Professional Documents
Culture Documents
STANDARD 1 6890-2
First edition
2016-12-01
Reference number
ISO 16890-2:2016(E)
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ISO 1 6890-2 : 2 01 6(E)
Contents Page
Foreword ........................................................................................................................................................................................................................................ vi
Introduction .............................................................................................................................................................................................................................. vii
1 Scope ................................................................................................................................................................................................................................. 1
Bibliography ............................................................................................................................................................................................................................. 5 9
Foreword
I SO (the I nternational O rganiz ation for Standardiz ation) is a worldwide federation of national s tandards
bodies (ISO member bodies). The work o f preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has b een es tablished has the right to b e represented on that committee. I nternational
organi zation s , governmental and non- governmental, in liaison with I SO, al so take p ar t in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters o f
elec trotechnical s tandardi z ation.
T he procedures used to develop this do cument and those intended for its fur ther maintenance are
describ ed in the I SO/I E C D irec tives , Par t 1 . I n p ar ticu lar the different approval criteria needed for the
di fferent types o f ISO documents should be noted. This document was dra fted in accordance with the
editorial ru les of the I SO/I E C D irec tives , Par t 2 (see www. iso . org/direc tives) .
Attention is drawn to the possibility that some o f the elements o f this document may be the subject o f
patent rights. ISO shall not be held responsible for identi fying any or all such patent rights. Details o f
any patent rights identified during the development o f the document will be in the Introduction and/or
on the I SO l is t of p atent declarations received (see www. iso . org/p atents) .
Any trade name used in this document is in formation given for the convenience o f users and does not
cons titute an endors ement.
For an explanation on the meaning o f ISO specific terms and expressions related to con formity assessment,
as well as information about I SO ’s adherence to the World Trade O rganization ( WTO) principles in the
Technical B arriers to Trade (TB T ) see the following URL: www.iso.org/iso/foreword. html .
T he committee res p ons ible for this do cument is I SO/ TC 142 , Cleaning equipment for air and other gases.
This first edition o f ISO 16890-2, together with ISO 16890-1, ISO 16890-3 and ISO 16890-4, cancels and
replaces ISO/TS 21220:2009, which has been technically revised.
I SO 16 8 9 0 cons is ts of the fol lowing p ar ts , under the general title Air filters for general ventilation :
— Part 1: Technical specifications, requirements and classification system based upon particulate matter
efficiency (ePM)
— Part 2: Measurement of fractional efficiency and air flow resistance
— Part 3: Determination of the gravimetric efficiency and the air flow resistance versus the mass of test
dust captured
— Part 4: Conditioning method to determine the minimum fractional test efficiency
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ISO 1 6890-2 : 2 01 6(E)
Introduction
The e ffects o f particulate matter (PM) on human health have been extensively studied in the past
decades. The results are that fine dust can be a serious health hazard, contributing to or even causing
respiratory and cardiovascular diseases. Di fferent classes o f particulate matter can be defined according
to the particle size range. The most important ones are PM10 , PM 2,5 and PM1 . The U.S. Environmental
Protection Agency (EPA), the World Health Organization (WHO) and the European Union define
PM10 as particulate matter which passes through a size-selective inlet with a 50 % efficiency cut-off
at 10 µm aerodynamic diameter. PM 2,5 and PM 1 are similarly defined. However, this definition is not
precise if there is no further characterization of the sampling method and the sampling inlet with a
clearly defined separation curve. In Europe, the re ference method for the sampling and measurement
of PM10 is described in EN 12341. The measurement principle is based on the collection on a filter of the
PM10 fraction of ambient particulate matter and the gravimetric mass determination (see EU Council
Directive 1999/30/EC of 22 April 1999).
As the precise definition o f PM10 , PM 2,5 and PM1 is quite complex and not simple to measure, public
authorities, like the U.S. EPA or the German Federal Environmental Agency (Umweltbundesamt),
increasingly use in their publications the more simple denotation o f PM10 as being the particle size
fraction less or equal to 10 µm. Since this deviation to the above mentioned complex “o fficial” definition
does not have a significant impact on a filter element’s particle removal e fficiency, the ISO 16890 series
re fers to this simplified definition o f PM10 , PM 2,5 and PM1 .
Particulate matter in the context of the ISO 16890 series describes a size fraction of the natural aerosol
(liquid and solid particles) suspended in ambient air. The symbol ePM x describes the e fficiency o f an air
cleaning device to particles with an optical diameter between 0,3 µm and x µm. The following particle
size ranges are used in the ISO 16890 series for the listed e fficiency values.
Table 1 — O ptical particle diameter size ranges for the definition o f the e fficiencies , ePM x
E fficiency Size range , µm
ePM10 0,3 ≤ × ≤10
ePM 2,5 0,3 ≤ × ≤2,5
e PM 1 0,3 ≤ × ≤1
Air filters for general ventilation are widely used in heating, ventilation and air-conditioning applications
o f buildings. In this application, air filters significantly influence the indoor air quality and, hence, the
health o f people, by reducing the concentration o f particulate matter. To enable design engineers and
maintenance personnel to choose the correct filter types, there is an interest from international trade
and manu facturing for a well-defined, common method o f testing and classi fying air filters according
to their particle e fficiencies, especially with respect to the removal o f particulate matter. Current
regional standards are applying totally di fferent testing and classification methods which do not allow
any comparison with each other, and thus hinder global trade with common products. Additionally,
the current industry standards have known limitations by generating results which o ften are far away
from filter per formance in service, i.e. overstating the particle removal e fficiency o f many products.
With this new ISO 16890 series, a completely new approach for a classification system is adopted, which
gives better and more meaningful results compared to the existing standards.
The ISO 16890 series describes the equipment, materials, technical specifications, requirements,
qualifications and procedures to produce the laboratory per formance data and e fficiency classification
based upon the measured fractional e fficiency converted into a particulate matter e fficiency (ePM)
reporting system.
Air filter elements according to the ISO 16890 series are evaluated in the laboratory by their ability to
remove aerosol particulate expressed as the e fficiency values ePM1 , ePM 2,5 and ePM10 . The air filter
elements can then be classified according to the procedures defined in ISO 16890-1. The particulate
removal e fficiency o f the filter element is measured as a function o f the particle size in the range o f
0,3 µm to 10 µm o f the unloaded and unconditioned filter element as per the procedures defined in
this part o f ISO 16890. A fter the initial particulate removal e fficiency testing, the air filter element is
© ISO 2016 – All rights reserved
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
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ISO 1 6890-2 : 2 01 6(E)
conditioned according to the procedures defined in ISO 16890-4 and the particulate removal e fficiency
is repeated on the conditioned filter element. This is done to provide in formation about the intensity o f
any electrostatic removal mechanism which may or may not be present with the filter element for test.
The average e fficiency o f the filter is determined by calculating the mean between the initial e fficiency
and the conditioned e fficiency for each size range. The average e fficiency is used to calculate the ePM x
e fficiencies by weighting these values to the standardized and normalized particle size distribution o f
the related ambient aerosol fraction. When comparing filters tested in accordance with the ISO 16890
series, the fractional e fficiency values shall always be compared among the same ePM x class (ex. ePM1
o f filter A with ePM1 o f filter B). The test dust capacity and the initial arrestance o f a filter element are
determined as per the test procedures defined in ISO 16890-3.
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INTERNATIONAL STANDARD ISO 1 6890-2 : 2 01 6(E)
It is intended for use in conjunction with ISO 16890-1, ISO 16890-3 and ISO 16890-4.
The test method described in this part o f ISO 16890 is applicable for air flow rates between 0,25 m 3/s
(900 m3/h, 530 ft3/min) and 1,5 m3/s (5 400 m3/h, 3 178 ft3/min), referring to a test rig with a nominal
face area of 610 mm × 610 mm (24,0 inch × 24,0 inch).
ISO 16890 (all parts) re fers to particulate air filter elements for general ventilation having an ePM 1
e fficiency less than or equal to 99 % and an ePM10 e fficiency greater than 20 % when tested as per the
procedures defined within ISO 16890 (all parts).
NOTE The lower limit for this test procedure is set at a minimum ePM10 e fficiency of 20 % since it will be very
di fficult for a test filter element below this level to meet the statistical validity requirements o f this procedure.
Air filter elements outside o f this aerosol fraction are evaluated by other applicable test methods, (see
ISO 29463 (all parts)).
Filter elements used in portable room-air cleaners are excluded from the scope.
The per formance results obtained in accordance with ISO 16890 (all parts) cannot by themselves be
quantitatively applied to predict per formance in service with regard to e fficiency and li fetime.
2 Normative references
The following documents, in whole or in part, are normatively re ferenced in this document and are
indispensable for its application. For dated re ferences, only the edition cited applies. For undated
re ferences, the latest edition o f the re ferenced document (including any amendments) applies.
ISO 16890-1, Air filters for general ventilation — Part 1: Technical specifications, requirements and
efficiency classification system based upon Particulate Matter (PM)
ISO 16890-3, Air filters for general ventilation — Part 3: Determination of the gravimetric efficiency and
the air flow resistance versus the mass of test dust captured
ISO 16890-4, Air filters for general ventilation — Part 4: Conditioning method to determine the minimum
fractional test efficiency
ISO 5167-1, Measurement of fluid flow by means of pressure differential devices inserted in circular cross-
section conduits running full — Part 1: General principles and requirements
ISO 21501-1, Determination of particle size distribution — Single particle light interaction methods —
Part 1: Light scattering aerosol spectrometer
ISO 21501-4, Determination of particle size distribution — Single particle light-interaction methods —
Part 4: Light scattering airborne particle counter for clean spaces
I SO 2 9 463 , High-efficiency filters and filter media for removing particles in air
[SOURC E: I SO 2 9 46 4: 2 011 , 3 . 2 . 3 8]
3 .1 . 2
nominal air flow rate
air flow rate (3 .1 .1 ) s p e ci fie d b y the manu fac tu rer
3 .1 . 3
resistance to airflow
d i fference i n pre s s ure b e twe en two p oi nts i n a n a i r flow s ys tem at s p e c i fie d cond ition s , e s p e c ia l ly when
3.2.2
filter element
s truc ture made o f the fi lteri ng materi a l, its s upp or ts and its i nter face s with the fi lter hou s i ng
3.2.3
upstream
U/S
re gion i n a pro ce s s s ys tem travers e d b y a flowi ng flu id b e fore it enters that p a r t o f the test device (3 . 2 .1)
3 . 2 .4
downstream
D/S
are a or re gion i nto wh ich flu id flows on le avi ng the test device (3 . 2 .1)
3.3 Aerosol
3 . 3 .1
liquid phase aerosol
liquid p ar ticles s us p ended in a gas
3.3.2
solid phase aerosol
sol id p ar ticles s us p ended in a gas
3.3.3
reference aerosol
defi ne d approve d aero s ol for te s t me a s urement with i n a s p e c i fic s i z e range
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ISO 1 6890-2 : 2 01 6(E)
3 . 3 .4
neutralization
action of bringing the aerosol to a Boltzmann charge equilibrium distribution with bipolar ions
3 .4 Particle counter
3 .4.1
particle counter
device for detecting and counting numbers of discrete airborne particles present in a sample of air
[SOURCE: ISO 29464:2011, 3.1.27]
3 .4. 2
optical particle counter
OPC
particle counter(3.4.1 f ) wh ich u nc tion s b y i l lum i nati ng a i rb orne p ar ticle s i n a s ample flow o f ai r,
conver ti ng the s c attere d l ight i mpu l s e s to ele c tric a l i mpu l s e data c ap able o f a na lys i s to provide data on
3 .4.4
particle size
ps
ge ome tric d i ame ter (e qu iva lent s pheric a l, op tic a l or aero dyna m ic, dep end i ng on contex t) of the
particles of an aerosol
[SOURCE: ISO 29464:2011, 3.1.126]
3 .4. 5
particle size distribution
presentation, in the form of tables, numbers or graphs, of the experimental results obtained using a
method or an apparatus capable of measuring the equivalent diameter of particles in a sample or capable
o f givi ng the prop or tion o f p ar ticles for wh ich the e qu iva lent di ame ter l ie s b etwe en defi ne d l i m its
3 . 5 .1
e fficiency
frac tion or p ercentage o f a ch a l lenge conta m i na nt that i s remove d b y a test device (3.2.1)
3.5.2
fractional e fficiency
abi l ity o f a n ai r cle an i ng device to remove p ar ticle s o f a s p e ci fic s i z e or s i z e range
N o te 1 to entr y: T he e ffic ienc y p lo tte d a s a fu nc tio n o f p a r ticle s i z e give s the p a r ticle s i z e e ffic ienc y s p e c tr u m .
3.5.3
penetration
P
ratio of p ar ticle count detec ted downs tream vers us the p ar ticle count up s tream
[SOURC E: I SO 2 9 46 4: 2 011 , 3 .1 .1 3 0]
3 . 5 .4
correlation ratio
R
ca lc u lation o f a ny p o tenti a l bi as b e twe en the up s tre am and down s tre am s ampl i ng s ys tem s
[SOURC E: I SO 2 9 46 4: 2 011 , 3 .1 . 8 8]
3 .6 . 2
reference filter
pri mar y de vice po s s es s ing acc u rate l y kno w n p a ra me ter s used as a s ta nd a rd fo r c a l ib rati n g
s e co nd a r y de vice s
[SOURC E: I SO 2 9 46 4: 2 011 , 3 . 3 9]
t ti me ( ye ars)
t0 , 5 h a l f-l i fe ti me ( ye a rs)
CV co e fficient o f variation
D c,i,ps downs tream correlation count for s ample i, and p ar ticle s ize, p s
D B , ps down s tre a m b ackground average count for e fficienc y s a mple, i, and for p ar ticle s i ze, ps
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ISO 1 6890-2 : 2 01 6(E)
D B,c, ps downstream background average count for correlation sample, , and for particle size, i ps
B b, , i ps , B f, ,
i ps f
meas ured b eginning or final ups tream b ackground count , and particle size,
or s ample, i ps
U B, , U B,c, up s tre am b ackground average cou nt for e fficienc y or correlation at a s p e ci fic p ar ticle
size,
ps ps
ps
Ui , ps f f
up s tre am e fic ienc y average , and for particle size,
or s ample, i ps
Di , ps f
down s tre am e ficienc y averagef , and for particle size,
or s ample, i ps
n number of samples
e c, ps 9 5 % u ncer tai nty o f the correlation va lue at a s p e c i fic p ar ticle s i z e, ps
R lcl, ps
lower con fidence l i m it o f the correlation ratio at a s p e ci fic p ar ticle s i ze, ps
R ucl, ps
upp er con fidence l i m it o f the correlation ratio at a s p e ci fic p ar ticle s i ze, ps
δ c, ps s tandard devi ation o f the correl ation va lue at a s p e ci fic p ar ticle s i ze, ps
Uc, i, ps correlation particles sampled for sample, , and for particle size,
i ps
P lcl, ps
lower con fidence l i m it o f the p ene tration at a s p e ci fic p a r ticle s i ze, ps
P ucl, ps
upp er con fidence l i m it o f the p ene tration at a s p e ci fic p a r ticle s i ze, ps
eps 9 5 % u ncer tai nty o f the p ene tration va lue at a s p e c i fic p ar ticle s i z e, ps
δps s tandard devi ation o f the p ene tration va lue at a s p e c i fic p ar ticle s i z e, ps
CL concentration limit
The complete test device (filter and frame) shall be made o f material suitable to withstand normal
usage and exposure to the range o f temperature, humidity and corrosive environments likely to be
encountered in ser vice.
T he complete tes t device shal l b e des igned so that it wi l l withs tand mechanical cons traints that are
likely to be encountered during normal use. Dust or fibre released from the test device media by air flow
through the tes t device shal l not cons titute a haz ard or nuis ance for the p eople (or devices) exp osed to
filtered air.
environmental equil ibrium with the tes t air weighed to the neares t gram . D evices requiring external
acces sories shal l b e op erated during the tes t with acces sories having charac teris tics equivalent to thos e
used in actual practice. The test device, including any normal mounting frame, shall be sealed into the
test rig in a manner that prevents leakage. The tightness shall be checked by visual inspection and no
visible leaks are acceptable. I f for any reason dimensions do not allow testing o f a test device under
standard test conditions, assembly o f two or more devices o f the same type or model is permitted,
provided no leaks occur in the resulting assembly. The operating conditions o f such accessory
equipment shal l b e recorded.
o f this part o f ISO 16890. All dimensions shown are mandatory unless otherwise indicated. Tolerances
are shown in the figures herein. Units are in mm (inch) unless otherwise indicated. The design
o f equipment not specified (including, but not limited to, blowers, valves and external piping) is
discretionary, but the equipment shall have adequate capacity to meet the per formance requirements
of this p ar t of I S O 16 8 9 0 .
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ISO 1 6890-2 : 2 01 6(E)
6 Test materials
The test aerosol shall consist of untreated and undiluted DEHS, or other liquid phase aerosols in
accordance with 6.3 aerosol reference.
Figure 1 gives an example of a system for generating the aerosol. It consists o f a small container
with DEHS liquid and a Laskin nozzle. The aerosol is generated by feeding compressed particle- free
air through the Laskin nozzle. The atomized droplets are then directly introduced into the test rig.
The pressure and air flow to the nozzle are varied according to the test flow and the required aerosol
concentration.
NOTE For a test air flow rate o f 0,944 m 3/s (2 000 ft3/min), the pressure is about 17 kPa (2,5 lb/in 2 ),
corresponding to an air flow o f about 0,39 dm 3/s [1,4 m 3/h, (0,82 ft3/min)] through the nozzle.
Any other generator capable o f producing droplets in su fficient concentrations in the particle size range
of 0,3 µm to 1,0 µm can be used.
Be fore testing, regulate the upstream concentration to reach steady-state and to have a concentration
below the coincidence level of the OPC.
Dimensions in millimetres
Key
The KCl test aerosol shall be polydisperse solid-phase (dry) potassium chloride (KCl) particles generated
from an aqueous solution. For example, a KCl solution can be prepared by combining 120 g o f reagent
grade KCl with 1 l of reagent grade distilled water. The solution is fed to the atomizing nozzle at around
1,2 ml/min (0,04 oz/min) by a metering pump. Varying the operating air pressure o f the generator and
the solution flow rate allows control o f the challenge aerosol concentration.
NOTE 1 Reagent grade water as defined by ASTM D1193.
NOTE 2 The 120 g KCl to 1 l o f water shown here is an example. The actual ratio used may vary depending on
the equipment used.
KCl
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ISO 1 6890-2 : 2 01 6(E)
The solid phase test aerosol generator shall be as illustrated in Figure 2. The aerosol generator shall
f f
provide a s table te s t aero s ol o s u fic ient concentration over the 0 , 3 0 µm to 10 µm p ar ticle s i z e range to
meet the minimum aerosol requirements of this part of ISO 16890 without overloading the OPC.
The nozzle is positioned at the top of a 305 mm (12,0 inch) diameter, 1 300 mm (51,0 inch) high
tran s p a rent ac r yl ic s pray tower. T he ta l l tower s er ve s two pu rp o s e s: it a l lows the KC l d rople ts to d r y
of the aerosol.
T he aero s ol sha l l b e brought to a B oltz man n ele c tro s tatic ch arge d i s tribution by an a lpha or b e ta
corona discharge ionizer shall have a minimum corona current of 3 µA and shall be balanced to provide
equal amounts of positive and negative ions.
NOTE 1 A Boltzmann charge distribution is the average charge found in ambient air. Electrostatic charging is
an unavoidable consequence of most aerosol generation methods of a solid phase aerosol.
NO TE 2 T he ac ti vity le vel o f a rad io ac tive s o u rce de c re a s e s with ti me . T he s ou rce s treng th o f 1 8 5 M B q (5 mC i)
is the minimum source strength at the end of the life. Thus, if the source strength is 370 MBq (10 mCi) when new,
the s ou rce s tren g th wi l l b e 1 8 5 M B q (5 mC i) a fter one h a l f-l i fe o f de c ay.
Key
Figure 2 — Schematic diagram o f the solid phase aerosol particle generator s ystem
For measuring the filtration per formance from 0,3 µm to 1,0 µm, the liquid phase aerosol listed in 6.1
shall be the reference material for this test method.
For measuring the filtration per formance from 1,0 µm to 10,0 µm, the solid phase aerosol listed in 6.2
shall be the reference material for this test method.
Only aerosols listed in 6.1 and 6.2 may be used to test devices as per this part o f ISO 16890. In order to
use an aerosol outside of the reference range for that aerosol, acceptable matching to the results of the
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ISO 1 6890-2 : 2 01 6(E)
reference aerosol for the particle size range being measured shall be achieved according to 6.3.4. Liquid
phase aerosol can only be used to measure filtration per formance in the particle size range from 1,0 µm
to 10,0 µm i f the test device media velocity is below 20 cm/s (39,4 ft/min).
7 Test equipment
7.1 Test rig
7.1.1 Dimensions
7.1.1.1 Cross dimensional area
The test rig (see Figure 3) consists of several square segments with 610 mm × 610 mm (24 inch × 24 inch)
nominal inner dimensions except for the test device section. The test device is located in section C and
may have nominal inner dimensions between 610 mm (24,0 inch) and 622 mm (24,5 inch).
Dimensions in millimetres
c c
Key
The test rig material shall be electrically conductive, electrically grounded, shall have a smooth interior
finish, and be su fficiently rigid to maintain its shape at the operating pressure. Smaller parts o f the test
rig could be made in glass or plastic to see the test device and equipment. Provision of windows to allow
monitoring of test progress is acceptable.
The entry plenum and the relative location o f high e fficiency filters and aerosol injections are
discretionary and a bend in the test rig is optional, thereby allowing both a straight test rig and a
U-shaped test rig configuration. Except for the bend itsel f, all dimensions and components are the same
for the straight and U-shaped configurations. A downstream mixing ba ffle shall be included in the test
rig a fter the bend. The length o f the test rig and individual sections are discretionary, but the test rig
shall meet all o f the apparatus qualification tests described in Clause 8.
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Dimensions in millimetres
Key
1 o rifice p late
rigid ele c tric a l ly conduc tive and ele c tric a l ly grou nde d me ta l l ic tubi ng havi ng a s mo o th i n s ide s u r face,
and sh a l l b e rigid ly s e c ure d to prevent movement duri ng te s ti ng. T he up s tre a m a nd down s tre a m
s a mple l i ne s sha l l b e nom i na l ly identic a l i n ge ome tr y ( b end s and s traight leng th s) . T he p or tion o f the
sampling lines inside the test rig shall block less than 10 % of the test rig cross-sectional area. The use
o f a shor t leng th [5 0 m m (2 , 0 i nch) ma xi mu m] o f s tra ight, flexible, ele c tric a l ly d i s s ip ative tubi ng to
NOTE 1 Particle losses in the test rig, aerosol transport lines and OPC need to be minimized because a smaller
nu mb er o f cou nte d p a r ticle s wi l l me a n l a rger s tati s tic a l er rors a nd le s s acc u rate re s u lts . T he i n fluence o f p a r ticle
losses on the result is minimized if the upstream and downstream sampling losses are made as near equal as
possible.
NO TE 2 T he u s e o f a s hor t fle xib le con ne c tio n o ften rel ie ve s s tre s s th at wo u ld b e p l ace d on the i n s tr u ment’s
inlet.
NO TE T h i s re fers to the average a i r velo c ity i n the te s t r ig a nd no t to the lo c a l velo c ity dep endent o n the
isokinetic sampling while meeting the requirements of 7.1.7.2, then the OPC pump can provide the
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ISO 1 6890-2 : 2 01 6(E)
sample air flow rate. The upstream and downstream sample air flow rate shall each be <2 % o f the test
rig air flow rate.
Key
1 test device
2 HEPA filter (clean air)
3 valve, upstream
4 valve, clean air
5 valve, downstream
6 computer
7 OPC
8 pump
Flow measurement shall be made by standardized flow measuring devices in accordance with
ISO 5167-1. The uncertainty o f measurement shall not exceed 5 % o f the measured value.
7.1 .9 Resistance to air flow measurement
Measurements o f resistance to air flow shall be taken between measuring points located in the test rig
wall as shown in Figure 3. Each measuring point shall comprise four interconnected static pressure
taps (see Figure 6 ) equally distributed around the periphery o f the test rig cross section. Figure 6 is
shown as an example of a static pressure tap. The static pressure tap hole shall be 2 mm ± 0,5 mm
(0,08 inch ± 0,02 inch). The complete system should pass the qualification testing in 8.2.
The pressure measuring equipment used shall be capable of measuring pressure differences with an
accuracy o f ±2 Pa (0,01 inch H 2 O) in the range of 0 Pa to 70 Pa (0,28 inch H 2 O). Above 70 Pa (0,28 inch
H 2 O), the accuracy shall be ±3 % o f the measured value.
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Dimensions in millimetres
The test apparatus shown in Figure 3 is designed for a test device with nominal face dimensions of
610 mm × 610 mm (24,0 inch × 24,0 inch). Transitions in accordance with Figure 7 shall be used for test
devices with face areas from 60 % to 150 % of the normal test rig cross section area of 0,37 m2 (4 ft2 ).
It is permitted to test a bank of several devices if the face area of an individual device is less than 60 %
o f f
the te s t rig are a . I t i s a l s o p erm itte d to te s t s p e c ia l ly s i z e d te s t device s dupl ic ati ng the s truc ture o
Key
1 tes t device dimens io ns s maller than tes t rig (asymmetrical dimens io ns are allowed)
2 tes t device dimens io ns larger than tes t rig (asymmetrical dimens io ns are allowed)
NOTE Even though this equipment is not used to measure the particle removal e fficiency, the equipment is
used to measure the filter element per formance as per the ISO 16890-3 test method. Listing o f the equipment and
requ irements are provide d i n I S O 16 8 9 0 -2 to help the u s er when as s embl i ng a tes t rig for b o th I S O 16 8 9 0 -2 and
I S O 16 8 9 0 -3 .
shown for the D/S mixing orifice in 7.1 . 6 and shown in Figure 4. I f an in let plenum is ins tal led in the tes t
rig, the orifice plate component in Figure 4 can be eliminated. The per forated plate mixing ba ffle shall
b e ins tal led and located as dimens ioned in Figure 4.
NOTE With an inlet plenum, the air is adequately mixed and use o f only the per forated plate allows the dust
to mix with a more uni form air flow distribution providing an even dust distribution on the face o f the test device.
These instruments are commonly known as optical particle counter spectrometers (OPC) and also as
op tical aerosol s p ec trometers .
test data set or 0,3 µm to 10,0 µm range for a full data set. The counting e fficiency o f the OPC shall be
≥50 % for 0,3 µm particles.
18
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
to 3,0 µm, and 3,0 µm to 10,0 µm. Particle size channel boundaries shall be located at 0,3 µm, 1,0 µm,
3,0 µm and 10,0 µm. The recommended particle size channels boundaries are shown in Table 2.
Table 2 — Recommended OPC(s) particle size range boundaries
Lower limit Upper limit Geometric mean
Size particle size limit
range µm µm µm
1 0,30 a 0,40 0,35
2 0,40 0,55 0,47
3 0,55 0,70 0,62
4 0,70 1,00 a 0,84
5 1,00 a 1,30 1,14
6 1,30 1,60 1,44
7 1,60 2,20 1,88
8 2,20 3,00 a 2,57
9 3,00 a 4,00 3,46
10 4,00 5,50 4,69
11 5,50 7,00 6,20
12 7,00 10,0 a 8,37
a Required channel boundaries.
7.2.4 Sizing resolution
The sizing resolution o f the OPC shall be ≤8 % (standard deviation/mean) and shall be measured in
accordance with ISO 21501-1. The resolution shall be measured at a particle size in the 0,5 µm to 0,7 µm
size range.
7.2.5 Calibration
The OPC shall be calibrated in accordance with ISO 21501-4. The calibration shall be performed with
monodisperse NIST-traceable PSL and the calibration shall include at least one particle diameter in each
of the ranges of 0,3 µm to 0,4 µm, the upper most channel of the range to be tested (either 2,20 µm to
3,00 µm for the minimum data range or 7,00 µm to 10,00 µm for the full data set range), and at least four
other sizes in between. The particle size calibration o f the OPC shall be per formed at least annually.
The temperature measurement device shall be accurate to within ±1 °C (1,8 °F). The relative humidity
measurement device shall be accurate to within ±2 %. The temperature and relative humidity
measurement devices shall be calibrated yearly.
8.1 .1 General
Apparatus qualification tests shall veri fy quantitatively that the test rig and sampling procedures
are capable o f providing reliable fractional e fficiency measurements and resistance to air flow
measurements. Maintenance testing shall keep the system in good operating order. Additional cleaning
and maintenance operations subject to any normal laboratory operation shall also be needed beyond
what is listed in Clause 8.
Full system qualification testing shall take place every two years or sooner i f any change is made to the
system that may alter per formance, such as changing a major component o f the system. It is suggested
that the qualification test be per formed in the order listed in Table 3.
A change to the system requiring requalification would include, but is not limited to, changing the
blower, reconfiguring the test rig dimensions, changing the locations o f the OPC, generators, etc. Also,
this order o f testing should allow the user to minimize potential retesting due to modifications that
may be required to pass sections o f the qualification testing. For example, not knowing the aerosol
generator response time could cause issues trying to pass the aerosol uni formity test.
8.1 .3 Qualification documentation
The test rig owner/operator shall always have a qualification testing report available documenting the
results o f the latest qualification testing.
Table 3 — Qualification testing requirements
Subclause
o f this
Qualification tes ting Requirement
part o f
I SO 16890
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ISO 1 6890-2 : 2 01 6(E)
Table 3 (continued)
Subclause
o f this
Qualification tes ting Requirement
p art o f
ISO 1689 0
Aerosol neutralizer — Radioactive service life Document source strength when new
8.2.7.3
verification Remaining life >185 Mbq (5 mCi)
Aerosol neutralizer — Radioactivity is present 8.2.7.4
Aerosol neutralizer — Corona discharge current 8.2.7.6 ≥3 µA
Aerosol neutralizer — Corona discharge bal- 8.2.7.7 As close as possible a reading of zero
anced output
Test rig — Air leakage test 8.2.8 <1 %
Test rig — Air velocity uni formity 8.2.9 CV < 10 %
Test rig — Aerosol uni formity 8.2.10 CV < 15 %
Test rig — Downstream mixing 8.2.11 CV < 10 %
Test rig — Empty test device section pressure 8.2.12 <5 Pa (0,02 inch H 2 O)
Test rig — 100 % e fficiency test 8.2.13 >99 % for all particle sizes
0,30 µm to 1,0 µm: 0,90 to 1,10
Test rig — Correlation ratio 8.2.14 1,0 µm to 3,0 µm: 0,80 to 1,20
3,0 µm to 10,0 µm: 0,70 to 1,30
a This test is required if an aerosol other than the reference one is used for a particle size range.
The test shall be made by calibrated pressure measuring devices or by the system described in Figure 8.
Care fully seal the pressure sample points in the test rig to be able to withstand a negative pressure o f
5 000 Pa (20,0 inch H 2 O). Disconnect the pressure sensor(s) and apply the negative pressure to each
individual sample line until all sample pressure lines have been tested.
For each pressure sensor connected to the system, apply the maximum pressure allowed by the
manu facturer to the sensor. This test shall be carried out sequentially on all pressure lines attached to
the test rig.
NOTE The pressure system test is to veri fy the lines, connectors and equipment used to measure pressure in
the test rig do not significantly a ffect the accuracy o f the measurements o f air flow rate or resistance to air flow.
For each sample line or sensor port, after 30 s of testing there shall be no change in the pressure from
the applied pressure value.
Key
1 sealed pressure inlet
2 test device section
3 Δ p = 5 000 Pa (20,0 inch H 2 O)
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I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
The zero count o f the OPC(s) shall be verified to be <10 total counts per minute in the 0,30 µm to 10,0 µm
size range.
NOTE The ability o f the OPC to zero count is a quick indication i f maintenance is needed on the OPC.
The sizing accuracy o f the OPC(s) shall be checked by sampling an aerosol containing monodisperse
polystyrene spheres (PSL) o f known particle size.
NOTE OPC(s) measure the particle count and the equivalent optical particle size. The indicated particle size
is strongly dependent on the calibration o f the OPC. Checks with PSL particles at the low and the high end o f the
OPC’s particle size range are especially meaning ful.
A relative maximum particle count shall appear in the OPC sizing channel that encompasses the PSL
particle diameter. This result is not intended to be an OPC calibration, but simply a sizing accuracy
check of the OPC.
8.2 .5 OPC — Overload test
8.2 .5 .1 General
OPCs may underestimate particle concentrations i f their concentration limit is exceeded. There fore, it is
necessary to know the concentration limit o f the OPC being used. The maximum aerosol concentration
used in the tests shall then be kept su fficiently below the concentration limit, so that the counting error
resulting from coincidence does not exceed 5 % .
NOTE The measured fractional e fficiency in the 0,30 µm to 0,40 µm particle size range o ften decreases as
the concentration begins to overload the OPC.
8.2 .5 .2 Overload test protocol
A series o f initial fractional e fficiency tests shall be per formed over a range o f challenge aerosol
concentration to determine a total concentration level for the fractional e fficiency test that does not
overload the OPC(s). I f the upstream concentration in the test rig cannot be reduced, a dilution system
may be used to reduce the aerosol concentrations below the OPC´s concentration limit. It is then
necessary to take upstream and downstream samples via the dilution system in order to eliminate
errors arising from uncertainty in the dilution factor’s value. The lowest total concentration level shall
be less than 1 % of the instrument’s stated total concentration limit. The tests shall be performed
following the procedures of 9.3 on a media-type air cleaner using a range of upstream aerosol
concentrations. The tests shall be performed at 0,944 m3/s (2 000 ft3/min). The filters selected for this
test shall have an initial fractional e fficiency in the range o f 30 % to 70 % as measured by the 0,30 µm
to 0,40 µm particle size range and >90 % for the 7,0 µm to 10 µm particle size range. The aerosol for
these tests shall be generated using the same system and procedures o f 9.3.
The tests shall be per formed over a su fficient range o f total aerosol challenge concentrations to
demonstrate that the OPC(s) is not overloaded at the intended test concentration. The measured
filtration e fficiencies should be equal over the concentration range where overloading is not significant.
s a mpl i ng from the up s tre am prob e . Si m i la rly, me a s u re the ti me i nter va l for the aero s ol to re tu rn to
s tate cond itio n fo r te s ti n g. T h i s i s to en s u re th at s u ffic ient ti me i s a l lowe d for the aero s ol concentration to
s tab i l i z e pr ior to b e gi n n i n g the up s tre a m/down s tre a m s a mp l i ng s e quence du ri n g the fi lter te s ti ng.
Us e the aero s ol generator defi ne d i n 6 .1 .4 and the OPC defi ne d i n 7. 2 to fi nd the aero s ol generator
res p ons e times for liquid phase aerosol . Rep eat this tes t us ing the solid phase aerosol generator in 6 . 2 .4.
generator and b eginning the OPC s ampling sequence and ( b) deac tivating the aerosol generator and
b eginning the OPC s ampling sequence for determination of b ackground aerosol concentrations .
I f a corona discharge ionizer is used, it shou ld have a minimum corona current of 3 µ A and shal l b e
NO TE W hen te s ti n g fi lters with a s o l id p h a s e aero s o l ele c tro s tatic ch a rge on , the aero s ol c a n a ffe c t the te s t
passed from date o f manu fac tu re, th at the c u rrent rad io ac tivity o f the s ou rce i s ab ove 1 8 5 M B q (5 mC i) .
− t
t0 5
Ra = Ra 0 ⋅ 2 ,
> 185 MBq ( 5 mCi ) (1)
where
Ra 0 origi na l rad io ac tivity o f the s ou rce (at d ate o f manu fac tu re) , M B q (mC i) ;
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I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
as the leak rate, and the test shall then be repeated for the other two test pressures. The measured leak
rates shall not exceed 1,0 % o f the corresponding test air flow rate. The highest pressure anticipated
by this part o f ISO 16890 is 3 200 Pa (13 inch H 2 O). The user should exercise caution and should not
pressurize the test rig beyond its design limit for personal sa fety.
where
δ is the standard deviation o f the nine averaged measuring points;
mean is the mean value of the nine measuring points.
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ISO 1 6890-2 : 2 01 6(E)
Dimensions in millimetres
upstream of the test device location using the grid points as shown in Figure 9.
T he travers e f
me as u rements s ha l l f be 3/s, 0,944 m 3/s and
p er orme d at ai r flow rate s o 0,236 m
1,416 m3/s (500 ft3/min, 2 000 ft3/min, and 3 000 ft3 /m i n) . T he travers e sh a l l b e made b y rep o s ition i ng
f f
a s i ngle prob e to ma i ntai n the s ame s ample l i ne con figu ration or e ach o the n i ne grid p oi nts . T he i n le t
nozzle of the sample probe shall be a tapered sharp edged sample probe and meet the requirements of
7.1.7.2 for isokinetic sampling at 0,944 m3/s (2 000 ft3/min). This same inlet nozzle diameter shall be
u s e d at a l l ai r flow rate s .
NO TE I f the aero s ol d i s tr ib ution i s no t u n i for m i n the te s t r ig , the re s u lts o f frac tion a l e ffic ienc y te s ti n g c a n
shown in 7.2 f . T he nu mb er o p ar ticle s cou nte d i n a s p e ci fie d s i z e ra nge i n a s i ngle me a s u rement sha l l
be >100 in order to reduce the statistical error. If both solid and liquid aerosols are used in testing, both
aero s ol s ys tem s sh a l l me e t th i s qua l i fic ation re qui rement.
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ISO 1 6890-2 : 2 01 6(E)
The CV of the corresponding nine grid point particle concentrations shall be less than 10 % for each
ai r flow rate i n e ach o f the 1 2 O PC p ar ticle s i ze ra nge s . I f the re qu i re d degre e o f down s tre am aero s ol
m i xi ng i s no t ach ieve d, veri fy th at the down s tre a m m i xi ng ori fice a nd b a ffle a re prop erly de s igne d
and centre d . C on fi rm th at the aero s ol nebu l i z er provide s a s table output b y i nj e c ti ng the aero s ol at
the centre o f the te s t rig lo c ation wh i le rep e ate d ly s ampl i ng down s tre am . I mprove the s tabi l ity o f the
mean ps is the mean value of the nine measuring points for particle size range, ps.
Dimensions in millimetres
S e t the te s t rig ai r flow rate to 0 ,9 4 4 m 3/s (2 000 ft3/min) with no test device in the test device section.
Re cord the re s i s tance to a i r flow o f the emp ty te s t device s e c tion .
T he me as u re d re s i s tance to ai r flow acro s s the emp ty te s t device s e c tion sha l l b e le s s than 5 Pa (0 , 02 i nch
H2 O) . S ys tem mai ntenance sha l l b e p er forme d unti l the res i s tance to ai r flow i s b elow th i s level .
NOTE Since there is a linear distance between the upstream and downstream pressure sampling points, there
can b e a s mal l tare pre s s u re or s ys tem e ffe c t due to thi s d is tance and the movement o f the ai r. T he s ys tem tare do e s
no t i nclude any fi lter mou nti ng hardware wh ich may b e u se d to hold the fi lter i n a normal in s ta l lation,5.2.
© ISO 2016 – All rights reserved
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
29
ISO 1 6890-2 : 2 01 6(E)
An initial fractional e fficiency test shall be per formed using a filter element with an e fficiency o f at least
H E PA according to I S O 2 9 463 -1 as the tes t device. T he tes t pro cedures for determination of frac tional
e fficiency given in 9. 3 shall be followed and the test shall be per formed at an air flow rate o f 0,944 m 3 /s
(2 0 0 0 ft3 /min) .
One parameter a ffecting the e fficiency during the 100 % e fficiency test is the purge time. The purge
time is to o shor t if, after s witching from the up s tream to the downs tream line, res idual p ar ticles from
the upstream sample are counted during the downstream sampling and yield an e fficiency o f <99 %. In
this case, the purge time shall be increased and the 100 % e fficiency test repeated.
NOTE The purpose o f this test is to ensure that the test rig and sampling system are capable o f providing
a 100 % e fficiency measurement. In addition, this test assesses the adequacy o f the aerosol generator response
ti me from 8 . 2 . 6 . I f the response time is insu fficient, residual particles from the relatively high concentration
The fractional e fficiency shall be greater than 99 % for all particle sizes. Determine an acceptable purge
time to meet this test requirement and double the time needed as a sa fety factor. Use this sa fety factor
value as the tes t purge time.
The correlation ratio test shall be per formed without a test device in place to check the adequacy o f the
overal l tes t rig, s ampling, meas urement and aerosol generator.
NOTE In a per fect system, the correlation ratios are 1,0 at all particle sizes. Deviations from 1,0 can occur
due to particle losses in the test rig, di fferences in the degree o f aerosol uni formity (i.e. mixing) at the upstream
and downstream probes, and di fferences in particle transport e fficiency in the upstream and downstream
s a mple l i nes .
The test shall be per formed as a normal fractional e fficiency test but with no test device installed. The
test air flow rate shall be 0,944 m /s (2 0 0 0 ft /min) . T he tes t pro cedures for determination of the
3 3
The correlation ratio for each particle size shall meet the data quality requirements from 10 . 3 . 3 .
NOTE I f the correlation ratio falls outside o f the required specification at the smaller particle sizes (<1,0 µm),
suspect incomplete mixing at the upstream probe location; the aerosol injection tube may need to be realigned or
additional mixing provided in the discretionary ductwork upstream o f the upstream mixing orifice. I f the small
p ar ticles are with i n requi red l im its but the larger p ar ticles are no t, s us p ec t une qua l s ample li ne lo s s es . For dua l
OPC systems, also suspect that one o f the OPCs may be out o f calibration or have air flow issues.
8.3 Maintenance
8.3 .1 General
Apparatus maintenance testing gives the user a way to check the system on a regular basis and keep
it in good operating order. Additional cleaning and maintenance operations subject to any normal
30
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
laboratory operation shall also be needed beyond what is listed in 8.3. The maintenance schedule is
shown in Table 4. Items are shown based on the proper time to perform each maintenance item with
references to the appropriate subclause of this part of ISO 16890. Several items listed here are also part
o f the qualification test requirements, but are listed here as they shall be per formed and documented
more o ften than the qualification requirement.
Subclause
o f this E ach Two Si x
M aintenance items Monthly Yearly
part o f tes t weeks months
I SO 16890
Test rig background counts are part o f the normal fractional e fficiency testing process defined in 9.3.1.
Regular monitoring o f these results enable the test rig owner/operator to find potential issues with the
system be fore they become a problem.
NOTE Increases in the background counts could be a sign o f an intake HEPA filter problem, an OPC problem,
or even a test rig leakage problem.
For each test rig, a minimum o f three identical re ference filters shall be maintained by the testing
facility solely for initial fractional e fficiency testing on a biweekly basis. The re ference filter shall be
o f structurally stable design. The fractional e fficiency o f the re ference filters shall pass through 50 %
e fficiency in the particle diameter range o f 0,7 µm to 3,0 µm and be <35 % at 0,30 µm to 0,40 µm
and >70 % in the 7,0 µm to 10,0 µm range. The three re ference filters shall be labelled as “primary,”
“secondary” and “reserve.” These re ference filters shall remain protected when not in use and stored in
a safe place from potential damage.
Testing a known re ference filter for fractional e fficiency enables the test rig owner/operator to find
potential issues with the system be fore they become a problem. Detecting shi fts in the e fficiency
curves becomes di fficult i f the e fficiency is either very high or very low for all particle sizes. Changes
in the filtration e fficiency o f electret media re ference filters may be due to reduced e ffectiveness o f the
neutralizer and its condition should then be checked.
The “primary” re ference filter shall be tested at an air flow rate o f 0,944 m 3/s (2 000 ft3/min) for
fractional e fficiency as defined in 9.3 every two weeks. I f the fractional e fficiency values shi ft by >5
percentage points for any o f the particle sizing channels, the “secondary” re ference filter shall be
tested. I f both the primary and secondary re ference filters show shi fts >5 percentage points for any o f
the particle sizing channels, system maintenance shall be per formed as needed (e.g. clean sample lines,
recalibrate the OPC, etc.) to restore the re ference filter fractional e fficiency test to a <5 percentage
point shi ft. The “reserve” re ference filter shall be used i f either the primary or secondary re ference
filter becomes unusable (e.g. damaged).
NOTE Percentage points is not to be con fused with percent. As an example, the di fference between e fficiency
values of 30 % and 35 % is 5 percentage points, not 5 %.
The re ference filters shall be tested as defined in 9.3 for fractional e fficiency and resistance to air flow.
These initial values shall be the re ference values for that re ference filter.
The measured resistance to air flow across the re ference filter shall be within 10 % o f the re ference value
for that re ference filter. I f the resistance to air flow deviates by more than 10 %, system maintenance
shall be per formed to restore the resistance to air flow to within 5 % o f the re ference value.
NOTE Examples o f system maintenance steps that can be per formed to restore the resistance to air flow
include (but are not limited to) checking for leaks in the ducting and around the flow nozzle, and checking the
manometer for proper zero and level.
Immediately a fter recalibration o f the OPC(s), retest each o f the re ference filters (or a new set o f
re ference filters) to establish new fractional e fficiency and resistance to air flow re ference values.
8.3 .3 .6 Re ference filter replacement
When either the primary or secondary re ference filter shows a shi ft >5 percentage points for any o f the
particle size ranges and the secondary or reserve re ference filter does not show the shi ft, the primary
32
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
and/or secondary re ference filter shall be replaced with an identical filter or filters, i f available, or a
new set o f identical re ference filters shall be obtained.
NOTE A re ference filter’s e fficiency may change with the collection o f test aerosol a fter repeated use.
9 Test methods
9.1 Air flow rate
The test device shall be tested at its nominal air volume flow rate for which the device has been specified
by the manu facturer.
I f the manu facturer does not speci fy a nominal air volume flow rate, the test device shall be tested
at 0,944 m3/s (2 000 ft3/min). The air flow velocity associated with this volumetric flow is 2,54 m/s
(500 ft/min). Unless otherwise specified, the test shall be per formed at 0,944 m 3/s (2 000 ft3/min).
For test devices that are not nominal 610 mm × 610 mm (24,0 inch × 24,0 inch) in face area, the nominal
f ace area shall be multiplied by 2,54 m/s (500 ft/min) to get the test air flow rate.
ru n at the te s t device ai r flow rate, a fter the frac tiona l e ffic ienc y te s ti ng , a nd with the aero s ol generator
off. E ach p ar ticle count for the b ackground s ampling shal l have a minimum s ample time of 3 0 s and al l
b ackground p ar ticle cou nts sh a l l have the s ame s ample ti me as the frac tiona l e fficienc y cou nts . T he
average b ackground count shal l b e les s than 5 % of the average meas ured up s tream count during the
fi lter element te s t.
NO TE C le a n i ng the i n s ide s u r face o f the te s t duc t b o th up s tre a m a nd down s tre a m o f the te s t device
up s tre a m co u nt.
a) I ns tal l the tes t device, un les s this is a correlation tes t, then no tes t device is ins tal led.
1) P urge the up s tream/downs tream l ines according to the purge time value determined from
8 . 2 .1 3 . 2 .
d) Star t the aeros ol generator and let s tabi l ize as p er the time determined in 8 . 2 . 6 .
e) M e a s u re e fficienc y counts . Rep e at 9. 3 . 3 .1 e) unti l 5 ups tream and 5 down s tream counts have b een
s ampled.
g) Stop the aerosol generator and let s tabi li ze as p er the time determined in 8 . 2 . 6 .
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ISO 1 6890-2 : 2 01 6(E)
i) 10.3.
C he ck the data qua l ity re qui rements a s defi ne d i n
1) I f the data qua l ity re qu i rements are go o d, s top the ai r flow and remove the te s t device .
2) I f the data qua l ity re qu i rements are no t accep table, rep e at item s c) to h) a s a comple te s e t and
Gen Off
Gen On
U/S Bb,1,ps Bb,2,ps N1, ps N2, ps N3, ps N4, ps N5, ps N6, ps Bf,1, ps Bf,2, ps
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
Purge
D/S db,ps D1, ps D2, ps D3, ps D4, ps D5, ps df, ps
For a s ingle OPC s ys tem, the ups tream counts from two s amples shall be averaged to obtain an es timate
of the upstream counts that would have occurred at the same time as the downstream counts were taken.
For the up s tre am b egi n ni ng and fi na l b ackgrou nd cou nts:
B b, i , ps + B b, i + 1 ,ps
U B,b, ps =
2
( )
(5)
B f, i , ps + B f, i + 1 ,ps
U B,f, ps =
2
( )
(6)
where
U B,b, ps is the beginning upstream background average count for particle size, ps ;
B b, , psi is the measured beginning upstream background count for particle size, ps ;
B f, , ps
i f
i s the me as u re d fi na l up s tre am b ackgrou nd cou nt ps. or p ar ticle s i z e,
T he up s tre am b ackgrou nd counts b e fore and a fter the e ffic ienc y or correlation s ample s sh a l l s i mply b e
averaged.
U B,b, ps + U B,f,ps
U B,c, ps or U B, ps =
2
(7)
where
U B, ps i s the up s tre a m b ackgrou nd average cou nt , and for particle size, ps for e ffic ienc y s a mple, i ;
U B,c, ps is the upstream background average count for correlation sample, , and for particle size, ps i ;
U B,b, ps is the beginning upstream background average count for sample, , and for particle size, ps i ;
U B,f, ps f
i s the fi na l up s tre am b ackgrou nd average cou nt , and for particle size, ps. or s ample, i
T he down s tre a m b ackgrou nd cou nts b e fore a nd a fter the e fficienc y or correl ation s ample s s ha l l s i mply
b e averaged.
d b, ps + d f,ps
D B,c, ps or D B, ps = (8)
2
where
s i ze, ps;
D B , c , ps is the downs tream b ackground average count for correlation s ample, i, and for p ar ticle
s i ze, ps;
db , ps is the b eginning downs tream b ackground average count for p ar ticle s i ze, ps;
df, ps i s the fi na l down s tre am b ackgrou nd average cou nt for p ar ticle s i z e, ps.
N i ps + N i +1 ps
U i ps = , ( ),
(9)
,
2
where
Ui, ps i s the up s tre am e fficienc y average for s a mple, i, and for p ar ticle s ize, ps;
Ni, ps i s the me a s u re d up s tre am e ffic ienc y cou nt for s ample, i, and for p ar ticle s i ze, ps.
a) I ns tal l the tes t device, un les s this is a correlation tes t, then no tes t device is ins tal led.
1) P urge the ups tream/downs tream lines as p er the purge time value determined from 8 . 2 .1 3 . 2 .
2) S ample the ups tream (UB , b ,1 ) and down s tream (db ,1 ) b ackground p ar ticles .
d) Star t the aeros ol generator and let s tabi l ize as p er the time determined in 8 . 2 . 6
e) M e a s u re e ffic ienc y cou nts . Rep e at 9. 3 .4.1 e) unti l 5 ups tream and 5 downs tream counts have b een
s ampled.
2) S ample the ups tream (Ui ) and the downs tream (D i ) p ar ticles .
f) Stop the aerosol generator and let s tabi li ze as p er the time determined in 8 . 2 . 6 .
36
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
2) Sample the upstream (UB,f,1) and the downstream (df,1) background particles.
h) 10.3.
C he ck the data qua l ity re qui rements a s defi ne d i n
1) I f the data qua l ity re qu i rements are go o d, s top the ai r flow and remove the te s t device .
2) I f the data qua l ity re qui rements are no t accep table, rep e at item s c) to g) as a comple te s e t and
Background, 1 2 3 4 5 Background,
beginning ?inal
Gen Off
Gen On
U/S UB,b,ps U1, ps U2, ps U3, ps U4, ps U5, ps UB,f, ps
Purge
Purge
Purge
D/S d b, ps D 1, ps D 2, ps D 3, ps D 4, ps D 5, ps d f, ps
T he up s tre am b ackgrou nd counts b e fore and a fter the e ffic ienc y or correlation s ample s sh a l l s i mply b e
averaged.
U B,b, ps + U B,f,ps
U B,c, ps or U B, ps =
2
(10)
where
UB, ps i s the up s tre a m b ackgrou nd average e ffic ienc y cou nt for p ar ticle s i ze, ps;
UB,c, ps is the upstream background average correlation count for particle size, ps ;
UB,b, ps is the beginning upstream background average count for particle size, ps ;
UB,f, ps f
i s the fi na l up s tre am b ackgrou nd average cou nt ps. or p ar ticle s i z e,
T he down s tre a m b ackgrou nd cou nts b e fore and a fter the e fficienc y or correlation s a mple s sh a l l s i mply
be averaged.
d b, ps + d f,ps
D B,c, ps or D B, ps =
2
(11)
where
DB, ps i s the down s tre am b ackground average e ffic ienc y count for p a r ticle s i ze , ps;
DB,c, ps is the downstream background average correlation count for particle size, ps ;
db, ps is the beginning downstream background average count for particle size, ps ;
df, ps f
i s the fi na l down s tre am b ackgrou nd average cou nt ps. or p ar ticle s i z e,
The correlation ratio, R , shal l b e us e d to corre c t for any bias b e twe en the up s tre am and downs tre am
s ampl i ng s ys tem s . T he correlation ratio sha l l b e e s tabl i she d from the ratio o f down s tre am to up s tre am
p ar ticle counts with the aero s ol generator on, but without any tes t device i ns ta l le d i n the te s t rig. T he
correlation ratio sha l l b e de term i ne d for e ach tes t device and at the ai r flow rate o f the tes t device . To
measure the correlation ratio, follow the sampling requirements of 9.3.1 without installing a test device.
downstream
R= (12)
upstream
where
The correlation ratio shall be calculated for each upstream and downstream sample in each particle
size range using the upstream and downstream values.
D c i ps
R i ps = , ,
(13)
,
U c i ps, ,
where
Ri,ps is the correlation ratio for sample, i, and for particle size, ps;
D c,i,ps is the downstream correlation count for sample, i, and for particle size ps;
Uc,i,ps is the upstream correlation count for sample, i, and for particle size ps.
particle size.
R ps =
∑= R n
i 1 i ps ,
(14)
n
where
Ri,ps is the correlation ratio for sample, i, and for particle size, ps;
n number of samples
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I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
δ ps =
∑= n
i 1
( R i ps
,
− R ps )
2
(15)
c,
n− 1
where
δ c, ps is the standard deviation of the correlation ratio for particle size ps ;
Ri, ps is the correlation ratio for sample and for particle size i ps ;
e ps =δ ps × st (16)
n
c, c,
where
e c, ps i s the correlation uncer ta i nty for p ar ticle s i z e, ps ;
de gre e s o f fre e do m . T he t d i s tr ib ution tab le (two ta i le d) for a 9 5 % con fidence le vel i s s hown .
R pslcl,
= R ps − e c, ps (17)
R ucl, ps = R ps + e c, ps (18)
where
i s the lower con fidence l i m it o f the correl ation ratio for
R ps lcl,
p ar ticle s i z e, ps ;
n v = n − 1
5 4 2,776
10 9 2,262
15 14 2,145
Table 7 (continued)
Number o f Number o f degrees o f
s amples freedom st
n v =n − 1
20 19 2 ,093
25 24 2 ,064
30 29 2 ,045
The sum of the particles sampled during the correlation counts shall be calculated.
U c,tot,ps = ∑= n
i 1
U c, i , ps (19)
where
Uc,tot, ps is the sum of the particles sampled during correlation for particle size, ps;
Uc, i, ps is the correlation particles sampled for sample, i, and for particle size, ps.
T he frac tiona l e fficienc y i s a me a s u re o f the frac tion o f p ar ticle s that the te s t device remove s from
the air that passes through it and is calculated from the amount of particulate that penetrates the
test device during the test. The general formulas for penetration (P) a nd frac tiona l e fficienc y (Eps) are
shown below.
P = downstream (20)
upstream
where
The observed penetration shall be calculated for each upstream and downstream sample in each
particle size range using the upstream and downstream values.
D i ps
Pi ,o, ps = ,
(22)
U i ps ,
40
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
where
is the observed penetration for sample and for particle size,
Pi ,o, ps i ps ;
is the downstream particle count for sample, , and for particle size,
D i, ps i ps ;
is the upstream particle count for sample, , and for particle size, .
Ui, ps i ps
These penetrations shall be averaged to determine the observed penetration value for each particle size.
Po,ps =
∑= P n
i 1 i ,o, ps (23)
n
where
Po,ps is the observed penetration for particle size, ps ;
Pi ,o, ps is the observed penetration for sample, , and for particle size, .
i ps
δ o, ps =
∑= n
(P
i 1 i ,o, ps
− Po,ps ) 2
(24)
n−1
where
δ o, ps is the standard deviation of the observed penetration for particle size, ps ;
Pi ,o, ps is the observed penetration for sample, , and for particle size, .
i ps
T he ob s er ved p ene tration s sha l l b e corre c te d b y the correl ation ratio to give the fi na l p ene tration
where
δ ps is the standard deviation of the observed penetration for particle size, ps;
δ c, ps is the standard deviation of the correlation ratio for particle size, ps;
δ o, ps is the standard deviation of the observed penetration for particle size, ps;
e ps = δ ps × st (27)
n
where
eps i s the p ene tration u ncer tai nty for p ar ticle s i ze, ps ;
P pslcl,
= Pps − e ps (28)
P psucl,
= Pps + e ps (29)
where
The sum of the upstream particle counts for particle size, ps, shall be calculated.
U tot,ps = ∑=U n
i 1 i ps
,
(30)
where
Utot, ps is the sum of the upstream particle counts for particle size, ps;
Ui, ps i s the e ffic ienc y p ar ticle s s a mple d for s a mple, i , and for particle size, ps.
42
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
The correlation background count values for each particle size shall be less than 5 % of the average
upstream particle measured during the correlation testing.
where
UB,c, ps is the upstream background average correlation count for particle size, ps ;
DB,c, ps is the downstream background average correlation count for particle size, ps ;
T he e fficienc y b ackground cou nt va lue s for e ach p a r ticle s i z e s ha l l b e le s s than 5 % o f the average
D B, ps or U B, ps <
∑= n
i 1
U i ps
,
× 0 05
, (32)
n
where
UB, p s i s the up s tre am b ackground average e ffic ienc y count for p a r ticle s i z e, ps ;
DB, ps i s the down s tre am b ackgrou nd average e ffic ienc y cou nt for p ar ticle s i z e, ps ;
T he correlation ratio s f
and uncer ta i nty s ha l l Table 3 and repeated
a l l with i n the l i m its s hown i n
below in Table 8. The minimum number of counts from Formula (19) for each particle size shall be
f f
gre ater tha n or e qua l to 5 0 0 . I f a s u ficient nu mb er o cou nts i s no t ob tai ne d, the s ample ti me or aero s ol
concentration shall be increased. The aerosol concentration shall not exceed the concentration limit of
ec,ps) is calculated from Formula (16).
the O PC (s) . T he correlation u ncer tai nty (
Table 8 (continued)
1 0.3 .4 Penetration
T he p ene tration u ncer tai nty sh a l l fa l l with i n the l i m its shown i n Table 9.
The minimum number of counts from Formula (30) for each particle size shall be greater than or equal
to 5 0 0 . I f a s u fficient nu mb er o f cou nts i s no t ob ta i ne d, the s a mple ti me or aero s ol concentration s ha l l
be increased. The aerosol concentration shall not exceed the concentration limit of the OPC(s).
T he p ene tration uncer ta i nty ( eps) is calculated from Formula (27) and shall be less than or equal to the
gre ater o f the s tatic l i m it or the dyna m ic l i m it shown f Table 9.
or th at p a r ticle s i z e i n
I f the p ene tration uncer ta i nty ca n no t me e t th i s data re qui rement, the p ene tration upp er con fidence
T he frac tiona l e ffic ienc y i s de term i ne d by one o f the fol lowi ng formu lae .
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I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
For all particle sizes that meet all o f the data quality requirements, the fractional e fficiency for the
particle size(s) is determined by:
E ps = (1 − Pps ) × 100 (33)
where
Eps is the fractional e fficiency particle size, ps, %;
Pps is the penetration for particle size, ps.
For any particle sizes that cannot meet all o f the data quality requirements, the fractional e fficiency for
the particle size(s) that cannot meet the data quality requirement is determined by:
E ps =( −P1
ucl, ps ) × 1 00 (34)
where
Eps is the fractional e fficiency particle size, ps, %;
P is the upper confidence limit o f the penetration for particle size, ps.
ucl, ps
1 1 Reporting results
1 1 .1 General
Test results shall be reported using the test report format shown in this part of ISO 16890. Figure 11
and Figure 12 comprise the complete test report, and are examples of acceptable forms. Use of this
exact format is not required, but the report shall include all of the items shown in 11.2.
1 1 .2 Required reporting elements
1 1 .2 .1 Report general
Every test report shall include the in formation listed in 11.2 . Any report not containing all required
elements shall be considered invalid.
1 1 .2 .2 Report values
All data values for particle removal e fficiency shall be reported as whole number values only (no
decimal or fractions).
Data values for resistance to airflow shall be reported as whole number values only (no decimal or
fractions) when displayed in SI units (Pa) or to 2 decimal places in IP units (in H 2 O).
1 1 .2 .3 Report summary
The one-page summary section o f the per formance report (see Figure 11) shall include the following
information:
a) laboratory in formation:
1) laboratory name;
2) laboratory location and contact in formation;
1) manufac turer’s name (or name of the marketing organiz ation, if different from the
manu facturer);
2) brand and model number as marked on the test device;
3) tes t device condition (e. g. clean, conditioned as p er I SO 16 8 9 0 - 4, lo aded as p er I SO 16 8 9 0 -3 ,
used, etc.);
4) dimensions (height, width, and depth);
5) physical description o f construction (e.g. pocket filter, number o f pockets; pleated panel,
number and depth o f pleats);
6) media descrip tion including:
i) type o f media with description and identification (e.g. glass fibre AB12, inorganic fibre
12AB);
ii) media colour;
iii) e ffective filter area;
iv) type and amount o f any additive to the media. I f this in formation is unknown, it shall be
shown as “Not Available”;
v) electrostatic charge. I f this in formation is unknown, it shall be shown as “Not Available”.
7) a photo o f the actual test device is highly recommended, but not required;
8) any other pertinent descriptive attributes.
d) test device literature data or operating data as stated by the manu facturer:
1) test device initial resistance to airflow at the test airflow rate;
2) rated final resistance to airflow at the test airflow rate;
3) initial particle removal e fficiency;
46
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
e) test conditions:
1) te s t ai r flow rate;
1 1 .2 .4 Report details
The report details shall include, but are not limited to the following information:
a) Measured results
1) T he re s i s tance to ai r flow data at e ach o f the re qu i re d ai r flow rate s s ha l l b e rep or te d i n table
b) Concluding statement
1) T he re s u lts o f th i s te s t relate on ly to the te s t device in the cond ition s tate d herei n . T he
48
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
Annex A
(informative)
Example
I n th i s exa mple te s t d ata, dua l OPC s were u s e d to te s t the fi lter element. P rior to the tes t device
i n s ta l lation, a correl ation ratio wa s de term i ne d by fol lowi ng the e ffic ienc y pro ce dure s with no te s t
device installed. The aerosol sampling followed the procedures for dual OPC testing. Each particle count
was a 3 0 s s a mple ti me . T he i n iti a l ( b e fore correlation te s ti ng) a nd fi na l (a fter correlation te s ti ng)
backgrounds counts are shown in Table A.1 with the particle counter channel sizes.
The KCl aerosol generator was turned on and allowed to stabilize for the proper time as per the test rig
Table A.2, Table A.3 and Table A.4.
qua l i fic ation pro ce du re s . T he correl ation ratio data a re s hown i n
50
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
10 0 % and 1 2 5 % o f the te s t a i r flow rate . T he d ata are s hown i n the te s t rep or t i n Figure A.1 and
Figure A.2 f f
. Nex t, the dua l OPC te s t s e quence wa s ol lowe d or the e ffic ienc y counts . T he b ackgrou nd
counts with the aerosol generator turned off are shown in Table A.5.
The KCl aerosol generator was turned on and allowed to stabilize for the proper time as per the test rig
Table A.6, Table A.7, and Table A.8.
qua l i fic ation pro ce du re s . T he e fficienc y cou nt d ata are s hown i n
52
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
µm P
δ e e ps ≤ 0 , 0 5 Limit Pass/fail
1 0,35 0,340 0,010 0,013 Pass 0,024 Pass 66
2 0,47 0,278 0,005 0,006 Pass 0,019 Pass 72
3 0,62 0,219 0,006 0,007 Pass 0,015 Pass 78
4 0,84 0,141 0,006 0,007 Pass 0,010 Pass 86
5 1,14 0,080 0,003 0,003 Pass 0,006 Pass 92
µm P
δ e e ps ≤ 0,05 Limit Pass/fail
54
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
Test ID: Unique Test Number Date of test: 4 July 201x Operator: Bill Filtergeek
Particle Counter Information Airflow measurement: Test sample obtained:
Manufacturer: Model: Coincidence Value
ABC 1234 (p/m 3): 71M XYX 23 Open Market
D E VI CE TE STE D
Test air flow rate (m 3/s): Test air temperature (ºC): Test air RH (%): Test aerosol: Loading dust or
0,944 23 47 KCl Conditioning method:
N/A
R E SU LTS
56
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
Annex B
(informative)
Resistance to air flow calculation
All pressure losses measured during the test should be corrected to a re ference air density o f 1,20
(1,198 7) kg/m3 (0,075 lb/ft3 ) which corresponds to standard air conditions: temperature 20 °C (68 °F),
barometric pressure 101,325 kPa (14,7 lb/in2 ), relative humidity 50 %. However, as long as the air
density is between 1,16 kg/m3 (0,072 lb/ft3 ) and 1,24 kg/m 3 (0,077 lb/ft3 ), no corrections need to be
made. All calculations are expressed in SI units only.
The pressure loss of a test device can be expressed as:
∆ p = c( q v ) n (B.1)
c = k × µ 2 − n × ρ n −1 (B.2)
where
Δ p is the pressure loss, Pa;
k is a constant;
qv is the air flow rate, m 3/s;
μ is the dynamic viscosity o f air, Pa.s;
n is an exponent;
ρ is the air density, kg/m3 .
The readings o f the air flow measuring system shall be convened to the volumetric air flow rate at the
conditions prevailing at the inlet o f the test device. With these air flow rate values and the measured
pressure losses, the exponent “n ” from Formula (B.1) could be determined by using at least a square
technique.
With a known value of exponent “n ”, the measured pressure losses can be corrected to standard air
conditions using Formula (B.3):
2 −n n −1
µ 1 20 ρ 1 20
Dp1 20 ,
= Dp
µ
,
×
ρ
,
(B.3)
where the unsubscripted quantities refer to the values at the test conditions and the subscripted
quantities to values at the standard air conditions and
ρ1,20 1,198 7 kg/m 3 ;
of temperature t (° C ) , b arome tric pre s s u re p (Pa) and relative hum id ity φ (%) c an b e ob ta i ne d by the
Formula (B.4):
p − 0, 378 pw
ρ = (B.4)
287, 06( t + 273, 15 )
where p w (Pa) i s the p ar ti a l vap our pre s s u re o f water i n ai r given b y Formu la (B . 5 ) :
pw = ϕ p ws (B.5)
100
and p ws (Pa) is the saturation vapour pressure of water in air at temperature t (° C ) ob ta i ne d from
Formula (B.6):
6 79 0, 49 8 5
p = − − × t + 2 73, 1 5 ) (B.6)
t + 2 73, 1 5
exp 5 9, 484 0 85 5, 0 2 8 0 2 ln (
ws
T he dyna mic vi s co s ity μ (Pa.s) at a temperature t (° C ) c a n b e ob tai ne d from Formula (B.7):
1, 455 ⋅ 10 −6 ( t + 273, 15 ) 0 5 ,
µ= (B.7)
1 + 110, 4 / ( t + 273, 15 )
58
I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n
ISO 1 6890-2 : 2 01 6(E)
Bibliography
[1] ISO 2854, Statistical interpretation of data — Techniques of estimation and tests relating to means
and variances
[2] ISO 12103-1, Road vehicles — Test contaminants for filter evaluation — Part 1: Arizona test dust
[3] ISO 14644-3, Cleanrooms and associated controlled environments — Part 3: Test methods
[4] EN 779, Particulate air filters for general ventilation — Determination of the filtration performance
[5] ASHRAE 52.2:2012, Method of testing general ventilation air-cleaning devices for removal efficiency
by particle size
[6] Ginestet, A.,Pugnet, D. , The fractional efficiency of air filters used in general ventilation, Journal of
Aerosol Science, Vol 28, Supplement 1, September 1997 Pages S293-S294
[7] N o JACA 37, Guideline of Substitute Materials for DOP
[8] JIS Z 8901, Test powders and test particles
[9] Hanley, James T. and Lawless, Phil A., Particle Counter Specifications for use with Filter
Performance Test Standard ANSI/ASHRAE/Standard 52.2, ASHRAE 1287-RP, June 15, 2010
[10] EU Council Directive 1999/30/EC of 22 April 1999
[11] ASTM D1193, Standard Specification for Reagent Water
ICS 91 .1 40.3 0
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I n tern ati o n al Org an i z ati o n fo r S tan d ard i z ati o n