CERTIFICATE OF ANALYSIS

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1. Identification

Catalogue
B689410 CAS Number: 17316-67-5
Number:
Synonym: P-[1-(Butylamino)-1-methylethyl]-phosphinic
Acid, ;[1-(Butylamino)-1-methylethyl]-
Product: Butafosfan
phosphinic Acid; 1-(Butylamino)-1-
methylethylphosphonous Acid; Butaphosphan
Structure: Molecular Formula:

C₇H₁₈NO₂P

Molecular weight:
179.2
Source of Product:
N/A
Solubility:
Methanol (Slightly)

Lot Number: 6-CGS-6-1 Purity: 98%

Shipping This Product Is Stable To Be Shipped At Room Storage Hygroscopic, -20°C Freezer, Under inert
Condition: Temperature Condition: atmosphere

2. Warning

Warning 1: Warning 2: Warning 3:

3. Analytical Information

Tests: Specifications: Results:

Appearance White to Off-White Solid White Solid
NMR Conforms to Structure Conforms
P NMR Conforms to Structure Conforms
MS Conforms to Structure Conforms
HPLC Purity >95% 98.93%

TLC Conditions: C18; Methanol : Water = 7 : 3; Visualized with KMnO4 and Ninhydrin; Single
Additional Information:
Spot, Rf = 0.75.
Purity is based on the analytical results of the tests performed. NMR and TLC may have an accuracy +-2%. Isotopic purity is
based on mass distribution observed.

4. Signatures

LotNumber Reviewed By Reviewed By C of A Approved By

6-CGS-6-1 Eric Beaton My Nguyen

Test Date Xhoana Gjergji

11/15/2018
Retest Date Date Date Date
11/13/2022 11/15/2018 11/15/2018 11/20/2018