Sample Code: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR

13C NMR
NICLOSAMIDE PIPERIZINE SALT

39.713
39.500
39.295
SIGMA CHEMI LABS
Solvent: dmso

43.113
40.130
SA-Varian 400MHz NMR

39.918
Date: Dec 25 2020

39.082
124.667
123.445
122.147
121.987
120.401
128.728
132.805

38.878
118.973
140.791
166.017
166.138

116.499
144.632

220 200 180 160 140 120 100 80 60 40 20 0 ppm

Plotname: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR_CARBON_20201225_01_plot01
Sample Code: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR
13C NMR
NICLOSAMIDE PIPERIZINE SALT
SIGMA CHEMI LABS
Solvent: dmso
SA-Varian 400MHz NMR
Date: Dec 25 2020

122.147
123.445
124.667

121.987
120.401
118.973
128.728
132.805
166.017
166.138

140.791

116.499
144.632

180 170 160 150 140 130 120 110 ppm

Plotname: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR_CARBON_20201225_01_plot02
Sample Code: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR
13C NMR
NICLOSAMIDE PIPERIZINE SALT
SIGMA CHEMI LABS
Solvent: dmso
SA-Varian 400MHz NMR
Date: Dec 25 2020

123.445
124.667

121.987

120.401
128.728

122.147
132.805

118.973

116.499
136 134 132 130 128 126 124 122 120 118 116 ppm

Plotname: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR_CARBON_20201225_01_plot03
Sample Code: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR
13C NMR
NICLOSAMIDE PIPERIZINE SALT
SIGMA CHEMI LABS
Solvent: dmso
SA-Varian 400MHz NMR
Date: Dec 25 2020

39.500
39.713

39.295
43.113

39.918

39.082
40.130

38.878
48 47 46 45 44 43 42 41 40 39 38 37 36 35 ppm

Plotname: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR_CARBON_20201225_01_plot04
 INDEX FREQUENCY PPM HEIGHT
13C NMR 1 16697.2 166.138 9.6
NICLOSAMIDE PIPERIZINE SALT 2 16685.0 166.017 12.9
SIGMA CHEMI LABS 3 14535.8 144.632 5.8
4 14149.7 140.791 13.7
5 13347.1 132.805 22.5
exp11 CARBON
6 12937.4 128.728 24.1
7 12529.2 124.667 34.7
SAMPLE PRESATURATION 8 12406.4 123.445 35.4
date Dec 25 2020 satmode n 9 12275.9 122.147 17.0
solvent dmso wet n 10 12259.9 121.987 25.3
file /home/spark/d~ SPECIAL 11 12100.5 120.401 26.6
12 11957.0 118.973 21.3
ata/2020/Dec/NICLO~ temp 27.0 13 11708.3 116.499 9.0
SAMIDE_PIPERIZINE_~ gain 30 14 4333.0 43.113 112.0
SALT-BATCH-5-13C-N~ spin 20 15 4033.1 40.130 23.2
MR_20201225_01/NIC~ hst 0.008 16 4011.8 39.918 68.5
LOSAMIDE_PIPERIZIN~ pw90 9.400 17 3991.2 39.713 137.9
18 3969.8 39.500 159.5
E_SALT-BATCH-5-13C~ alfa 10.000
19 3949.2 39.295 137.2
-NMR_CARBON_202012~ FLAGS 20 3927.9 39.082 68.3
25_01.fid il n 21 3907.3 38.878 22.9
ACQUISITION in n
sw 25000.0 dp y
at 1.311 hs nn
np 65536 PROCESSING
fb 17000 lb 2.00
bs 4 fn not used
ss 8 DISPLAY
d1 3.000 sp -1490.5
nt 1000 wp 24999.2
ct 512 rfl 5461.1
TRANSMITTER rfp 3969.8
tn C13 rp 49.8
sfrq 100.513 lp 0
tof 1530.3 PLOT
tpwr 56 wc 268
pw 4.700 sc 0
DECOUPLER vs 159
dn H1 th 3
dof 0 nm cdc ph
dm yyy
decwave w
dpwr 42
dmf 9524

Plotname: NICLOSAMIDE_PIPERIZINE_SALT-BATCH-5-13C-NMR_CARBON_20201225_01_plot05