CHT356 – Pre-Lab Questions - Day 3

Name: Baiq Desy Ratnasari

Date: 04/03/2017

1) I will use 2.5 mmol of phenyl hydrazine weighing 0.29 mg [1]

2) I will use 2.5 mmol of 1,3 dicarbonyl weighing 405 mg [1]

3) For a molecule to be UV active it should possess (circle only those that apply):

a fluorine atom an N-N bond an aromatic ring

a double bond a carbon atom a conjugated system

[1]

4) I’m quietly confident that 10 % Ethyl Acetate in Petroleum ether will give me a good
separation based on the previous 2 days, or at least serve as a good starting point.

[1]

5) An aromatic CF3 group comes at - 75 ppm in the 19F NMR spectra

[1]

Reaction Scheme: provide the identity of A

[1]
☐
May enter lab
See demonstrator ☐
May not enter lab ☐