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Procedia Manufacturing 00 (2019) 000–000
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Procedia
Procedia Manufacturing
Manufacturing 00
00 (2019)
(2019) 000–000
000–000 www.elsevier.com/locate/procedia
www.elsevier.com/locate/procedia
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Abstract
Abstract
Abstract
In Selective Laser Sintering and Melting it is necessary to protect metal powder deposited on the powder bed from contact with atmospheric
In
air,Selective
In Selective
which may Laser
leadSintering
Laser Sintering and
and Melting
to oxidation Melting it
it is
and downgradingis necessary
necessary
of theto protect
protect metal
to propertiesmetal powder
powder
of the deposited
deposited
powder on
on the
the powder
in the presence of highbed
powder bed from
from contactthatwith
contact
temperature with atmospheric
atmospheric
is necessary for
air,
air, which may
mayorlead
which full
achieving lead to
to oxidation
partialoxidation and
and downgrading
melting. Thus, the buildingof
downgrading the
the properties
ofchamberproperties of
of the
the powder
of commercially powder in
in the
available presence
theSLS/SLM of
of high
high temperature
presence machines temperature that
that is
is fully isolated necessary
isand
necessary for
for
filled with
achieving
achieving full
full or
or partial
partial melting.
melting. Thus,
Thus, the
the building
building chamber
chamber of
of commercially
commercially available
available SLS/SLM
SLS/SLM machines
machines is
is
inert shielding gas which may need to be replenished before each build session thereby raising both machine building and consumables costs. fully
fully isolated
isolated and
and filled
filled with
with
inert
In thisshielding
inert paper, itgas
shielding gas which
which may
is examined may need to
to be
be replenished
needComputational
using Fluidbefore
replenished before each
each build
Dynamics build session
session thereby
how protection of the raising
thereby powderboth
raising areamachine
both machine building
building
around the and consumables
and can
laser spot consumables
be achievedcosts.
costs.
by
In
In this
this paper,
paper, it
it is
is examined
examined using
using Computational
Computational Fluid
Fluid Dynamics
Dynamics how
how protection
protection of
of the
the powder
powder area
area around
around the
the laser
laser
locally insulating it from air by gas circulation in a suitably designed box moving with the laser beam. Full coverage of the respective area and spot
spot can
can be
be achieved
achieved by
by
locally
locally
at the sameinsulating
insulating
time no it
it from
from air
air by
by gas
disturbance gas circulation
circulation
of the in
in aa suitably
powder particles suitably
withindesigned
designed box
box moving
moving
it are critical with
with the
requirements. laser
theTwo beam.
beam. Full
laserconcept Full coverage
coverage
variants of
of the
the respective
are studied respective
and simulatedarea and
areawith
and
at
at the
the same
promising time
time no
sameresults.no disturbance
disturbance ofof the
the powder
powder particles
particles within
within itit are
are critical
critical requirements.
requirements. TwoTwo concept
concept variants
variants are
are studied
studied and
and simulated
simulated with
with
promising
promising results.
results.
© 2020 The Authors. Published by Elsevier Ltd.
© 2020
©
© 2021
2020
This is an The
The
The Authors.
Authors.
Authors.
open Published
accessPublished
Published
article by by
the Elsevier
by Elsevier
under Elsevier Ltd. Ltd. license https://creativecommons.org/licenses/by-nc-nd/4.0/)
Ltd.
CC BY-NC-ND
Thisis
This
This isisan
Peer-review anopen
an open
open access
access
access
under article
article
article under
under
under
responsibility of the theBY-NC-ND
CC CC BY-NC-ND
the scientific
CC BY-NC-ND
committee oflicense
license
license (https://creativecommons.org/licenses/by-nc-nd/4.0/)
https://creativecommons.org/licenses/by-nc-nd/4.0/)
https://creativecommons.org/licenses/by-nc-nd/4.0/)
the FAIM 2020.
Peer-reviewunder
Peer-review
Peer-review underresponsibility
under responsibility
responsibility of of
of thethe
the scientific
scientific
scientific committee
committee
committee of of FAIM
of the
the the FAIM
FAIM 2020.2021.
2020.
Keywords: Selective Laser Sintering; inert gas; protection; insulation; metal powder
Keywords: Selective
Keywords: Selective Laser
Laser Sintering;
Sintering; inert
inert gas;
gas; protection;
protection; insulation;
insulation; metal
metal powder
powder
In order to circumvent this problem, atmospheric air is each use is certainly not negligible; to make savings special
replaced by a non-reacting shielding gas. Moreover, in order storage reservoirs may be used in an airtight recirculating
to divert vaporised powder from the laser beam path (thereby system together with appropriate filters which increase the
safeguarding the latter’s nominal properties) an artificially machine acquisition cost [15].
created flow of the shielding gas may be required. In the latter Following these basic considerations, this paper studies the
case, it is important to realize that flow properties depend on creation of a local protective gas flow solution by using
several parameters: (a) particle size, shape and distribution (b) computational fluid dynamics (CFD) simulation. Section 2
chemical composition (c) moisture (d) temperature [1]. discusses gas flow over deposited non-sintered powder layer
Uniformity of gas flow is needed in order to achieve and how the latter may be disturbed locally. Section 3
consistency of mechanical properties of the porous products presents and evaluates a device based on one inflow and one
[2]. outflow orifice, whilst Section 4 presents and evaluates an
There have been various studies on the effects of the improved device. Section 5 briefly discusses findings,
shielding gas on the different facets of SLM, and secondarily summarizes conclusions and points to further work.
of SLS, focusing on specific powder materials and specific
gas types, but formulation of a full and generally applicable 2. Lift and drag forces on powder particles
theory cannot be claimed yet [3].
The type of gas used, e.g. Argon or Nitrogen, does not Flowability of a powder particle is influenced by the
seem to affect the mechanical properties of the built part [4] adhesive forces between individual particles. These for fine-
but according to other studies, Argon seems to favour a grained, dry bulk solids, are essentially due to Van der Waals
promoted microstructure compared to Nitrogen when interactions. By contrast, for moist bulk solids, liquid bridges
processing Inconel [5] and a sounder surface morphology are formed in the contact area of particles where low capillary
when processing TiC/AlSi10Mg by SLM [6]. Helium was pressure prevails due to surface tension effects. Whichever the
claimed to promote build rate increase of 304L stainless steel nature of adhesive forces is, the size of the particles and the
through better control of the melt profiles via a smaller distance between them are very important.
plasma [7]. Similarly, a mixture of 50% Argon and 50% Whether a bulk solid flows well or poorly depends on the
Helium was proved to increase build rate of Ti-6Al-4V by relationship of the adhesive forces to the other forces acting
44% and achieve density of 99.98%, yet at the expense of on it. If powder particles are pressed against each other, due to
increased residual stresses [8]. the miniscule size of contact area large stresses prevail
Typically, the build chamber of the SLS/SLM machine is locally, leading to plastic deformation, a greater area of
initially flooded with non-reactive gas, so as to reduce oxygen contact, lower inter-particle distance and an increase in
below 0.1%, and then, the flow is maintained throughout adhesive forces.
processing. There are various ways to deliver inert gas in the In addition, it is proven that as the particle diameter
build chamber, e.g. nozzles, a gas rail or annular flow reduces, adhesive forces increase. As a result, the finer the
systems, all of which generally maintain a clear direction of powder, the harder it is to flow. Moreover, since adhesive
flow [2]. forces are connected to the exerted loading, time is inherently
A very recent coupled CFD-DPM simulation study tried to relevant to cohesion of powders and so is stress history [16].
identify the critical flow velocity at a distance of 1 mm above An initial investigation was carried out on the magnitude
the powder bed that causes displacement of powder particles. of gas flow velocity that is expected to create enough force to
Velocities between 0.2 and 1 m/s were examined. An inlet blow away powder grains. For this reason powder grains were
and an outlet nozzle rail were placed at the ends of the build considered as spheres, arranged as in Fig. 2(a).
chamber. Downward bending of the velocity vector was
observed and was counteracted by additional nozzles as well
as appropriate positioning of the outlet nozzles [9].
At velocities in the range 0 to 5 m/sec [10] it has been
clearly observed that some powder particles are spattered;
these may be blown away by the gas flow [11] and/or may
cause beam scattering, thereby lowering the energy available
for sintering or melting the powder bed [12]. Thus, in the
presence of high gas flow velocities the scanning (feed)
direction of the laser is closely related to the gas flow
direction. Spatter concentration was examined by CFD
simulation in a build chamber with an inlet and an outlet flow
nozzle rail with average flow velocity over the powder bed
ranging between 0.6 and 1.5 m/s [13]. In some cases pressure
of the inert gas may be varied, typically between 10 and 105
Pa (0.01 mbar to 1 bar), low pressure dictating scanning speed Fig. 2. Idealized powder particle model (a) arrangement (b) stream lines.
adjustment to safeguard integrity of the built product [14].
From a cost point of view, using large amounts of Five spheres of 15 µm radius were examined
shielding gas to fill the build chamber and replenish it after corresponding to the top surface of the spread out powder and
90 Iason Sideris et al. / Procedia Manufacturing 55 (2021) 88–95
Author name / Procedia Manufacturing 00 (2019) 000–000 3
the particles just underneath it. It was assumed that after be estimated under some assumptions. The flow adjacent to
application of a compressive force by the roller the spheres the powder bed pushes the material beads to slide against the
will have acquired the most stable position depicted in Fig. 2. previous layer of particles, see Fig. 4.
It was also assumed, according to preliminary calculations
and engineering intuition, that at each contact point between
sphere pairs a displacement of 1 µm in the radial direction
resulted from such compressive forces.
ANSYS Fluent 18 was employed to set up and solve this
model. At first, an orthogonal control volume was defined
around the spheres. The control volume surfaces were
selected sufficiently far from the beads so that their effect to
the flow at the area of interest is trivial. Then, a mesh was
created. tested and refined until the final solutions were
independent from node density. The final mesh consisted of
665000 tetrahedral elements.
To increase precision and reduce computational time, there
were two consecutive solutions, namely one for initializing
data and the other one to obtain the final solution. For the first
solution, Laplace’s equation is solved for the velocity
potential and pressure given the boundary conditions of the
control volume. For the second and most precise solution, the
Fig. 4. Force balance in material beads exposed to an external flow. The
equations of mass and momentum conservation for laminar lower beads are considered to be homogeneously dispersed.
flow are solved. The small crevices around the material
spheres induce a very low Reynolds number and for this The forces opposing the particle migration are the cohesive
reason a turbulence model is avoided. The solver used for forces 𝐹𝐹𝑐𝑐 and the gravitational pull w, counteracted by the
initialization was able to achieve residuals less than 10-4, aerodynamic drag and lift, 𝐹𝐹𝑑𝑑 and 𝐹𝐹𝑙𝑙 . By considering the
while the second solver reduced the residuals to values geometry of Fig. 4, we assume that the moment arms
smaller than 10-6. contributing to the formation of the relevant moments are
Gas flow was assumed to be horizontal, i.e. parallel to the roughly the same and that lift and weight are negligible
powder bed and there were no vertical components. Typical compared to cohesive forces.
stream lines produced can be seen in Fig. 2(b). Under the mentioned assumption, a lower bound for the
The calculated lift and drag forces on the top middle sphere critical drag force that results in the material particles being
are shown in Fig. 3. Note that negative sign in the lift force blown away can be found by calculating the force balance on
corresponds to pushing the sphere towards the powder bed. the central bead. Bead movement from its current position
between spheres 1,2,3,4 to the next stable equilibrium point is
equivalent to separating the central sphere from the substrate
spheres 1 and 2. Thus, the bead is free to slide against the
surface if:
𝐹𝐹⃗𝑐𝑐1 ,𝑥𝑥 + 𝐹𝐹⃗𝑐𝑐2 ,𝑥𝑥 ≤ 𝐹𝐹⃗𝑑𝑑 (1)
Notice that the simplifications made only represent a
conservative scenario, where just a fraction of the cohesion
forces is active and the distribution of the particles on the
substrate does not hinder sliding of the bead.
Following the analysis provided in [17], the predominant
cohesion forces for conductive powder materials with particle
diameters less than 100μm are the Van Der Waals forces. The
interaction force between any two spheres of effective radius
𝑟𝑟𝑒𝑒𝑒𝑒𝑒𝑒 can be calculated as:
𝐹𝐹𝑐𝑐𝑖𝑖 = 𝐴𝐴𝑟𝑟𝑒𝑒𝑒𝑒𝑒𝑒 / 6𝑠𝑠02 = −4𝜋𝜋𝜋𝜋𝑟𝑟𝑒𝑒𝑒𝑒𝑒𝑒 (2)
Fig. 3. Lift and drag forces on top middle sphere for different flow velocities.
where: index i defines the interaction between the main
As can be clearly seen in Fig. 3, the lift force is always and the i-th substrate sphere, A is the Hamaker constant of the
negative, as anticipated because the free area in the bottom material, 𝑠𝑠0 is the contact distance (typically considered to be
half of the sphere is less than its upper half counterpart and, in 𝑠𝑠0 = 4 Å), and γ is the surface energy.
addition, it is a lot harder for the gas to flow between the grain Typical A values for many metallic materials are in the
gaps, thus velocity in the bottom half ia much lower. order of 10-19J, [18]. Taking 𝑟𝑟𝑒𝑒𝑒𝑒𝑒𝑒 = 15𝜇𝜇𝜇𝜇 , the interaction
Τhe necessary force exerted from a gas flow to a particle force value for metallic powders is calculated approximately
for the latter to lose contact with its neighboring material can as 𝐹𝐹𝑐𝑐𝑖𝑖 ~10−4 𝑁𝑁.
Iason Sideris et al. / Procedia Manufacturing 55 (2021) 88–95 91
4 Author name / Procedia Manufacturing 00 (2019) 000–000
For calculating the 𝐹𝐹𝑐𝑐,𝑥𝑥 term, a simple projection of the net to use [20]. The lower end of the cylindrical chamber is fully
force 𝐹𝐹𝑐𝑐 on the plane of 𝐹𝐹𝑑𝑑 is needed, see Fig. 5. After open, see Fig. 6(a).
applying simple geometrical calculations, we can prove that:
Fig. 6. Local insulation chamber (a) concept (b) CAD model (c) orifices.
Fig. 8. Typical velocity vectors at the gap between device and powder bed
(a) full gap (b) partial detail
Table 1 Critical inflow velocity (vin) causing chamber insulation for different 4. Four orifice design of insulation device
feed values (fz and fz) and orifice inclination angle values (φ).
4.1. Design concept
fx fz φ vin VP VV
(mm/s) (mm/s) (ο) (mm/s) (μm/s) (μm/s)
According to the simulation results of the two orifice
0 34 -8.6 -11.8
system, see Table 1, it is evident that this design limits the
1.0 - 30 30 -17.6 -10.7 range of the applicable feed rates. At high feeds, there is no
60 30 -67.7 -11.2 inert gas flow input angle φ that can guaranty the isolation of
0 110 -20.3 -11.8 the device chamber from atmospheric air for an arbitrary
movement direction. This proves that the two orifice design is
2.5 - 30 100 -20.2 -30.7
inefficient, and that more gas inlet surfaces have to be
60 70 -64.2 -28.9
introduced for better controlling the flow inside the chamber
0 250 -6.8 -37.6 and reaching higher laser scanning rates.. Thereby, several
4.5 - 30 - - - new designs were simulated, with the simplest one achieving
60 - - - sufficiently good performance was the four orifice design
depicted in Fig. 11.
0 30 -17.5 -59.4
- 1.0 30 30 -17.1 -11.4
60 30 -5.9 -11.4
0 58 -4.6 -22.3
- 2.5 30 58 -46.4 -22.3
60 70 -86.7 -29.5
0 90 -210.0 -43.4
- 4.5 30 90 -210.0 -32.7 Fig. 11. Four orifice design of the insulation device
60 125 -88.8 -42.3
In this case, the orifices work in pairs. Each pair comprises
In addition, the reason for not expanding this study to juxtaposed orifices, namely one for inflow and one for
higher feed values was that for movement in x direction, the outflow. Outflow rate is 90% of the inflow rate.
insulating capabilities of the device reached their maximum Let θ denote the angle of feed vector f to x axis; then
and, thus, there is no reason to explore further. f=(fx2+fz2)1/2 and tanθ=fz/fx.
Note that for the highest value of fx examined simulations The goal is to create an internal flow that will constantly
demonstrate that chamber insulation is impossible. In keep the chamber isolated and keep, at the same time, keep
particular, Vp reaches its minimum at approximately vin = 120 the velocity field intensity low. To this end, the inflow
mm/s, but it is pointing inwards (Vp > 0) for both inclination velocity at the respective orifices should change in accordance
angles 30o and 60o, see Fig. 10. to θ angle, namely: vinx = vinz tanθ. As a result, the main flow
will always be in the same direction as the feed.
4.2. Results
Table 2 Critical inflow velocity in x and z directions (vin x vin z) causing An issue that is worth investigating pertains to the amount
chamber insulation for different feed magnitude and direction (f and θ). of atmospheric air trapped amongst powder particles and to
what extent this might affect the integrity of the result. In
f θ vin x vin z VP VV
(mm/s) (ο) (mm/s) (mm/s) (μm/s) (μm/s)
addition to the first principles theoretical calculation of
Section 2, experimental evidence is needed to determine the
5 0 111 0 -124 -45.6
maximum flow velocity that disturbs the deposited powder
23 90 38 -88.5 -45.6 layers, which according to this linear relationship will
45 80 80 -920 -55.9 effectively determine the upper limit in laser feed that the
7.5 0 148 0 -79 - insulating system can handle. Thus, a device that follows the
advocated design should be constructed in near future and
23 120 51 -250 -59.2
tested on the prototype SLS/SLM machine on which this is
45 90 90 -470 -60.9
intended to use [20]. The exact way in which the shell will be
10 0 170 0 -24 -59.2 attached to the laser head at an appropriate distance in order to
23 140 59 -110 -67.4 avoid disturbance of the roller-based powder spreading
45 100 100 -71 -66.9 mechanism will be decided as part of the design
implementation exercise.
12.5 0 192 0 -110 -67.4
23 160 68 -99.9 -75.7
45 120 120 -440 -77.7 CRediT author statement
15 0 219 0 -142 -75.7
Iason Sideris: Methodology, Formal analysis, Writing-
23 180 76 -210 -83.6
Original draft preparation. George-Cristopher Vosniakos:
45 130 130 -180 -84.1 Conceptualization, Supervision, Writing-Reviewing and
20 0 258 0 -22 -83.6 editing.
23 220 93 -820 -97.4
45 160 160 -730 -98.9
References
100 45 380 380 -870 -230
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