Si02 All

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

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Sample: SiO2 | Sample:
Operator: wawan | Operator:
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File:
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Started: 1/31/2019 12: Analysis AdsorN2 | Started:
Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C | Completed:
Report Time: 7/25/2019 10: Thermal Correc No | Report Time:
Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ Measured | Sample Mass:
Cold Free Spa32.0438 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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Summary Report | Isotherm Tabular Report
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| Relative Press
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Surface Area | 0.012931432
| 0.116178332
Single point s 43.6585 m²/g | 0.209428125
| 0.300513217
BET Surface A44.3672 m²/g | 0.402673862
| 0.501120678
t-Plot Micropo 3.7000 m²/g | 0.599116155
| 0.696451609
t-Plot External 40.6672 m²/g | 0.800450054
| 0.903034652
BJH Adsorption | 0.989112292
between 1.70038.147 m²/g | 0.899949646
| 0.793429967
BJH Desorption | 0.703397249
between 1.70035.4378 m²/g | 0.599400852
| 0.487485183
D-H Adsorption | 0.409757634
between 1.70034.147 m²/g | 0.301968303
| 0.209994768
D-H Desorption | 0.11024705
between 1.70035.2607 m²/g | 0.009837572
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Pore Volume |
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Single point ad |
less than 177. 0.153786 cm³/g |
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t-Plot micropo 0.001968 cm³/g |
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BJH Adsorption |
between 1.7000.148936 cm³/g |
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BJH Desorption |
between 1.7000.146999 cm³/g |
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Pore Size |
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Adsorption ave13.86487 nm |
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BJH Adsorption
15.6169 nm |
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BJH Desorption
16.5923 nm |
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D-H Adsorption17.0490 nm |
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D-H Desorption16.5315 nm |
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Freundlich |
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Qm·C: 4.7208 ± 0.1013 cm³/g STP |
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m: 5.0005 ± 0.2755 |
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Temkin |
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q·alpha/Qm: 0.281286 ± 0.037867 kJ/mol·(cm³/g STP) |
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A: 2.2840 ± 1.4853 mmHg |
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DFT Pore Size |
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Volume in Por < 1.483 nm : 0.00457 cm³/ |
Total Volume i<= 117.233 nm : 0.15004 cm³/ |
Area in Pores > 117.233 nm : 0.000 m²/g |
Total Area in >= 1.483 nm : 20.015 m²/g |
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DFT Surface Energy |
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Total Area : 40.438 m²/g |
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Nanoparticle Size: |
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Average Partic135.2351 nm |
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Horvath-Kawazoe |
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Maximum pore0.153786 cm³/g |
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Median pore wi66.4043 nm |
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MP-Method |
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Cumulative sur |
1.89998 nm and
0.0000 m²/g |
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Cumulative po |
1.89998 nm and
0.000000 cm³/g |
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Average pore h0.00000 nm |
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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SiO2 | Sample: SiO2
wawan | Operator: wawan
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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1/31/2019 12: Analysis AdsorN2 | Started: 1/31/2019 12:
1/31/2019 7:5 Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5
7/25/2019 10: Thermal Correc No | Report Time: 7/25/2019 10:
0.1781 g Warm Free Sp11.1152 cm³ Measured | Sample Mass:0.1781 g
32.0438 cm³ Equilibration In5 s | Cold Free Spa32.0438 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
No | Automatic DegNo
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otherm Tabular Report | Isotherm Linear Plot
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Absolute Pres Quantity AdsoElapsed Time S( aturation Pr |
760 | SiO2 - Adsorption
9.827888489 7.521682702 00:36 | Relative PressQuantity Adso
88.29553223 11.2630366 00:40 | 0.012931432 7.521682702
159.1653748 12.91880126 00:42 | 0.116178332 11.2630366
228.39 14.33775115 00:44 | 0.209428125 12.91880126
306.032135 15.9250009 00:46 | 0.300513217 14.33775115
380.8517151 17.608932 00:48 | 0.402673862 15.9250009
455.3282776 19.58553313 00:50 | 0.501120678 17.608932
529.3032227 22.09115784 00:52 | 0.599116155 19.58553313
608.342041 26.22560443 00:56 | 0.696451609 22.09115784
686.3063354 36.42213023 01:02 | 0.800450054 26.22560443
751.7253418 99.42221883 01:13 | 0.903034652 36.42213023
683.961731 39.39765872 01:32 | 0.989112292 99.42221883
603.0067749 26.39537359 01:38 |
534.5819092 22.56734996 01:41 |
455.5446472 19.77524702 01:43 |
370.488739 17.51928866 01:47 |
311.415802 16.1637073 01:48 |
229.4959106 14.46555118 01:50 |
159.5960236 13.02920423 01:52 |
83.78775787 11.21571086 01:56 |
7.476554871 7.170665712 02:08 |
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Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
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| Sample: SiO2
| Operator: wawan
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu
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Analysis AdsorN2 | Started: 1/31/2019 12: Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 7/25/2019 10: Thermal CorrecNo
Warm Free Sp11.1152 cm³ M| Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ M
Equilibration In5 s | Cold Free Spa32.0438 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
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| Isotherm Log Plot
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SiO2 - Desorption | SiO2 - Adsorption SiO2 - Desorption
Relative PressQuantity Adso| Relative PressQuantity AdsoRelative PressQuantity Adso
0.989112292 99.42221883 | 0.012931432 7.521682702 0.989112292 99.42221883
0.899949646 39.39765872 | 0.116178332 11.2630366 0.899949646 39.39765872
0.793429967 26.39537359 | 0.209428125 12.91880126 0.793429967 26.39537359
0.703397249 22.56734996 | 0.300513217 14.33775115 0.703397249 22.56734996
0.599400852 19.77524702 | 0.402673862 15.9250009 0.599400852 19.77524702
0.487485183 17.51928866 | 0.501120678 17.608932 0.487485183 17.51928866
0.409757634 16.1637073 | 0.599116155 19.58553313 0.409757634 16.1637073
0.301968303 14.46555118 | 0.696451609 22.09115784 0.301968303 14.46555118
0.209994768 13.02920423 | 0.800450054 26.22560443 0.209994768 13.02920423
0.11024705 11.21571086 | 0.903034652 36.42213023 0.11024705 11.21571086
0.009837572 7.170665712 | 0.989112292 99.42221883 0.009837572 7.170665712
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| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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| Sample: SiO2 | Sample:
| Operator: wawan | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu| File:
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| Started: 1/31/2019 12: Analysis AdsorN2 | Started:
| Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C | Completed:
| Report Time: 7/25/2019 10: Thermal Correc No | Report Time:
| Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ M| Sample Mass:
| Cold Free Spa32.0438 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
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| Isotherm Linear Absolute Plot | Isotherm Log Absolute Plot
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| SiO2 - Adsorption SiO2 - Desorption | SiO2 - Adsorption
| Absolute Pres Quantity AdsoAbsolute Pres Quantity Adso| Absolute Pres
| 9.827888489 7.521682702 751.7253418 99.42221883 | 9.827888489
| 88.29553223 11.2630366 683.961731 39.39765872 | 88.29553223
| 159.1653748 12.91880126 603.0067749 26.39537359 | 159.1653748
| 228.39 14.33775115 534.5819092 22.56734996 | 228.39
| 306.032135 15.9250009 455.5446472 19.77524702 | 306.032135
| 380.8517151 17.608932 370.488739 17.51928866 | 380.8517151
| 455.3282776 19.58553313 311.415802 16.1637073 | 455.3282776
| 529.3032227 22.09115784 229.4959106 14.46555118 | 529.3032227
| 608.342041 26.22560443 159.5960236 13.02920423 | 608.342041
| 686.3063354 36.42213023 83.78775787 11.21571086 | 686.3063354
| 751.7253418 99.42221883 7.476554871 7.170665712 | 751.7253418
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
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SiO2 | Sample: SiO2
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu
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1/31/2019 12: Analysis AdsorN2 | Started: 1/31/2019 12: Analysis Adsor
1/31/2019 7:5 Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5 Analysis Bath
7/25/2019 10: Thermal Correc No | Report Time: 7/25/2019 10: Thermal Correc
0.1781 g Warm Free Sp11.1152 cm³ M| Sample Mass:0.1781 g Warm Free Sp
32.0438 cm³ Equilibration In5 s | Cold Free Spa32.0438 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
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otherm Log Absolute Plot | Isotherm Pressure Composition
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O2 - Adsorption SiO2 - Desorption | SiO2 - Adsorption SiO2 - Desorption
Quantity AdsoAbsolute Pres Quantity Adso| Weight % N2 Absolute Pres Weight % N2
7.521682702 751.7253418 99.42221883 | 0.067115634 9.827888489 0.887139959
11.2630366 683.961731 39.39765872 | 0.100499566 88.29553223 0.351543526
12.91880126 603.0067749 26.39537359 | 0.115273879 159.1653748 0.235524724
14.33775115 534.5819092 22.56734996 | 0.127935105 228.39 0.201367442
15.9250009 455.5446472 19.77524702 | 0.142098062 306.032135 0.176453634
17.608932 370.488739 17.51928866 | 0.157123703 380.8517151 0.15632382
19.58553313 311.415802 16.1637073 | 0.174760826 455.3282776 0.144228029
22.09115784 229.4959106 14.46555118 | 0.197118402 529.3032227 0.129075459
26.22560443 159.5960236 13.02920423 | 0.234009882 608.342041 0.116259
36.42213023 83.78775787 11.21571086 | 0.32499302 686.3063354 0.100077209
99.42221883 7.476554871 7.170665712 | 0.887139959 751.7253418 0.063983526
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Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
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| Sample: SiO2 |
| Operator: wawan |
| Submitter: |
0\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Janu|
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N2 | Started: 1/31/2019 12: Analysis AdsorN2 |
-195.850 °C | Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C |
No | Report Time: 7/25/2019 10: Thermal Correc No |
11.1152 cm³ M| Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ M|
5s | Cold Free Spa32.0438 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
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| BET Surface Area Report |
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| BET Surface A44.3672 ± 0.6360 m²/g |
O2 - Desorption | Slope: 0.097766 ± 0.001381 g/cm³ STP |
Absolute Pres | Y-Intercept: 0.000351 ± 0.000266 g/cm³ STP |
751.7253418 | C: 279.392190 |
683.961731 | Qm: 10.1919 cm³/g STP |
603.0067749 | Correlation Coe
0.9998004 |
534.5819092 | Molecular Cros0.1620 nm² |
455.5446472 | |
370.488739 | |
311.415802 | |
229.4959106 | |
159.5960236 | Relative PressQuantity Adso1/[Q(Po/P - 1)] |
83.78775787 | 0.012931432 7.521682702 0.001741744 |
7.476554871 | 0.116178332 11.2630366 0.011670917 |
| 0.209428125 12.91880126 0.02050555 |
| 0.300513217 14.33775115 0.029964223 |
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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Sample: SiO2 | Sample: SiO2
Operator: wawan | Operator: wawan
File: C:\TriStar II 3020\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\J
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Started: 1/31/2019 12: Analysis AdsorN2 | Started: 1/31/2019 12:
Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5
Report Time: 7/25/2019 10: Thermal Correc No | Report Time: 7/25/2019 10:
Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ M| Sample Mass:0.1781 g
Cold Free Spa32.0438 cm³ Equilibration In5 s | Cold Free Spa32.0438 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
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BET Surface Area Plot | BET Isotherm Plot
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SiO2 Not Fitted | SiO2
Relative Press1/[Q(Po/P - 1)]Relative Press1/[Q(Po/P - 1)]| Relative PressQuantity Adso
0.012931432 0.001741744 | 0.012931432 7.521682702
0.116178332 0.011670917 | 0.116178332 11.2630366
0.209428125 0.02050555 | 0.209428125 12.91880126
0.300513217 0.029964223 | 0.300513217 14.33775115
| 0.402673862 15.9250009
| 0.501120678 17.608932
| 0.599116155 19.58553313
| 0.696451609 22.09115784
| 0.800450054 26.22560443
| 0.903034652 36.42213023
| 0.989112292 99.42221883
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| Sample: SiO2
| Operator: wawan
| Submitter:
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| Automatic DegNo
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| Langmuir Reports
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| Primary Data
SiO2 - BET Equation |
Relative PressQuantity Adso|
0.012931432 8.109762119 |
0.116178332 11.22590993 |
0.209428125 12.71989162 |
0.300513217 14.45007813 |
0.402673862 16.97235257 |
0.501120678 20.35696698 |
0.599116155 25.36272314 |
0.696451609 33.52342591 |
0.800450054 51.02868103 |
0.903034652 105.0678536 |
0.989112292 936.0514437 |
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| Freundlich Tabular Report | Freundlich Plot
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| Qm·C: 4.7208 ± 0.1013 cm³/g STP |
| m: 5.0005 ± 0.2755 | SiO2
| Correlation Coe
0.996979 | log(P)
| | 0.99246022
| | 1.945938729
| | 2.201848596
| | 2.35867717
| Absolute Pres Quantity Adsolog(P) log(Q) |
| 9.827888489 7.521682702 0.99246022 0.876315009 |
| 88.29553223 11.2630366 1.945938729 1.051655495 |
| 159.1653748 12.91880126 2.201848596 1.111222217 |
| 228.39 14.33775115 2.35867717 1.156481038 |
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SiO2 | Sample: SiO2
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reundlich Plot | Temkin Tabular Report
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| q·alpha/Qm: 0.281286 ± 0.037867 kJ/mol·(cm³/g STP)
| A: 2.2840 ± 1.4853 1/mmHg
log(Q) | Correlation Coe
0.973876
0.876315009 |
1.051655495 |
1.111222217 |
1.156481038 |
| Absolute Pres Quantity Adsoln(P)
| 9.827888489 7.521682702 2.285224108
| 88.29553223 11.2630366 4.480689509
| 159.1653748 12.91880126 5.069943755
| 228.39 14.33775115 5.431054892
| 306.032135 15.9250009 5.723690113
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| Sample: SiO2 |
| Operator: wawan |
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| Automatic DegNo |
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| Temkin Plot |
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7867 kJ/mol·(cm³/g STP) | |
| SiO2 |
| ln(P) Quantity Adsorbed (cm³/g STP) |
| 2.285224108 7.521682702 |
| 4.480689509 11.2630366 |
| 5.069943755 12.91880126 |
| 5.431054892 14.33775115 |
| 5.723690113 15.9250009 |
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t-Plot Report | t-Plot
| Harkins and Jura
Micropore Vol 0.001968 cm³/g |
Micropore Area3.7000 m²/g | SiO2
External Surfa40.6672 m²/g | Thickness (nmQuantity Adso
Slope: 26.291177 ± 0.000000 cm³/g·nm STP | 0.379992489 11.2630366
Y-Intercept: 1.272587 ± 0.000000 cm³/g STP | 0.442970447 12.91880126
Correlation Coe 1.000000 |
Surface Area C1.000 |
Density Conver0.0015468 |
Total Surface 44.3672 m²/g |
Thickness Ran0.35000 nm to 0.50000 nm |
Thickness Equa Harkins and Jura |
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Thickness Curve |
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t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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t-Plot Report - Data |
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Relative PressStatistical Thi Quantity AdsoFitted |
0.012931432 0.269769126 7.521682702 |
0.116178332 0.379992489 11.2630366 * |
0.209428125 0.442970447 12.91880126 * |
0.300513217 0.501554566 14.33775115 |
0.402673862 0.571027002 15.9250009 |
0.501120678 0.647139828 17.608932 |
0.599116155 0.738540831 19.58553313 |
0.696451609 0.855594976 22.09115784 |
0.800450054 1.034732178 26.22560443 |
0.903034652 1.336719312 36.42213023 |
0.989112292 1.899976995 99.42221883 |
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| Sample: SiO2
| Operator: wawan
| Submitter:
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| Automatic DegNo
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| Alpha-S Method
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| 4029- At least two fitted data points are needed for Alpha
Not Fitted |
Thickness (nmQuantity Adso|
0.269769126 7.521682702 |
0.501554566 14.33775115 |
0.571027002 15.9250009 |
0.647139828 17.608932 |
0.738540831 19.58553313 |
0.855594976 22.09115784 |
1.034732178 26.22560443 |
1.336719312 36.42213023 |
1.899976995 99.42221883 |
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| f-Ratio Method | BJH Adsorption Pore Distribution Repor
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| Primary Data |
| A reference file has not been chosen. |
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| Diameter Rang
| Adsorbate Prop
| Density Conver
| Fraction of Po
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| Pore Diameter
| 177.8 - 21.3
| 21.3 - 10.6
| 10.6 - 6.9
| 6.9 - 5.1
| 5.1 - 4.0
| 4.0 - 3.2
| 3.2 - 2.5
| 2.5 - 2.0
| 2.0 - 1.6
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TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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SiO2 | Sample:
wawan | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File:
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1/31/2019 12: Analysis AdsorN2 | Started:
1/31/2019 7:5 Analysis Bath -195.850 °C | Completed:
7/25/2019 10: Thermal Correc No | Report Time:
0.1781 g Warm Free Sp11.1152 cm³ Measured | Sample Mass:
32.0438 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
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JH Adsorption Pore Distribution Report | BJH Desorption Pore Distribution Repo
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Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
0.00 | Fraction of Po
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Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
23.1345507 0.123798834 0.123798834 21.40501208 21.40501208 | 177.8 - 20.6
12.46941942 0.014132481 0.137931315 4.533484767 25.93849685 | 20.6 - 10.2
7.933806682 0.003456199 0.141387514 1.742517407 27.68101425 | 10.2 - 7.0
5.733151995 0.001594858 0.142982373 1.112727112 28.79374137 | 7.0 - 5.1
4.399088865 0.001216412 0.144198784 1.106057708 29.89979907 | 5.1 - 3.8
3.474686398 0.001051964 0.145250748 1.211003444 31.11080252 | 3.8 - 3.2
2.76322826 0.001044075 0.146294824 1.511384767 32.62218729 | 3.2 - 2.5
2.222607282 0.001083989 0.147378813 1.950842381 34.57302967 | 2.5 - 2.0
1.742530377 0.001557064 0.148935877 3.574259283 38.14728895 |
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SiO2 | Sample:
wawan | Operator:
| Submitter:
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No | Automatic Deg
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JH Desorption Pore Distribution Report | Dollimore-Heal Adsorption Pore Distribu
|
Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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| Diameter Rang
1.7000 nm to 300.0000 nm | Adsorbate Prop
0.95300 nm | Density Conver
0.0015468 |
0.00 |
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| Pore Diameter
| 177.9 - 21.4
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| 21.4 - 10.6
22.35935933 0.118258113 0.118258113 21.15590365 21.15590365 | 10.6 - 7.0
12.01168474 0.020363475 0.138621588 6.781221872 27.93712552 | 7.0 - 5.2
8.003603536 0.003187361 0.141808949 1.592963038 29.53007813 | 5.2 - 4.1
5.733138021 0.001570016 0.143378965 1.095397343 30.62548591 | 4.1 - 3.2
4.25881064 0.001111653 0.144490618 1.044097443 31.66958335 | 3.2 - 2.6
3.439776551 0.000722575 0.145213194 0.840258444 32.50984179 | 2.6 - 2.1
2.745852218 0.000900272 0.146113465 1.311464145 33.82130594 | 2.1 - 1.6
2.190290285 0.000885128 0.146998593 1.616457323 35.43776326 |
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SiO2 | Sample:
wawan | Operator:
| Submitter:
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No | Automatic Deg
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|
ollimore-Heal Adsorption Pore Distribution Report | Dollimore-Heal Desorption Pore Distribu
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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|
1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
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|
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
99.63288092 0.101711315 0.101711315 4.083443682 4.083443682 | 177.9 - 20.7
15.99669076 0.018412133 0.120123447 4.603985429 8.687429111 | 20.7 - 10.3
8.806277104 0.00725503 0.127378478 3.295390379 11.98281949 | 10.3 - 7.1
6.088740034 0.004317679 0.131696157 2.836501055 14.81932054 | 7.1 - 5.2
4.625263198 0.003380718 0.135076875 2.923697515 17.74301806 | 5.2 - 3.9
3.645191109 0.002838664 0.137915539 3.114968959 20.85798702 | 3.9 - 3.3
2.912933691 0.002607702 0.140523241 3.580860099 24.43884712 | 3.3 - 2.6
2.346775237 0.002333225 0.142856466 3.976903535 28.41575065 | 2.6 - 2.1
1.87525618 0.00268694 0.145543405 5.731355337 34.14710599 | 2.1 - 1.6
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SiO2 | Sample:
wawan | Operator:
| Submitter:
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No | Automatic Deg
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|
ollimore-Heal Desorption Pore Distribution Report | Horvath-Kawazoe Report
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
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|
| Maximum Pore
1.7000 nm to 300.0000 nm | at Relative Pr
0.95300 nm | Median Pore W
0.0015468 | Relative Press
|
| Diameter of Ad
| Diameter of Ad
| Diameter of S
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Diameter of Sa
99.31705071 0.096845982 0.096845982 3.900477547 3.900477547 | Interaction Pa
15.50304078 0.024032603 0.120878585 6.200745605 10.10122315 |
8.712573454 0.006690392 0.127568977 3.071603133 13.17282628 | Density Conver
6.174880078 0.004608353 0.13217733 2.985226077 16.15805236 |
4.563024763 0.003624773 0.135802103 3.177517756 19.33557012 |
3.606514559 0.002233173 0.138035275 2.476820764 21.81239088 |
2.942665687 0.002636688 0.140671963 3.584080312 25.39647119 |
2.352341788 0.002227608 0.14289957 3.787897715 29.18436891 | Absolute Pres
1.861769673 0.002828191 0.145727762 6.076350311 35.26071922 | 9.827888489
| 88.29553223
| 159.1653748
| 228.39
| 306.032135
| 380.8517151
| 455.3282776
| 529.3032227
| 608.342041
| 686.3063354
| 751.7253418
|
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SiO2 | Sample:
wawan | Operator:
| Submitter:
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No | Automatic Deg
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|
orvath-Kawazoe Report |
|
Slit Pore Geometry (Original H-K) |
|
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|
|
0.153786 cm³/g |
0.989112292 |
66.4043 nm |
1.293e-002 to 9.891e-001 | Volume in Por
| Total Volume i
0.3000 nm | Area in Pores
0.2574 nm | Total Area in
0.3040 nm |
0.2609 nm |
3.49e-043 erg·cm^4 | Pore Size Table
|
0.0015468 | Pore Width (n
| 1.483289338
| 1.590515054
| 1.715611708
| 1.8585793
Relative PressQuantity AdsoPore Width (n Cumulative PoDifferential P | 2.001546978
0.012931432 7.521682702 1.06859 0.011634539 0.010887748 | 2.16238568
0.116178332 11.2630366 1.88665364 0.017421665 0.007074176 | 2.341095234
0.209428125 12.91880126 2.489083391 0.019982802 0.004251345 | 2.519804789
0.300513217 14.33775115 3.151044155 0.022177633 0.003315652 | 2.734256221
0.402673862 15.9250009 4.066630856 0.024632791 0.002681513 | 2.948707652
0.501120678 17.608932 5.259813079 0.027237496 0.00218299 | 3.181030107
0.599116155 19.58553313 6.984595134 0.030294903 0.001772634 | 3.431223586
0.696451609 22.09115784 9.76154988 0.034170603 0.001395666 | 3.699287918
0.800450054 26.22560443 15.70022431 0.040565765 0.001076867 | 4.003093956
0.903034652 36.42213023 34.26512451 0.056337751 0.000849559 | 4.324771359
0.989112292 99.42221883 290.0766459 0.153786288 0.000380939 | 4.664319445
| 5.039609578
| 5.432770394
| 5.879544281
| 6.344189191
| 6.844575808
| 7.398575836
| 7.98831723
| 8.631671354
| 9.310767526
| 10.06134779
| 10.86554079
| 11.72334651
| 12.65263702
| 13.67128093
| 14.76140894
| 15.94089173
| 17.20973066
| 18.58579369
| 20.06908354
| 21.65959748
| 23.39307962
| 25.25166062
| 27.27107913
| 29.45133516
| 31.79242869
| 34.33010654
| 37.06436055
| 40.03094025
| 43.22984018
| 46.67893786
| 50.39609442
| 54.4170594
| 58.75969939
| 63.44189191
| 68.49937012
| 73.96788359
| 79.86529889
| 86.24523218
| 93.12554458
| 100.5598686
| 108.5660545
| 117.2334679
|
|
|
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
SiO2 | Sample: SiO2
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
1/31/2019 12: Analysis AdsorN2 | Started: 1/31/2019 12:
1/31/2019 7:5 Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5
7/25/2019 10: Thermal Correc No | Report Time: 7/25/2019 10:
0.1781 g Warm Free Sp11.1152 cm³ Measured | Sample Mass:0.1781 g
32.0438 cm³ Equilibration In5 s | Cold Free Spa32.0438 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
|
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Porosity Distribution by Original Density Functional Theor | Porosity Distribution by Original Density
Model: N2 @ 77K on Carbon, Slit Pores | Model: N2 @ 77K on Carbon, Slit Pores
Method: Non-negative Regularization: 0.00000 | Method: Non-negative Regularization:
Standard Deviation of Fit: 0.54271 cm³/g STP |
|
|
|
| Standard Deviation of Fit: 0.54271 cm³/
< 1.483 nm : 0.00457 cm³/ |
<= 117.233 nm : 0.15004 cm³/ |
> 117.233 nm : 0.000 m²/g | Isotherm Table
>= 1.483 nm : 20.015 m²/g | Relative Pressure
| (P/Po) Experimental
| 0.01451552 7.593672712
ore Size Table | 0.017706521 7.738336214
| 0.02139844 7.904971523
Cumulative VoIncremental VoCumulative AreIncremental Ar| 0.02563123 8.094790884
0.004751812 0.000182389 0.245925197 0.245925197 | 0.03044224 8.308568231
0.00528922 0.000537408 0.921691434 0.675766236 | 0.035865448 8.546483571
0.005846867 0.000557647 1.571776992 0.650085449 | 0.041930798 8.807944428
0.006599996 0.000753129 2.382212284 0.810435292 | 0.048663601 9.091384002
0.007240734 0.000640737 3.022454381 0.640242097 | 0.056084011 9.394038213
0.007474831 0.000234097 3.23897154 0.216517159 | 0.064206667 9.711711296
0.007802416 0.000327586 3.518828522 0.279856983 | 0.073040441 10.03853459
0.008376415 0.000573999 3.974418537 0.455590015 | 0.082588248 10.36672821
0.009163035 0.00078662 4.54979988 0.575381343 | 0.092847057 10.68638238
0.009901778 0.000738742 5.050861598 0.501061718 | 0.103808001 10.98526872
0.010602316 0.000700538 5.49130883 0.440447232 | 0.115456402 11.24869129
0.011315725 0.000713409 5.907142466 0.415833636 | 0.127772301 11.4889658
0.011879116 0.000563391 6.21173676 0.304594294 | 0.140730694 11.73530526
0.012608024 0.000728908 6.575909098 0.364172337 | 0.154301897 11.98594833
0.013458465 0.000850441 6.969197555 0.393288458 | 0.168452203 12.23887082
0.01449386 0.001035395 7.413161723 0.443964168 | 0.183144197 12.49191956
0.015570031 0.001076171 7.840246684 0.427084961 | 0.198337302 12.74284343
0.016683878 0.001113847 8.250294023 0.410046387 | 0.213988706 12.98987263
0.017882088 0.001198211 8.65788031 0.407586287 | 0.230053101 13.24025363
0.018966609 0.00108452 8.999774351 0.341894041 | 0.246484801 13.49636017
0.020241934 0.001275326 9.372427305 0.372652954 | 0.263235897 13.75739202
0.021557367 0.001315433 9.728018088 0.355590783 | 0.280259013 14.02253781
0.022914223 0.001356856 10.06772818 0.339710089 | 0.297506303 14.29097685
0.0233722 0.000457977 10.1738436 0.106115428 | 0.314930797 14.56190234
0.0233722 0 10.1738436 0| 0.332486212 14.83462739
0.0233722 0 10.1738436 0| 0.35012731 15.10856393
0.0233722 0 10.1738436 0| 0.367810607 15.38315671
0.0233722 0 10.1738436 0| 0.385494202 15.65787673
0.0233722 0 10.1738436 0| 0.40313831 15.93223195
0.0233722 0 10.1738436 0| 0.420704991 16.21299204
0.025286078 0.001913878 10.43315188 0.259308278 | 0.4381589 16.50400743
0.034765466 0.009479388 11.62246909 1.18931721 | 0.455466807 16.80161781
0.046272845 0.011507379 12.95977987 1.337310775 | 0.472598106 17.10228471
0.057202075 0.01092923 14.13586415 1.176084283 | 0.489524394 17.40263698
0.067110424 0.009908349 15.1232883 0.987424149 | 0.506219923 17.70057244
0.076105799 0.008995375 15.95390164 0.830613337 | 0.522661209 18.00835302
0.084277359 0.00817156 16.65253217 0.698630531 | 0.5388273 18.32642057
0.091696877 0.007419518 17.24017813 0.587645961 | 0.5546996 18.65
0.098425534 0.006728657 17.73364279 0.493464659 | 0.570261598 18.97482262
0.103064141 0.004638607 18.04864424 0.31500145 | 0.585499227 19.29688149
0.107327117 0.004262977 18.31681983 0.268175595 | 0.60040009 19.61284841
0.112553986 0.005226869 18.62132623 0.304506397 | 0.614954293 19.93989658
0.117293386 0.0047394 18.87706518 0.255738952 | 0.629153311 20.28543568
0.121594108 0.004300722 19.09193507 0.214869891 | 0.642990828 20.64144751
0.124563855 0.002969747 19.22932846 0.137393388 | 0.656461716 21.00086044
0.127297661 0.002733806 19.34646076 0.117132296 | 0.669562697 21.35753825
0.130653177 0.003355516 19.47962648 0.13316572 | 0.682291925 21.70623071
0.133693604 0.003040427 19.59137183 0.11174535 | 0.694648683 22.04251747
0.135792587 0.002098984 19.6628148 0.071442972 | 0.706633508 22.38858928
0.137725542 0.001932955 19.72375103 0.060936232 | 0.71824801 22.7784894
0.140101058 0.002375516 19.79310979 0.069358762 | 0.729494929 23.19841106
0.141742287 0.001641229 19.83748659 0.044376796 | 0.740377605 23.63575248
0.143254431 0.001512144 19.87535394 0.037867355 | 0.750900388 24.07980739
0.145112042 0.001857612 19.91843137 0.043077434 | 0.761068285 24.52158862
0.146797501 0.001685459 19.95462894 0.036197564 | 0.770887017 24.95366916
0.147962477 0.001164975 19.97779873 0.023169789 | 0.780362606 25.37
0.149036361 0.001073884 19.99758178 0.019783054 | 0.789501607 25.76580425
0.150036926 0.001000617 20.01465228 0.017070497 | 0.798311174 26.13736901
| 0.806798697 26.2975029
| 0.814971626 26.22560443
| 0.822837889 26.22560443
| 0.830405474 26.22560443
| 0.837682605 26.22560443
| 0.844677329 26.22560443
| 0.851397991 26.22560443
| 0.857852995 26.22560443
| 0.864050388 26.22560443
| 0.869998574 26.22560443
| 0.875705481 26.22560443
| 0.881179392 26.22560443
| 0.886428118 27.26181007
| 0.891459525 29.44168647
| 0.896281302 31.99902264
| 0.9009009 34.91346445
| 0.90532577 38.09899621
| 0.909563184 41.20035239
| 0.913620114 44.16961344
| 0.917503417 47.01179619
| 0.921219707 49.73174296
| 0.924775481 52.33420884
| 0.928177178 54.82390526
| 0.931430817 57.20523832
| 0.934542298 59.48252683
| 0.937517405 61.66
| 0.940361619 63.74167844
| 0.943080306 65.7314812
| 0.945678592 67.63316238
| 0.948161721 69.45056093
| 0.950534225 71.18699233
| 0.95280093 72.84599017
| 0.954966187 74.43073902
| 0.957034409 75.94446712
| 0.959009588 77.39
| 0.960896015 78.77077054
| 0.962697208 80.08906067
| 0.964416981 81.34775968
| 0.96605891 82.54948503
| 0.967626274 83.69663607
| 0.969122529 84.79174303
| 0.970550597 85.83694351
| 0.971913695 86.83459324
| 0.973214507 87.78665531
| 0.974455774 88.69513647
| 0.975640416 89.56217431
| 0.976770699 90.38942656
| 0.977849126 91.17872546
| 0.978878021 91.93177236
| 0.979859591 92.65018137
| 0.980795979 93.33552298
| 0.981689274 93.98932404
| 0.982541502 94.61306779
| 0.98335427 95.20793208
| 0.984129488 95.77531292
| 0.984869003 96.31656265
| 0.985574186 96.83268465
| 0.986246824 97.32498764
| 0.986888289 97.794475
| 0.987500012 98.24219371
| 0.988083303 98.66910351
| 0.988639593 99.07625139
|
|
|
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
| Sample: SiO2
| Operator: wawan
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File: C:\TriStar II 3020\data\SAMPEL\2019\Janu
|
|
Analysis AdsorN2 | Started: 1/31/2019 12: Analysis Adsor
Analysis Bath -195.850 °C | Completed: 1/31/2019 7:5 Analysis Bath
Thermal Correc No | Report Time: 7/25/2019 10: Thermal Correc
Warm Free Sp11.1152 cm³ Measured | Sample Mass:0.1781 g Warm Free Sp
Equilibration In5 s | Cold Free Spa32.0438 cm³ Equilibration In
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
| Automatic DegNo
|
|
|
|
|
|
|
| Cumulative Surface Area vs. Pore Width
|
orosity Distribution by Original Density Functional Theor |
odel: N2 @ 77K on Carbon, Slit Pores | Cumulative Surface Area
ethod: Non-negative Regularization: 0.00000 | Pore Width (n Cumulative Surface Area (m²/g)
| 1.483289338 0.245925197
| 1.590515054 0.921691434
| 1.715611708 1.571776992
| 1.8585793 2.382212284
tandard Deviation of Fit: 0.54271 cm³/g STP | 2.001546978 3.022454381
| 2.16238568 3.23897154
| 2.341095234 3.518828522
| 2.519804789 3.974418537
| 2.734256221 4.54979988
Fitted Quantit Absolute ResidRelative Resid| 2.948707652 5.050861598
7.590116354 0.003556358 0.000468332 | 3.181030107 5.49130883
7.771859043 -0.03352283 -0.00433205 | 3.431223586 5.907142466
7.910312608 -0.00534108 -0.00067566 | 3.699287918 6.21173676
8.055137427 0.039653457 0.004898639 | 4.003093956 6.575909098
8.34545408 -0.03688585 -0.0044395 | 4.324771359 6.969197555
8.510058594 0.03641102 0.004260351 | 4.664319445 7.413161723
8.852486205 -0.04454178 -0.005057 | 5.039609578 7.840246684
9.045818265 0.045565737 0.005011969 | 5.432770394 8.250294023
9.475530753 -0.08149254 -0.00867492 | 5.879544281 8.65788031
9.707691745 0.004019551 0.000413887 | 6.344189191 8.999774351
9.959732099 0.078802489 0.007849999 | 6.844575808 9.372427305
10.41260245 -0.04587424 -0.00442514 | 7.398575836 9.728018088
10.68136345 0.005018926 0.000469656 | 7.98831723 10.06772818
10.94468093 0.040587783 0.003694747 | 8.631671354 10.1738436
11.26354373 -0.01485244 -0.00132037 | 9.310767526 10.1738436
11.49696445 -0.00799865 -0.0006962 | 10.06134779 10.1738436
11.7146747 0.020630559 0.001757991 | 10.86554079 10.1738436
12.01697669 -0.03102835 -0.00258873 | 11.72334651 10.1738436
12.20823755 0.030633275 0.002502949 | 12.65263702 10.1738436
12.56963504 -0.07771548 -0.00622126 | 13.67128093 10.1738436
12.74344979 -0.00060636 -4.75845E-05 | 14.76140894 10.43315188
12.91239463 0.077478 0.005964493 | 15.94089173 11.62246909
13.33485203 -0.09459839 -0.00714476 | 17.20973066 12.95977987
13.49793272 -0.00157256 -0.00011652 | 18.58579369 14.13586415
13.6615225 0.095869519 0.006968582 | 20.06908354 15.1232883
14.07355902 -0.05102121 -0.00363851 | 21.65959748 15.95390164
14.24095595 0.050020752 0.003500174 | 23.39307962 16.65253217
14.65558679 -0.09368445 -0.00643353 | 25.25166062 17.24017813
14.83249163 0.002135756 0.000143971 | 27.27107913 17.73364279
15.01703193 0.091531997 0.006058286 | 29.45133516 18.04864424
15.45982862 -0.07667191 -0.00498415 | 31.79242869 18.31681983
15.65611434 0.001762389 0.000112556 | 34.33010654 18.62132623
15.85733804 0.074893912 0.00470078 | 37.06436055 18.87706518
16.25980569 -0.04681365 -0.00288742 | 40.03094025 19.09193507
16.45858491 0.045422523 0.002752212 | 43.22984018 19.22932846
16.91835829 -0.11674048 -0.00694817 | 46.67893786 19.34646076
17.10403838 -0.00175366 -0.00010254 | 50.39609442 19.47962648
17.2835437 0.119093282 0.006843404 | 54.4170594 19.59137183
17.77227887 -0.07170643 -0.00405108 | 58.75969939 19.6628148
17.93793031 0.070422714 0.003910558 | 63.44189191 19.72375103
18.49462768 -0.1682071 -0.00917839 | 68.49937012 19.79310979
18.65060019 -0.00057243 -3.0693E-05 | 73.96788359 19.83748659
18.80531635 0.169506266 0.00893322 | 79.86529889 19.87535394
19.37920645 -0.08232496 -0.00426623 | 86.24523218 19.91843137
19.53182035 0.081028056 0.004131376 | 93.12554458 19.95462894
20.13224707 -0.19235048 -0.00964651 | 100.5598686 19.97779873
20.28718681 -0.00175112 -8.63241E-05 | 108.5660545 19.99758178
20.44632605 0.195121467 0.009452897 | 117.2334679 20.01465228
21.09781433 -0.09695389 -0.00461666 |
21.2617798 0.095758448 0.00448359 |
21.88043114 -0.17420043 -0.00802537 |
22.04561545 -0.00309798 -0.00014055 |
22.21048312 0.178106156 0.00795522 |
22.91126664 -0.13277724 -0.00582906 |
23.06671326 0.131697795 0.005677018 |
23.78603356 -0.15028108 -0.00635821 |
23.93046527 0.149342118 0.006201965 |
24.67020006 -0.14861145 -0.00606043 |
24.80601037 0.147658788 0.005917318 |
25.14685879 0.223148002 0.008795741 |
25.28014919 0.485655067 0.018848822 |
25.41426812 0.723100894 0.027665405 |
25.55030855 0.747194359 0.02841313 |
25.68920068 0.536403755 0.020453437 |
25.83172024 0.393884196 0.01501907 |
25.97816248 0.247441949 0.009435129 |
26.12826722 0.097337217 0.003711534 |
26.28102609 -0.05542166 -0.00211327 |
26.4347614 -0.20915696 -0.0079753 |
26.58781839 -0.36221395 -0.01381146 |
26.7387503 -0.51314587 -0.0195666 |
26.88665304 -0.6610486 -0.02520623 |
27.03146618 -0.80586174 -0.03072805 |
27.17354975 -0.94794531 -0.03614579 |
28.2771421 -1.01533204 -0.03724375 |
28.4134581 1.028228363 0.034924235 |
33.38795246 -1.38892982 -0.04340538 |
33.51219823 1.401266219 0.04013541 |
39.58754189 -1.48854567 -0.03907047 |
39.70051066 1.499841728 0.036403614 |
45.53428386 -1.36467042 -0.03089614 |
45.6373244 1.374471791 0.029236743 |
50.98302018 -1.25127721 -0.02516053 |
51.07454455 1.259664294 0.024069616 |
55.97224102 -1.14833575 -0.02094589 |
56.04981297 1.155425352 0.020197894 |
60.53613042 -1.05360359 -0.01771282 |
60.60051383 1.05948855 0.017182752 |
64.70698335 -0.96530491 -0.01514401 |
64.76120419 0.970277004 0.014761222 |
68.51619196 -0.88302959 -0.01305616 |
68.56327166 0.887289273 0.01277584 |
71.18459859 0.002393747 3.36261E-05 |
73.61658412 -0.77059395 -0.0105784 |
73.65677046 0.77396856 0.010398507 |
76.64776815 -0.70330103 -0.00926073 |
76.68384539 0.706251913 0.009125869 |
79.41316439 -0.64239386 -0.00815523 |
79.44413998 0.644920689 0.008052544 |
81.93466325 -0.58690357 -0.00721475 |
81.96046157 0.589023455 0.007135398 |
83.6954434 0.001192667 1.42499E-05 |
85.30341039 -0.51166737 -0.0060344 |
85.32365791 0.513285604 0.005979775 |
87.30096685 -0.46637361 -0.00537083 |
87.31885835 0.467796966 0.005328794 |
89.12 -0.42486933 -0.00479022 |
89.13603708 0.426137229 0.004758005 |
90.38871243 0.000714131 7.90058E-06 |
91.54833996 -0.36961451 -0.00405374 |
91.56116073 0.370611626 0.004031377 |
92.9870895 -0.33690813 -0.00363635 |
92.99776803 0.337754948 0.003618718 |
93.98882557 0.000498464 5.3034E-06 |
94.90598792 -0.29292014 -0.00309598 |
94.91434699 0.293585094 0.00308362 |
96.04202721 -0.26671429 -0.00278479 |
96.0492539 0.267308753 0.002775315 |
97.07550711 -0.24282247 -0.00250765 |
97.08163506 0.243352582 0.002500412 |
97.79416565 0.000309349 3.16326E-06 |
98.45318533 -0.21099162 -0.00214767 |
98.45770191 0.211401597 0.002142531 |
99.07300389 0.0032475 3.27778E-05 |
|
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| |
| Sample: SiO2 |
| Operator: wawan |
| Submitter: |
| |
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| Automatic DegNo |
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| Incremental Surface Area vs. Pore Width |
| |
| |
| Incremental Surface Area |
ace Area (m²/g) | Pore Width (n Incremental Surface Area (m²/g) |
| 1.483289338 0.245925197 |
| 1.590515054 0.675766236 |
| 1.715611708 0.650085449 |
| 1.8585793 0.810435292 |
| 2.001546978 0.640242097 |
| 2.16238568 0.216517159 |
| 2.341095234 0.279856983 |
| 2.519804789 0.455590015 |
| 2.734256221 0.575381343 |
| 2.948707652 0.501061718 |
| 3.181030107 0.440447232 |
| 3.431223586 0.415833636 |
| 3.699287918 0.304594294 |
| 4.003093956 0.364172337 |
| 4.324771359 0.393288458 |
| 4.664319445 0.443964168 |
| 5.039609578 0.427084961 |
| 5.432770394 0.410046387 |
| 5.879544281 0.407586287 |
| 6.344189191 0.341894041 |
| 6.844575808 0.372652954 |
| 7.398575836 0.355590783 |
| 7.98831723 0.339710089 |
| 8.631671354 0.106115428 |
| 9.310767526 0 |
| 10.06134779 0 |
| 10.86554079 0 |
| 11.72334651 0 |
| 12.65263702 0 |
| 13.67128093 0 |
| 14.76140894 0.259308278 |
| 15.94089173 1.18931721 |
| 17.20973066 1.337310775 |
| 18.58579369 1.176084283 |
| 20.06908354 0.987424149 |
| 21.65959748 0.830613337 |
| 23.39307962 0.698630531 |
| 25.25166062 0.587645961 |
| 27.27107913 0.493464659 |
| 29.45133516 0.31500145 |
| 31.79242869 0.268175595 |
| 34.33010654 0.304506397 |
| 37.06436055 0.255738952 |
| 40.03094025 0.214869891 |
| 43.22984018 0.137393388 |
| 46.67893786 0.117132296 |
| 50.39609442 0.13316572 |
| 54.4170594 0.11174535 |
| 58.75969939 0.071442972 |
| 63.44189191 0.060936232 |
| 68.49937012 0.069358762 |
| 73.96788359 0.044376796 |
| 79.86529889 0.037867355 |
| 86.24523218 0.043077434 |
| 93.12554458 0.036197564 |
| 100.5598686 0.023169789 |
| 108.5660545 0.019783054 |
| 117.2334679 0.017070497 |
| |
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Differential Surface Area vs. Pore Width | Cumulative Pore Volume vs. Pore Width
|
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Differential Surface Area | Cumulative Pore Volume
Pore Width (n Differential Surface Area (m²/g) | Pore Width (n Cumulative Pore Volume (cm³/g)
1.483289338 8.113154397 | 1.483289338 0.004751812
1.590515054 21.38733357 | 1.590515054 0.00528922
1.715611708 19.22098543 | 1.715611708 0.005846867
1.8585793 24.21132764 | 1.8585793 0.006599996
2.001546978 19.47443444 | 2.001546978 0.007240734
2.16238568 6.363164799 | 2.16238568 0.007474831
2.341095234 8.425146044 | 2.341095234 0.007802416
2.519804789 13.51495551 | 2.519804789 0.008376415
2.734256221 16.85733133 | 2.734256221 0.009163035
2.948707652 15.24639018 | 2.948707652 0.009901778
3.181030107 13.38393464 | 3.181030107 0.010602316
3.431223586 12.68745652 | 3.431223586 0.011315725
3.699287918 9.099597093 | 3.699287918 0.011879116
4.003093956 10.73541866 | 4.003093956 0.012608024
4.324771359 11.84737558 | 4.324771359 0.013458465
4.664319445 13.36562311 | 4.664319445 0.01449386
5.039609578 12.89642761 | 5.039609578 0.015570031
5.432770394 12.24995087 | 5.432770394 0.016683878
5.879544281 12.1026694 | 5.879544281 0.017882088
6.344189191 10.3599746 | 6.344189191 0.018966609
6.844575808 11.16195205 | 6.844575808 0.020241934
7.398575836 10.59744675 | 7.398575836 0.021557367
7.98831723 10.14866304 | 7.98831723 0.022914223
8.631671354 3.189993703 | 8.631671354 0.0233722
9.310767526 0 | 9.310767526 0.0233722
10.06134779 0 | 10.06134779 0.0233722
10.86554079 0 | 10.86554079 0.0233722
11.72334651 0 | 11.72334651 0.0233722
12.65263702 0 | 12.65263702 0.0233722
13.67128093 0 | 13.67128093 0.0233722
14.76140894 7.774963834 | 14.76140894 0.025286078
15.94089173 35.69044029 | 15.94089173 0.034765466
17.20973066 40.11822014 | 17.20973066 0.046272845
18.58579369 35.23665009 | 18.58579369 0.057202075
20.06908354 29.71069653 | 20.06908354 0.067110424
21.65959748 24.95838659 | 21.65959748 0.076105799
23.39307962 20.96744057 | 23.39307962 0.084277359
25.25166062 17.64307215 | 25.25166062 0.091696877
27.27107913 14.77106437 | 27.27107913 0.098425534
29.45133516 9.45646696 | 29.45133516 0.103064141
31.79242869 8.056930671 | 31.79242869 0.107327117
34.33010654 9.139834102 | 34.33010654 0.112553986
37.06436055 7.665962243 | 37.06436055 0.117293386
40.03094025 6.430619684 | 40.03094025 0.121594108
43.22984018 4.118187446 | 43.22984018 0.124563855
46.67893786 3.516786648 | 46.67893786 0.127297661
50.39609442 3.998123864 | 50.39609442 0.130653177
54.4170594 3.351555234 | 54.4170594 0.133693604
58.75969939 2.144112833 | 58.75969939 0.135792587
63.44189191 1.829724208 | 63.44189191 0.137725542
68.49937012 2.080750366 | 68.49937012 0.140101058
73.96788359 1.331206494 | 73.96788359 0.141742287
79.86529889 1.135590763 | 79.86529889 0.143254431
86.24523218 1.291469928 | 86.24523218 0.145112042
93.12554458 1.085553468 | 93.12554458 0.146797501
100.5598686 0.695525974 | 100.5598686 0.147962477
108.5660545 0.593845728 | 108.5660545 0.149036361
117.2334679 0.511743025 | 117.2334679 0.150036926
|
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| Sample: SiO2
| Operator: wawan
| Submitter:
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| Automatic DegNo
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e Volume vs. Pore Width | Incremental Pore Volume vs. Pore Width
|
|
| Incremental Pore Volume
umulative Pore Volume (cm³/g) | Pore Width (n Incremental Pore Volume (cm³/g)
| 1.483289338 0.000182389
| 1.590515054 0.000537408
| 1.715611708 0.000557647
| 1.8585793 0.000753129
| 2.001546978 0.000640737
| 2.16238568 0.000234097
| 2.341095234 0.000327586
| 2.519804789 0.000573999
| 2.734256221 0.00078662
| 2.948707652 0.000738742
| 3.181030107 0.000700538
| 3.431223586 0.000713409
| 3.699287918 0.000563391
| 4.003093956 0.000728908
| 4.324771359 0.000850441
| 4.664319445 0.001035395
| 5.039609578 0.001076171
| 5.432770394 0.001113847
| 5.879544281 0.001198211
| 6.344189191 0.00108452
| 6.844575808 0.001275326
| 7.398575836 0.001315433
| 7.98831723 0.001356856
| 8.631671354 0.000457977
| 9.310767526 0
| 10.06134779 0
| 10.86554079 0
| 11.72334651 0
| 12.65263702 0
| 13.67128093 0
| 14.76140894 0.001913878
| 15.94089173 0.009479388
| 17.20973066 0.011507379
| 18.58579369 0.01092923
| 20.06908354 0.009908349
| 21.65959748 0.008995375
| 23.39307962 0.00817156
| 25.25166062 0.007419518
| 27.27107913 0.006728657
| 29.45133516 0.004638607
| 31.79242869 0.004262977
| 34.33010654 0.005226869
| 37.06436055 0.0047394
| 40.03094025 0.004300722
| 43.22984018 0.002969747
| 46.67893786 0.002733806
| 50.39609442 0.003355516
| 54.4170594 0.003040427
| 58.75969939 0.002098984
| 63.44189191 0.001932955
| 68.49937012 0.002375516
| 73.96788359 0.001641229
| 79.86529889 0.001512144
| 86.24523218 0.001857612
| 93.12554458 0.001685459
| 100.5598686 0.001164975
| 108.5660545 0.001073884
| 117.2334679 0.001000617
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| Differential Pore Volume vs. Pore Width | Goodness of Fit
| | Standard Deviation of Fit: 0.54271 cm³/
| |
| Differential Pore Volume | Input Data
| Pore Width (n Differential Pore Volume (cm³/g) | Relative Press
| 1.483289338 0.006017078 | 0.012931432
| 1.590515054 0.017008438 | 0.116178332
| 1.715611708 0.016487874 | 0.209428125
| 1.8585793 0.022499336 | 0.300513217
| 2.001546978 0.019489498 | 0.402673862
| 2.16238568 0.006879808 | 0.501120678
| 2.341095234 0.009862035 | 0.599116155
| 2.519804789 0.017027525 | 0.696451609
| 2.734256221 0.023046132 | 0.800450054
| 2.948707652 0.022478574 | 0.903034652
| 3.181030107 0.02128735 | 0.989112292
| 3.431223586 0.02176675 |
| 3.699287918 0.016831015 |
| 4.003093956 0.021487445 |
| 4.324771359 0.025618595 |
| 4.664319445 0.031170768 |
| 5.039609578 0.03249648 |
| 5.432770394 0.033275585 |
| 5.879544281 0.03557909 |
| 6.344189191 0.032862819 |
| 6.844575808 0.038199413 |
| 7.398575836 0.039203007 |
| 7.98831723 0.04053537 |
| 8.631671354 0.013767489 |
| 9.310767526 0 |
| 10.06134779 0 |
| 10.86554079 0 |
| 11.72334651 0 |
| 12.65263702 0 |
| 13.67128093 0 |
| 14.76140894 0.05738471 |
| 15.94089173 0.284468722 |
| 17.20973066 0.345211882 |
| 18.58579369 0.327450554 |
| 20.06908354 0.298133225 |
| 21.65959748 0.270294304 |
| 23.39307962 0.245246503 |
| 25.25166062 0.222758435 |
| 27.27107913 0.201411433 |
| 29.45133516 0.139252789 |
| 31.79242869 0.128074697 |
| 34.33010654 0.156885739 |
| 37.06436055 0.142066994 |
| 40.03094025 0.128711876 |
| 43.22984018 0.089014293 |
| 46.67893786 0.082079933 |
| 50.39609442 0.100744914 |
| 54.4170594 0.09119089 |
| 58.75969939 0.062993713 |
| 63.44189191 0.058040583 |
| 68.49937012 0.071265045 |
| 73.96788359 0.049233264 |
| 79.86529889 0.045347148 |
| 86.24523218 0.055691562 |
| 93.12554458 0.050546379 |
| 100.5598686 0.034971 |
| 108.5660545 0.032235744 |
| 117.2334679 0.029996705 |
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SiO2 | Sample: SiO2
| Submitter:
|
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|
oodness of Fit | Goodness of Fit
tandard Deviation of Fit: 0.54271 cm³/g STP | Standard Deviation of Fit: 0.54271 cm³/g STP
|
Model Fit | Input Data Model Fit
Quantity AdsoRelative PressQuantity Adso| Relative PressQuantity AdsoRelative Press
7.521682702 0.01451552 7.590116354 | 0.012931432 7.521682702 0.01451552
11.2630366 0.017706521 7.771859043 | 0.116178332 11.2630366 0.017706521
12.91880126 0.02139844 7.910312608 | 0.209428125 12.91880126 0.02139844
14.33775115 0.02563123 8.055137427 | 0.300513217 14.33775115 0.02563123
15.9250009 0.03044224 8.34545408 | 0.402673862 15.9250009 0.03044224
17.608932 0.035865448 8.510058594 | 0.501120678 17.608932 0.035865448
19.58553313 0.041930798 8.852486205 | 0.599116155 19.58553313 0.041930798
22.09115784 0.048663601 9.045818265 | 0.696451609 22.09115784 0.048663601
26.22560443 0.056084011 9.475530753 | 0.800450054 26.22560443 0.056084011
36.42213023 0.064206667 9.707691745 | 0.903034652 36.42213023 0.064206667
99.42221883 0.073040441 9.959732099 | 0.989112292 99.42221883 0.073040441
0.082588248 10.41260245 | 0.082588248
0.092847057 10.68136345 | 0.092847057
0.103808001 10.94468093 | 0.103808001
0.115456402 11.26354373 | 0.115456402
0.127772301 11.49696445 | 0.127772301
0.140730694 11.7146747 | 0.140730694
0.154301897 12.01697669 | 0.154301897
0.168452203 12.20823755 | 0.168452203
0.183144197 12.56963504 | 0.183144197
0.198337302 12.74344979 | 0.198337302
0.213988706 12.91239463 | 0.213988706
0.230053101 13.33485203 | 0.230053101
0.246484801 13.49793272 | 0.246484801
0.263235897 13.6615225 | 0.263235897
0.280259013 14.07355902 | 0.280259013
0.297506303 14.24095595 | 0.297506303
0.314930797 14.65558679 | 0.314930797
0.332486212 14.83249163 | 0.332486212
0.35012731 15.01703193 | 0.35012731
0.367810607 15.45982862 | 0.367810607
0.385494202 15.65611434 | 0.385494202
0.40313831 15.85733804 | 0.40313831
0.420704991 16.25980569 | 0.420704991
0.4381589 16.45858491 | 0.4381589
0.455466807 16.91835829 | 0.455466807
0.472598106 17.10403838 | 0.472598106
0.489524394 17.2835437 | 0.489524394
0.506219923 17.77227887 | 0.506219923
0.522661209 17.93793031 | 0.522661209
0.5388273 18.49462768 | 0.5388273
0.5546996 18.65060019 | 0.5546996
0.570261598 18.80531635 | 0.570261598
0.585499227 19.37920645 | 0.585499227
0.60040009 19.53182035 | 0.60040009
0.614954293 20.13224707 | 0.614954293
0.629153311 20.28718681 | 0.629153311
0.642990828 20.44632605 | 0.642990828
0.656461716 21.09781433 | 0.656461716
0.669562697 21.2617798 | 0.669562697
0.682291925 21.88043114 | 0.682291925
0.694648683 22.04561545 | 0.694648683
0.706633508 22.21048312 | 0.706633508
0.71824801 22.91126664 | 0.71824801
0.729494929 23.06671326 | 0.729494929
0.740377605 23.78603356 | 0.740377605
0.750900388 23.93046527 | 0.750900388
0.761068285 24.67020006 | 0.761068285
0.770887017 24.80601037 | 0.770887017
0.780362606 25.14685879 | 0.780362606
0.789501607 25.28014919 | 0.789501607
0.798311174 25.41426812 | 0.798311174
0.806798697 25.55030855 | 0.806798697
0.814971626 25.68920068 | 0.814971626
0.822837889 25.83172024 | 0.822837889
0.830405474 25.97816248 | 0.830405474
0.837682605 26.12826722 | 0.837682605
0.844677329 26.28102609 | 0.844677329
0.851397991 26.4347614 | 0.851397991
0.857852995 26.58781839 | 0.857852995
0.864050388 26.7387503 | 0.864050388
0.869998574 26.88665304 | 0.869998574
0.875705481 27.03146618 | 0.875705481
0.881179392 27.17354975 | 0.881179392
0.886428118 28.2771421 | 0.886428118
0.891459525 28.4134581 | 0.891459525
0.896281302 33.38795246 | 0.896281302
0.9009009 33.51219823 | 0.9009009
0.90532577 39.58754189 | 0.90532577
0.909563184 39.70051066 | 0.909563184
0.913620114 45.53428386 | 0.913620114
0.917503417 45.6373244 | 0.917503417
0.921219707 50.98302018 | 0.921219707
0.924775481 51.07454455 | 0.924775481
0.928177178 55.97224102 | 0.928177178
0.931430817 56.04981297 | 0.931430817
0.934542298 60.53613042 | 0.934542298
0.937517405 60.60051383 | 0.937517405
0.940361619 64.70698335 | 0.940361619
0.943080306 64.76120419 | 0.943080306
0.945678592 68.51619196 | 0.945678592
0.948161721 68.56327166 | 0.948161721
0.950534225 71.18459859 | 0.950534225
0.95280093 73.61658412 | 0.95280093
0.954966187 73.65677046 | 0.954966187
0.957034409 76.64776815 | 0.957034409
0.959009588 76.68384539 | 0.959009588
0.960896015 79.41316439 | 0.960896015
0.962697208 79.44413998 | 0.962697208
0.964416981 81.93466325 | 0.964416981
0.96605891 81.96046157 | 0.96605891
0.967626274 83.6954434 | 0.967626274
0.969122529 85.30341039 | 0.969122529
0.970550597 85.32365791 | 0.970550597
0.971913695 87.30096685 | 0.971913695
0.973214507 87.31885835 | 0.973214507
0.974455774 89.12 | 0.974455774
0.975640416 89.13603708 | 0.975640416
0.976770699 90.38871243 | 0.976770699
0.977849126 91.54833996 | 0.977849126
0.978878021 91.56116073 | 0.978878021
0.979859591 92.9870895 | 0.979859591
0.980795979 92.99776803 | 0.980795979
0.981689274 93.98882557 | 0.981689274
0.982541502 94.90598792 | 0.982541502
0.98335427 94.91434699 | 0.98335427
0.984129488 96.04202721 | 0.984129488
0.984869003 96.0492539 | 0.984869003
0.985574186 97.07550711 | 0.985574186
0.986246824 97.08163506 | 0.986246824
0.986888289 97.79416565 | 0.986888289
0.987500012 98.45318533 | 0.987500012
0.988083303 98.45770191 | 0.988083303
0.988639593 99.07300389 | 0.988639593
|
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| Sample: SiO2 |
| Operator: wawan |
| Submitter: |
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| Automatic DegNo |
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271 cm³/g STP | |
| Surface Energy Distribution by Modified De|
| Model: N2 @ 77K, Surface Energy Distribut|
Quantity Adso| Method: Non-negative Regularization: 0.0 |
7.590116354 | Standard Deviation of Fit: 0.04774 cm³/g S |
7.771859043 | |
7.910312608 | |
8.055137427 | |
8.34545408 | |
8.510058594 | Total Area : 40.438 m²/g |
8.852486205 | |
9.045818265 | |
9.475530753 | Surface Energy Table |
9.707691745 | |
9.959732099 | Energy (e/k) Cumulative AreIncremental Area (m²/g) |
10.41260245 | 20 0 0 |
10.68136345 | 22 0 0 |
10.94468093 | 24 0 0 |
11.26354373 | 26 0 0 |
11.49696445 | 28 0 0 |
11.7146747 | 30 0 0 |
12.01697669 | 32 0 0 |
12.20823755 | 34 0 0 |
12.56963504 | 36 0 0 |
12.74344979 | 38 0 0 |
12.91239463 | 40 11.46456049 11.46456049 |
13.33485203 | 42 17.08442876 5.619868264 |
13.49793272 | 44 17.08442876 0 |
13.6615225 | 46 17.08442876 0 |
14.07355902 | 48 17.08442876 0 |
14.24095595 | 50 17.08442876 0 |
14.65558679 | 52 17.08442876 0 |
14.83249163 | 54 17.08442876 0 |
15.01703193 | 56 17.08442876 0 |
15.45982862 | 58 17.08442876 0 |
15.65611434 | 60 17.08442876 0 |
15.85733804 | 62 18.98577712 1.901348366 |
16.25980569 | 64 24.72498471 5.739207584 |
16.45858491 | 66 24.72498471 0 |
16.91835829 | 68 24.72498471 0 |
17.10403838 | 70 24.72498471 0 |
17.2835437 | 72 26.46355689 1.738572177 |
17.77227887 | 74 26.46355689 0 |
17.93793031 | 76 26.46355689 0 |
18.49462768 | 78 26.46355689 0 |
18.65060019 | 80 26.46355689 0 |
18.80531635 | 82 32.63356205 6.17 |
19.37920645 | 84 32.63356205 0 |
19.53182035 | 86 32.63356205 0 |
20.13224707 | 88 32.63356205 0 |
20.28718681 | 90 37.7353781 5.101816047 |
20.44632605 | 92 37.7353781 0 |
21.09781433 | 94 37.7353781 0 |
21.2617798 | 96 37.7353781 0 |
21.88043114 | 98 40.43771851 2.702340412 |
22.04561545 | 100 40.43771851 0 |
22.21048312 | |
22.91126664 | |
23.06671326 | |
23.78603356 | |
23.93046527 | |
24.67020006 | |
24.80601037 | |
25.14685879 | |
25.28014919 | |
25.41426812 | |
25.55030855 | |
25.68920068 | |
25.83172024 | |
25.97816248 | |
26.12826722 | |
26.28102609 | |
26.4347614 | |
26.58781839 | |
26.7387503 | |
26.88665304 | |
27.03146618 | |
27.17354975 | |
28.2771421 | |
28.4134581 | |
33.38795246 | |
33.51219823 | |
39.58754189 |
39.70051066 |
45.53428386 |
45.6373244 |
50.98302018 |
51.07454455 |
55.97224102 |
56.04981297 |
60.53613042 |
60.60051383 |
64.70698335 |
64.76120419 |
68.51619196 |
68.56327166 |
71.18459859 |
73.61658412 |
73.65677046 |
76.64776815 |
76.68384539 |
79.41316439 |
79.44413998 |
81.93466325 |
81.96046157 |
83.6954434 |
85.30341039 |
85.32365791 |
87.30096685 |
87.31885835 |
89.12 |
89.13603708 |
90.38871243 |
91.54833996 |
91.56116073 |
92.9870895 |
92.99776803 |
93.98882557 |
94.90598792 |
94.91434699 |
96.04202721 |
96.0492539 |
97.07550711 |
97.08163506 |
97.79416565 |
98.45318533 |
98.45770191 |
99.07300389 |
|
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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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Sample: SiO2 | Sample:
Operator: wawan | Operator:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP | File:
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Started: 1/31/2019 12: Analysis AdsorN2 | Started:
Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C | Completed:
Report Time: 7/25/2019 10: Thermal Correc No | Report Time:
Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ Measured | Sample Mass:
Cold Free Spa32.0438 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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| Cumulative Surface Area vs. Energy
|
Surface Energy Distribution by Modified Density Function |
Model: N2 @ 77K, Surface Energy Distribution | Cumulative Surface Area
Method: Non-negative Regularization: 0.00000 | Energy (e/k)
| 20
| 22
| 24
| 26
Standard Deviation of Fit: 0.04774 cm³/g STP | 28
| 30
| 32
Isotherm Table | 34
Relative Pressure | 36
(P/Po) Experimental Fitted Quantit Absolute ResidRelative Resid| 38
0.013335214 7.540039063 7.395184084 0.144858427 0.019211885 | 40
0.014125375 7.575951985 7.467007449 0.108944536 0.01438031 | 42
0.014962357 7.613960148 7.536526003 0.077434145 0.010170022 | 44
0.015848932 7.654185181 7.6040554 0.050129781 0.006549329 | 46
0.01678804 7.696751016 7.669902359 0.026848657 0.00348831 | 48
0.017782794 7.741787435 7.734381815 0.00740562 0.000956578 | 50
0.018836491 7.789430123 7.79780082 -0.0083707 -0.00107462 | 52
0.019952623 7.839820664 7.860472077 -0.02065141 -0.00263417 | 54
0.02113489 7.893106479 7.922713449 -0.02960697 -0.00375099 | 56
0.022387211 7.949440669 7.984863977 -0.03542331 -0.00445608 | 58
0.023713737 8.008981758 8.047287006 -0.03830525 -0.00478279 | 60
0.025118864 8.071893309 8.110393833 -0.03850052 -0.0047697 | 62
0.026607251 8.138343377 8.17465778 -0.0363144 -0.00446214 | 64
0.028183829 8.208503765 8.240658426 -0.03215466 -0.00391724 | 66
0.029853826 8.282549054 8.309120776 -0.02657172 -0.00320816 | 68
0.031622777 8.360655333 8.380984996 -0.02032966 -0.00243159 | 70
0.033496544 8.442998591 8.45748195 -0.01448336 -0.00171543 | 72
0.035481339 8.52975268 8.540078125 -0.01034435 -0.00121274 | 74
0.03758374 8.621086775 8.630078125 -0.00899448 -0.00104331 | 76
0.039810717 8.717162226 8.727064902 -0.00990268 -0.001136 | 78
0.04216965 8.818128663 8.828507606 -0.01037894 -0.001177 | 80
0.044668359 8.924119233 8.932403665 -0.00828443 -0.00092832 | 82
0.047315126 9.035244766 9.039320995 -0.00407623 -0.00045115 | 84
0.050118723 9.151586682 9.151604466 -1.77846E-05 -1.94333E-06 | 86
0.053088444 9.273188368 9.272035039 0.001153329 0.000124372 | 88
0.056234133 9.400039063 9.402045655 -0.00200091 -0.00021286 | 90
0.059566214 9.532089675 9.539359083 -0.00726941 -0.00076262 | 92
0.063095734 9.66918072 9.679025452 -0.00984473 -0.00101816 | 94
0.066834392 9.811080875 9.818341085 -0.00726021 -0.00074 | 96
0.070794578 9.95743654 9.958367439 -0.0009309 -9.34876E-05 | 98
0.074989421 10.10775111 10.10208578 0.005665328 0.000560493 | 100
0.079432823 10.26135327 10.25230924 0.009044022 0.000881367 |
0.084139514 10.41735904 10.40913187 0.008227168 0.000789756 |
0.089125094 10.57462633 10.56825622 0.00637011 0.000602396 |
0.094406088 10.73170056 10.72407218 0.007628371 0.000710826 |
0.1 10.88674966 10.87405757 0.012692087 0.001165829 |
0.105925373 11.03748645 11.01881671 0.018669743 0.001691485 |
0.112201845 11.18107594 11.16031675 0.020759192 0.001856636 |
0.118850223 11.31555258 11.30084336 0.014709223 0.001299912 |
0.125892541 11.45268289 11.44255613 0.010126762 0.000884226 |
0.133352143 11.5958565 11.58704982 0.008806684 0.000759468 |
0.141253754 11.74510716 11.73494245 0.010164711 0.000865442 |
0.149623566 11.90041778 11.88637822 0.014039561 0.001179754 |
0.158489319 12.0617085 12.04226027 0.019448234 0.001612395 |
0.167880402 12.22882247 12.2047028 0.024119676 0.001972363 |
0.177827941 12.40150892 12.37655833 0.024950588 0.002011899 |
0.188364909 12.57940307 12.56033439 0.01906868 0.001515865 |
0.199526231 12.76200234 12.75639404 0.005608297 0.000439453 |
0.211348904 12.94873365 12.96170428 -0.01297063 -0.00100169 |
0.223872114 13.14391027 13.17157565 -0.02766538 -0.00210481 |
0.237137371 13.3506708 13.38267082 -0.03200002 -0.00239688 |
0.251188643 13.5696685 13.59438987 -0.02472137 -0.00182181 |
0.266072506 13.80158457 13.8085529 -0.00696833 -0.00050489 |
0.281838293 14.0471273 14.0286319 0.018495406 0.001316668 |
0.298538262 14.30703052 14.25934561 0.047684916 0.003332971 |
0.316227766 14.58205757 14.50676219 0.07529538 0.005163563 |
0.334965439 14.87313009 14.77838601 0.094744074 0.00637015 |
0.354813389 15.18132603 15.08187205 0.099453978 0.006551073 |
0.375837404 15.50783293 15.42232747 0.085505454 0.005513695 |
0.398107171 15.85396523 15.80223652 0.051728712 0.003262825 |
0.421696503 16.22922923 16.22161046 0.007618762 0.000469447 |
0.446683592 16.64964171 16.6788365 -0.0291948 -0.00175348 |
0.473151259 17.11206312 17.1728922 -0.06082907 -0.00355475 |
0.501187234 17.61011541 17.70687053 -0.09675512 -0.00549429 |
0.530884444 18.16846558 18.29561927 -0.12715369 -0.00699859 |
0.562341325 18.80879501 18.96537427 -0.15657926 -0.00832479 |
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SiO2 | Sample: SiO2
| Submitter:
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umulative Surface Area vs. Energy | Incremental Surface Area vs. Energy
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umulative Surface Area | Incremental Surface Area
Cumulative Surface Area (m²/g) | Energy (e/k) Incremental Surface Area (m²/g)
0 | 20 0
0 | 22 0
0 | 24 0
0 | 26 0
0 | 28 0
0 | 30 0
0 | 32 0
0 | 34 0
0 | 36 0
0 | 38 0
11.46456049 | 40 11.46456049
17.08442876 | 42 5.619868264
17.08442876 | 44 0
17.08442876 | 46 0
17.08442876 | 48 0
17.08442876 | 50 0
17.08442876 | 52 0
17.08442876 | 54 0
17.08442876 | 56 0
17.08442876 | 58 0
17.08442876 | 60 0
18.98577712 | 62 1.901348366
24.72498471 | 64 5.739207584
24.72498471 | 66 0
24.72498471 | 68 0
24.72498471 | 70 0
26.46355689 | 72 1.738572177
26.46355689 | 74 0
26.46355689 | 76 0
26.46355689 | 78 0
26.46355689 | 80 0
32.63356205 | 82 6.17
32.63356205 | 84 0
32.63356205 | 86 0
32.63356205 | 88 0
37.7353781 | 90 5.101816047
37.7353781 | 92 0
37.7353781 | 94 0
37.7353781 | 96 0
40.43771851 | 98 2.702340412
40.43771851 | 100 0
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| Sample: SiO2 |
| Operator: wawan |
| Submitter: |
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| Automatic DegNo |
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| Differential Surface Area vs. Energy |
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| Differential Surface Area |
face Area (m²/g) | Energy (e/k) Differential Surface Area (m²/g-K) |
| 20 0 |
| 22 0 |
| 24 0 |
| 26 0 |
| 28 0 |
| 30 0 |
| 32 0 |
| 34 0 |
| 36 0 |
| 38 0 |
| 40 5.732280247 |
| 42 2.809934132 |
| 44 0 |
| 46 0 |
| 48 0 |
| 50 0 |
| 52 0 |
| 54 0 |
| 56 0 |
| 58 0 |
| 60 0 |
| 62 0.950674183 |
| 64 2.869603792 |
| 66 0 |
| 68 0 |
| 70 0 |
| 72 0.869286089 |
| 74 0 |
| 76 0 |
| 78 0 |
| 80 0 |
| 82 3.085002583 |
| 84 0 |
| 86 0 |
| 88 0 |
| 90 2.550908023 |
| 92 0 |
| 94 0 |
| 96 0 |
| 98 1.351170206 |
| 100 0 |
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Goodness of Fit | Goodness of Fit
Standard Deviation of Fit: 0.04774 cm³/g STP | Standard Deviation of Fit: 0.04774 cm³/g STP
|
Input Data Model Fit | Input Data
Relative PressQuantity AdsoRelative PressQuantity Adso| Relative PressQuantity Adso
0.012931432 7.521682702 0.013335214 7.395184084 | 0.012931432 7.521682702
0.116178332 11.2630366 0.014125375 7.467007449 | 0.116178332 11.2630366
0.209428125 12.91880126 0.014962357 7.536526003 | 0.209428125 12.91880126
0.300513217 14.33775115 0.015848932 7.6040554 | 0.300513217 14.33775115
0.402673862 15.9250009 0.01678804 7.669902359 | 0.402673862 15.9250009
0.501120678 17.608932 0.017782794 7.734381815 | 0.501120678 17.608932
0.599116155 19.58553313 0.018836491 7.79780082 | 0.599116155 19.58553313
0.696451609 22.09115784 0.019952623 7.860472077 | 0.696451609 22.09115784
0.800450054 26.22560443 0.02113489 7.922713449 | 0.800450054 26.22560443
0.903034652 36.42213023 0.022387211 7.984863977 | 0.903034652 36.42213023
0.989112292 99.42221883 0.023713737 8.047287006 | 0.989112292 99.42221883
0.025118864 8.110393833 |
0.026607251 8.17465778 |
0.028183829 8.240658426 |
0.029853826 8.309120776 |
0.031622777 8.380984996 |
0.033496544 8.45748195 |
0.035481339 8.540078125 |
0.03758374 8.630078125 |
0.039810717 8.727064902 |
0.04216965 8.828507606 |
0.044668359 8.932403665 |
0.047315126 9.039320995 |
0.050118723 9.151604466 |
0.053088444 9.272035039 |
0.056234133 9.402045655 |
0.059566214 9.539359083 |
0.063095734 9.679025452 |
0.066834392 9.818341085 |
0.070794578 9.958367439 |
0.074989421 10.10208578 |
0.079432823 10.25230924 |
0.084139514 10.40913187 |
0.089125094 10.56825622 |
0.094406088 10.72407218 |
0.1 10.87405757 |
0.105925373 11.01881671 |
0.112201845 11.16031675 |
0.118850223 11.30084336 |
0.125892541 11.44255613 |
0.133352143 11.58704982 |
0.141253754 11.73494245 |
0.149623566 11.88637822 |
0.158489319 12.04226027 |
0.167880402 12.2047028 |
0.177827941 12.37655833 |
0.188364909 12.56033439 |
0.199526231 12.75639404 |
0.211348904 12.96170428 |
0.223872114 13.17157565 |
0.237137371 13.38267082 |
0.251188643 13.59438987 |
0.266072506 13.8085529 |
0.281838293 14.0286319 |
0.298538262 14.25934561 |
0.316227766 14.50676219 |
0.334965439 14.77838601 |
0.354813389 15.08187205 |
0.375837404 15.42232747 |
0.398107171 15.80223652 |
0.421696503 16.22161046 |
0.446683592 16.6788365 |
0.473151259 17.1728922 |
0.501187234 17.70687053 |
0.530884444 18.29561927 |
0.562341325 18.96537427 |
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| Sample: SiO2
| Operator: wawan
| Submitter:
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| Automatic DegNo
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| Dubinin Reports
ion of Fit: 0.04774 cm³/g STP |
| 4035- Cannot calculate optimized Astakhov exponent:
Model Fit | 4031- Not enough points with a relative pressure in the r
Relative PressQuantity Adso| 4026- Cannot calculate Dubinin-Astakhov: bad least squa
0.013335214 7.395184084 | 1017- (INTERNAL) Cannot calculate Radushkevich: bad le
0.014125375 7.467007449 |
0.014962357 7.536526003 |
0.015848932 7.6040554 |
0.01678804 7.669902359 |
0.017782794 7.734381815 |
0.018836491 7.79780082 |
0.019952623 7.860472077 |
0.02113489 7.922713449 |
0.022387211 7.984863977 |
0.023713737 8.047287006 |
0.025118864 8.110393833 |
0.026607251 8.17465778 |
0.028183829 8.240658426 |
0.029853826 8.309120776 |
0.031622777 8.380984996 |
0.033496544 8.45748195 |
0.035481339 8.540078125 |
0.03758374 8.630078125 |
0.039810717 8.727064902 |
0.04216965 8.828507606 |
0.044668359 8.932403665 |
0.047315126 9.039320995 |
0.050118723 9.151604466 |
0.053088444 9.272035039 |
0.056234133 9.402045655 |
0.059566214 9.539359083 |
0.063095734 9.679025452 |
0.066834392 9.818341085 |
0.070794578 9.958367439 |
0.074989421 10.10208578 |
0.079432823 10.25230924 |
0.084139514 10.40913187 |
0.089125094 10.56825622 |
0.094406088 10.72407218 |
0.1 10.87405757 |
0.105925373 11.01881671 |
0.112201845 11.16031675 |
0.118850223 11.30084336 |
0.125892541 11.44255613 |
0.133352143 11.58704982 |
0.141253754 11.73494245 |
0.149623566 11.88637822 |
0.158489319 12.04226027 |
0.167880402 12.2047028 |
0.177827941 12.37655833 |
0.188364909 12.56033439 |
0.199526231 12.75639404 |
0.211348904 12.96170428 |
0.223872114 13.17157565 |
0.237137371 13.38267082 |
0.251188643 13.59438987 |
0.266072506 13.8085529 |
0.281838293 14.0286319 |
0.298538262 14.25934561 |
0.316227766 14.50676219 |
0.334965439 14.77838601 |
0.354813389 15.08187205 |
0.375837404 15.42232747 |
0.398107171 15.80223652 |
0.421696503 16.22161046 |
0.446683592 16.6788365 |
0.473151259 17.1728922 |
0.501187234 17.70687053 |
0.530884444 18.29561927 |
0.562341325 18.96537427 |
|
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| |
| MP Tabular Report | Options Report
| |
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
| 4059- Fewer than 2 points available for MP|
| | Analysis Conditions
| |
| |
| |
| Preparation
|
| Fast evacuatio
| Evacuation rat
| Evacuation tim
| Leak test:
| Use TranSeal:
|
|
| Free Space
|
| Measured
| Lower dewar fo
| Evacuation tim
| Outgas test:
|
|
| Po and Temperature
|
| Po and T type:
| Po:
| Temperature:
|
|
| Dosing
|
| Use first press
| Use maximum v
| Target toleran
|
|
| Equilibration
|
| Equilibration
| Minimum equili
|
|
| Sample Backfill
|
| Backfill at star
| Backfill at end
| Backfill gas:
|
|
| Adsorptive Properties
|
| Adsorptive:
| Maximum manif
| Non-ideality fa
| Density conver
| Therm. tran. h
| Molecular cros
| Adsorbate Mol
|
|
| Inside diamete
|
|
|
|
|
SiO2 | Sample: SiO2
| Submitter:
|
|
|
|
|
|
|
|
|
ptions Report | Sample log
|
| Date Time Log Message
| 1/31/2019 12:18:04 PM Started analysis of file Si02.
nalysis Conditions | 1/31/2019 12:18:04 PM System volume: 18.1544 cm³
| 1/31/2019 12:29:46 PM Pressure transducer zeroed.
| 1/31/2019 12:29:46 PM Helium Purged: 30 seconds
| 1/31/2019 12:37:57 PM Measured free space on port
| 1/31/2019 12:48:57 PM Pressure transducer zeroed.
| 1/31/2019 7:56:22 PM Finished a sample analysis f
No |
5.0 mmHg/s |
0.10 h |
No |
No |
|
|
|
|
|
Yes |
0.10 h |
No |
|
|
o and Temperature |
|
Enter Po below. Enter the Analysis Bath T |
760.000 mmHg |
-195.850 °C |
|
|
|
|
No |
No |
5.0% or 5.000 mmHg |
|
|
|
|
5s |
600 s |
|
|
ample Backfill |
|
Yes |
Yes |
N2 |
|
|
dsorptive Properties |
|
Nitrogen |
1,050.00 mmHg |
0.0000620 |
0.0015468 |
0.38600 nm |
0.162 nm² |
2.00 |
|
|
9.53 mm |
|
|
|
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiO2
| Operator: wawan
| Submitter:
0\data\SAMPEL\2019\Janu| File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\Si02.SMP
|
|
N2 | Started: 1/31/2019 12: Analysis AdsorN2
-195.850 °C | Completed: 1/31/2019 7:5 Analysis Bath -195.850 °C
No | Report Time: 7/25/2019 10: Thermal CorrecNo
11.1152 cm³ M| Sample Mass:0.1781 g Warm Free Sp11.1152 cm³ Measured
5s | Cold Free Spa32.0438 cm³ Equilibration In5 s
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
| Validation Report
|
|
tarted analysis of file Si02. |
ystem volume: 18.1544 cm³| Isotherm Reports
ressure transducer zeroed. |
elium Purged: 30 seconds | Free Space: Low free space values may be
easured free space on port| observed when using liquid argon or ice baths.
ressure transducer zeroed. |
nished a sample analysis f | Po Passed
|
|
| Pressure/Volu Passed
|
|
| Desorption Not within limits. Increase the sample mass, increase
| the equilibration interval, or check the free space.
|
|
|
|
| BET Reports
|
| C Value: Passed
|
|
| Correlation Coe
Passed
|
|
| Surface area: Passed
|
|
| Pressure RangThe selected BET relative pressure range is outside the
| recommended values of 0.05 to 0.30.
|
|
|
|

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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

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