Pages 1 of 3

DR. REDDY'S LABORATORY - FTO 9, DUVVADA, VIZAG

ANFD PROCESS SYSTEM

Process Name : Feed, Filtration & Spent Transfer (Process/Solvent Rinse)

User name : Administrator
Equipment ID : 1701075

Batch Data
Batch Number : PR-FT09-001645
Batch Name : Placebo
Progressive Number : 551
Start Date & Time : 2022-09-02 11:11:47
End Date & Time : 02-09-2022 11:57:13

Parameters
Steps Setpoint Ranges Unit
Slot Quantity 16.0 0-30 Kg.
ANFD Jacket Temp. Setpoint 5.0 -20 - 150 °C
Agitator RPM Setpoint 80 5-100 RPM
Agitator direction Forward - -
Pressure Setpoint 1000 1000-3000 mbar
Pressure Filtration ML Tank Level Setpoint 15.0 0-50 Ltrs.
CP-01 RPM Setpoint 1500 50-2800 RPM

Date-Time CV-05(KG) PT-101 (mbar) TT-101 (°C) TT-103 (°C) HCS_201(°C) LT-101 (Ltr) Agi(RPM) CP-01 (RPM) STAGE
2022-09-02 11:11:47 341.0 -11 17.0 25 7 0 80.0 0
2022-09-02 11:12:47 337.0 52 16.4 25 7 0 80.0 0
2022-09-02 11:13:07 326.0 40 13.5 25 6 0 80.0 0 Filtration
2022-09-02 11:13:47 324.0 1333 11.5 12 6 2 80.0 0 Filtration
2022-09-02 11:14:47 325.0 912 13.1 9 6 2 0.0 0 Filtration
2022-09-02 11:15:47 326.0 1284 13.7 13 7 2 80.0 0 Filtration
2022-09-02 11:16:47 325.0 1066 13.7 12 6 2 80.0 0 Filtration
2022-09-02 11:17:47 324.0 1373 13.7 12 6 2 80.0 0 Filtration
2022-09-02 11:18:16 325.0 1337 13.6 13 6 2 80.0 0 Spent Transfer
2022-09-02 11:18:19 324.0 1155 13.6 13 6 1 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:18:21 326.0 1154 13.6 13 6 1 0.0 0 Stage 1- Feed transfer
2022-09-02 11:18:47 314.0 45 10.9 14 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:19:01 308.0 37 9.9 15 6 1 80.0 0 Filtration
2022-09-02 11:19:47 308.0 1815 8.6 9 6 8 80.0 0 Filtration
2022-09-02 11:20:47 308.0 1277 9.0 9 6 16 80.0 0 Filtration
2022-09-02 11:21:36 307.0 1259 9.9 9 6 15 80.0 0 Spent Transfer
2022-09-02 11:21:47 307.0 1110 10.0 10 6 8 0.0 1500 Spent Transfer
2022-09-02 11:22:16 307.0 1106 10.3 12 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:22:20 306.0 1106 10.4 13 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:22:47 296.0 44 8.3 14 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:22:57 289.0 42 7.9 15 6 1 80.0 0 Filtration
2022-09-02 11:23:47 289.0 1127 7.0 8 6 9 80.0 0 Filtration
2022-09-02 11:24:47 290.0 1447 8.0 8 6 13 80.0 0 Filtration
2022-09-02 11:25:47 289.0 1428 8.8 8 6 13 80.0 0 Filtration
2022-09-02 11:25:50 289.0 1155 8.8 8 6 14 80.0 1500 Spent Transfer
2022-09-02 11:26:30 290.0 1045 9.1 11 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:26:34 289.0 843 9.1 11 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:26:47 285.0 62 8.1 12 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:27:09 274.0 543 7.2 13 6 0 80.0 0 Filtration
2022-09-02 11:27:47 271.0 1324 6.6 8 6 3 80.0 0 Filtration
2022-09-02 11:28:47 271.0 1440 6.7 8 5 11 80.0 0 Filtration
2022-09-02 11:29:08 272.0 1119 7.0 8 5 11 80.0 1500 Spent Transfer
2022-09-02 11:29:45 270.0 954 7.6 11 5 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:29:47 272.0 954 7.6 11 6 0 0.0 0 Stage 1- Feed transfer
2022-09-02 11:29:47 272.0 954 7.6 11 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:30:25 253.0 42 6.2 13 6 0 80.0 0 Filtration
2022-09-02 11:30:47 254.0 1075 6.0 8 6 2 80.0 0 Filtration
2022-09-02 11:31:47 255.0 1114 6.0 7 6 12 80.0 0 Filtration
2022-09-02 11:32:13 255.0 1099 6.4 7 6 12 80.0 0 Spent Transfer
2022-09-02 11:32:47 254.0 1281 6.9 10 6 1 0.0 1500 Stage 1 - Achieving temp
Done By Checked By Reviewed By
(Production) (Production) (QA)

Sign and Date Sign and Date Sign and Date

 Pages 2 of 3

DR. REDDY'S LABORATORY - FTO 9, DUVVADA, VIZAG

ANFD PROCESS SYSTEM
2022-09-02 11:32:50 254.0 1281 6.9 10 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:33:27 237.0 1285 5.9 12 6 1 80.0 0 Filtration
2022-09-02 11:33:47 237.0 1215 5.7 8 6 2 80.0 0 Filtration
2022-09-02 11:34:48 237.0 1468 5.7 7 6 13 80.0 0 Filtration
2022-09-02 11:35:48 228.0 1185 6.6 8 6 13 80.0 0 Filtration
2022-09-02 11:36:48 202.0 1165 7.2 8 6 13 80.0 0 Filtration
2022-09-02 11:37:48 176.0 1359 7.6 9 6 12 80.0 0 Filtration
2022-09-02 11:38:48 153.0 1156 7.9 11 6 13 80.0 0 Filtration
2022-09-02 11:39:48 132.0 1239 8.1 11 5 13 80.0 0 Filtration
2022-09-02 11:40:10 123.0 1296 8.2 12 6 12 80.0 0 Spent Transfer
2022-09-02 11:40:48 115.0 1137 8.3 13 6 5 0.0 1500 Spent Transfer
2022-09-02 11:41:31 115.0 1132 8.4 15 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:41:33 115.0 1132 8.4 15 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:41:48 109.0 90 7.7 15 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:42:02 98.0 63 6.9 15 6 1 80.0 0 Filtration
2022-09-02 11:42:48 84.0 1044 6.0 8 6 5 80.0 0 Filtration
2022-09-02 11:43:48 61.0 992 6.0 8 6 14 80.0 0 Filtration
2022-09-02 11:44:28 54.0 1315 6.6 8 6 12 80.0 1500 Spent Transfer
2022-09-02 11:44:48 54.0 1262 6.8 9 6 5 0.0 1500 Spent Transfer
2022-09-02 11:45:25 54.0 1252 7.1 12 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:45:27 54.0 1251 7.1 12 6 0 0.0 0 Stage 1- Feed transfer
2022-09-02 11:45:48 54.0 -5 6.9 12 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:46:48 45.0 285 5.7 15 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:47:35 37.0 70 5.2 15 6 0 80.0 0 Filtration
2022-09-02 11:47:48 36.0 1147 5.2 8 6 1 80.0 0 Filtration
2022-09-02 11:48:48 36.0 1299 5.0 7 6 10 80.0 0 Filtration
2022-09-02 11:49:34 36.0 1419 5.6 7 6 11 80.0 1500 Spent Transfer
2022-09-02 11:49:48 36.0 1242 5.8 9 6 5 0.0 1500 Spent Transfer
2022-09-02 11:50:16 36.0 1232 6.2 11 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:50:20 36.0 1232 6.2 11 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:50:48 29.0 103 5.0 12 5 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:51:18 20.0 106 4.5 14 5 0 80.0 0 Filtration
2022-09-02 11:51:48 20.0 1465 4.2 6 6 2 80.0 0 Filtration
2022-09-02 11:52:48 19.0 1496 4.3 6 6 11 80.0 0 Filtration
2022-09-02 11:53:16 19.0 1375 4.8 7 6 11 80.0 1500 Spent Transfer
2022-09-02 11:53:48 19.0 1109 5.2 9 6 1 0.0 1500 Spent Transfer
2022-09-02 11:53:50 19.0 1109 5.3 9 6 0 0.0 0 Stage 1 - Achieving temp
2022-09-02 11:53:54 19.0 1109 5.3 10 6 0 80.0 0 Stage 1- Feed transfer
2022-09-02 11:54:48 6.0 51 4.1 13 6 1 80.0 0 Stage 1- Feed transfer
2022-09-02 11:54:56 2.0 80 4.0 13 6 1 80.0 0 Filtration
2022-09-02 11:55:48 2.0 1359 3.6 6 6 6 80.0 0 Filtration
2022-09-02 11:56:33 2.0 1377 3.9 6 6 12 80.0 1500 Spent Transfer
2022-09-02 11:56:48 2.0 1222 4.2 7 6 5 0.0 1500 Spent Transfer
2022-09-02 11:57:13 2.0 1215 4.6 9 6 0 0.0 0 Cycle Completed
2022-09-02 11:57:14 2.0 1215 4.6 9 6 0 0.0 0 Cycle Completed

Done By Checked By Reviewed By

(Production) (Production) (QA)

Sign and Date Sign and Date Sign and Date

 TEMPERATURE (°C)

Done By
(Production)

Sign and Date

0.0
5.0
30.0

10.0
15.0
20.0
25.0
2022-09-02 11:11:47

TT 103
TT 101
PT-101

HCS-201
2022-09-02 11:14:47
2022-09-02 11:18:16
2022-09-02 11:19:01
2022-09-02 11:21:47
2022-09-02 11:22:57

ANFD PRESSURE
2022-09-02 11:25:50

ANFD TEMPERATURE
ANFD TEMPERATURE
2022-09-02 11:27:09

ANFD Jacket Temperature

2022-09-02 11:29:45

Legends
2022-09-02 11:30:47
2022-09-02 11:32:50
2022-09-02 11:35:48
2022-09-02 11:39:48

DATE & TIME

2022-09-02 11:41:33

-20 - 150
2022-09-02 11:43:48
GRAPH -FEED TRANSFER

2022-09-02 11:45:27
2022-09-02 11:47:48
2022-09-02 11:50:16
2022-09-02 11:51:48
2022-09-02 11:53:50
2022-09-02 11:55:48
2022-09-02 11:57:14

Checked By
(Production)

Sign and Date

0
500

-500
2000

1000
1500

PRESSURE (mbar)
Pages 3 of 3

Sign and Date

Reviewed By
(QA)