 20.06908354 0.234587909
21.65959748 15.85283897 | 21.65959748 0.240301509
23.39307962 13.10996321 | 23.39307962 0.245410804
25.25166062 10.85735646 | 25.25166062 0.249976696
27.27107913 8.849088358 | 27.27107913 0.254007717
29.45133516 5.468584193 | 29.45133516 0.256690179
31.79242869 4.394257675 | 31.79242869 0.25901521
34.33010654 4.653766679 | 34.33010654 0.261676596
37.06436055 3.599661012 | 37.06436055 0.263902049
40.03094025 2.863063878 | 40.03094025 0.265816832
43.22984018 1.770772453 | 43.22984018 0.267093789
46.67893786 1.415580934 | 46.67893786 0.268194203
50.39609442 1.43784523 | 50.39609442 0.269400947
54.4170594 0.892739431 | 54.4170594 0.270210813
58.75969939 0.408010943 | 58.75969939 0.270610236
63.44189191 0 | 63.44189191 0.270610236
68.49937012 0 | 68.49937012 0.270610236
73.96788359 0 | 73.96788359 0.270610236
79.86529889 0 | 79.86529889 0.270610236
86.24523218 0 | 86.24523218 0.270610236
93.12554458 0 | 93.12554458 0.270610236
100.5598686 0 | 100.5598686 0.270610236
108.5660545 0 | 108.5660545 0.270610236
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| Sample: SiNP3N
| Operator: NHA
| Submitter:
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| Automatic DegNo
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e Volume vs. Pore Width | Incremental Pore Volume vs. Pore Width
|
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| Incremental Pore Volume
umulative Pore Volume (cm³/g) | Pore Width (n Incremental Pore Volume (cm³/g)
| 1.483289338 0.000647701
| 1.590515054 0.002865511
| 1.715611708 0.002925279
| 1.8585793 0.003798047
| 2.001546978 0.002131025
| 2.16238568 0
| 2.341095234 0.001426078
| 2.519804789 0.003528083
| 2.734256221 0.005315161
| 2.948707652 0.004985783
| 3.181030107 0.005400662
| 3.431223586 0.006747472
| 3.699287918 0.005973119
| 4.003093956 0.007528914
| 4.324771359 0.008668232
| 4.664319445 0.009596834
| 5.039609578 0.01071974
| 5.432770394 0.011524345
| 5.879544281 0.010888765
| 6.344189191 0.009716035
| 6.844575808 0.008881008
| 7.398575836 0.006587848
| 7.98831723 0.00612904
| 8.631671354 0.006893662
| 9.310767526 0.006047062
| 10.06134779 0.004465382
| 10.86554079 0.00470476
| 11.72334651 0.005282775
| 12.65263702 0.00604692
| 13.67128093 0.006828826
| 14.76140894 0.007498659
| 15.94089173 0.007987569
| 17.20973066 0.008097789
| 18.58579369 0.007322081
| 20.06908354 0.006446952
| 21.65959748 0.0057136
| 23.39307962 0.005109295
| 25.25166062 0.004565892
| 27.27107913 0.004031022
| 29.45133516 0.002682462
| 31.79242869 0.002325032
| 34.33010654 0.002661386
| 37.06436055 0.002225452
| 40.03094025 0.001914783
| 43.22984018 0.001276957
| 46.67893786 0.001100415
| 50.39609442 0.001206744
| 54.4170594 0.000809865
| 58.75969939 0.000399423
| 63.44189191 0
| 68.49937012 0
| 73.96788359 0
| 79.86529889 0
| 86.24523218 0
| 93.12554458 0
| 100.5598686 0
| 108.5660545 0
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| Differential Pore Volume vs. Pore Width | Goodness of Fit
| | Standard Deviation of Fit: 0.66885 cm³/
| |
| Differential Pore Volume | Input Data
| Pore Width (n Differential Pore Volume (cm³/g) | Relative Press
| 1.483289338 0.021367889 | 0.010688695
| 1.590515054 0.090690579 | 0.107216454
| 1.715611708 0.086491301 | 0.212697862
| 1.8585793 0.113464661 | 0.296486624
| 2.001546978 0.064820016 | 0.406271523
| 2.16238568 0 | 0.498046433
| 2.341095234 0.042932353 | 0.60548947
| 2.519804789 0.104659636 | 0.707751304
| 2.734256221 0.15572183 | 0.794603769
| 2.948707652 0.151708249 | 0.903093679
| 3.181030107 0.164110705 | 0.988631078
| 3.431223586 0.205871418 |
| 3.699287918 0.178443854 |
| 4.003093956 0.221944501 |
| 4.324771359 0.261120817 |
| 4.664319445 0.288914469 |
| 5.039609578 0.323697551 |
| 5.432770394 0.344283821 |
| 5.879544281 0.323325714 |
| 6.344189191 0.294412481 |
| 6.844575808 0.266009918 |
| 7.398575836 0.196333462 |
| 7.98831723 0.183101894 |
| 8.631671354 0.207234144 |
| 9.310767526 0.181699124 |
| 10.06134779 0.13316407 |
| 10.86554079 0.14171936 |
| 11.72334651 0.159770118 |
| 12.65263702 0.18116047 |
| 13.67128093 0.204007648 |
| 14.76140894 0.224835867 |
| 15.94089173 0.239700447 |
| 17.20973066 0.242926985 |
| 18.58579369 0.219376809 |
| 20.06908354 0.193982947 |
| 21.65959748 0.171683056 |
| 23.39307962 0.153341207 |
| 25.25166062 0.13708314 |
| 27.27107913 0.120662094 |
| 29.45133516 0.080528553 |
| 31.79242869 0.069852062 |
| 34.33010654 0.079882153 |
| 37.06436055 0.066709567 |
| 40.03094025 0.05730557 |
| 43.22984018 0.038275105 |
| 46.67893786 0.033038907 |
| 50.39609442 0.036230892 |
| 54.4170594 0.024290127 |
| 58.75969939 0.0119873 |
| 63.44189191 0 |
| 68.49937012 0 |
| 73.96788359 0 |
| 79.86529889 0 |
| 86.24523218 0 |
| 93.12554458 0 |
| 100.5598686 0 |
| 108.5660545 0 |
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NHA | Operator: NHA
| Submitter:
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oodness of Fit | Goodness of Fit
tandard Deviation of Fit: 0.66885 cm³/g STP | Standard Deviation of Fit: 0.66885 cm³/g STP
|
Model Fit | Input Data Model Fit
Quantity AdsoRelative PressQuantity Adso| Relative PressQuantity AdsoRelative Press
36.28838566 0.01178367 36.50663292 | 0.010688695 36.28838566 0.01178367
55.36015678 0.01451552 37.26342277 | 0.107216454 55.36015678 0.01451552
65.80209914 0.017706521 38.18022848 | 0.212697862 65.80209914 0.017706521
73.62407577 0.02139844 38.94347158 | 0.296486624 73.62407577 0.02139844
84.91082142 0.02563123 39.73834952 | 0.406271523 84.91082142 0.02563123
96.08583999 0.03044224 41.3071795 | 0.498046433 96.08583999 0.03044224
112.2580179 0.035865448 42.20441948 | 0.60548947 112.2580179 0.035865448
131.2188895 0.041930798 44.03454734 | 0.707751304 131.2188895 0.041930798
147.7759088 0.048663601 45.08352489 | 0.794603769 147.7759088 0.048663601
181.8617453 0.056084011 47.33017516 | 0.903093679 181.8617453 0.056084011
232.1851007 0.064206667 48.58741928 | 0.988631078 232.1851007 0.064206667
0.073040441 49.95202829 | 0.073040441
0.082588248 52.01765983 | 0.082588248
0.092847057 53.48443271 | 0.092847057
0.103808001 54.92338892 | 0.103808001
0.115456402 56.29352666 | 0.115456402
0.127772301 57.57756407 | 0.127772301
0.140730694 58.77634785 | 0.140730694
0.154301897 60.32843477 | 0.154301897
0.168452203 61.3849663 | 0.168452203
0.183144197 63.4943114 | 0.183144197
0.198337302 64.45628666 | 0.198337302
0.213988706 65.39262297 | 0.213988706
0.230053101 68.04673831 | 0.230053101
0.246484801 68.95076534 | 0.246484801
0.263235897 69.85856753 | 0.263235897
0.280259013 72.44136909 | 0.280259013
0.297506303 73.36923875 | 0.297506303
0.314930797 76.19204833 | 0.314930797
0.332486212 77.16771341 | 0.332486212
0.35012731 78.1852362 | 0.35012731
0.367810607 81.61316548 | 0.367810607
0.385494202 82.68 | 0.385494202
0.40313831 83.77200404 | 0.40313831
0.420704991 86.98628631 | 0.420704991
0.4381589 88.04729956 | 0.4381589
0.455466807 91.82377066 | 0.455466807
0.472598106 92.79704412 | 0.472598106
0.489524394 93.73708314 | 0.489524394
0.506219923 97.85702878 | 0.506219923
0.522661209 98.70764193 | 0.522661209
0.5388273 103.1972107 | 0.5388273
0.5546996 103.9816896 | 0.5546996
0.570261598 104.7580234 | 0.570261598
0.585499227 109.7074885 | 0.585499227
0.60040009 110.4517169 | 0.60040009
0.614954293 115.8129101 | 0.614954293
0.629153311 116.5423104 | 0.629153311
0.642990828 117.2875315 | 0.642990828
0.656461716 122.4826588 | 0.656461716
0.669562697 123.2240386 | 0.669562697
0.682291925 128.0204876 | 0.682291925
0.694648683 128.7438161 | 0.694648683
0.706633508 129.4630995 | 0.706633508
0.71824801 133.9177127 | 0.71824801
0.729494929 134.5818104 | 0.729494929
0.740377605 138.071202 | 0.740377605
0.750900388 138.682835 | 0.750900388
0.761068285 141.9830165 | 0.761068285
0.770887017 142.5542528 | 0.770887017
0.780362606 146.2239874 | 0.780362606
0.789501607 146.7695937 | 0.789501607
0.798311174 147.3164425 | 0.798311174
0.806798697 150.6327565 | 0.806798697
0.814971626 151.1797912 | 0.814971626
0.822837889 153.8182222 | 0.822837889
0.830405474 154.3787159 | 0.830405474
0.837682605 157.1797646 | 0.837682605
0.844677329 157.7483306 | 0.844677329
0.851397991 160.8613655 | 0.851397991
0.857852995 161.4161266 | 0.857852995
0.864050388 164.9167658 | 0.864050388
0.869998574 165.4388617 | 0.869998574
0.875705481 169.3368679 | 0.875705481
0.881179392 169.8248813 | 0.881179392
0.886428118 174.0796249 | 0.886428118
0.891459525 174.5442191 | 0.891459525
0.896281302 179.0850824 | 0.896281302
0.9009009 179.5416291 | 0.9009009
0.90532577 184.1917438 | 0.90532577
0.909563184 184.6546498 | 0.909563184
0.913620114 188.9606346 | 0.913620114
0.917503417 189.4368215 | 0.917503417
0.921219707 193.3331351 | 0.921219707
0.924775481 193.8135648 | 0.924775481
0.928177178 197.3459876 | 0.928177178
0.931430817 197.8094799 | 0.931430817
0.934542298 201.0216699 | 0.934542298
0.937517405 201.4593433 | 0.937517405
0.940361619 204.3784071 | 0.940361619
0.943080306 204.7989436 | 0.943080306
0.945678592 207.4372018 | 0.945678592
0.948161721 207.8575822 | 0.948161721
0.950534225 209.7758028 | 0.950534225
0.95280093 211.5177058 | 0.95280093
0.954966187 211.97 | 0.954966187
0.957034409 213.9404162 | 0.957034409
0.959009588 214.4166379 | 0.959009588
0.960896015 216.1620071 | 0.960896015
0.962697208 216.6362909 | 0.962697208
0.964416981 218.1973088 | 0.964416981
0.96605891 218.65 | 0.96605891
0.967626274 219.8301179 | 0.967626274
0.969122529 220.9085442 | 0.969122529
0.970550597 221.3494087 | 0.970550597
0.971913695 222.5022753 | 0.971913695
0.973214507 222.9648823 | 0.973214507
0.974455774 223.942778 | 0.974455774
0.975640416 224.447031 | 0.975640416
0.976770699 225.2033005 | 0.976770699
0.977849126 225.7308088 | 0.977849126
0.978878021 226.2538888 | 0.978878021
0.979859591 226.7658899 | 0.979859591
0.980795979 227.2666029 | 0.980795979
0.981689274 227.7614083 | 0.981689274
0.982541502 228.2566825 | 0.982541502
0.98335427 228.7621227 | 0.98335427
0.984129488 229.288009 | 0.984129488
0.984869003 229.8396465 | 0.984869003
0.985574186 230.4184087 | 0.985574186
0.986246824 231.0145153 | 0.986246824
0.986888289 231.5894789 | 0.986888289
0.987500012 232.1999252 | 0.987500012
0.988083303 232.771839 | 0.988083303
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| Sample: SiNP3N |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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885 cm³/g STP | |
| Surface Energy Distribution by Modified De|
| Model: N2 @ 77K, Surface Energy Distribut|
Quantity Adso| Method: Non-negative Regularization: 0.0 |
36.50663292 | Standard Deviation of Fit: 0.06582 cm³/g S |
37.26342277 | |
38.18022848 | |
38.94347158 | |
39.73834952 | |
41.3071795 | Total Area : 426.143 m²/g |
42.20441948 | |
44.03454734 | |
45.08352489 | Surface Energy Table |
47.33017516 | |
48.58741928 | Energy (e/k) Cumulative AreIncremental Area (m²/g) |
49.95202829 | 20 188.0154242 188.0154242 |
52.01765983 | 22 188.0154242 0 |
53.48443271 | 24 188.0154242 0 |
54.92338892 | 26 188.0154242 0 |
56.29352666 | 28 188.0154242 0 |
57.57756407 | 30 188.0154242 0 |
58.77634785 | 32 238.3560857 50.34066151 |
60.32843477 | 34 238.3560857 0 |
61.3849663 | 36 238.3560857 0 |
63.4943114 | 38 238.3560857 0 |
64.45628666 | 40 238.3560857 0 |
65.39262297 | 42 238.3560857 0 |
68.04673831 | 44 238.3560857 0 |
68.95076534 | 46 330.8285844 92.47249864 |
69.85856753 | 48 330.8285844 0 |
72.44136909 | 50 330.8285844 0 |
73.36923875 | 52 330.8285844 0 |
76.19204833 | 54 330.8285844 0 |
77.16771341 | 56 352.1352976 21.30671319 |
78.1852362 | 58 352.1352976 0 |
81.61316548 | 60 359.1755153 7.040217773 |
82.68 | 62 359.1755153 0 |
83.77200404 | 64 378.7955223 19.62 |
86.98628631 | 66 378.7955223 0 |
88.04729956 | 68 378.7955223 0 |
91.82377066 | 70 389.2062708 10.41074853 |
92.79704412 | 72 389.2062708 0 |
93.73708314 | 74 389.2062708 0 |
97.85702878 | 76 389.2062708 0 |
98.70764193 | 78 389.2062708 0 |
103.1972107 | 80 389.2062708 0 |
103.9816896 | 82 389.2062708 0 |
104.7580234 | 84 406.3725119 17.16624108 |
109.7074885 | 86 406.3725119 0 |
110.4517169 | 88 412.6462851 6.273773178 |
115.8129101 | 90 412.6462851 0 |
116.5423104 | 92 412.6462851 0 |
117.2875315 | 94 412.6462851 0 |
122.4826588 | 96 412.6462851 0 |
123.2240386 | 98 412.6462851 0 |
128.0204876 | 100 426.1429272 13.49664212 |
128.7438161 | |
129.4630995 | |
133.9177127 | |
134.5818104 | |
138.071202 | |
138.682835 | |
141.9830165 | |
142.5542528 | |
146.2239874 | |
146.7695937 | |
147.3164425 | |
150.6327565 | |
151.1797912 | |
153.8182222 | |
154.3787159 | |
157.1797646 | |
157.7483306 | |
160.8613655 | |
161.4161266 | |
164.9167658 | |
165.4388617 | |
169.3368679 | |
169.8248813 | |
174.0796249 | |
174.5442191 | |
179.0850824 | |
179.5416291 | |
184.1917438 | |
184.6546498 | |
188.9606346 |
189.4368215 |
193.3331351 |
193.8135648 |
197.3459876 |
197.8094799 |
201.0216699 |
201.4593433 |
204.3784071 |
204.7989436 |
207.4372018 |
207.8575822 |
209.7758028 |
211.5177058 |
211.97 |
213.9404162 |
214.4166379 |
216.1620071 |
216.6362909 |
218.1973088 |
218.65 |
219.8301179 |
220.9085442 |
221.3494087 |
222.5022753 |
222.9648823 |
223.942778 |
224.447031 |
225.2033005 |
225.7308088 |
226.2538888 |
226.7658899 |
227.2666029 |
227.7614083 |
228.2566825 |
228.7621227 |
229.288009 |
229.8396465 |
230.4184087 |
231.0145153 |
231.5894789 |
232.1999252 |
232.771839 |
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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Sample: SiNP3N | Sample:
Operator: NHA | Operator:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.S | File:
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ Measured | Sample Mass:
Cold Free Spa32.3094 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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| Cumulative Surface Area vs. Energy
|
Surface Energy Distribution by Modified Density Function |
Model: N2 @ 77K, Surface Energy Distribution | Cumulative Surface Area
Method: Non-negative Regularization: 0.00000 | Energy (e/k)
| 20
| 22
| 24
| 26
Standard Deviation of Fit: 0.06582 cm³/g STP | 28
| 30
| 32
Isotherm Table | 34
Relative Pressure | 36
(P/Po) Experimental Fitted Quantit Absolute ResidRelative Resid| 38
0.011220185 36.41957841 36.22324886 0.196329551 0.005390769 | 40
0.011885022 36.58363642 36.45497475 0.128661672 0.003516919 | 42
0.012589254 36.75734568 36.68733519 0.070010376 0.001904667 | 44
0.013335214 36.94125878 36.92096012 0.020298656 0.000549485 | 46
0.014125375 37.13595661 37.15651399 -0.02055738 -0.00055357 | 48
0.014962357 37.3420492 37.39468822 -0.05263902 -0.00140964 | 50
0.015848932 37.56017632 37.63628889 -0.07611257 -0.00202642 | 52
0.01678804 37.7910079 37.88213417 -0.09112627 -0.00241132 | 54
0.017782794 38.03524422 38.1331818 -0.09793758 -0.00257492 | 56
0.018836491 38.29361585 38.3904778 -0.09686196 -0.00252945 | 58
0.019952623 38.56688313 38.65525262 -0.0883695 -0.00229133 | 60
0.02113489 38.85583522 38.92890162 -0.0730664 -0.00188045 | 62
0.022387211 39.16128852 39.21312747 -0.05183895 -0.00132373 | 64
0.023713737 39.48408442 39.50995891 -0.02587449 -0.00065531 | 66
0.025118864 39.82508606 39.82191324 0.003172816 7.96686E-05 | 68
0.026607251 40.18517406 40.15220808 0.032965979 0.000820352 | 70
0.028183829 40.56524088 40.50504526 0.060195612 0.001483921 | 72
0.029853826 40.96618356 40.88591614 0.080267422 0.001959358 | 74
0.031622777 41.38889447 41.30178572 0.087108747 0.002104641 | 76
0.033496544 41.83424968 41.75959647 0.074653205 0.0017845 | 78
0.035481339 42.30309441 42.26042312 0.042671292 0.001008704 | 80
0.03758374 42.79622508 42.79267593 0.003549156 8.29315E-05 | 82
0.039810717 43.31436708 43.34048398 -0.0261169 -0.00060296 | 84
0.04216965 43.85814756 43.89807346 -0.0399259 -0.00091034 | 86
0.044668359 44.42806219 44.46850688 -0.04044469 -0.00091034 | 88
0.047315126 45.02443465 45.05724902 -0.03281437 -0.00072881 | 90
0.050118723 45.64736744 45.66905223 -0.02168479 -0.00047505 | 92
0.053088444 46.29668234 46.30719556 -0.01051322 -0.00022708 | 94
0.056234133 46.97184842 46.97364706 -0.00179864 -3.82919E-05 | 96
0.059566214 47.67189515 47.66926237 0.002632779 5.5227E-05 | 98
0.063095734 48.39530785 48.39295266 0.002355192 4.86657E-05 | 100
0.066834392 49.13990184 49.14065142 -0.00074958 -1.52541E-05 |
0.070794578 49.90267131 49.90804678 -0.00537546 -0.00010772 |
0.074989421 50.67960803 50.69101711 -0.01140908 -0.00022512 |
0.079432823 51.4654839 51.47860398 -0.01312008 -0.00025493 |
0.084139514 52.25359068 52.25404446 -0.00045378 -8.68418E-06 |
0.089125094 53.03542837 53.00741429 0.028014078 0.000528214 |
0.094406088 53.80033258 53.7393009 0.061031679 0.001134411 |
0.1 54.53502914 54.45580658 0.07922256 0.001452691 |
0.105925373 55.22310202 55.16457211 0.058529918 0.001059881 |
0.112201845 55.87897205 55.87352745 0.005444598 9.74354E-05 |
0.118850223 56.56682144 56.59076831 -0.02394686 -0.00042334 |
0.125892541 57.29043797 57.32486439 -0.03442642 -0.00060091 |
0.133352143 58.05137077 58.08478003 -0.03340926 -0.00057551 |
0.141253754 58.85119849 58.87886252 -0.02766403 -0.00047007 |
0.149623566 59.69152483 59.71214428 -0.02061945 -0.00034543 |
0.158489319 60.57397329 60.58500112 -0.01102783 -0.00018206 |
0.167880402 61.50018112 61.49779457 0.002386547 3.88054E-05 |
0.177827941 62.47179239 62.45639579 0.015396593 0.000246457 |
0.188364909 63.49045009 63.47 0.020393917 0.000321212 |
0.199526231 64.5577874 64.54389856 0.013888844 0.000215138 |
0.211348904 65.67541782 65.67462902 0.000788792 1.20105E-05 |
0.223872114 66.84659731 66.85747019 -0.01087288 -0.00016265 |
0.237137371 68.07871968 68.09515796 -0.01643827 -0.00024146 |
0.251188643 69.38018013 69.39755445 -0.01737431 -0.00025042 |
0.266072506 70.76152851 70.77866185 -0.01713334 -0.00024213 |
0.281838293 72.23602435 72.2550516 -0.01902725 -0.0002634 |
0.298538262 73.82042775 73.84152708 -0.02109933 -0.00028582 |
0.316227766 75.54319636 75.54996925 -0.00677289 -8.96556E-05 |
0.334965439 77.4206262 77.39616687 0.024459331 0.000315928 |
0.354813389 79.45901601 79.39770706 0.061308956 0.00077158 |
0.375837404 81.66293859 81.57204507 0.090893526 0.001113033 |
0.398107171 84.03455254 83.95966438 0.074888165 0.000891159 |
0.421696503 86.61491563 86.62508866 -0.01017303 -0.00011745 |
0.446683592 89.55022803 89.62409862 -0.07387059 -0.00082491 |
0.473151259 92.8504401 92.97530161 -0.1248615 -0.00134476 |
0.501187234 96.50081004 96.65242994 -0.1516199 -0.00157118 |
0.530884444 100.5277554 100.6126918 -0.0849364 -0.00084491 |
0.562341325 105.1138723 104.8629219 0.250950346 0.002387414 |
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NHA | Operator: NHA
| Submitter:
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umulative Surface Area vs. Energy | Incremental Surface Area vs. Energy
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umulative Surface Area | Incremental Surface Area
Cumulative Surface Area (m²/g) | Energy (e/k) Incremental Surface Area (m²/g)
188.0154242 | 20 188.0154242
188.0154242 | 22 0
188.0154242 | 24 0
188.0154242 | 26 0
188.0154242 | 28 0
188.0154242 | 30 0
238.3560857 | 32 50.34066151
238.3560857 | 34 0
238.3560857 | 36 0
238.3560857 | 38 0
238.3560857 | 40 0
238.3560857 | 42 0
238.3560857 | 44 0
330.8285844 | 46 92.47249864
330.8285844 | 48 0
330.8285844 | 50 0
330.8285844 | 52 0
330.8285844 | 54 0
352.1352976 | 56 21.30671319
352.1352976 | 58 0
359.1755153 | 60 7.040217773
359.1755153 | 62 0
378.7955223 | 64 19.62
378.7955223 | 66 0
378.7955223 | 68 0
389.2062708 | 70 10.41074853
389.2062708 | 72 0
389.2062708 | 74 0
389.2062708 | 76 0
389.2062708 | 78 0
389.2062708 | 80 0
389.2062708 | 82 0
406.3725119 | 84 17.16624108
406.3725119 | 86 0
412.6462851 | 88 6.273773178
412.6462851 | 90 0
412.6462851 | 92 0
412.6462851 | 94 0
412.6462851 | 96 0
412.6462851 | 98 0
426.1429272 | 100 13.49664212
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| Sample: SiNP3N |
| Operator: NHA |
| Submitter: |
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| Automatic DegNo |
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| Differential Surface Area vs. Energy |
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| Differential Surface Area |
face Area (m²/g) | Energy (e/k) Differential Surface Area (m²/g-K) |
| 20 94.00771212 |
| 22 0 |
| 24 0 |
| 26 0 |
| 28 0 |
| 30 0 |
| 32 25.17033075 |
| 34 0 |
| 36 0 |
| 38 0 |
| 40 0 |
| 42 0 |
| 44 0 |
| 46 46.23624932 |
| 48 0 |
| 50 0 |
| 52 0 |
| 54 0 |
| 56 10.6533566 |
| 58 0 |
| 60 3.520108886 |
| 62 0 |
| 64 9.81 |
| 66 0 |
| 68 0 |
| 70 5.205374267 |
| 72 0 |
| 74 0 |
| 76 0 |
| 78 0 |
| 80 0 |
| 82 0 |
| 84 8.58312054 |
| 86 0 |
| 88 3.136886589 |
| 90 0 |
| 92 0 |
| 94 0 |
| 96 0 |
| 98 0 |
| 100 6.748321061 |
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Goodness of Fit | Goodness of Fit
Standard Deviation of Fit: 0.06582 cm³/g STP | Standard Deviation of Fit: 0.06582 cm³/g STP
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Input Data Model Fit | Input Data
Relative PressQuantity AdsoRelative PressQuantity Adso| Relative PressQuantity Adso
0.010688695 36.28838566 0.011220185 36.22324886 | 0.010688695 36.28838566
0.107216454 55.36015678 0.011885022 36.45497475 | 0.107216454 55.36015678
0.212697862 65.80209914 0.012589254 36.68733519 | 0.212697862 65.80209914
0.296486624 73.62407577 0.013335214 36.92096012 | 0.296486624 73.62407577
0.406271523 84.91082142 0.014125375 37.15651399 | 0.406271523 84.91082142
0.498046433 96.08583999 0.014962357 37.39468822 | 0.498046433 96.08583999
0.60548947 112.2580179 0.015848932 37.63628889 | 0.60548947 112.2580179
0.707751304 131.2188895 0.01678804 37.88213417 | 0.707751304 131.2188895
0.794603769 147.7759088 0.017782794 38.1331818 | 0.794603769 147.7759088
0.903093679 181.8617453 0.018836491 38.3904778 | 0.903093679 181.8617453
0.988631078 232.1851007 0.019952623 38.65525262 | 0.988631078 232.1851007
0.02113489 38.92890162 |
0.022387211 39.21312747 |
0.023713737 39.50995891 |
0.025118864 39.82191324 |
0.026607251 40.15220808 |
0.028183829 40.50504526 |
0.029853826 40.88591614 |
0.031622777 41.30178572 |
0.033496544 41.75959647 |
0.035481339 42.26042312 |
0.03758374 42.79267593 |
0.039810717 43.34048398 |
0.04216965 43.89807346 |
0.044668359 44.46850688 |
0.047315126 45.05724902 |
0.050118723 45.66905223 |
0.053088444 46.30719556 |
0.056234133 46.97364706 |
0.059566214 47.66926237 |
0.063095734 48.39295266 |
0.066834392 49.14065142 |
0.070794578 49.90804678 |
0.074989421 50.69101711 |
0.079432823 51.47860398 |
0.084139514 52.25404446 |
0.089125094 53.00741429 |
0.094406088 53.7393009 |
0.1 54.45580658 |
0.105925373 55.16457211 |
0.112201845 55.87352745 |
0.118850223 56.59076831 |
0.125892541 57.32486439 |
0.133352143 58.08478003 |
0.141253754 58.87886252 |
0.149623566 59.71214428 |
0.158489319 60.58500112 |
0.167880402 61.49779457 |
0.177827941 62.45639579 |
0.188364909 63.47 |
0.199526231 64.54389856 |
0.211348904 65.67462902 |
0.223872114 66.85747019 |
0.237137371 68.09515796 |
0.251188643 69.39755445 |
0.266072506 70.77866185 |
0.281838293 72.2550516 |
0.298538262 73.84152708 |
0.316227766 75.54996925 |
0.334965439 77.39616687 |
0.354813389 79.39770706 |
0.375837404 81.57204507 |
0.398107171 83.95966438 |
0.421696503 86.62508866 |
0.446683592 89.62409862 |
0.473151259 92.97530161 |
0.501187234 96.65242994 |
0.530884444 100.6126918 |
0.562341325 104.8629219 |
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| Sample: SiNP3N
| Operator: NHA
| Submitter:
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| Automatic DegNo
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| Dubinin Reports
ion of Fit: 0.06582 cm³/g STP |
| 4035- Cannot calculate optimized Astakhov exponent:
Model Fit | 4031- Not enough points with a relative pressure in the r
Relative PressQuantity Adso| 4026- Cannot calculate Dubinin-Astakhov: bad least squa
0.011220185 36.22324886 | 1017- (INTERNAL) Cannot calculate Radushkevich: bad le
0.011885022 36.45497475 |
0.012589254 36.68733519 |
0.013335214 36.92096012 |
0.014125375 37.15651399 |
0.014962357 37.39468822 |
0.015848932 37.63628889 |
0.01678804 37.88213417 |
0.017782794 38.1331818 |
0.018836491 38.3904778 |
0.019952623 38.65525262 |
0.02113489 38.92890162 |
0.022387211 39.21312747 |
0.023713737 39.50995891 |
0.025118864 39.82191324 |
0.026607251 40.15220808 |
0.028183829 40.50504526 |
0.029853826 40.88591614 |
0.031622777 41.30178572 |
0.033496544 41.75959647 |
0.035481339 42.26042312 |
0.03758374 42.79267593 |
0.039810717 43.34048398 |
0.04216965 43.89807346 |
0.044668359 44.46850688 |
0.047315126 45.05724902 |
0.050118723 45.66905223 |
0.053088444 46.30719556 |
0.056234133 46.97364706 |
0.059566214 47.66926237 |
0.063095734 48.39295266 |
0.066834392 49.14065142 |
0.070794578 49.90804678 |
0.074989421 50.69101711 |
0.079432823 51.47860398 |
0.084139514 52.25404446 |
0.089125094 53.00741429 |
0.094406088 53.7393009 |
0.1 54.45580658 |
0.105925373 55.16457211 |
0.112201845 55.87352745 |
0.118850223 56.59076831 |
0.125892541 57.32486439 |
0.133352143 58.08478003 |
0.141253754 58.87886252 |
0.149623566 59.71214428 |
0.158489319 60.58500112 |
0.167880402 61.49779457 |
0.177827941 62.45639579 |
0.188364909 63.47 |
0.199526231 64.54389856 |
0.211348904 65.67462902 |
0.223872114 66.85747019 |
0.237137371 68.09515796 |
0.251188643 69.39755445 |
0.266072506 70.77866185 |
0.281838293 72.2550516 |
0.298538262 73.84152708 |
0.316227766 75.54996925 |
0.334965439 77.39616687 |
0.354813389 79.39770706 |
0.375837404 81.57204507 |
0.398107171 83.95966438 |
0.421696503 86.62508866 |
0.446683592 89.62409862 |
0.473151259 92.97530161 |
0.501187234 96.65242994 |
0.530884444 100.6126918 |
0.562341325 104.8629219 |
|
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| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNP3N
| Operator: NHA
| Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N.SMP
|
|
| Started: 1/24/2019 3:1 Analysis AdsorN2
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
| Report Time: 1/24/2019 7:1 Thermal CorrecNo
| Sample Mass:0.2927 g Warm Free Sp11.1935 cm³ Measured
| Cold Free Spa32.3094 cm³ Equilibration In5 s
| Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
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| MP Tabular Report
|
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
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| Total Pore Sur232.9974 m²/g
| Density Conver0.0015468
|
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| Pore HydraulicAverage Pore Incremental PoCumulative PoDifferential P Incremental Po
| 0.000 - 0.745 0.37262369 0 0 0 0
| 0.745 - 0.760 0.75262369 -0.02205076 -0.02205076 -1.49470155 -29.2985232
| 0.760 - 0.780 0.77 0.002864946 -0.01918582 0.143247308 3.720709308
| 0.780 - 0.800 0.79 0.006488081 -0.01269774 0.324404067 8.212761198
| 0.800 - 0.820 0.81 0.010140942 -0.00255679 0.507047115 12.51968186
| 0.820 - 0.840 0.83 0.01396608 0.011409287 0.698304005 16.82660253
| 0.840 - 0.860 0.85 0.017963495 0.029372782 0.898174736 21.1335232
| 0.860 - 0.880 0.87 0.02004425 0.049417035 1.00221263 23.03937079
| 0.880 - 0.900 0.89 0.004671067 0.054088102 0.233553368 5.248390286
| 0.900 - 0.920 0.91 0.000625833 0.054713935 0.031291673 0.687729078
| 0.920 - 0.940 0.93 0.000575029 0.055288965 0.028751468 0.618311136
| 0.940 - 0.960 0.95 0.000521449 0.055810413 0.026072427 0.548893194
| 0.960 - 0.980 0.97 0.000465091 0.056275504 0.02325455 0.479475253
| 0.980 - 1.000 0.99 0.000405957 0.056681461 0.020297837 0.410056152
| 1.000 - 1.020 1.01 0.000344046 0.057025507 0.017202288 0.34063937
| 1.020 - 1.040 1.03 -0.00109388 0.05593163 -0.05469384 -1.0620164
| 1.040 - 1.060 1.05 -0.00290565 0.053025978 -0.14528261 -2.76728781
| 1.060 - 1.080 1.07 -0.00227972 0.050746262 -0.11398577 -2.13057507
| 1.080 - 1.100 1.09 -0.00160065 0.049145616 -0.08003204 -1.46848282
| 1.100 - 1.120 1.11 -0.00089509 0.048250523 -0.04475468 -0.80639056
| 1.120 - 1.140 1.13 -0.00016306 0.048087466 -0.00815285 -0.1442983
| 1.140 - 1.160 1.15 0.000595463 0.048682929 0.029773152 0.517793952
| 1.160 - 1.180 1.17 0.001380467 0.050063324 0.069023343 1.179886208
| 1.180 - 1.200 1.19 0.002191954 0.05225535 0.109597719 1.841978464
| 1.200 - 1.220 1.21 0.003029926 0.055285275 0.151496279 2.50407072
| 1.220 - 1.240 1.23 0.00389438 0.059179656 0.194719023 3.166162976
| 1.240 - 1.260 1.25 0.004785319 0.063964975 0.239265952 3.828255232
| 1.260 - 1.280 1.27 0.005702741 0.069667716 0.285137066 4.490347488
| 1.280 - 1.300 1.29 0.006646647 0.076314363 0.332332364 5.152439744
| 1.300 - 1.320 1.31 0.007617037 0.0839314 0.380851846 5.814532001
| 1.320 - 1.340 1.33 0.008505382 0.092436782 0.425269079 6.395023744
| 1.340 - 1.360 1.35 0.003326092 0.095762874 0.166304596 2.46377179
| 1.360 - 1.380 1.37 2.99821E-15 0.095762874 1.4991E-13 2.18847E-12
| 1.380 - 1.400 1.39 0 0.095762874 0 0
| 1.400 - 1.420 1.41 -3.08574E-15 0.095762874 -1.54287E-13 -2.18847E-12
| 1.420 - 1.440 1.43 3.12951E-15 0.095762874 1.56476E-13 2.18847E-12
| 1.440 - 1.460 1.45 0 0.095762874 0 0
| 1.460 - 1.480 1.47 -3.21705E-15 0.095762874 -1.60852E-13 -2.18847E-12
| 1.480 - 1.500 1.49 3.26082E-15 0.095762874 1.63041E-13 2.18847E-12
| 1.500 - 1.520 1.51 -3.30459E-15 0.095762874 -1.65229E-13 -2.18847E-12
| 1.520 - 1.540 1.53 3.34836E-15 0.095762874 1.67418E-13 2.18847E-12
| 1.540 - 1.560 1.55 0 0.095762874 0 0
| 1.560 - 1.580 1.57 -3.4359E-15 0.095762874 -1.71795E-13 -2.18847E-12
| 1.580 - 1.600 1.59 3.47967E-15 0.095762874 1.73983E-13 2.18847E-12
| 1.600 - 1.620 1.61 0 0.095762874 0 0
| 1.620 - 1.640 1.63 -3.5672E-15 0.095762874 -1.7836E-13 -2.18847E-12
| 1.640 - 1.660 1.65 3.61098E-15 0.095762874 1.80549E-13 2.18847E-12
| 1.660 - 1.680 1.67 0 0.095762874 0 0
| 1.680 - 1.700 1.69 -3.69851E-15 0.095762874 -1.84925E-13 -2.18847E-12
| 1.700 - 1.720 1.71 3.74229E-15 0.095762874 1.87114E-13 2.18847E-12
| 1.720 - 1.740 1.73 -3.78605E-15 0.095762874 -1.89303E-13 -2.18847E-12
| 1.740 - 1.760 1.75 3.82982E-15 0.095762874 1.91491E-13 2.18847E-12
| 1.760 - 1.780 1.77 0 0.095762874 0 0
| 1.780 - 1.800 1.79 -3.91736E-15 0.095762874 -1.95868E-13 -2.18847E-12
| 1.800 - 1.820 1.81 3.96113E-15 0.095762874 1.98056E-13 2.18847E-12
| 1.820 - 1.840 1.83 -4.00489E-15 0.095762874 -2.00245E-13 -2.18847E-12
| 1.840 - 1.860 1.85 4.04867E-15 0.095762874 2.02434E-13 2.18847E-12
| 1.860 - 1.880 1.87 0 0.095762874 0 0
| 1.880 - 1.900 1.89 0.068336677 0.164099551 3.416833847 36.15697192
|
|
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| Options Report | Sample log
| |
| | Date
| | 1/24/2019
| Analysis Conditions | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| Preparation | 1/24/2019
| | 1/24/2019
| Fast evacuatioNo |
| Evacuation rat5.0 mmHg/s |
| Evacuation tim0.10 h |
| Leak test: No |
| Use TranSeal:No |
| |
| |
| Free Space |
| |
| Measured |
| Lower dewar foYes |
| Evacuation tim0.10 h |
| Outgas test: No |
| |
| |
| Po and Temperature |
| |
| Po and T type:Enter Po below. Enter the Analysis Bath T |
| Po: 760.000 mmHg |
| Temperature: -195.850 °C |
| |
| |
| Dosing |
| |
| Use first pressNo |
| Use maximumNo v |
| Target toleran 5.0% or 5.000 mmHg |
| |
| |
| Equilibration |
| |
| Equilibration 5 s |
| Minimum equili600 s |
| |
| |
| Sample Backfill |
| |
| Backfill at star Yes |
| Backfill at end Yes |
| Backfill gas: N2 |
| |
| |
| Adsorptive Properties |
| |
| Adsorptive: Nitrogen |
| Maximum manif 1,050.00 mmHg |
| Non-ideality fa0.0000620 |
| Density conver0.0015468 |
| Therm. tran. h 0.38600 nm |
| Molecular cros0.162 nm² |
| Adsorbate Mol2.00 |
| |
| |
| Inside diamete9.53 mm |
| |
| |
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|
|
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNP3N
|
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|
|
| Validation Report
|
Time Log Message |
3:11:07 PM Started analysis of file SiNP |
3:11:07 PM System volume: 18.1544 cm³| Isotherm Reports
3:22:31 PM Pressure transducer zeroed. |
3:22:31 PM Helium Purged: 30 seconds | Free Space: Low free space values may be
3:30:18 PM Measured free space on port| observed when using liquid argon or ice baths.
3:41:17 PM Pressure transducer zeroed. |
7:14:39 PM Finished a sample analysis | Po Passed
|
|
| Pressure/Volu Passed
|
|
| Desorption Not within limits. Increase the sample mass, increase
| the equilibration interval, or check the free space.
|
|
|
|
| BET Reports
|
| C Value: Passed
|
|
| Correlation Coe
Passed
|
|
| Surface area: Passed
|
|
| Pressure RangThe selected BET relative pressure range is outside th
| recommended values of 0.05 to 0.30.
|
|
|
|
Page 1
0\data\SAMPEL\2019\Januari\SiNP3N.SMP
N2
-195.850 °C
No
11.1935 cm³ Measured
5s
1.000 g/cm³
values may be
using liquid argon or ice baths.
Increase the sample mass, increase

interval, or check the free space.
ET relative pressure range is outside the
alues of 0.05 to 0.30.

Si NP3 N

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Si NP3 N

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

Increase the sample mass, increase

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