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Fibre reinforced geopolymer concrete products for underground infrastructure

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Don Wimpenny Peter Duxson


CH2M Hill Coogee Chemicals
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REINFORCEMENT

Fibre reinforced geopolymer

FRGC - concrete (FRGC) has no


Portland cement or steel re-
inforcement, but instead

an innovative used synthetic fibre rein-


forcement and geopolymer
binder. Here, Dom

material for Wimpenny, Associate Direc-


tor CH2M Hill, and Malcolm
Chappell, Director of Tun-

tunnel segments nelling, Asia Pacific CH2M


Hill, discuss the development
of FRGC during a project
part-funded by the Victorian
THIS PAPER EXAMINES the combined use Government and a consortium of five organisations. The work
of two emerging technologies in the involves laboratory and field trials and the production of
production of precast tunnel segments:
geopolymer binder and fibre reinforcement.
prototype tunnel segments which have been subject to fire
Precast concrete is the predominant mate- testing. The results indicate that FRGC has the potential to
rial for segmental tunnel linings, with a typical produce precast concrete products with increased durability
6m internal diameter (ID) tunnel utilising ap-
proximately 4,500 cubic metres of concrete and substantially reduced carbon emissions compared to the
per kilometre. The major contribution of con- Portland cement based concrete with steel reinforcement.
crete to underground infrastructure is accom-
panied by significant embodied greenhouse and reduced impact damage during han- cement based concrete. This paper sum-
gas emissions. Concrete in construction re- dling. There has also been development in marises the findings of a 3 year Australian
portedly generating more than 5% of world- the use of non-corrodible synthetic macrofi- project to develop Fibre Reinforced Geopoly-
wide carbon dioxide (CO2) emissions, over bres as an alternative to steel fibres, primarily mer Concrete (FRGC) precast products for un-
three-quarters deriving from the Portland ce- for sprayed concrete linings in mines, but also derground infrastructure funded by Victoria’s
ment binder. Approximately half the CO2 for potential use in segmental linings. Fibre Science Agenda Investment Fund and a con-
emissions from Portland cement are associ- reinforced segments have a lower resistance sortium of five organisations (Halcrow Group,
ated with energy used in the heating and to bending moments than conventionally re- Elasto Plastic Concrete, Zeobond, University
grinding processes. The remaining emissions inforced concrete and the lower elastic mod- of Melbourne and Humes).
derive from the chemical de-carbonation of ulus of synthetic fibres influences their ability
the limestone. The cement industry has made to control cracking and deflection under load. Methodology
considerable improvements in energy effi- These effects need to be considered in the The introduction of new products in the con-
ciency and use of alternative fuel sources. design and handling of segments. Guidance struction industry is controlled by the under-
However, if worldwide emissions targets are on the use of steel and synthetic fibres was standably conservative nature of the
to be met, some radical changes are required published by the UK, Concrete Society in engineering profession and the need to meet
to further reduce the CO2 emissions derived 2007 and a design method based on work by existing industry specifications. Some of the
from the use of concrete. Geopolymer binder Rilem is included in New Zealand Standard issues relating to adoption of geopolymer
contains no Portland cement but instead uses NZS 3101. and fibre technology are indicated in Table 1.
industrial by-products such as fly ash and slag The combination of geopolymer binder In order to address these issues, the project
which are activated by an alkaline agent. The and synthetic fibre reinforcement presents the pre-empted the normal approvals process by
hardened binder includes alumino silicates opportunity to produce concrete with en- testing the FRGC products against the re-
similar to those produced by Portland cement hanced durability and reduced environmental quirements of a typical performance specifi-
based binders, but no calcium compounds. impact. However, it necessitates the design, cation. In addition, the project developed
There are currently no international standards testing and construction procedures to be guidance on structural and durability design
for the use of geopolymer in construction, modified compared to bar reinforced Portland and produced prototype products.
but guidance was recently published by the
Concrete Institute of Australia (CIA 2011).
Table 1: Key issues to address in the adoption of FRGC technology.
Steel fibres have become the preferred re-
inforcement for segmental linings constructed Geopolymer Synthetic fibres
in the last 10 years. Halcrow has been at the
forefront of this development (King 2005, Absence of structural design parameters Absence of structural design parameters
Angerer and Chappell 2008 and Harding and Practical constraints (e.g. controlling workability, Uncertainty over long-term performance (eg creep)
Chappell 2012). In addition to increased pro- setting time and strength development)
ductivity by the elimination of steel fixing,
Uncertainty over long-term performance Urgent need to identify appropriate test methods
steel fibre reinforced concrete (SFRC) has en-
(eg permeability and diffusion properties and acid and limits to control properties but avoid
hanced durability due to the absence of gal- resistance) unacceptably high rates of non-compliance
vanic and stray current corrosion (ACI 1996)

TUNNELLING JOURNAL 35
REINFORCEMENT

Typical performance requirements for concrete with 40kg/m3 steel fibres provided gave a 100mm target slump 60 minutes
fibre reinforced tunnel segments were two control mixes. The Portland cement after mixing (allowing for permissible toler-
adopted as shown in Table 2. The tests in- control mix was based on an existing pro- ances). The main laboratory mixes were
clude American and Australian strength duction mix, with 20% fly ash in the binder 0.35m3 in size to allow a large number of
and durability tests, such as residual flexural and a water/binder ratio of less than 0.4. specimens to be produced. The key findings
strength and apparent volume of perme- The synthetic fibres are manufactured from the laboratory trials are discussed
able voids (AVPV), as well as European tests from polyolefin and are 60mm long and 0.5- below.
for water penetration and chloride migra- 1mm in diameter with an embossed profile.
tion. Specimens were also subject to expo- The steel fibres are formed from cold drawn Strength - The strength results are sum-
sure tests to acid, chloride and sulfate high tensile carbon steel and are 60mm long marised in Table 3.
solutions for 2 years. and 0.75mm in diameter with hooked ends. It can be observed that the compressive and
tensile splitting strengths of the geopolymer
concrete are lower than those of the Portland
Table 2: Summary of performance specification requirements. cement based control and the typical specifi-
cation requirements. However, flexural
Parameter Requirement strength is of primary importance in the per-
STRENGTH formance of tunnel segments, and the flexural
strength and equivalent post-crack residual
Minimum 28-day cylinder strength (MPa) 50 flexural strength value at 3mm deflection of
Minimum cylinder strength for demoulding (MPa) 10 the geopolymer with synthetic fibres slightly
Minimum 28-day tensile splitting strength (MPa) 4.2 exceeds those of both the Portland cement
Minimum 28-day flexural strength (MPa) 4.6
based control with synthetic fibres and the
Minimum 28-day equivalent post-crack residual flexural strength Fe3.0 (MPa) 3.2
geopolymer mix with steel fibres. This is
DURABILITY shown in Figure 1.
Conventional concrete mixes with steel fi-
Maximum AVPV rodded (%) 13 bres have shown a tendency to become brittle
Maximum 56-day chloride migration coefficient (m2/s) 4x10-12 as the concrete strength increases due to fibre
Maximum 91-day chloride migration coefficient (m2/s) 2x10-12
rupture rather than gradual pull-out. The
Maximum sorptivity (mm) 8
good equivalent post-crack residual flexural
Maximum 56-day drying shrinkage (microstrain) 600
strength values of the geopolymer mix with
synthetic fibres is en-
Following laboratory testing, field trials couraging, and this
Fig 1: Flexural strength results (y-axis units in MPa).
were undertaken at the precast plant to value would not be
allow prototype segments to be produced expected to be re-
as well, as large beams for bending tests to Flexural strength duced by long-term
Eq. (Post-crack) Residual Strength, Fe0.75
validate the design method. Standard and strength gain of the
Eq. (Post-crack) Residual Strength, Fe3.0
accelerated curing were used to determine concrete in the same
8
the effect on the early strength gain for de- way as steel fibres be-
7
moulding. Prototype segments were subject cause of the lower
to simulated hydrocarbon fire to assess 6 elastic modulus of
spalling resistance. ASTM C1550 round 5 synthetic fibres.
panels were tested for toughness and 4
cracked panels were centrally loaded in a 3 Durability - The
rig to monitor deflection due to creep. 2 durability test results
1 are summarised in
Discussion 0 Table 4.
Laboratory Trials - The initial laboratory tri- Conventional concrete Geopolymer concrete Geopolymer concrete The Apparent Vol-
with synthetic fibres with steel fibres with synthetic fibres
als assessed the workability characteristics of ume of Permeable
FRGC mixes using different fibre types, and Voids of the geopoly-
doses of synthetic fibres from 8-12kg/m3. A Based on the initial trials a geopolymer mer mixes is higher than that of the Portland
Portland cement based concrete containing mix with 8kg/m3 of synthetic fibre was se- cement based control, and also exceeds the
8kg/m3 of synthetic fibres and geopolymer lected for further development. This mix specified limit. In contrast, the chloride migra-
tion, sorptivity and dying shrinkage of the
Table 3: Summary of strength results for laboratory trials. geopolymer mixes are better than those of
the Portland cement based control.
Conventional Geopolymer Geopolymer Exposure of specimens to acid and sulfate
Parameter concrete with concrete with concrete with solutions and periodic abrasion resulted in
synthetic fibres steel fibres synthetic fibres similar deterioration to FRGC as the control
28-day cylinder strength (MPa) 52.5 46.0 49.5 mix containing Portland cement and 20% fly
ash. In contrast, the chloride ingress into
1-day cylinder strength for demoulding (MPa)* 25.0 24.0 25.0 FRGC is much lower than that of the control
28-day tensile splitting strength (MPa)* 4.8 4.0 3.4 and this is consistent with the chloride migra-
tion test results.
28-day flexural strength (MPa)* 5.5 6.4 7.4
Geopolymer concrete lacks a conventional
28-day equivalent post-crack residual flexural capillary pore structure and this may mean
strength Fe3.0 (MPa)* 3.7 3.8 3.9 that parameters which are heavily influenced
Note: * denotes accelerated curing by capillary porosity and capillary transport of

36 TUNNELLING JOURNAL
REINFORCEMENT

The creep deflection of the FRGC mix is ap-


Table 4: Summary of durability test results for laboratory trials.
proximately a factor of three greater than
Conventional Geopolymer Geopolymer the conventional SFRC control mix and
Parameter concrete with concrete with concrete with creep coefficients are approximately 1.5 for
synthetic fibres steel fibres synthetic fibres the control mix and 4.3 for the FRGC mix.
56-day chloride migration coefficient (m2/s) 3.5x10-12 Not tested 1.1x10-12
This indicates that creep deformation needs
to be taken into consideration in the design
91-day chloride migration coefficient (m2/s) 1.9x10-12 Not tested 0.9x10-12 when there is a potential for cracked FRGC
Sorptivity (mm) 9.0 6.1 6.2 segments to be subject to sustained
bending.
56-day drying shrinkage (microstrain) 530 240 400

Fig 4: Creep data, y-axis = deflection (mm)


moisture, such as sorptivity and diffusion, Strength - The compressive strength devel-
could be beneficially influenced. However, be- opment of the FRGC mix is shown in Figure 3.
1.4
cause there is no hydration in geopolymer Early strength development of the FRGC was Conventional concrete
concrete it is important that the water content very good and segments were successfully 1.2 with steel fibres
Geopolymer concrete
is carefully controlled to minimise overall stripped to allow a single casting cycle every 1.0 with synthetic fibres
porosity to benefit AVPV and strength. 24 hours at an ambient temperature at cast- 0.8
ing of 22°C without heat curing. Compressive
0.6
Field Trials strength and tensile splitting at 28 days in the
Field trials of up to 2.5m3 size were under- FRGC mix is approximately 20% lower than 0.4
taken at a precast plant. Tunnel segment conventional SFRC control mix. Flexural 0.2
moulds were already available at this plant strength and residual flexural strength in the 0
from a recently completed 2.4m ID tunnel FRGC mix are 5-10% lower than the SFRC 0 20 40 60 80 100
with a 200mm thick lining. The objective of control, but met the performance require- Time (days)
the field trials was to produce prototype FRGC ments.
segments, as well as larger specimens for fur-
ther testing, including large beams for bend- Beam Tests - Notched beams of different
ing tests. A conventional concrete control mix Fig 3: Compressive strength development dimensions (100x200x700mm,
(y-axis in MPa).
with steel fibres was also included. 250x200x1750mm and 400x200x2800mm)
The field trials used a FRGC with 8kg/m3 of were cast from the FRGC mix and subject
8.0
synthetic fibres and Portland cement based to bending at approximately 3 months age
Conventional concrete
concrete with 40kg/m3 of steel fibres (with 7.0 with steel fibres using a modification of the three -point
and without the addition of 1kg/m3 of syn- 6.0 Geopolymer concrete method in TC162-TDF (Rilem 2003). Figure
with synthetic fibres
thetic microfibres for improved fire spalling re- 5 shows the testing arrangement for the
5.0
sistance). largest of the beams. The load and crack
Four rectangular bolted segments (each ap- 4.0 mouth opening deflections were recorded
proximately 0.4m3 and 0.8 tonnes in weight) 3.0 and the results were analysed to verify the
and four smaller tapered key segments (each 2.0
size factor in the NZS 3101 design method.
approximately 0.1m3 and 0.2 tonnes in This factor takes into consideration bound-
weight) were produced from the FRGC mix. 1.0 ary effects in thinner sections, including a
Figure 2 shows the typical condition of the de- 0.0 predominant fibre orientation. The beam
1 day 7 days 28 days
moulded segments and a sawn cross-section. tests mimic research undertaken in the Brite
The surface of the segments displayed accept- EuRam Project “Test and Design Methods
able finish and the cross-section indicated Creep - ASTM C1550 round panels were for Steel Fibre Reinforced Concrete.”
good uniformity and compaction. However, loaded to induce cracking and then a load The tests confirm that there is a size fac-
care has to be taken to evenly disperse the representing 20-30% of the static capacity tor effect for FRGC similar to that for SFRC,
fibres during mixing and to appropriately cure was applied over 100 days the central deflec- although its magnitude is influenced by the
the concrete. tion monitored (see Figure 4). fibre type and should be established for the
intended fibre in order to modify the NZS
Fig 2: Prototype tunnel segments and sawn cross-section 3101 design method.

Fire Tests - Four segments were subject to


a simulated hydrocarbon fire involving ex-
posure to furnace temperatures of up to
1100°C over approximately 1 hour. Table 5
summarises the condition of the intrados
exposed to fire testing.
The steel fibre mix without synthetic
microfibres displayed extensive explosive
spalling, whereas the geopolymer concrete
with macrosynthetic fibres had little or no
spalling indicating acceptable fire perform-
ance. However, the potential impact of a
fire event upon the performance of the syn-
thetic macrofibres should be assessed as
part of the design process.

TUNNELLING JOURNAL 37
REINFORCEMENT

Fig 5: Bending test on FRGC beams

Table 5: Summary of fire tests on segments. forcement type predominate over trans-
portation.
Segment Performance
Summary and further work
Conventional SFRC Explosive spalling to approximately 40% of exposed area
The findings of the project are sum-
Conventional SFRC and synthetic microfibres No spalling marised in Table 6. An estimate of cost of
FRGC compared to conventional concrete
FRGC (6 months old) Non-explosive spalling to approximately 10% of exposed area
has been included based on the experi-
FRGC (8 months old) No spalling ence of the consortium partners in
Victoria. The cost will be influenced by
Carbon emissions fibres and conventional concrete assumes the availability and cost of suitable indus-
Reducing the carbon emissions of concrete 40kg/m3 of steel reinforcing bar or steel trial by-products and alkali activators.
is a key driver for the project. In order to as- fibres. The next step in the development of
sess the impact of using FRGC compared to The calculations allow for the embodied FRGC following the successful laboratory
conventional concrete, two scenarios were carbon in the constituent materials (includ- and field trials is to undertake project
considered: ing obtaining and processing the raw mate- trials. It is proposed that precast FRGC
a) Casting segments at Echuca, Victoria rials), transportation to the precast plant,
for transport by road 220km to a project production of the segments and their trans-
site in Melbourne, Victoria; and portation to the project site. The calcula- Fig 6: Carbon emissions associated with
b) Casting segments for transport at tions do not assess the effects of segments delivered to Melbourne and
Echuca, Victoria by road 3,310km to a proj- carbonation, or the carbon emission associ- Perth (y-axis = total emissions: tonne
ect site in Perth, Western Australia. ated with demolition and reuse of tunnel CO2/tonne segment)
The first case represents a realistic supply segments.
situation for precast segments, whereas the Figure 6 shows the comparison between 0.5
Conventional concrete
second case is intended to represent a max- FRGC and conventional concrete. The CO2 0.45
with steel rebar/fibres
imum transport distance in order to assess emissions of segments using FRGC are 0.4
Geopolymer concrete
the influence of haulage on carbon 34% and 60% of the values for conven- 0.35 with synthetic fibres
emissions. 0.3
tional concrete segments delivered to sites
0.25
The carbon emissions were calculated in Melbourne and Perth respectively, repre-
0.2
using published values for converting senting a reduction of up to approximately
0.15
energy and fuel to CO2. The calculations 70% in emissions. The CO2 emissions for
0.1
assumed that the strength and durability FRGC segments transported to Perth are 0.05
performance of the FRGC and conven- slightly less than those associated with con- 0
tional concrete mixes are similar. The ventional concrete segments delivered to Melbourne Perth
FRGC concrete has 8kg/m3 of synthetic Melbourne, indicating that binder and rein-

38 TUNNELLING JOURNAL
REINFORCEMENT

than control mixes using synthetic and


Table 6: Summary of FRGC characteristics steel fibres respectively and met the
Segment Performance specified requirements. Durability and fire
spalling performance are significantly
Characteristic FRGC comparison to conventional SFRC enhanced.
Compressive strength and tensile split-
Compressive strength Equal or better at early ages
ting strength are lower than the control
20% lower at later ages (50MPa possible with care) and care is needed over control of water
Tensile splitting strength 20% lower consistent with compressive strength content and curing. Creep of cracked
FRGC ASTM C1550 round panels is a fac-
Flexural strength Slightly lower tor of three higher than the control and
Residual flexural strength Slightly lower this should be allowed for in the design.
The embodied carbon dioxide emissions
Drying shrinkage Reduced
associated with synthetic fibre reinforced
Creep Factor of three times higher for cracked FRGC panels FRGC segments are approximately 70%
lower than conventional concrete using
Fire resistance Improved resistance to spalling compared to SFRC without
synthetic macrofibres. steel reinforcement for a realistic
transport distance.
Effect of fire event on synthetic macrofibres to be assessed The next stage in the development of
in design. FRGC segments is a field trial maybe as
Durability: part of a major project. In addition the
bolted connections in the segmental
AVPV Slightly higher
lining need to be replaced to maintain a
Sorptivity Reduced
minimum carbon footprint. An internal
Chloride migration Significant reduction in chloride ingress research project is currently underway to
Acid resistance Similar develop alternative connection details.
Sulfate resistance Similar

Carbon emissions 70% reduction allowing for practical transport distances ACKNOWLEDGEMENT
Design code NZS 3101 but with modified size factor and allowance for
increased creep The authors acknowledge the substantial
contributions made by Dr Van Bui in
Specification Similar to SFRC but no need for chloride migration testing management of the project and the
if synthetic macrofibres used financial support of the Victorian
Additional care over control of water content and curing Government through the Victoria’s
Science Agenda program.
Cost Cost up to 10% lower than conventional SFRC

products using synthetic or steel fibres


are used in non-critical applications, such REFERENCES
as a back shunt tunnel or precast head- ACI 1996. Report on Fiber Reinforced Concrete, Report by ACI Committee 544, Reapproved
wall. The products would be designed to 2002. Farmington Hills, MI: American Concrete Institute.
NZS 3101 and subject to load testing as
necessary. The products would be Angerer W., and Chappell M. 2008. Design of steel fibre reinforced segmental lining for the
inspected and tested periodically and/or Gold Coast Desalination Tunnels, Presented at 13th Australian Tunnelling Conference,
include sensors, such as corrosion Melbourne, May 4-7.
ladders, to allow long-term monitoring of
ASTM C1550-08.2009. Standard Test Method for Flexural Toughness of Fiber Reinforced
performance.
Concrete (Using Centrally Loaded Round Panel). West Conshohocken, PA: ASTM International.

Conclusions Concrete Institute of Australia. 2011. Geopolymer Recommended Practice Handbook. ISBN
A 3 year study has been undertaken to 1921093560. Rhodes NSW 2138 Australia: Concrete Institute of Australia.
develop concrete which has no Portland
cement or steel reinforcement, but Concrete Society. 2007. Technical Report 63, Guidance on the design of steel-fibre-reinforced
instead used synthetic fibre reinforcement concrete. ISBN 1-904482-32-5. Camberley, Surrey, UK: The Concrete Society.
and geopolymer binder.
Laboratory and field trials have been Concrete Society. 2007. Technical Report 65, Guidance on the use of macro synthetic-fibre-
undertaken to assess the strength and reinforced concrete. ISBN 1-904482-34-1. Camberley, Surrey, UK: The Concrete Society.
Harding A., and Chappell M, 2012. The design of steel fibre reinforced segmental linings –
durability of FRGC against a typical per-
reflections on design challenges, Presented at the World Tunnelling Congress.
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forced concrete segments and control King, M.R. 2005. The design and use of steel fiber reinforced concrete segments, Proceedings
mixes using Portland cement and 20% fly of Rapid Excavation and Tunnelling Conference, Seattle, June 27-29.
ash. Prototype segments have also been NZS 3101: 2006. Concrete Structures Standard. Wellington: Standards New Zealand.
produced.
The work indicates that acceptable Rilem 2003.TC 162-TDF: Test and Design Methods for Steel Fibre Reinforced Concrete- Design
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duced. Flexural and residual flexural October 2003, 36:560-567.
strength are slightly higher and lower

TUNNELLING JOURNAL 39
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