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THERMAL
CONDUCTIVITY
∙∙ What is the heating/cooling load of a building?
∙∙
How does this change with the weather and how can you improve it?
How can you optimize the heat transfer from an electronic component?
How do you design a heat exchanger system to achieve the required
efficiency and what are the best materials to use?
The HFM 446 Lambda Series is based on various relevant standards, e.g.,
ASTM C518, ISO 8301, JIS A1412, DIN EN 12664* and DIN EN 12667.
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2
The HFM is an exact, fast and easy-to-use
instrument for measuring the low thermal
conductivity λ of insulation materials.
PRINCIPLE OF OPERATION
In a heat flow meter (HFM), the test specimen is placed between two
heated plates controlled to a user-defined mean sample temperature and .
Q L λ in SI unit [W/(m·K)] or
temperature gradient to measure heat flowing through the specimen. The λ = – –– British Thermal Units
A ΔT
sample thickness L is measured by an internal thickness gauge. Alterna- [Btu in/(h·ft2·°F)]
tively, the user can enter and drive to the desired thickness,
. which is of
particular interest for compressible samples. The heat flow Q through the R in SI unit [(m2·K/W)] or
L
sample is measured by two calibrated heat flux transducers covering a large R=– British Thermal Units
λ [(h·ft2·°F)/Btu]
area of both sides of the specimen.
After reaching thermal equilibrium, the test is done. The heat flux trans-
ducer output is calibrated using a reference standard. For the calculation of U=1
– U in SI unit [W/(m²·K)]
the thermal conductivity λ and the thermal resistance R, the average heat R
flux Q/A, the sample thickness L, and the temperature gradient ΔT are used,
in accordance with Fourier’s Law (see formulas on the right). The thermal
transmittance, also known as U-value, is the reciprocal of the total thermal
resistance. The lower the U-value, the better the insulating ability.
Thickness gauge
Load
Load
Hoisting device
Hot plate
Heat flux transducer
Cold plate
Peltier system
Lower heat sink
Cooling system
3
HFM 446 Lambda Series
dedicated to small, medium and large-sized specimens ...
4
equipped with great features
Saving Ressources in
Eco-Mode
In standby, the HFM 446 Lambda
can be switched to the energy-
saving Eco-Mode or to Idle-Mode
for a quick measurement start. The
timing for when each mode is
active can be adjusted via a
scheduler.
5
HFM 446 Lambda Series
The λ Solution
Fast sample change
without affecting the
plate temperatures
Three thermocouple Various plate openings of the HFM 446 Lambda are possible when changing the specimen
positions in the lower
and upper plates
6
Measuring the thermal conductivity of
compressible materials at variable density
Precise control regulates thickness and therefore, also the density of compressible materials
7
Materials beyond the routine capability of the HFM method can be tested by insertion of
additional thermocouples and rubber interface pads – eliminating the impact of interface
resistance for low thermal resistance and accordingly higher thermal conductivity materials.
The HFM 446 Lambda series can be equipped with an optional instrumen-
tation kit* that expanding its range to lower thermal resistances (down to
0.02 (m2·K)/W) like concrete, wood products, brick, etc.
The optional kit includes thin, compressible rubber pads for use at both
interfaces, and auxiliary thermocouples to be fixed on both surfaces of
the specimen. This increases the temperature accuracy – especially for
applications which require enhanced temperature sensing.
8
The instrument is delivered calibrated and a reference specimen is optio-
nally included for verification. Of course, the list of available reference
materials can be extended by the operator.
ACCESSORIES
AND MORE
Pre-calibrated with Certified
Reference Materials
The design of the testing chamber Along with the thermal conduc-
of the HFM 446 Lambda Series tivity, the HFM 446 Lambda Small
minimizes influences from the and Medium instruments allow for
environment and reduces conden- determination of the specific heat
sation effects inside the testing capacity cp by using the calibration
chamber and on the plate surfaces. factors and accounting for contri-
Optionally, the testing chamber bution of the thermal mass of the
can be purged with dry gas. plates.
9
Software Interface
SmartMode is the user-friendly, For calibration purposes, the The “Wizards” button allows for
smoothly running user interface of thermal conductivity values of the manual parameter input, while the
the HFM Proteus® software. It is most common certified reference User Methods button retrieves
characterized by a logical structure materials, such as NIST SRM 1450d, parameter sets defined by the user
which quickly gives a clear overview are already stored in the software. beforehand. Such “User Methods”
of the current measurement status However, AutoCalibration also can also be transferred to
and provides various report and offers the ability to create cali- “Favorites” for faster access if they
export possibilities. After bration curves for any user-defined are used frequently.
completing the test, all relevant material on the basis of up to 99
results can be directly printed out freely selectable temperatures.
by the integrated printer or a report
can be created by the software
when a PC is connected.
10
Printout of the results
obtained by the
integrated printer
The button “Reports” allows for The λ90/90 value is the basis for Any measurement can be
reports to be generated quickly determination of the declared started by using the pre-defined
and easily by granting access to value of the thermal conductivity instrument parameters (including
various templates; one of these within the realm of CE declarations number and position of thermo-
templates meets all of the require- of building materials. It is calcu- couples, stability criteria, etc.).
ments stipulated by ASTM C518. lated from a measurement series However, experienced users who
Each report can be adapted to the of at least 10 measurements and wish to apply their own parameter
customer‘s own corporate identity. states which thermal conductivity sets can define them under “Setup
In addition, data can easily be values to a probability of 90%, can & Control”.
exported into either Word or Excel be achieved for 90% of the output
format with just a few mouse production volume. The integrated
clicks. The “Full” export button report calculates the λ90/90 value by
exports data, graphs and results a mouse mouse click. The calcu-
together into a single file. Measure- lation is based on your measure-
ment data is stored in binary ments; no additional documen-
format and is thus fully tamper- tation and calculation are required.
proof.
11
Performance & Applications
Performance Checked on EPS Material
0,0350
EPS (expanded polystyrene). 24°C
0,0340
0,0345
Conductivity
0,0330 8 °C
dimensions of 600 mm x 600 mm x
25 mm (HFM 446 Lambda Large), 0,0320
0,0325
8 °C
300 mm x 300 mm x 25 mm 0,0315
(HFM 446 Lambda Medium) and 0,0320
-2,50 -2,00 -1,50 -1,00 -0,50 0,00 0,50 1,00 1,50 2,00 2,50
300 mm x 300 mm x 25 mm (HFM 0,0315 Density minus 26 [kg/m³]
446 Lambda Small) is reproducible -2,50 -2,00 -1,50 -1,00 -0,50 0,00 0,50 1,00 1,50 2,00 2,50
to within about ± 0.5%. The mean Temperature- and density-dependent thermal
Density minus 26conductivity
[kg/m³] of 30 different
NETZSCH EPS specimens.
thermal conductivity (formula
stored also in the software)
depends on the temperature
and also slightly on the specimen 1,00%
density (mean value 26 kg/m3).
NETZSCH EPS
0,80%
1,00%
NIST SRM 1450d
The lower figure is also evidencing
NETZSCH EPS
the thermal conductivity's 0,60%
0,80%
NIST SRM 1450d
excellent reproducibility of better
than ± 0.5%. During a period of 2 0,40%
0,60%
to 3 weeks, 100 different NETZSCH
0,20%
0,40%
EPS specimens were measured.
0,00%
0,20%
0 10 20 30 40 50 60 70 80 90 100
-0,20%
0,00%
0 10 20 30 40 50 60 70 80 90 100
-0,40%
-0,20%
-0,60%
-0,40%
-0,60%
0.03
0.045 0.03 Pressure (kPa)
[W/(m·K)]
12 0.040
0.03 Pressure (kPa)
0.03
0 10 20 30 40 50 60 70 80 90 100
-0,20%
0,40%
-0,40%
0,20%
-0,60%
0,00%
Investigation of the Correlation Between0Density
10 and
20 30 40 50 60 70 80 90 100
-0,40%
0.050
With the “Variable Load” feature, -0,60%
the density-conductivity corre- 0.03
lation of compressible materials 0.045
Thermal conductivity/[W/(m·K)]
can be investigated. The case
study presented here validates 0.03 Pressure (kPa)
the expected multi-mode heat 0.050
0.040
0.03
transfer within glass-fiber insula-
0.03
tions. While the specimen is 0.19
progressively compressed with an
Thermal conductivity/[W/(m·K)] 0.045
0.035
0.68 21.3
increasing load, represented here 10.9
1.51Pressure (kPa)
4.63
0.03
by the equivalent surface pressure,
0.040
the combined conductivity first 0.030 0.03
decreases due to a reduction
0.19
in radiative heat transfer, and
0.035
0.025
then increases as conductive heat 21.3
0 20 0.68
40 1.51 60 804.63 100 10.9
120 140 160 180
transfer becomes more pre-
Density [kg/m3]
dominant.
0.030
Thermal conductivity of a glass-fiber as a function of density
1,30
Conductivity / W/(m·K)
0.025
1,25
Low Thermal Resistance – Measurable in0 the HFM
1,20
20 446
40 Lambda
60 Series100
80 120 140 160 180
Density [kg/m3]
1,15
The use of the instrumentation kit
(see page 8) is crucial for materials 1,10
1,30
/ W/(m·K)
1,00
1,20 Sample C in HFM
thickness of 25 mm and a thermal Sample B1 in LFA
Sample B2 in LFA
Thermal Conductivity
50
150 Temperature 40,0
2.8%. Therefore, both measurement
20,0
methods are within the stated uncer- Interface pad 35,0
tainty of ± 5% for this material. 1000 15,0
0Sample5 10 15 20 25 30 35
Qupper 40 45 30,0
TimeQ/lower
min
Interface pad Qtotal 10,0
25,0
Q / W/m²
-50
50 Temperature
Literature : [1] I. Williams, R. E. Shawyer: 5,0
Certification report for a pyrex glass reference 20,0
material for thermal conductivity between -100
0 0,0
-75°C and 195°C; Commission of the European 0 5 10 15 20 25 30 35 40 45 15,0
Communities; Luxembourg; 1991 Use and comoponents of the Time
instrumentation
/ min kit
10,0
-50
5,0
13
1,2
-100 0,0
0
0 20
20 40
40 60
60 80
80 100
100 120
120 140
140 160
160 180
180
Density [kg/m
Density [kg/m3]]
3
Cp Measurement
1,30
1,30
W/(m·K)
Conductivity//W/(m·K)
1,25
1,25
1,20
1,20
ThermalConductivity
1,15
1,15
1,10
For measurement of the specific heat capacity,
1,10cp, with the HFM 446 Lambda, both plates are held at exactly the
same temperature. When there is no more 1,05heat flux between the two plates,
1,05 Sample aAtemperature
Sample A in
in HFM
HFM
step is initialized.
Heat-flux transducers measure the resulting heat flux into the sample and the plates,
Sample
Sample B
B in the signal is integrated and
in HFM
HFM
Thermal
1,00 Sample CC in
in HFM
evaluated. By performing a so-called empty1,00
stack measurement (system Sample
without
Sample
Sample B1
B1 in
in
HFM
sample)
LFA
LFA prior to the sample
0,95 Sample B2
B2 in LFA
in
measurement, the specific heat of the system is taken into consideration. Sample
0,95 LFA
Literature CRM - European Commission ± 5% Literature CRM - European Commission ± 5%
0,90
0,90
The HFM 446 Lambda Small and Medium versions 0 can
0 5 measure
5 10 15 the
10 15 20 specific
20 25
25 3030heat
35capacity
35 40 45(Si50
40 45 unit55
50 J/(g·K))
55 60 of
60 65 solid
65 70
70
Temperature // °C
polymers such as polyamide or PVC, and of insulation materials such asTemperature
glass wool.°C
°C
Qtotal 25,0
W/m²
Temperature//°C
25,0
QQ//W/m²
50 total
of an insulation material can 50 Temperature
Temperature
Temperature
dampen temperature changes of the 20,0
20,0
outer environment and contribute 0
0 15,0
to a constant indoor climate. 0
0 5
5 10
10 15
15 20
20 25
25 30
30 35
35 40
40 45
45 15,0
Time // min
Time min
10,0
10,0
Glass wool was investigated with -50
-50
two different HFM 446 Lambda 5,0
5,0
Medium devices within a temper-
ature range of 0°C to 70°C and -100
-100 0,0
0,0
different temperature steps (10 K Heat flux and temperature of one temperature step between 25°C and 35°C
and 20 K). during a cp measurement with the HFM 446 Lambda Medium on a glass fiber
insulation featuring sample dimensions of approx. 30 cm x 30 cm x 2.5 cm and
a mass of approx. 300 g
The upper figure shows the measure-
1,2
ment signals of the temperature and 1,2
heat flux of one temperature step
versus time of the glass fiber sample. 1,1
1,1
J/(g·K)
14
Technical Specifications
HFM 446 Lambda Series
Standards ASTM C518, ISO 8301, JIS A1412, DIN EN 12667, DIN EN 12664*
Type Stand-alone, with integrated printer
∙
Medium: 0.002 to 2 W/(m·K)**
Large: 0.001 to 0.5 W/(m·K)**
Small and Medium: 2.0 W/(m·K) achievable with optional instrumentation kit,
Thermal conductivity recommended for hard materials and those with higher thermal conductivity
∙∙
range Performance data:
Accuracy: ± 1% to 2%
∙
Repeatability: ± 0.25 %
Reproducibility: ± 0.5%
→ All performance data is verified with NIST SRM 1450 D (thickness 25 mm)
Plate temperature range -20°C to 90°C, optional for the HFM 446 Lambda Medium: -30° to 90°C
Air-tight system Sample compartment with possibility to introduce purge gas
Metering area heat
flux transducer
∙∙ Small/Medium: 102 mm x 102 mm
Large: 254 mm x 254 mm
Chiller system External; constant temperature setpoint over plate temperature range
Plate temperature control Peltier system
Plate motion Motorized
Three thermocouples on each plate, type K (two extra thermocouples with
Plate thermocouples
instrumentation kit)
Thermocouple resolution ± 0.01°C
Number of setpoints Up to 99
∙
Medium: 305 mm x 305 mm x 105 mm
(max.)
Large: 611 mm x 611 mm x 200 mm
∙∙
Small: 0 to 854 N (21 kPa on 203 x 203 mm²)
∙
Medium: 0 to 1930 N (21 kPa on 305 x 305 mm²)
Variable load/
Large: 0 to 1900 N (5 kPa on 611 x 611 mm2)
contact force
Force-controlled adjustment of the contact force or the desired thickness, and
thus density, of compressible materials
∙∙
Automatic measurement of mean sample thickness
∙
Thickness determination Four-corner thickness determination via inclinometer
Compliance to non-parallel specimen surfaces
∙
SmartMode (incl. AutoCalibration, report generation, data export, wizards,
user methods, predefined user definable parameters, user-defined parameters,
∙∙
cp determination, etc.)
Storage and restoration of calibration and measurement files
Software features
∙∙
λ90/90 Report
Plot of plate/mean temperatures and thermal conductivity values
∙
Monitoring of heat flux transducer signal
Creation/selection of configurations for stand-alone-operation (without PC)
15
The NETZSCH Group is an owner-managed, international technology
company with headquarters in Germany. The Business Units Analyzing &
Testing, Grinding & Dispersing and Pumps & Systems represent customized
solutions at the highest level. More than 3,800 employees in 36 countries and
a worldwide sales and service network ensure customer proximity and
competent service.
NGB · HFM 446 Lambda Series · EN · 0321 · NWS · Technical specifications are subject to change.
NETZSCH-Gerätebau GmbH
Wittelsbacherstraße 42
95100 Selb
Germany
Tel.: +49 9287 881-0
Fax: +49 9287 881 505
at@netzsch.com