Certificate of analysis

Toltrazuril 98~102%

Batch Number: CP004-220506 Manufacturing Date: 2022-05-05

Quantity: 204.23Kg Report Date: 2022-05-09

Test Standard QS-CP004-06 Expiration Date 2025-05-04

Testing Items Specifications Results

Appearance White or off-white crystalline powder White crystalline powder

IR: IR spectrum of sample corresponds to Conform

that of reference standard HPLC: The
retention time of the main
Identification
peak corresponds to that of reference standard Conform

Clarity The solution is clear Conform

This solution is not more intensely than reference
Degree of coloration solution B7 Conform

Melting point 192~196℃ 193.5~194.5℃

Loss on drying Not more than 0.50% 0.06%

Sulphated Ash Not more than 0.10% 0.02%

Heavy metals Not more than 10ppm Conform

Single max impurity Not more than 0.20% 0.10%

Total impurities Not more than 1.0% 0.30%

It should be 98.0%~102.0%(Calculated with dried

Assay (HPLC) substance) 99.6%

Residual Solvent Methanol: Not more than 3000ppm 128ppm

Conclusion
Complies specification.

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