JCD China Co.

,Ltd
Certificate of Analysis
Name of Product: Vitamin D3 Crystal (Cholecalciferol)
Batch No.: B-1-51-M210401
Quantity: 80kg
Mfg Date: 2021-04-02
Expiry Date: 2024-04-01___

Items Standard Result

Appearance White or almost white crystals White crystals
Solubility Practically insoluble in water, freely Corresponding
soluble in ethanol (96 %), soluble in
trimethylpentane and fatty oils.
Identification Infrared absorption spectrophotometry. Corresponding
Comparison: cholecalciferol CRS.

Pre-cholecalciferol 0.05% max Corresponding

Trans-cholecalciferol 0.1% max Corresponding
Light absorption 465-495 490
Specific optical rotation +105°- +112° +108.0°
Loss on Drying 0.10% max 0.090%
Orgnic Methanol Max.3,000 ppm Not detected
Volatile Hexane Max. 290 ppm Not detected
Impurities Chlorobenzene Max. 360 ppm Not detected
Assay 97.0-103.0% 98.1%
38,800,000-41,200,000IU/G 39,240,000 IU/G
Impurities Trans-VD3, Pro-VD3, L3, Iso-T3, T3 Corresponding
conclusion The batch tested complies with Ph.Eur 8.0 and USP 31
Examiner: Jinfu shi Checked by:Chunhua Sun