IGUACU VIETNAM CO., LTD.

REPORT SAMPLE RESULT

Sample Name: INSTANT COFFEE - RECOVERY VALIDATION

SKU: VT-11 PROSOL (068.22 HIGH DENSITY) BB 310 KG

S/N LOT: 001522305170003

Equipment name Shimadzu Sample Type Sample

Instrument Name LC-2050 Method Name Ochratoxin A (OTA)
Part No: Waters PSS831915 Name of STD: Ochratoxin A
Serial No: 01973129414072
Analysis: NGUYEN DUC TRUNG
Date acquired: 24/08/2023

ASSAY QUANTITY
<< Detector B >>
ID#1 Compound Name: OTA
Sample Name Sample Peak Area Dilution Factor Assay(ppb)
OTA RECOVERY-LEVEL 1.lcd 236900 1.000000 1.02
OTA RECOVERY-LEVEL 2 REP.lcd 533681 1.000000 2.32
OTA RECOVERY-LEVEL 3 REP.lcd 1058318 1.000000 4.63

Retention Time
8.356
8.359
8.362

Calibration Curve

ID# :1
Name : OTA
Quantitative Method : External Standard
Function : f(x)=227414*x+5827.60
Rr1=0.9999831 Rr2=0.9999662(8.430534e+007!=--)
FitType : Linear

Area # Concentration (ppb) Area

1 0.205 53685
[*10^6] 2 0.522 119827
2.0 6
3 1.043 249960
4 2.087 478328
1.6 5 4.174 952502
6 8.348 1905486
1.2
5
0.8
4
0.4 3
1 2
0.0
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0
Conc. [*10^0]

Conclusion

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Pass Not Pass Signature:

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 Chromatogram
OTA RECOVERY-LEVEL 1.lcd
uV
50000

8.356 / 236900 / OTA

1 Detector B Ex:333nm,Em:477nm

40000

Chromatogram
30000

20000

0.0 2.5 5.0 7.5 10.0 12.5 15.0

min

Chromatogram
OTA RECOVERY-LEVEL 2 REP.lcd
uV
75000

8.359 / 533681 / OTA

1 Detector B Ex:333nm,Em:477nm

50000

25000

0.0 2.5 5.0 7.5 10.0 12.5 15.0

min

Chromatogram
OTA RECOVERY-LEVEL 3 REP.lcd
uV
8.362 / 1058318 / OTA

1 Detector B Ex:333nm,Em:477nm

100000

50000

0.0 2.5 5.0 7.5 10.0 12.5 15.0

min

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