<Sample Information>

Sample Name
Sample ID
mix
MIX; Met 100%
Data Filename KA2 3.lcd
Method Filename : Workshop PT .Icm
Batch Filename
Vial # 1-1 Sample Type : Unknown
Injection Volume: 20 uL
Date Acquired 11/29/2021 12:17:16 PM Acquired by
Date Processed :11/29/2021 2:34:39 PM Processed by
System Administrato
:SystemAdministrator

<Chromatogram>
mAU

PDA Multi 1 254nm,4nm

50

25

0.0 2.5 5.0 7.5

min

mAU

PDA Multi 2 271nm,4nm

150

100

50

0.0 2.5 5.0 7.5

min
mAU

PDA Multi 3
-
278nm 4nm

150

100

50

0.0
2.5 5.0 7.5
min
<Peak Table>
PDA Ch1 254nm
Peak# Ret. Time Area Height Conc. Unit Mark Name
1.725 4765 273 0.646
2.096 721759 70308 97.873
2.731 10922 886 1.481
*

Total 737446 71467

PDA Ch2 271nmn
Peak# Ret. Timne Area Height Conc. Unit Mark Name
1.696 3497 277 0.192
2.091 1817950 179839 99.620 V
2.743 3435 250 0.188
Total 1824882 180366

PDA Ch3 278nm

Peak# Ret. Time Area Height Conc Unit Mark Name
1.693 3341 262 0.177
2.089 1881842 187364 99.684 SV
2.781 1109 117 0.059 T
4 3.501 1511 122 0.080
Total 1887803 187865
 SHIMADZU

LabSolutions Analysis Report

<Sample Information>
Sample Name Mix
Sample ID Mix Met OH60%
Data Filename KA2 7 Icd
Method Filename : Workshop PT Icm
Batch Filename
Vial # 1-1 Sample Type Unknown
Injection Volume 20 uL
System Administrator
Date Acquired 11/29/2021 2:11:12 PM Acquired by System Administrator
Date Processed 11/29/2021 2:36:56 PM Processed by

<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
20

15

10

0.0 2.5 5.0 7.5

min

mAU

PDA Multi 2 271nm,4nm

25

0.0 2.5 5.0 7.5

min
 mAU
PDA Multi 3 278nm, 4nm
75

50

25

0.0 25 5.0 7.5

min
<Peak Table>
PDA Ch1 254nm
Peak# Ret. Time Area
1
Height Conc Unit Mark Name
2.033 8779 874 1.309
2 2.301 264329 15625 39 400 V
3 2.789 397782 20608 59 292
Total 670890 37107

PDA Ch2 271nm

Peak# Ret. Time Area Height Conc Unit Mark Name
1 2.027 7430 797 0425
2 2.301 496419 29715 28 420 V
3 2.789 1242906 64750 71.155
Total 1746755 95262

PDA Ch3 278nm

Peak# Ret. Time Area Height Conc Unit Mark Name
2.027 7049 756 0.374
2 2.302 414051 24889 21.969 V
3 2.789 1463588 76294 77.657 V
Total 1884688 101940
 SHIMADZU
LabSolutions Analysis Report
<Sample lInformation>
Sample Name
Sample ID
mix
mix Met OH50%
Data Filename KA2 11.lcd
Method Filename Workshop PT.Icmn
Batch Filename
Vial # 1-1 Sample Type Unknown
Injection Volume 20 uL
Date Acquired 11/29/2021 3:54:23 PM Acquired by System Administrator
Date Processed :11/29/2021 4:04:26 PM Processed by System Administrator

<Chromatogram>
mAU

PDA Multi 1 271nm,4nm

50-

40

30 L
N

20

10

0.0 2.5 5.0 7.5

min

mAU

PDAMulti2 278nm,4nm

50

25

0.0 2.5 5.0 7.5

min

Peak Table>
PDA Ch1 271nm
Peak# Ret. Time Area Height Conc Unit Mark
1.991
2.536
2209
502012
213
25459
0.129
29.256
V Name
3.581 1211738 52343 70.616
Total 1715959 78015
PDA Ch2 278nm
Peak# Ret. Time Area Height Conc. Unit Mark
1.991 1951 195 Name
2.535 422532
0.105 V
3.581 21374 22.778B
Total
1430514 61747 77.117
1854997 83316
 SHIMADZU

LabSolutions Analysis Report

<Sample Information>
Sample Name : Mix
Sample ID Mix Air100%
Data Filename KA2 15.lcd
Method Filename Workshop PT.lcm
Batch Fitename
Vial # 1-1
Injection Volume :20 uL Sample Type :Unknown
Date Acquired :11/29/2021 5:23:46 PM
Date Processed 11/29/2021 5:33:49 PM Acquired by System Administrator
Processed by System Administrator

<Chromatogram>
mAU

PDA Multi 1 278nm,4nm

7.5

5.0

2.5

0.0

0.0 2.5 5.0 7.5

min

mAU

PDA Multi 2 271nm,4nm

7.5

5.0

2.5

0.0

0.0 2.5 5.0 7.5

min

<Peak Table>
PDA Ch1 278nm
 11/29/2021 5:36:59 PM Pag

Peak# Ret. Time Area Height Conc. UnitMark Name

2.244 18687 8723 100.000O
Total 18687 8723
PDA Ch2 271nm
Peak# Ret. Time Area Height Conc. Unit Mark Name
2.244 18564 8704 100.000
Total 18564 8704