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Effect of strain rate and fibre rotation on the in-plane shear response
of ±45 laminates in tension and compression tests
Hao Cui a, *, Daniel Thomson a, Antonio Pellegrino a, Jens Wiegand b, Nik Petrinic a
a
Department of Engineering Science, University of Oxford, Parks Road, Oxford, OX1 3PJ, UK
b
COMPACT Composite Impact Engineering LTD, Manchester, UK
a r t i c l e i n f o a b s t r a c t
Article history: This work focuses on the effect of strain rate and fibre rotation on the in-plane shear properties of
Received 28 June 2016 composite laminates. The effect of fibre rotation on the measured shear properties, was for the first time
Received in revised form experimentally quantified with the comparison between compression and tension tests of the ±45
5 September 2016
laminate samples. Significant increase of shear strength and decrease of final failure strain was observed
Accepted 19 September 2016
Available online 20 September 2016
with the increase in strain rate from 5e-4 1/s to 1300 1/s. The nonlinear shear model was developed to
simulate the large deformation process, in which the fibre orientation was updated as a function of the
in-plane shear strain. The results of this investigation should motivate the updating of procedures for
Keywords:
In-plane shear
experimental characterization as well as analytical and numerical modelling of in-plane shear response
Fibre rotation of laminates.
Rate-dependent © 2016 Elsevier Ltd. All rights reserved.
Hopkinson bar
±45 laminate
1. Introduction once damage has initiated [1,2]. The ±45 laminates yield quite
uniform shear stress distribution over the whole gauge area [7], and
Carbon fibre composite laminates feature high stiffness and provide stable damage evolution for large deformation. However,
strength in fibre orientation, while their elastic moduli as well as the tension test of ±45 exhibit significant fibre rotation [8]. The
strength in transverse direction are relatively weak. Inter-fibre reinforcement fibres get more aligned with the loading axis as the
failure is one of the dominating failure modes for composite lam- shear strain increases during tests, resulting in the overestimation
inates, and significant nonlinearities may occur prior to fracture in of the shear stress, as confirmed with analytical and numerical
composite structures. Considerable nonlinearity of in-plane work [9,10]. The opposite trend may be observed when the
behaviour has been observed in off-axis compression tests of uni- compression loading is applied, and this can be used in comparison
directional laminates, and it has been found to be dependent on the with tension tests to evaluate the influence of fibre rotation on
strain rate [1,2]. The shear properties of laminated composites are measured shear response.
very important for predicting permanent deformation and damage, This paper aims to study the rate-dependence in in-plane
and several models have been developed [3e6]. In this study, the shear, and to reveal the effect of fibre rotation on the laminate
rate dependent in-plane shear properties were characterized using response in both experiments and modelling. The experimental
±45 laminates, in order to gain deeper understanding of their setups and related data processing methods are introduced in
nonlinear deformation behaviour, and to support the development Section 2. The corresponding numerical models of the specimens
of constitutive models for simulation of composites subjected to and the developed constitutive model used to simulate the con-
impact loading. ducted experiments are outlined in Section 3. All results and
The in-plane shear response can be obtained from off-axis discussions are presented in Section 4, followed by concluding
compression/tension tests. Achieving large deformations poses remarks in Section 5.
several challenges, as the deformation process becomes unstable
* Corresponding author.
E-mail address: hao.cui@eng.ox.ac.uk (H. Cui).
http://dx.doi.org/10.1016/j.compscitech.2016.09.016
0266-3538/© 2016 Elsevier Ltd. All rights reserved.
H. Cui et al. / Composites Science and Technology 135 (2016) 106e115 107
The Zwick/Roell Z250 screw driven testing machine with 20 KN 2.3. In-plane shear data processing
loading cell was used in quasi-static tests. The displacement
controlled loading rate was 0.01 mm/s. An in-house built Split- The displacement (extension and contraction) across the lami-
Hopkinson-Tension and Compression Bar systems [11] were used nate specimens gauge section and the corresponding strain can be
for dynamic tests (Fig. 2). The striker velocity was approximately evaluated from the images taken during tests by means of the DIC
5 m/s in compression tests, and 11 m/s in tension tests. Strain method. The strain distribution within gauge area is reasonably
gauges were used to acquire the strain history on the split Hop- uniform over the gauge section. The average normal strains in both
kinson bars, from which the force histories applied upon all sam- x and y directions were calculated from the changing of edge length
ples were calculated. These dynamic experiments are considered of the gauge area as:
valid for the purpose of classical characterisation of mechanical
εxx ¼ Dlx =l
x (1)
εyy ¼ Dly ly
where Dlx and Dly are the elongations, while lx and ly are the length
and width of the gauge area in the direction of parallel and
perpendicular to the loading direction. The shear strain is then
calculated as:
F
t12 ¼ ð1 þ εxx Þ (3)
2A
where l is equal to 1 for compression tests and 1 for tension tests. 3.1. Laminate model
The stiffness constants Qij are calculated from material proper-
ties of unidirectional laminates: The tension and compression experiments were simulated
numerically using the finite element method as illustrated in Fig. 3.
Q11 ¼ E11 =ð1 v12 v21 Þ The experimentally acquired boundary conditions were used as
Q12 ¼ Q21 ¼ E11 v21 =ð1 v12 v21 Þ (7) input data for modelling. The laminates were modelled with three
Q22 ¼ E22 =ð1 v12 v21 Þ dimensional 8 node reduced integration solid ‘brick’ element
The material constants in Eq (7) are listed in Table 1. (C3D8R) in Abaqus 6.14, material properties are listed in Table 1.
During large in-plane shear deformation, the moduli in trans- Due to large in-plane shear, the inter-laminar shear stress txz
verse direction, E22, also get degraded. However, the degraded and tyz may also exceed its yielding limit in ±45 laminates,
whereby this transverse shear deformation concentrates at the
resin-rich interface between two layers. To avoid large distortion of
Table 1 bulk elements, the cohesive zone model was used to simulate the
Elastic properties of IM7/8552 laminate [15].
nonlinear deformation in XeZ and YeZ directions. The imple-
E11 162095 MPa mented (as user-defined in Abaqus/Explicit) cohesive law features
E22 9721 MPa very high initial stiffness (1e5MPa/mm) before exceeding its
E33 9721 MPa
reversible limit, to avoid non-physical contribution to the out-of-
G12 4688 MPa
G13 4688 MPa plane deformation. The inter-laminar cohesive stress after
G23 5000 MPa yielding is determined using experimentally determined in-plane
v12 0.362 shear behaviour.
v13 0.362 All simulations were done using Abaqus/Explicit. The quasi-
v23 0.3
static simulation was carried out using the true density for a long
H. Cui et al. / Composites Science and Technology 135 (2016) 106e115 109
1 εxx
q ¼ arctan (10)
1 εyy
where εxx is the strain along loading axis and εyy is the strain
normal to the loading axis this equation provided very close esti-
Fig. 3. Numerical models for (a) compression tests and (b) tension tests. mation of fibre rotation in comparison to the Eq (6) used in pro-
cessing experimental results.
Within the VUMAT, the strain tensor in global coordinates ~ε was
time to avoid any inertia effect generated during rapid fracture updated first. The following equation was used to compute the
processes. strain in local material coordinates
Fig. 4. Fibre rotation during shear deformation of unidirectional laminate: the patterns indicate fibre orientation, and the 1e2 axis is the local material coordinate system used FEM.
110 H. Cui et al. / Composites Science and Technology 135 (2016) 106e115
2 3
c2 s2 0 2s1 c1 0 0
6 s2 c2 0 2s1 c1 0 07
6 7
6 0 0 1 0 0 07
RðqÞ ¼ 6
6 s1 c1
7 (12)
6 s1 c 1 0 c 2 s2 0 07 7
4 0 0 0 0 c1 s1 5
0 0 0 0 s1 c1
c ¼ E11E22 E11 E33v223 .2E22 E33 v13 v23 E22 E33 v213
C11 ¼ E22 E33 v223 E11 2
c
C12 ¼ C21 ¼ ðE22 v12 þ E33 v13 v23 ÞE11 E22 =c
C13 ¼ C
31 ¼ ðv12 v23 þ v13.ÞE11 E22 E33 =c (14)
C22 ¼ E11 E33 v213 E22 2
c
C23 ¼ C
32 ¼ ðE v
11 23 þ E v
22 12.v13 ÞE22 E33 =c
C33 ¼ E11 E22 v212 E22 E33 c
~ ¼ RðqÞ$s
s (16) the dynamic tests produced similar macroscopic failure pattern as
that in quasi-static tests. Detailed investigation on the failure
mechanisms in tension tests will be presented in Section 4.5. The
cross-section of compression samples in quasi-static tests was
4. Results and discussions analysed and illustrated in Fig. 7. Although the delamination
seemed to trigger the final failure of the ±45 laminates in both
4.1. Force-displacement tension and compression load, the number of delamination planes
in compression tests was much less than that in tension tests. Be-
The edge surface of the specimens was monitored in quasi-static sides, the number of in-plane cracks in compression tests was
tests, and the representative damage evolution processes were considerably smaller than in tension. This could be due to the fact
depicted in Fig. 5 at each stage of the load-displacement curves. In that the high hydro-static stress in compression experiments might
tension tests, there is no visible damage occurring at the moment of have prevented the opening of cracks and growth of voids within
yielding. The load dropped slightly after yielding, and micro cracks the epoxy matrix.
started to emerge at displacement of 0.6 mm. The load carried by In the dynamic tests, the force at both ends of the sample,
the specimen then kept growing causing an increasing number of calculated from the signal on the input bar and output bar [13], are
micro cracks in each ply to appear. There were no delamination plotted in Fig. 8. The force on one end of the specimen is very
cracks observed until the extension of about 1.5 mm was reached, similar to that on the other, showing that dynamic equilibrium
which was followed by catastrophic failure. In compression testing, conditions were achieved from the early stage during experiments.
the stiffness appears higher because of the shorter length of the After an initial ramp-up period where the strain rate rapidly in-
sample. There were not many visible cracks on the edge of creases, a constant strain rate is reached long before failure. Hence,
compression samples, until the contraction of 0.9 mm was reached the sample and test setup produced valid measurement of the
when delamination between layers appeared. nonlinear deformation response.
Samples after tension and compression tests in different loading
rates are all presented in Fig. 6. The delamination between plies of
different angles has resulted in the complete break of tension, and
H. Cui et al. / Composites Science and Technology 135 (2016) 106e115 111
Fig. 6. Samples after tests (a) quasi-static tension; (b) quasi-static compression; (c) dynamic tension; (d) dynamic compression.
Fig. 8. The equilibrium and shear strain in (a) dynamic compression and (b) dynamic
4.3. Rate dependence of corrected shear response tension tests.
Fig. 9. The original stress from tension and compression tests in (a) quasi-static and Fig. 10. Corrected shear from (a) tension tests and (b) compression tests.
(b) dynamic rate.
Fig. 11. Comparison of force-displacement curves from experiments and simulations, (a) quasi-static tension; (b) quasi-static compression; (c) dynamic tension; (d) dynamic
compression.
taking into account the rotation of fibre not only results in an in-
crease in the apparent stress calculated using small strain theory,
but it also causes the apparent reduction in stiffness in the original
fibre orientation and a change in the in-plane distribution of
stresses. With the growing demand for more accurate tools for
predictive modelling of composite systems and structures, the fibre
rotation should be considered both in experiments and in numer-
ical simulations, such that the true in-plane shear properties could
be utilised. Further accounting for nonlinearities in the transverse
direction, should lead to an even more accurate characterisation
and modelling of the intrinsic material behaviour.
Fig. 13. The deformation and fracture of tension samples from (a) dynamic tests and (b) quasi-static tests.
5. Conclusions Acknowledgements
The in-plane shear behaviour was characterised with ±45 The authors would like to acknowledge Rolls-Royce plc, for their
laminates loaded in both compression and tension at two distinct continuing support through the Solid Mechanics University Tech-
loading rates. The split Hopkinson bar system and high-speed nology Centre at the University of Oxford.
camera enabled the successful measurement of the shear defor-
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