HPCL-MITTAL ENERGY LIMITED

DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC1-5001 LT. Kerosene 19/09/2023 6:00 Doctor Test IS 1448:P 19 Negative
501-SC1-5201 Hot HGO 19/09/2023 6:00 Initial Boling Point ASTM D 86 °C 202.4
Temperature at 5% Volume ASTM D 86 °C 269.6
Recovery
Temperature at 10% Volume ASTM D 86 °C 291.7
Recovery
Temperature at 30% Volume ASTM D 86 °C 326.6
Recovery
Temperature at 50% Volume ASTM D 86 °C 346.7
Recovery
Temperature at 70% Volume ASTM D 86 °C 362.7
Recovery
Temperature at 90% Volume ASTM D 86 °C 381.3
Recovery
Temperature at 95% Volume ASTM D 86 °C 388.7
Recovery
Final Boiling Point ASTM D 86 °C 392.0
501-SC2-059 HVGO 19/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m³ 940.4
Temperature at 5% Mass Recovery ASTM D 6352 °C 393.0
Temperature at 10% Mass Recovery ASTM D 6352 °C 414.0
Temperature at 20% Mass Recovery ASTM D 6352 °C 41.0
Temperature at 30% Mass Recovery ASTM D 6352 °C 61.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 478.0
Temperature at 50% Mass Recovery ASTM D 6352 °C 493.0
Temperature at 60% Mass Recovery ASTM D 6352 °C 508.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 522.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 537.0

Page 1 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-059 HVGO 19/09/2023 6:00 Temperature at 90% Mass Recovery ASTM D 6352 °C 556.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 569.0
Temperature at Max. Recovery ASTM D 6352 °C 598.0
501-SC2-060 VGO 19/09/2023 6:00 Temperature at 5% Volume ASTM D 6352 °C 381.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 401.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 420.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 433.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 444.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 458.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 475.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 489.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 506.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 527.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 542.0
Recovery
Temperature at 5% Mass Recovery ASTM D 6352 °C 362.0
Temperature at 10% Mass Recovery ASTM D 6352 °C 382.0
Temperature at 20% Mass Recovery ASTM D 6352 °C 408.0
Temperature at 30% Mass Recovery ASTM D 6352 °C 425.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 442.0

Page 2 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-060 VGO 19/09/2023 6:00 Temperature at 50% Mass Recovery ASTM D 6352 °C 459.0
Temperature at 60% Mass Recovery ASTM D 6352 °C 475.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 492.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 511.0
Temperature at 90% Mass Recovery ASTM D 6352 °C 535.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 552.0
Temp at FBP for Vol% ASTM D 6352 °C 556.0
Temp at FBP for Mass% ASTM D 6352 °C 586.0
501-SC2-086 Vacuum diesel 19/09/2023 6:00 Initial Boling Point ASTM D 86 °C 243.1
Temperature at 5% Volume ASTM D 86 °C 272.0
Recovery
Temperature at 10% Volume ASTM D 86 °C 283.3
Recovery
Temperature at 30% Volume ASTM D 86 °C 305.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 322.3
Recovery
Temperature at 70% Volume ASTM D 86 °C 337.5
Recovery
Temperature at 90% Volume ASTM D 86 °C 355.6
Recovery
Temperature at 95% Volume ASTM D 86 °C 363.4
Recovery
Final Boiling Point ASTM D 86 °C 369.7
501-SC2-096B Crude-2nd Stage 19/09/2023 6:00 BS&W ASTM D 4007 Vol % 0.3 0.10
Desalter Outlet
Salt Content IP 77 PTB 1.3 0.79
501-SC2-5601 Vacuum Residue 19/09/2023 6:00 Temperature at 5% Mass Recovery ASTM 1160 °C 550 554.0
Equivalent

Page 3 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC2-5601 Vacuum Residue 19/09/2023 6:00 Temperature at 10% Mass Recovery ASTM 1160 °C 597.0
Equivalent
Temperature at 20% Mass Recovery ASTM 1160 °C 609.0
Equivalent
Temperature at 30% Mass Recovery ASTM 1160 °C 635.0
Equivalent
Temperature at 40% Mass Recovery ASTM 1160 °C 656.0
Equivalent
Temperature at 50% Mass Recovery ASTM 1160 °C 687.0
Equivalent
Temperature at 55% Mass Recovery ASTM 1160 °C 708.0
Equivalent
501-SC3-056 HOT Diesel to 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 854.5
DHDT
Nitrogen Content ASTM D 4629 mg/kg 185.0
Total Sulphur ASTM D 4294 Wt% 1.48
501-SC3-5301 MP steam Blow 19/09/2023 6:00 Conductivity ASTM D 1125 µS/cm 16.80
down
Phosphate APHA 4500 mg/l 6.55
P.D
pH ASTM D 1293 9.7
501-SC3-5401 LP steam Blow 19/09/2023 6:00 Conductivity ASTM D 1125 µS/cm 17.70
down
Phosphate APHA 4500 mg/l 6.96
P.D
pH ASTM D 1293 9.7
501-Hot Well Hot Well Gas 19/09/2023 10:00 Methane UOP 539 Vol % 40.39
Gas
Ethane UOP 539 Vol % 17.02
C2 UNSAT UOP 539 Vol % 1.58
Propane UOP 539 Vol % 8.95
C3 UNSAT UOP 539 Vol % 2.45
Page 4 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-Hot Well Hot Well Gas 19/09/2023 10:00 Iso Butane UOP 539 Vol % 1.03
Gas
N Butane UOP 539 Vol % 3.19
C4 Unsaturated UOP 539 Vol % 1.6
Iso Pentane UOP 539 Vol % 0.90
n-Pentane UOP 539 Vol % 0.64
C5 Unsaturated UOP 539 Vol % 0.3
C6+ heaviers UOP 539 Vol % 0.55
Carbon Dioxide UOP 539 Vol % 1.28
Oxygen UOP 539 Vol % 1.89
Nitrogen UOP 539 Vol % 12.92
Carbon Monoxide UOP 539 Vol % 2.00
Hydrogen UOP 539 Vol % 3.38
Hydrogen Sulfide UOP 539 ppm <0.5
501-SC1-5001 LT. Kerosene 19/09/2023 14:00 Copper Strip Corrosion for 3 hrs @ ASTM D 130 Rating 3a
50°C
Doctor Test IS 1448:P 19 Positive
501-SC3-084 Stabilised naphtha 19/09/2023 14:00 Initial Boling Point ASTM D 86 °C 39.1
(UnTreated to
Temperature at 5% Volume ASTM D 86 °C 55.9
NHT)
Recovery
Temperature at 10% Volume ASTM D 86 °C 60.6
Recovery
Temperature at 30% Volume ASTM D 86 °C 75.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 90.4
Recovery
Temperature at 70% Volume ASTM D 86 °C 104.7
Recovery

Page 5 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

501-CDU & VDU

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
501-SC3-084 Stabilised naphtha 19/09/2023 14:00 Temperature at 90% Volume ASTM D 86 °C 120.2
(UnTreated to Recovery
NHT) Temperature at 95% Volume ASTM D 86 °C 123 140 125.0
Recovery
Final Boiling Point ASTM D 86 °C 138.0
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 50 45.4
501-SC1-1401 Brine to ETP at 19/09/2023 22:00 Oil & Grease IS 3025:P 39 mg/l 100 47.0
B/L
pH Vendor 5.7
Method
501-SC4-2901 Reflux Drum sour 19/09/2023 22:00 Chloride IS 3025:P 32 mg/l 40 12.6
water
Iron Content ASTM D 1068 mg/kg 1.0 0.33
pH ASTM D 1293 7.5
501-V-107 Hot well Drum sour 19/09/2023 22:00 Chloride IS 3025:P 32 mg/l 5.9
water
Iron Content ASTM D 1068 mg/l 0.37
Sulphide IS 3025:P 29 mg/l 310.0
pH ASTM D 1293 6.1
# of Samples in Unit: 16
# of Analytes in Unit: 113

Page 6 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.4-8202 PSA product gas 19/09/2023 6:00 Methane UOP 539 ppm 5000 71.00
Carbon Dioxide UOP 539 ppm 5 3.0
Carbon Monoxide UOP 539 ppm 20 <0.2
Hydrogen UOP 539 Vol % 99.5 99.99
502-SC.A-1101 SR Naphtha From 19/09/2023 6:00 Bromine Number ASTM D 1159 gm/100g 0.3
Storage m
Density at 15°C ASTM D 4052 kg/m3 690 720 712.0
Initial Boling Point ASTM D 86 °C 38.2
Temperature at 5% Volume ASTM D 86 °C 60 65 54.3
Recovery
Temperature at 10% Volume ASTM D 86 °C 60.8
Recovery
Temperature at 30% Volume ASTM D 86 °C 81.4
Recovery
Temperature at 50% Volume ASTM D 86 °C 107.9
Recovery
Temperature at 70% Volume ASTM D 86 °C 130.7
Recovery
Temperature at 90% Volume ASTM D 86 °C 143.9
Recovery
Temperature at 95% Volume ASTM D 86 °C 150 160 147.5
Recovery
Final Boiling Point ASTM D 86 °C 155.7
Nitrogen Content ASTM D 4629 ppm(w) 0.2
Total Sulphur ASTM D 4239 ppm(w) 200 500 368.00
Bromine Number ASTM D 1159 gm/100g 1 0.3
m
Density at 15°C ASTM D 4052 kg/m3 690 720 712.0
Nitrogen Content ASTM D 4629 ppm(w) 1 0.2
Page 7 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.A-1101 SR Naphtha From 19/09/2023 6:00 Total Sulphur ASTM D 4239 ppm(w) 200 500 368.00
Storage
502-SC.A-1901 Hydrotreated 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 630 730 737.8
Naphtha from
Total Sulphur ASTM D 5453 ppm(w) 0.3 0.10
Storage
502-SC.B-1701 HDT Separator 19/09/2023 6:00 Ammonia IS 3025:P 34 mg/l 86.00
Boot
Chloride IS 3025:P 32 mg/l 15 35 13.0
H2S IS 3025:P 29 mg/l 90.0
Iron Content ASTM D 1068 mg/l 0.5 1.5 1.45
pH IS 3025:P 11 5.5 8.5 7.5
502-SC.B-2302 Stripper Reflux 19/09/2023 6:00 Ammonia ASTM D 1426 mg/l 711.00
Drum Boot
Chloride IS 3025:P 32 mg/l 15 40 13.5
H2S IS 3025:P 29 mg/l 1183.0
Iron Content APHA 3500 D mg/l 2 0.59
pH IS 3025:P 11 5.5 8.5 6.4
502-SC.B-2701 Light Hydrotreated 19/09/2023 6:00 Iso Butane ASTM D 5443 Wt% 0.05
Naphtha
N Butane ASTM D 5443 Wt% 3.44
Iso Pentane ASTM D 5443 Wt% 20.32
n-Pentane ASTM D 5443 Wt% 24.54
22 Dimethyl Butane ASTM D 5443 Wt% 0.24
23 Dimethyl Butane ASTM D 5443 Wt% 4.00
2 Methyl Pentane ASTM D 5443 Wt% 10.18
3 Methyl Pentane ASTM D 5443 Wt% 7.22
n-Hexane ASTM D 5443 Wt% 16.89
Methyl CycloPentane ASTM D 5443 Wt% 5.53
Benzene ASTM D 5443 Wt% 2.05
Page 8 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.B-2701 Light Hydrotreated 19/09/2023 6:00 Cyclo Hexane ASTM D 5443 Wt% 2.24
Naphtha
2-Methyl Hexane ASTM D 5443 Wt% 0.69
3-Methyl Hexane ASTM D 5443 Wt% 0.67
n-Heptane ASTM D 5443 Wt% 0.44
Methyl Cyclohexane ASTM D 5443 Wt% 0.08
Other Hydorcarbons ASTM D 5443 Wt% 1.42
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 80 95 85.5
502-SC.B-2703 Hexane Cut 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 685 695 695.8
502-SC.E-1901 Heavy 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 0.3 0.10
Hydrotreated
Naphtha
502-SC.G-2401 Splitter Inlet Feed 19/09/2023 6:00 Nitrogen Content ASTM D 4629 mg/kg 0.2 0.1
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
502-SC.H-1101 SR Naphtha From 19/09/2023 6:00 Bromine Number ASTM D 1159 gm/100g 0.3
CDU/VDU m
Density at 15°C ASTM D 4052 kg/m³ 685 710 700.1
Nitrogen Content ASTM D 4629 mg/kg 1 0.5
502-SC.K-1201 NHT Combined 19/09/2023 6:00 Bromine Number ASTM D 1159 gm/100g 10 5.2
Feed m
C 4 Iso Paraffins ASTM D 5443 Wt% 0.05
C 4 n- Paraffins ASTM D 5443 Wt% 0.71
C 4 Olefins ASTM D 5443 Wt% 0.11
Total C4 ASTM D 5443 Wt% 0.87
C 5 Naphthenes ASTM D 5443 Wt% 0.90
C 5 Iso Paraffins ASTM D 5443 Wt% 6.67
C 5 n- Paraffins ASTM D 5443 Wt% 9.18
Page 9 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.K-1201 NHT Combined 19/09/2023 6:00 C 5 Olefins ASTM D 5443 Wt% 2.12
Feed
Total C 5 ASTM D 5443 Wt% 18.87
C 6 Naphthenes ASTM D 5443 Wt% 4.90
C 6 Iso Paraffins ASTM D 5443 Wt% 8.47
C 6 n- Paraffins ASTM D 5443 Wt% 8.68
C 6 Olefins ASTM D 5443 Wt% 0.89
C 6 Aromatics ASTM D 5443 Wt% 1.06
Total C 6 ASTM D 5443 Wt% 24.03
C 7 Naphthenes ASTM D 5443 Wt% 6.92
C 7 Iso Paraffins ASTM D 5443 Wt% 7.01
C 7 n- Paraffins ASTM D 5443 Wt% 7.88
C 7 Olefins ASTM D 5443 Wt% 0.36
C 7 Aromatics ASTM D 5443 Wt% 2.22
Total C 7 ASTM D 5443 Wt% 24.39
C 8 Naphthenes ASTM D 5443 Wt% 5.73
C 8 Iso Paraffins ASTM D 5443 Wt% 7.16
C 8 n- Paraffins ASTM D 5443 Wt% 5.90
C 8 Olefins ASTM D 5443 Wt% 0.17
C 8 Aromatics ASTM D 5443 Wt% 2.83
Total C 8 ASTM D 5443 Wt% 21.79
C 9 Naphthenes ASTM D 5443 Wt% 2.40
C 9 Iso Paraffins ASTM D 5443 Wt% 4.47
C 9 n- Paraffins ASTM D 5443 Wt% 1.85
C 9 Aromatics ASTM D 5443 Wt% 0.54

Page 10 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.K-1201 NHT Combined 19/09/2023 6:00 Total C 9 ASTM D 5443 Wt% 9.26
Feed
C 10 Naphthenes ASTM D 5443 Wt% 0.20
C 10 Iso Paraffins ASTM D 5443 Wt% 0.29
C 10 n- Paraffins ASTM D 5443 Wt% 0.29
Total C 10 ASTM D 5443 Wt% 0.78
Naphthenes ASTM D 5443 Wt% 21.05
i-Paraffin ASTM D 5443 Wt% 34.12
n Paraffin ASTM D 5443 Wt% 34.49
Paraffins ASTM D 5443 Wt% 68.61
Olefines ASTM D 5443 Wt% 11 3.65
Aromatics ASTM D 5443 Wt% 6.69
Density at 15°C ASTM D 4052 kg/m³ 685 710 701.5
Initial Boling Point ASTM D 86 °C 38.0
Temperature at 5% Volume ASTM D 86 °C 53 57 55.6
Recovery
Temperature at 10% Volume ASTM D 86 °C 60.0
Recovery
Temperature at 30% Volume ASTM D 86 °C 72.3
Recovery
Temperature at 50% Volume ASTM D 86 °C 89.0
Recovery
Temperature at 70% Volume ASTM D 86 °C 106.6
Recovery
Temperature at 90% Volume ASTM D 86 °C 125.8
Recovery
Temperature at 95% Volume ASTM D 86 °C 135 145 132.3
Recovery
Final Boiling Point ASTM D 86 °C 144.6

Page 11 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC.K-1201 NHT Combined 19/09/2023 6:00 Nitrogen Content ASTM D 4629 mg/kg 1 0.5
Feed
Total Chloride ASTM D 4929 mg/kg 1 <0.3
Total Sulphur ASTM D 4294 mg/kg 300 600 321
502-SC-7201 Surface 19/09/2023 6:00 TOC APHA 5310 D ppm 0.2
Condensate
502-SC-8201 PSA feed 19/09/2023 6:00 Methane UOP 539 Vol % 4.70
Ethane UOP 539 Vol % 3.46
Propane UOP 539 Vol % 2.08
Iso Butane UOP 539 Vol % 0.39
N Butane UOP 539 Vol % 1.21
Iso Pentane UOP 539 Vol % 0.26
n-Pentane UOP 539 Vol % 0.32
C6+ heaviers UOP 539 Vol % 0.16
Carbon Dioxide UOP 539 Vol % <0.01
Oxygen UOP 539 Vol % 0.11
Nitrogen UOP 539 Vol % 1.01
Carbon Monoxide UOP 539 Vol % <0.01
Hydrogen UOP 539 Vol % 85 95 86.27
Molecular Weight UOP 539 6.27
Hydrogen Sulfide Dragger ppm 1 <0.5
502-SC-8203 PSA off gas 19/09/2023 6:00 Methane UOP 539 Vol % 22.15
Ethane UOP 539 Vol % 14.82
Propane UOP 539 Vol % 6.78
Propylene UOP 539 Vol % 0.03

Page 12 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

502-NHU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
502-SC-8203 PSA off gas 19/09/2023 6:00 Iso Butane UOP 539 Vol % 1.54
N Butane UOP 539 Vol % 4.85
Iso Pentane UOP 539 Vol % 1.07
n-Pentane UOP 539 Vol % 1.32
C6+ heaviers UOP 539 Vol % 3 0.82
Carbon Dioxide UOP 539 Vol % 0.07
Oxygen UOP 539 Vol % 0.13
Nitrogen UOP 539 Vol % 2.98
Carbon Monoxide UOP 539 Vol % 0.15
Hydrogen UOP 539 Vol % 20 50 43.29
Molecular Weight UOP 539 18.98
Hydrogen Sulfide DRAEGER Vol % 0.0010
TUBE
Total Volatile Sulphur ASTM D 3246 ppm(w) 16.0
# of Samples in Unit: 15
# of Analytes in Unit: 147

Page 13 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

503-ISOM
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
503-SC.B-1102 Fresh Feed+DIH 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 650 675 663.8
Recycle
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
503-SC.D-2104 Isomerate product 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 670 654.7
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 96.3
Research Octane Number (RON) ASTM D 2699 84 87 86.8
503-SC.K-2403 SCRUBBER 19/09/2023 6:00 % strength UOP 209 Wt% 2 2.8
CIRCULATING
CAUSTIC
503-SC.D-2104 Isomerate product 19/09/2023 14:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 89.6
503-SC.K-2403 SCRUBBER 19/09/2023 14:00 % strength UOP 209 Wt% 2 2.0
CIRCULATING
CAUSTIC
503-SC-2402 Scrubber off-gas 19/09/2023 14:00 Methane UOP 603 Vol % 0.93
Ethane UOP 603 Vol % 0.60
Propane UOP 603 Vol % 7.91
Iso Butane UOP 603 Vol % 9.58
N Butane UOP 603 Vol % 12.09
C4 Unsaturated UOP 603 Vol % 0.1
Iso Pentane UOP 603 Vol % 5.33
n-Pentane UOP 603 Vol % 0.34
Carbon Dioxide UOP 603 Vol % <0.01
Oxygen UOP 603 Vol % 0.01
Nitrogen UOP 603 Vol % 3.66
Carbon Monoxide UOP 603 Vol % <0.01
Hydrogen UOP 603 Vol % 45 65 59.42

Page 14 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

503-ISOM
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
503-SC-2402 Scrubber off-gas 19/09/2023 14:00 Hydrogen Sulfide UOP 603 ppm(v) <0.5
Molecular Weight UOP 603 22.80
503-SC.D-2104 Isomerate product 19/09/2023 22:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 95.0 97.2
503-SC.K-2403 SCRUBBER 19/09/2023 22:00 % strength UOP 209 Wt% 2 2.8
CIRCULATING
CAUSTIC
503-SC.C-2301 CAUSTIC 20/09/2023 0:00 % strength IS 252 Wt% 18.5
PREPERATION
TANK
# of Samples in Unit: 9
# of Analytes in Unit: 26

Page 15 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

504-CCR
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
504-SC.K-1101 CCR Feed 19/09/2023 6:00 Naphthenes ASTM D 6839 Wt% 19 31.23
i-Paraffin ASTM D 6839 Wt% 31.16
n Paraffin ASTM D 6839 Wt% 27.81
Paraffins ASTM D 6839 Wt% 74 58.97
Aromatics ASTM D 6839 Wt% 9 9.81
C 6 Naphthenes ASTM D 6839 Wt% 0.60
C 6 n- Paraffins ASTM D 6839 Wt% 0.01
Total C 6 ASTM D 6839 Wt% 0.61
C 7 Naphthenes ASTM D 6839 Wt% 11.95
C 7 Iso Paraffins ASTM D 6839 Wt% 8.72
C 7 n- Paraffins ASTM D 6839 Wt% 13.30
C 7 Aromatics ASTM D 6839 Wt% 3.89
Total C 7 ASTM D 6839 Wt% 37.85
C 8 Naphthenes ASTM D 6839 Wt% 12.40
C 8 Iso Paraffins ASTM D 6839 Wt% 14.73
C 8 n- Paraffins ASTM D 6839 Wt% 11.58
C 8 Aromatics ASTM D 6839 Wt% 5.24
Total C 8 ASTM D 6839 Wt% 43.94
C 9 Naphthenes ASTM D 6839 Wt% 5.13
C 9 Iso Paraffins ASTM D 6839 Wt% 7.53
C 9 n- Paraffins ASTM D 6839 Wt% 2.91
C 9 Aromatics ASTM D 6839 Wt% 0.68
Total C 9 ASTM D 6839 Wt% 16.25
C 10 Naphthenes ASTM D 6839 Wt% 1.16

Page 16 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

504-CCR
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
504-SC.K-1101 CCR Feed 19/09/2023 6:00 C 10 Iso Paraffins ASTM D 6839 Wt% 0.18
Total C 10 ASTM D 6839 Wt% 1.34
N+2A ASTM D 6839 Wt% 44 50.85
Density at 15°C ASTM D 4052 kg/m³ 730 740 737.4 @10:00hrs
Total Sulphur ASTM D 5453 ppm(w) 0.2 0.5 0.7
504-SC-2602 Reformate 19/09/2023 6:00 Benzene Content ASTM D 3606 Vol % 0.6 1.0 0.80
Density at 15°C ASTM D 4052 kg/m3 800.0 805 799.4
Initial Boling Point ASTM D 86 °C 40.0
Temperature at 5% Volume ASTM D 86 °C 89.9
Recovery
Temperature at 10% Volume ASTM D 86 °C 99.7
Recovery
Temperature at 30% Volume ASTM D 86 °C 113.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 122.2
Recovery
Temperature at 70% Volume ASTM D 86 °C 133.8
Recovery
Temperature at 90% Volume ASTM D 86 °C 151.1
Recovery
Temperature at 95% Volume ASTM D 86 °C 159.4
Recovery
Final Boiling Point ASTM D 86 °C 185.5
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 20 30 26.1
Research Octane Number (RON) ASTM D 2699 95.0
504-SC-3301 Continuous blow 19/09/2023 6:00 Chloride Vendor ppb(v) 220 <50
down drum sample Method
Iron Content ASTM D 1068 mg/l 0.37

Page 17 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

504-CCR
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
504-SC-3301 Continuous blow 19/09/2023 6:00 Phosphate APHA 4500 mg/l 1.48
down drum sample P.D
Silica ASTM D 859 mg/l 0.04
pH ASTM D 1293 9.0
504-SC-2301 Hydrogen rich gas 19/09/2023 14:00 Methane UOP 539 Vol % 3 1.87
Ethane UOP 539 Vol % 2.5 1.79
Propane UOP 539 Vol % 1.2 0.90
N Butane UOP 539 Vol % 0.14
Iso Butane UOP 539 Vol % 0.23
Iso Pentane UOP 539 Vol % 0.06
n-Pentane UOP 539 Vol % 0.02
C6+ heaviers UOP 539 Vol % 0.03
Carbon Dioxide UOP 539 Vol % <0.01
Oxygen UOP 539 Vol % 0.01
Nitrogen UOP 539 Vol % 0.87
Carbon Monoxide UOP 539 Vol % <0.01
Hydrogen UOP 539 Vol % 90 98 94.05
Molecular Weight UOP 539 Wt% 5 3.69
Hydrogen Sulfide UOP 163 ppm(v) 0.20 <0.5
504-SC-2602 Reformate 19/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 0.6 1.0 0.86
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 20 30 21.8
504-SC.K-1101 CCR Feed 19/09/2023 18:00 Total Sulphur ASTM D 5453 ppm(w) 0.2 0.5 0.1
504-SC-2602 Reformate 19/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 0.6 1.0 0.88

Page 18 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

504-CCR
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 7
# of Analytes in Unit: 66

Page 19 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

505-CCR Regeneration
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
505-SC-1103 Caustic Recycle 19/09/2023 6:00 % strength UOP 209 % 0.2 1.0 0.7 10:00
Solution
505-SC-2101 Spent Catalyst 19/09/2023 6:00 Carbon Content UOP 703 Wt% 4 6 3.40
Chloride IS 3025:P 32 Wt% 0.9 1.0 0.85
505-SC-2301 Regenerated 19/09/2023 6:00 Carbon Content UOP 703 Wt% 1 <0.05
Catalyst
Chloride IS 3025:P 32 Wt% 1.0 1.1 1.03
# of Samples in Unit: 3
# of Analytes in Unit: 5

Page 20 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

506-HRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
506-SC.3-1901 Stripped Naphtha 19/09/2023 2:00 Initial Boling Point ASTM D 1078 °C 64.1
(C-03 bottom)
Dry Point ASTM D 1078 °C 0.1 67.4
Recovery up to 70°C (E70) ASTM D 1078 Vol % 95.6
Total Sulphur ASTM D 5453 mg/kg 0.2 0.10
506-SC.1-2305 Hexane(FG) 19/09/2023 6:00 Benzene Content ASTM D 6229 ppm(v) 20 <1.0
Density at 20°C ASTM D 4052 gm/cc 0.660 0.687 0.6682
Initial Boling Point ASTM D 1078 °C 63 64.3
Dry Point ASTM D 1078 °C 69.0
Distillation between 64 to 70°C ASTM D 1078 Vol % 95 97.9
Total Sulphur ASTM D 5453 mg/kg 0.5 0.1
506-SC.1-2305 Hexane(FG) 19/09/2023 10:00 Benzene Content ASTM D 6229 ppm(v) 20 <1.0
Density at 20°C ASTM D 4052 gm/cc 0.660 0.687 0.6660
Initial Boling Point ASTM D 1078 °C 63 63.8
Distillation between 64 to 70°C ASTM D 1078 Vol % 95 97.5
Dry Point ASTM D 1078 °C 68.4
506-SC.1-2305 Hexane(FG) 19/09/2023 14:00 Benzene Content ASTM D 6229 ppm(v) 20 <1.0
Density at 20°C ASTM D 4052 gm/cc 0.660 0.687 0.6670
Initial Boling Point ASTM D 1078 °C 63 63.8
Dry Point ASTM D 1078 °C 68.6
Distillation between 64 to 70°C ASTM D 1078 Vol % 95 96.0
Total Sulphur ASTM D 5453 mg/kg 0.5 0.1
506-SC.1-2305 Hexane(FG) 19/09/2023 22:00 Benzene Content ASTM D 6229 ppm(v) 20 <1
Density at 20°C ASTM D 4052 gm/cc 0.660 0.687 0.6684
Initial Boling Point ASTM D 1078 °C 63 64.5

Page 21 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

506-HRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
506-SC.1-2305 Hexane(FG) 19/09/2023 22:00 Dry Point ASTM D 1078 °C 69.3
Distillation between 64 to 70°C ASTM D 1078 Vol % 95 97.4
Total Sulphur ASTM D 5453 mg/kg 0.5 0.1
# of Samples in Unit: 5
# of Analytes in Unit: 27

Page 22 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
507-SC-C-3803 Diesel Product 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 820 860 829.7
Total Sulphur ASTM D 5453 mg/kg 5 10 5.00
507-SC-C-4002 Kerosene Product 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 775 840 792.9
Flash Point, Abel IP 170 °C 45 42.0
Total Sulphur ASTM D 5453 mg/kg 10 0.50
507-SC-G-8401 DHDT Light 19/09/2023 6:00 Doctor Test ASTM D 4952 Negative
Naphtha
507-SC-H-1201 Feed TO DHDT 19/09/2023 6:00 Bromine Number ASTM D 1159 gm/100g 11.7 10.2
m
Density at 15°C ASTM D 4052 kg/m³ 850 840.2
Initial Boling Point ASTM D 86 °C 65.6
Temperature at 5% Volume ASTM D 86 °C 136.7
Recovery
Temperature at 10% Volume ASTM D 86 °C 175.1
Recovery
Temperature at 30% Volume ASTM D 86 °C 238.5
Recovery
Temperature at 50% Volume ASTM D 86 °C 274.4
Recovery
Temperature at 70% Volume ASTM D 86 °C 307.5
Recovery
Temperature at 90% Volume ASTM D 86 °C 346.9
Recovery
Temperature at 95% Volume ASTM D 86 °C 361 364.0
Recovery
Final Boiling Point ASTM D 86 °C 374.0
Nitrogen Content ASTM D 4629 mg/kg 400 268.0
Cetane Index ASTM D 4737 10 46.7 47.8

Page 23 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

507-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
507-SC-C-3803 Diesel Product 19/09/2023 14:00 Total Sulphur ASTM D 5453 mg/kg 5 10 5.00
507-SC-C-3803 Diesel Product 19/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 5 10 5.50

# of Samples in Unit: 6
# of Analytes in Unit: 21

Page 24 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

508-DCU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
508-SC-2-1902 Hot HCGO 19/09/2023 11:00 Density at 15°C ASTM D 1298 kg/m³ 967.7
Temperature at 5% Volume ASTM D 6352 °C 355 347.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 367.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 392.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 408.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 421.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 431.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 455.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 464.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 481.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 502.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 522.0
Recovery
Temp at FBP for Vol% ASTM D 6352 °C 539.0
Temperature at 5% Mass Recovery ASTM D 6352 °C 325.0
Temperature at 10% Mass Recovery ASTM D 6352 °C 348.0
Temperature at 20% Mass Recovery ASTM D 6352 °C 377.0
Temperature at 30% Mass Recovery ASTM D 6352 °C 397.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 416.0
Temperature at 50% Mass Recovery ASTM D 6352 °C 430.0

Page 25 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

508-DCU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
508-SC-2-1902 Hot HCGO 19/09/2023 11:00 Temperature at 60% Mass Recovery ASTM D 6352 °C 450.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 467.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 486.0
Temperature at 90% Mass Recovery ASTM D 6352 °C 511.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 533.0
Temp at FBP for Mass% ASTM D 6352 °C 592.0
Micro Carbon Residue ASTM D 4530 Wt% 1.0 0.98
508-SC-3-3601 Hot LCGO 19/09/2023 11:00 Density at 15°C ASTM D 4052 kg/m³ 872.7
Initial Boling Point ASTM D 86 °C 200.7
Temperature at 5% Volume ASTM D 86 °C 217.0
Recovery
Temperature at 10% Volume ASTM D 86 °C 224.2
Recovery
Temperature at 30% Volume ASTM D 86 °C 250.5
Recovery
Temperature at 50% Volume ASTM D 86 °C 280.2
Recovery
Temperature at 70% Volume ASTM D 86 °C 309.4
Recovery
Temperature at 90% Volume ASTM D 86 °C 347.6
Recovery
Temperature at 95% Volume ASTM D 86 °C 350 370 367.8
Recovery
Final Boiling Point ASTM D 86 °C 380.8
Flash Point, PMCC ASTM D 93 °C 84.0
Total Sulphur ASTM D 4294 Mass% 2.500
# of Samples in Unit: 2
# of Analytes in Unit: 38
Page 26 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-B-4102 VGO Naphtha 19/09/2023 6:00 Total Sulphur ASTM D 5453 mg/kg 20 5.5
Product
Doctor Test ASTM D 4952 Negative
509-SC-D-2101 Recycle Gas 19/09/2023 6:00 Hydrogen UOP 539 Vol % 88.61
Methane UOP 539 Vol % 6.96
Ethane UOP 539 Vol % 2.23
Propane UOP 539 Vol % 1.27
Hydrogen Sulfide UOP 539 Vol % 0.0050
N Butane UOP 539 Vol % 0.46
Iso Butane UOP 539 Vol % 0.11
n-Pentane UOP 539 Vol % 0.12
Iso Pentane UOP 539 Vol % 0.08
C6+ heaviers UOP 539 Vol % 0.14
Molecular Weight Default Vol % 4.74
509-SC-F-4302 HDT VGO Product 19/09/2023 6:00 Density at 15°C ASTM D 1298 kg/m3 894.5
Temperature at 5% Volume ASTM D 6352 °C 363.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 387.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 402.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 419.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 427.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 439.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 459.0
Recovery
Page 27 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-F-4302 HDT VGO Product 19/09/2023 6:00 Temperature at 70% Volume ASTM D 6352 °C 472.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 489.0
Recovery
Temperature at 90% Volume ASTM D 6352 °C 510.0
Recovery
Temperature at 95% Volume ASTM D 6352 °C 529.0
Recovery
Temperature at Max. Recovery ASTM D 6352 °C 547.0
Total Sulphur ASTM D 4294 mg/kg 230 172
509-SC-G-4401 Sweet Gas 19/09/2023 6:00 H2S DRAEGER Vol % 0.0010 0.0014
Sample TUBE
509-SC-B-4102 VGO Naphtha 19/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 770.0 734.1
Product
Initial Boling Point ASTM D 86 °C 33.8
Temperature at 5% Volume ASTM D 86 °C 54.9
Recovery
Temperature at 10% Volume ASTM D 86 °C 63.5
Recovery
Temperature at 30% Volume ASTM D 86 °C 89.7
Recovery
Temperature at 50% Volume ASTM D 86 °C 108.7
Recovery
Temperature at 70% Volume ASTM D 86 °C 128.4
Recovery
Temperature at 90% Volume ASTM D 86 °C 167.8
Recovery
Temperature at 95% Volume ASTM D 86 °C 188.8
Recovery
Final Boiling Point ASTM D 86 °C 202.0
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 50 52.0

Page 28 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-B-4102 VGO Naphtha 19/09/2023 14:00 Total Sulphur ASTM D 5453 mg/kg 20 5.0
Product
Doctor Test ASTM D 4952 Negative
509-SC-E-3603 Diesel Product 19/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 880.0 874.1
Initial Boling Point ASTM D 86 °C 166.7
Temperature at 5% Volume ASTM D 86 °C 182.2
Recovery
Temperature at 10% Volume ASTM D 86 °C 203.4
Recovery
Temperature at 30% Volume ASTM D 86 °C 256.2
Recovery
Temperature at 50% Volume ASTM D 86 °C 285.8
Recovery
Temperature at 70% Volume ASTM D 86 °C 309.1
Recovery
Temperature at 90% Volume ASTM D 86 °C 333.1
Recovery
Temperature at 95% Volume ASTM D 86 °C 378 344.3
Recovery
Final Boiling Point ASTM D 86 °C 348.6
Total Sulphur ASTM D 5453 mg/kg 50 30.0
509-SC-F-4302 HDT VGO Product 19/09/2023 14:00 Asphaltenes (Heptane Insoluble) IFP 9313 mg/kg 216.00
Nitrogen Content ASTM D 4629 mg/kg 293.0
Total Sulphur ASTM D 4294 mg/kg 230 192
509-SC-G-4401 Sweet Gas 19/09/2023 14:00 H2S DRAEGER Vol % 0.0010 0.0016
Sample TUBE
509-SC-J-1201 Total Feed 19/09/2023 14:00 Asphaltenes (Heptane Insoluble) IFP 9313 mg/kg 500 434
DownStream of
Density at 15°C ASTM D 1298 kg/m³ 952.4 942.3
Filter
Temperature at 5% Mass Recovery ASTM D 6352 °C 330.0

Page 29 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-J-1201 Total Feed 19/09/2023 14:00 Temperature at 10% Mass Recovery ASTM D 6352 °C 369.0
DownStream of
Temperature at 20% Mass Recovery ASTM D 6352 °C 403.0
Filter
Temperature at 30% Mass Recovery ASTM D 6352 °C 423.0
Temperature at 40% Mass Recovery ASTM D 6352 °C 442.0
Temperature at 50% Mass Recovery ASTM D 6352 °C 460.0
Temperature at 60% Mass Recovery ASTM D 6352 °C 476.0
Temperature at 70% Mass Recovery ASTM D 6352 °C 494.0
Temperature at 80% Mass Recovery ASTM D 6352 °C 513.0
Temperature at 90% Mass Recovery ASTM D 6352 °C 537.0
Temperature at 95% Mass Recovery ASTM D 6352 °C 554.0
Temp at FBP for Mass% ASTM D 6352 °C 600 590.0
Temperature at 5% Volume ASTM D 6352 °C 368.0
Recovery
Temperature at 10% Volume ASTM D 6352 °C 398.0
Recovery
Temperature at 20% Volume ASTM D 6352 °C 419.0
Recovery
Temperature at 30% Volume ASTM D 6352 °C 434.0
Recovery
Temperature at 40% Volume ASTM D 6352 °C 448.0
Recovery
Temperature at 50% Volume ASTM D 6352 °C 462.0
Recovery
Temperature at 60% Volume ASTM D 6352 °C 477.0
Recovery
Temperature at 80% Volume ASTM D 6352 °C 491.0
Recovery
Temperature at 70% Volume ASTM D 6352 °C 509.0
Recovery
Page 30 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-J-1201 Total Feed 19/09/2023 14:00 Temperature at 90% Volume ASTM D 6352 °C 529.0
DownStream of Recovery
Filter Temperature at 95% Volume ASTM D 6352 °C 545.0
Recovery
Temp at FBP for Vol% ASTM D 6352 °C 565 559.0
Micro Carbon Residue ASTM D 4530 Wt% 0.85 0.55
Nitrogen Content ASTM D 4629 mg/kg 1824 1293
Total Sulphur ASTM D 4294 Mass% 3.5 2.920
509-SC-3-7001 Condensate from 19/09/2023 22:00 Chloride IS 3025:P 32 ppm 3 0.9
Condensate Drum
Iron Content ASTM D 1068 ppm 0.2 0.09
pH IS 3025:P 11 9 8.90
509-SC-B-2202 Cold LP Separator 19/09/2023 22:00 Ammonia IS 3025:P 34 mg/l 8787.00
Sour Water
Chloride IS 3025:P 32 mg/l 50 15
H2S IS 3025:P 29 Wt% 10897.0
Iron Content ASTM D 1068 mg/l 1.0 1.21
pH IS 3025:P 11 9.0 8.50
509-SC-B-2903 Stripper Reflux 19/09/2023 22:00 Ammonia IS 3025:P 34 mg/l 9115.0
Drum Sour Water
Chloride IS 3025:P 32 mg/l 20 8
Iron Content ASTM D 1068 mg/l 0.9 0.97
Sulphide IS 3025:P 29 mg/l 16669.0
pH IS 3025:P 11 9 8.6
509-SC-B-4102 VGO Naphtha 19/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 20 6.0
Product
Doctor Test ASTM D 4952 Negative
509-SC-F-4302 HDT VGO Product 19/09/2023 22:00 Total Sulphur ASTM D 4294 mg/kg 230 204
509-SC-G-2301 Washing Water 19/09/2023 22:00 Ammonia IS 3025:P 34 mg/l 20 4.80

Page 31 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

509-VGO HDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
509-SC-G-2301 Washing Water 19/09/2023 22:00 Chloride IS 3025:P 32 mg/l 20 12
Iron Content ASTM D 1068 mg/l 0.4 0.85
TSS IS 3025:P 17 mg/l 15
pH IS 3025:P 11 8.5 8.40
509-SC-G-4401 Sweet Gas 19/09/2023 22:00 H2S DRAEGER Vol % 0.0010 0.0016
Sample TUBE
509-SC-H-3401 Sour Water 19/09/2023 22:00 Ammonia IS 3025:P 34 mg/l 5 5.10
(Fractionator
Chloride IS 3025:P 32 mg/l 5 1
Reflux Drum Boot)
Iron Content ASTM D 1068 mg/l 1 0.4
Sulphide IS 3025:P 29 mg/l 6.7
pH IS 3025:P 11 7 6.40
# of Samples in Unit: 17
# of Analytes in Unit: 112

Page 32 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-FB-8302 FCCU PP MIX 19/09/2023 6:00 Methane ASTM D 2712 ppm(v) <100
Ethane ASTM D 2712 ppm(v) 200 <200
Ethylene ASTM D 2712 ppm(v) <100
Propane ASTM D 2712 Vol % 13 11.53
Propylene ASTM D 2712 Vol % 87 88.37
Propadiene ASTM D 2712 ppm(v) 5 <5
Acetylene ASTM D 2712 ppm(v) <3
C4 Saturates ASTM D 2712 ppm(v) <200
C4 Unsaturated ASTM D 2712 ppm(v) <10
C5 Saturated ASTM D 2712 ppm(v) <200
Methyl Acetylene ASTM D 2712 ppm(v) <3
1,3 Butadiene ASTM D 2712 ppm(v) <5
C5 Unsaturated ASTM D 2712 ppm(v) <10
Moisture Content ASTM D 1142 ppm(w) 1788 17
COS ASTM D 5504 ppm(v) <0.02
Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
Methyl Mercaptan ASTM D 5504 ppm(v) <0.5
Ethyl Mercaptan ASTM D 5504 ppm(v) <0.5
510-FV-8402 FCCU FV MIX 19/09/2023 6:00 Propane ASTM D 2163 Vol % 1.04
Propylene ASTM D 2163 Vol % 0.584 0.35
Iso Butane ASTM D 2163 Vol % 18.37
N Butane ASTM D 2163 Vol % 5.66
trans-2-Butene ASTM D 2163 Vol % 16.52
Butene ASTM D 2163 Vol % 14.31

Page 33 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-FV-8402 FCCU FV MIX 19/09/2023 6:00 Iso Butylene ASTM D 2163 Vol % 30.26
cis-2-Butene ASTM D 2163 Vol % 12.20
Iso Pentane ASTM D 2163 Vol % 0.30
1,3 Butadiene ASTM D 2163 Vol % 0.38
Trance-2-Pentene ASTM D 2163 Vol % 0.55
2 Methyl 2 Butene ASTM D 2163 Vol % 0.02
1 Pentene ASTM D 2163 Vol % 0.04
C5+ heaviers ASTM D 2163 Vol % 0.91
Density at 15°C IP 432 kg/m³ 596.1
Vapour Pressure at 40°C IP 432 kPa 352
Hydrogen Sulfide ASTM D 5504 Negative
510-SC-1-8001 Circulating Caustic 19/09/2023 6:00 % strength IS 252 Wt% 5 8 6.6
Mercaptide UOP 209 ppm(w) 124.00
Sulphide IS 3025:P 29 ppm(w) 568.00
510-SC-1-9002 LCN 19/09/2023 6:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 110 107.4
Benzene Content ASTM D 3606 Vol % 4.7 3.06
510-SC-1-8001 Circulating Caustic 19/09/2023 14:00 % strength IS 252 Wt% 5 8 7.4
510-SC-1-8002 Circulating Wash 19/09/2023 14:00 Free Caustic IS 252 Wt% 0.4 0.16
Water (LPG Wash
Section)
510-SC-1-9002 LCN 19/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 4.7 3.84
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 110 97.9
510-SC-1-9101 Caustic 19/09/2023 16:00 % strength IS 252 % 5.9
510-SC-4-7301 Fuel gas 19/09/2023 16:00 Methane UOP 539 Vol % 32.02

Page 34 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-SC-4-7301 Fuel gas 19/09/2023 16:00 Ethane UOP 539 Vol % 10.30
Ethylene UOP 539 Vol % 33.90
Propane UOP 539 Vol % 0.08
Propylene UOP 539 Vol % 1.83 0.85
Iso Butane UOP 539 Vol % 0.05
N Butane UOP 539 Vol % 0.04
C4 Unsaturated UOP 539 Vol % 0.3
Iso Pentane UOP 539 Vol % 0.02
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 1.36
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 9.00
Carbon Monoxide UOP 539 Vol % 0.50
Hydrogen UOP 539 Vol % 11.50
Hydrogen Sulfide UOP 539 Vol % 0.05 0.030
Gross Calorific Value ASTM D 3588 Kcal/kg 10809.00
Net Calorific Value ASTM D 4868 Kcal/kg 9941.00
Molecular Weight Default Wt% 21.90
510-SC-1-8001 Circulating Caustic 19/09/2023 22:00 % strength IS 252 Wt% 5 8 7.0
510-SC-5401 Sour Water 19/09/2023 22:00 Ammonia IS 3025:P 34 ppm 397 361.00
Oil & Grease IS 3025:P 39 ppm 300 34
Total Iron ASTM D 1068 ppm(w) 1.1
pH IS 3025:P 11 8.4
510-SC-1-9002 LCN 20/09/2023 2:00 Benzene Content ASTM D 3606 Vol % 4.7 3.10

Page 35 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

510-FCCU PC
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
510-SC-1-9002 LCN 20/09/2023 2:00 Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 110 106.4
# of Samples in Unit: 13
# of Analytes in Unit: 71

Page 36 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-1155 Naphtha feed to 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 692 733 710.4
PDS section
Initial Boling Point ASTM D 86 °C 35.8
Temperature at 5% Volume ASTM D 86 °C 51.5
Recovery
Temperature at 10% Volume ASTM D 86 °C 56 80 57.7
Recovery
Temperature at 30% Volume ASTM D 86 °C 80.0
Recovery
Temperature at 50% Volume ASTM D 86 °C 107.4
Recovery
Temperature at 70% Volume ASTM D 86 °C 130.0
Recovery
Temperature at 90% Volume ASTM D 86 °C 143.8
Recovery
Temperature at 95% Volume ASTM D 86 °C 147.2
Recovery
Final Boiling Point ASTM D 86 °C 177 159.5
Total Chloride UOP 779 ppm(w) 2 <0.3
Total Sulphur ASTM D 5453 ppm(w) 5 500 296.00
C/H Ratio ASTM D 6839 5.78 5.4
511-SC-1754 Hydrogenated 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 709.5
naphtha to E-003
Total Sulphur ASTM D 5453 ppm(w) 132.0
A/B/C
511-SC-2255 Naphtha (liquid) to 19/09/2023 6:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.4
HDS section
511-SC-2752-Ga Feed + H2 d/s 19/09/2023 6:00 Hydrogen Sulphide DRAEGER ppm(v) <0.2
s 511-R-101 TUBE
Total Sulphur ASTM D 5504 ppm(w) <1.0
511-SC-2955 Process gas 19/09/2023 6:00
prereformed (511-
Page 37 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R-103 O/L) Methane UOP 539 Vol % 57.4 66.10
Carbon Dioxide UOP 539 Vol % 19.87 15.82
Carbon Monoxide UOP 539 Vol % 0.88 0.64
Hydrogen UOP 539 Vol % 21.85 17.44
511-SC-3355 Boiler blow-down 19/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 6.36
from steam
Phosphate APHA 4500 mg/l 2.06
drum-Train 1
P.D
Silica ASTM D 859 mg/l <0.02
pH IS 3025:P 11 9.2
511-SC-3551 Process gas I/L to 19/09/2023 6:00 Methane UOP 539 Vol % 4.26 3.55
MT shift
Carbon Dioxide UOP 539 Vol % 6.88 8.20
convertor-Train 1
Carbon Monoxide UOP 539 Vol % 21.66 17.46
Hydrogen UOP 539 Vol % 67.2 70.79
511-SC-3704 Reformer O/L to 19/09/2023 6:00 Methane UOP 539 Vol % 3.78 3.26
Heater I/L
Carbon Dioxide UOP 539 Vol % 8.79 8.42
Carbon Monoxide UOP 539 Vol % 19.7 18.09
Hydrogen UOP 539 Vol % 67.73 70.23
511-SC-4752-Ga Feed + H2 d/s 19/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.2
s 511-R-201
Total Sulphur ASTM D 5504 ppm(w) <1.0
511-SC-4758-Ga Feed+ H2 d/s 19/09/2023 6:00 Hydrogen Sulfide UOP 539 ppm(v) <0.2
s 511-R-202A
Total Sulphur ASTM D 5504 ppm(w) <1.0
511-SC-4955 Process gas 19/09/2023 6:00 Methane UOP 539 Vol % 57.82 80.86
prereformed (511-
Carbon Dioxide UOP 539 Vol % 20.8 2.55
R-203 O/L)
Carbon Monoxide UOP 539 Vol % 0.82 0.05

Page 38 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-4955 Process gas 19/09/2023 6:00 Hydrogen UOP 539 Vol % 20.56 16.54
prereformed (511-
511-SC-5355 Boiler 19/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 13.56
R-203 blow-down
O/L)
from steam
Phosphate APHA 4500 mg/l 2.67
drum-Train 2
P.D
Silica ASTM D 859 mg/l 0.04
pH IS 3025:P 11 9.3
511-SC-5551 Process gas I/L to 19/09/2023 6:00 Methane UOP 539 Vol % 4.83 4.90
MT shift
Carbon Dioxide UOP 539 Vol % 10.18 6.00
convertor-Train 2
Carbon Monoxide UOP 539 Vol % 17.8 14.64
Hydrogen UOP 539 Vol % 67.19 74.46
511-SC-5704 Reformal O/L 19/09/2023 6:00 Methane UOP 539 Vol % 3.78 3.51
Carbon Dioxide UOP 539 Vol % 8.79 8.81
Carbon Monoxide UOP 539 Vol % 19.7 21.40
Hydrogen UOP 539 Vol % 67.73 66.28
511-SC-6853 Boiler feed water 19/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 4.58
from
Silica ASTM D 859 mg/l 0.02 <0.02
Dearator-Train 1
pH IS 3025:P 11 8.3 9.3
511-SC-7853 Boiler feed water 19/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 43.00
from
Silica ASTM D 859 ppm 0.02 <0.02
Dearator-Train 2
pH IS 3025:P 11 8.3 9.6
511-SC-2255 Naphtha (liquid) to 19/09/2023 14:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.4
HDS section
511-SC-2255 Naphtha (liquid) to 19/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) 2 5 0.2
HDS section
511-SC-2752-Liq Feed + H2 d/s 19/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) <0.05
uid 511-R-101
Page 39 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

511-HGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
511-SC-2758-Ga Feed+ H2 d/s 19/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(w) <0.2
s 511-R-102A
Total Sulphur ASTM D 5504 ppm(w) <1
511-SC-2764-Liq Feed+ H2 d/s 19/09/2023 22:00 Total Sulphur ASTM D 7183 ppm(w) 0.05 <0.05
uid 511-R-102B
511-SC-3580 R-105 outlet 19/09/2023 22:00 Methane UOP 603 Vol % 3.59
Carbon Dioxide UOP 603 Vol % 19.42
Carbon Monoxide UOP 603 Vol % 1.83
Hydrogen UOP 603 Vol % 75.16
511-SC-5580 Process gas O/L of 19/09/2023 22:00 Methane UOP 539 Vol % 4.2 4.04
MT shift convertor-
Carbon Dioxide UOP 539 Vol % 22.3 15.30
2
Carbon Monoxide UOP 539 Vol % 1.9 1.80
Hydrogen UOP 539 Vol % 71.6 78.86
# of Samples in Unit: 23
# of Analytes in Unit: 74

Page 40 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-1301 PP mix 19/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5 <0.5
COS ASTM D 5504 ppm(v) <0.02 <0.02
Methyl Mercapton ASTM D 5504 ppm(v) <0.5 <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5 <0.5
Moisture Content ASTM D 1142 ppm(w) 0.60
512-SC-4-1302 PP mix 19/09/2023 6:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
COS ASTM D 5504 ppm(v) <0.02
Methyl Mercapton ASTM D 5504 ppm <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5
Moisture Content ASTM D 1142 ppm(w) 1 0.60
512-SC-4-1401 LPG product from 19/09/2023 6:00 Propane ASTM D 2163 Vol % 99.15
C3 stripper bottom
Propylene ASTM D 2163 Vol % 2 0.77
Iso Butane ASTM D 2163 Vol % 0.08
Density at 15°C IP 432 kg/m³ 507.5
512-SC-4-2202 PGP product 19/09/2023 6:00 Ammonia Dragger ppm 2.0 <2
Arsine GC-MS ppm(v) 0.03 <0.03
Methane ASTM D 2712 ppm(v) 100.0 <100
Ethane ASTM D 2712 ppm(v) 279.9 <279.9
Ethylene ASTM D 2712 ppm(v) 100.0 <100
Propane ASTM D 2712 Vol % 0.4 0.340
Propylene ASTM D 2712 Vol % 99.50 99.56
Iso Butane ASTM D 2712 ppm(v) 100 <100
N Butane ASTM D 2712 ppm(v) 100 <100
Propadiene ASTM D 2712 ppm(v) 5.0 <5

Page 41 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-2202 PGP product 19/09/2023 6:00 Acetylene ASTM D 2712 ppm(v) 4.85 <3
C4 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Iso Pentane ASTM D 2712 ppm(v) 100 <100
n-Pentane ASTM D 2712 ppm(v) 100 <100
1,3 Butadiene ASTM D 2712 ppm(v) 3.89 <3.89
Methyl Acetylene ASTM D 2712 ppm(v) 3.0 <3
C5 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Hexane + Nonene ASTM D 2712 ppm(v) 1.98 <1.98
Cyclopentadiene Vendor ppm(v) 0.05 <0.05
Method
Green Oil (C6,C9,C12) Vendor ppm(v) 20.0 <20
Method
H2S DRAEGER ppm(v) 0.50 <0.5
TUBE
Moisture Content By SHAW ppm(w) 1.0 0.4
Dew Point
Total Sulphur ASTM D 3246 ppm(w) 0.5 0.5
Carbon Dioxide ASTM D 8098 ppm(v) 1.91 <1.91
Hydrogen ASTM D 8098 ppm(v) 2.0 <2
Oxygen ASTM D 8098 ppm(v) 1.0 <1
Nitrogen ASTM D 8098 ppm(v) 100.0 <100
Carbon Monoxide ASTM D 8098 ppm(v) 0.03 <0.03
COS Default ppm(v) 0.02 <0.02
Isopropyl alcohol UOP 960 ppm(v) 0.91 <0.91
Methanol UOP 960 ppm(v) 1.0 <1
Phosphine GC-MS ppm(v) 0.03 <0.03

Page 42 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-1301 PP mix 19/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5 <0.5
COS ASTM D 5504 ppm(v) <0.02 <0.02
Methyl Mercapton ASTM D 5504 ppm(v) <0.5 <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5 <0.5
Moisture Content ASTM D 1142 ppm(w) 0.60
512-SC-4-1302 PP mix 19/09/2023 22:00 Hydrogen Sulfide ASTM D 5504 ppm(v) <0.5
COS ASTM D 5504 ppm(v) <0.02
Methyl Mercapton ASTM D 5504 ppm <0.5
Mercaptan Sulfur ASTM D 5504 ppm(v) <0.5
Moisture Content ASTM D 1142 ppm(w) 1 0.60
512-SC-4-2202 PGP product 19/09/2023 22:00 Arsine GC-MS ppm(v) 0.03 <0.03
Methane ASTM D 2712 ppm(v) 100.0 <100
Ethane ASTM D 2712 ppm(v) 279.9 <279.9
Ethylene ASTM D 2712 ppm(v) 100.0 <100
Propane ASTM D 2712 Vol % 0.4 0.400
Propylene ASTM D 2712 Vol % 99.50 99.50
Iso Butane ASTM D 2712 ppm(v) 100 <100
N Butane ASTM D 2712 ppm(v) 100 <100
Propadiene ASTM D 2712 ppm(v) 5.0 <5
Acetylene ASTM D 2712 ppm(v) 4.85 <3
C4 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
Iso Pentane ASTM D 2712 ppm(v) 100 <100
n-Pentane ASTM D 2712 ppm(v) 100 <100
1,3 Butadiene ASTM D 2712 ppm(v) 3.89 <3.89

Page 43 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

512-PRU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
512-SC-4-2202 PGP product 19/09/2023 22:00 Methyl Acetylene ASTM D 2712 ppm(v) 3.0 <3
C5 Unsaturated ASTM D 2712 ppm(v) 10.0 <10
H2S DRAEGER ppm(v) 0.50 <0.5
TUBE
Moisture Content By SHAW ppm(w) 1.0 0.4
Dew Point
COS Default ppm(v) 0.02 <0.02
Phosphine GC-MS ppm(v) 0.03 <0.03
# of Samples in Unit: 7
# of Analytes in Unit: 76

Page 44 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331A Reactor1 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 4.24
Xylene Solubility by NMR Default % 3.68
513-S-331B Reactor2 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 4.04
513-S-415 Reactor 3 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.63
R03RR PP Pellet 19/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.29
513-S-331A Reactor1 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.83
Xylene Solubility ASTM D 5492 Wt% 3.52
Xylene Solubility by NMR Default % 3.64
513-S-331B Reactor2 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.90
Xylene Solubility ASTM D 5492 Wt% 3.55
Xylene Solubility by NMR Default % 3.89
513-S-415 Reactor 3 19/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.53
Xylene Solubility ASTM D 5492 Wt% 3.38
Xylene Solubility by NMR Default % 3.51
R03RR PP Pellet 19/09/2023 4:00 Irg 1010 ASTM D 6247 ppm 380 520 360
I 168 ASTM D 6247 ppm 750 1050 550
DHT 4A ASTM D 6247 ppm 250 350 230
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.69
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 15
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
Page 45 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331A Reactor1 19/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.31
Xylene Solubility by NMR Default % 3.00
513-S-331B Reactor2 19/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.84
513-S-415 Reactor 3 19/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.41
R03RR PP Pellet 19/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.47
513-S-331A Reactor1 19/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.472
Aluminium Content ASTM D 6247 ppm 60.0
Magnesium Content ASTM D 6247 ppm 13.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 26.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 2.94
Retention on 10 mesh ASTM D 1921 Wt% 1.00
Retention on 18 mesh ASTM D 1921 Wt% 1.30
Retention on 35 mesh ASTM D 1921 Wt% 22.20
Retention on 60 mesh ASTM D 1921 Wt% 61.20
Retention on 120 mesh ASTM D 1921 Wt% 10.00
Retention on 230 mesh ASTM D 1921 Wt% 4.00
Retention on Pan ASTM D 1921 Wt% 0.30
APS ASTM D 1921 µ 458
Xylene Solubility ASTM D 5492 Wt% 3.07
Xylene Solubility by NMR Default % 3.09
513-S-331B Reactor2 19/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.468
Aluminium Content ASTM D 6247 ppm 60.0
Page 46 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331B Reactor2 19/09/2023 8:00 Magnesium Content ASTM D 6247 ppm 14.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 29.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 3.79
Retention on 10 mesh ASTM D 1921 Wt% 0.40
Retention on 18 mesh ASTM D 1921 Wt% 0.70
Retention on 35 mesh ASTM D 1921 Wt% 20.20
Retention on 60 mesh ASTM D 1921 Wt% 63.80
Retention on 120 mesh ASTM D 1921 Wt% 12.00
Retention on 230 mesh ASTM D 1921 Wt% 2.60
Retention on Pan ASTM D 1921 Wt% 0.30
APS ASTM D 1921 µ 434
Xylene Solubility ASTM D 5492 Wt% 3.62
Xylene Solubility by NMR Default % 3.70
513-S-415 Reactor 3 19/09/2023 8:00 Bulk Density ASTM D 1895 g/cc 0.470
Aluminium Content ASTM D 6247 ppm 61.0
Magnesium Content ASTM D 6247 ppm 14.0
Titanium Content ASTM D 6247 ppm 1.0
Chloride Content ASTM D 6247 ppm 35.0
Iron Content ASTM D 6247 ppm 1.0
Melt Flow Rate ASTM D 1238 g/10min 3.48
Xylene Solubility ASTM D 5492 Wt% 3.11
Xylene Solubility by NMR Default % 3.35

Page 47 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 19/09/2023 8:00 Irg 1010 ASTM D 6247 ppm 380 520 420
I 168 ASTM D 6247 ppm 750 1050 865
DHT 4A ASTM D 6247 ppm 250 350 280
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.40
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 7
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 35
Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 1.7
Size Default Wt% 98 98.3
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -4.09
513-S-331A Reactor1 19/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.14
Xylene Solubility by NMR Default % 3.20
513-S-331B Reactor2 19/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.84
513-S-415 Reactor 3 19/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.54
R03RR PP Pellet 19/09/2023 10:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.21
513-S-331A Reactor1 19/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.78
Xylene Solubility ASTM D 5492 Wt% 3.24
Xylene Solubility by NMR Default % 3.49
Page 48 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331B Reactor2 19/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.53
Xylene Solubility ASTM D 5492 Wt% 3.48
Xylene Solubility by NMR Default % 3.55
513-S-415 Reactor 3 19/09/2023 12:00 Melt Flow Rate ASTM D 1238 g/10min 3.44
Xylene Solubility ASTM D 5492 Wt% 3.29
Xylene Solubility by NMR Default % 3.50
R03RR PP Pellet 19/09/2023 12:00 Irg 1010 ASTM D 6247 ppm 380 520 415
I 168 ASTM D 6247 ppm 750 1050 860
DHT 4A ASTM D 6247 ppm 250 350 265
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.18
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 15
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
513-S-331A Reactor1 19/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.66
Xylene Solubility by NMR Default % 3.19
513-S-331B Reactor2 19/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.45
513-S-415 Reactor 3 19/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.45
R03RR PP Pellet 19/09/2023 14:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.22
513-S-331A Reactor1 19/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 3.40
Xylene Solubility ASTM D 5492 Wt% 3.23
Xylene Solubility by NMR Default % 3.43
Page 49 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-331B Reactor2 19/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 3.50
Xylene Solubility ASTM D 5492 Wt% 3.33
Xylene Solubility by NMR Default % 3.54
513-S-415 Reactor 3 19/09/2023 16:00 Melt Flow Rate ASTM D 1238 g/10min 3.50
Retention on 10 mesh ASTM D 1921 Wt% 0.10
Retention on 18 mesh ASTM D 1921 Wt% 0.30
Retention on 35 mesh ASTM D 1921 Wt% 26.80
Retention on 60 mesh ASTM D 1921 Wt% 59.60
Retention on 120 mesh ASTM D 1921 Wt% 10.20
Retention on 230 mesh ASTM D 1921 Wt% 2.6
Retention on Pan ASTM D 1921 Wt% 0.40
APS ASTM D 1921 µ 453
Xylene Solubility ASTM D 5492 Wt% 3.18
Xylene Solubility by NMR Default % 3.44
R03RR PP Pellet 19/09/2023 16:00 Irg 1010 ASTM D 6247 ppm 380 520 400
I 168 ASTM D 6247 ppm 750 1050 895
DHT 4A ASTM D 6247 ppm 250 350 265
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.23
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 12
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0

Page 50 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 19/09/2023 16:00 pellet Count Default No/Gm 34 42 34
Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 1.5
Size Default Wt% 98 98.5
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -4.58
513-S-331A Reactor1 19/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.41
513-S-331B Reactor2 19/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.46
513-S-415 Reactor 3 19/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.64
R03RR PP Pellet 19/09/2023 18:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.16
513-S-331A Reactor1 19/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.67
Xylene Solubility ASTM D 5492 Wt% 3.21
Xylene Solubility by NMR Default % 3.41
513-S-331B Reactor2 19/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.76
Xylene Solubility ASTM D 5492 Wt% 3.23
Xylene Solubility by NMR Default % 3.36
513-S-415 Reactor 3 19/09/2023 20:00 Melt Flow Rate ASTM D 1238 g/10min 3.54
Xylene Solubility ASTM D 5492 Wt% 3.34
Xylene Solubility by NMR Default % 3.53
R03RR PP Pellet 19/09/2023 20:00 I 168 ASTM D 6247 ppm 750 1050 950
DHT 4A ASTM D 6247 ppm 250 350 295
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.10
Fines Default Not Present

Page 51 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 19/09/2023 20:00 Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 14
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
513-S-331A Reactor1 19/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.91
513-S-331B Reactor2 19/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.50
513-S-415 Reactor 3 19/09/2023 22:00 Melt Flow Rate ASTM D 1238 g/10min 3.60
513-LZ-110B-I/L Propylene Dryer 20/09/2023 0:00 Methane UOP 539 ppm(v) 100 <5
I/L
Ethane UOP 539 ppm(v) 200 <5
Ethylene UOP 539 ppm(v) 100 <5
Propane UOP 539 Vol % 0.4 0.350
Propylene UOP 539 Vol % 99.6 99.64
Propadiene UOP 539 ppm(v) 5 <5
Acetylene UOP 539 ppm(v) 3 <3
Iso Butane UOP 539 ppm(v) <5
N Butane UOP 539 ppm(v) <5
C4 Unsaturated UOP 539 ppm(v) 650 <5
Iso Pentane UOP 539 ppm(v) <5
n-Pentane UOP 539 ppm(v) <5
1,3 Butadiene UOP 539 ppm(v) 5 <5
Methyl Acetylene UOP 539 ppm(v) 3 <3
C5 Unsaturated UOP 539 ppm(v) 200 <5
Hydrogen Sulfide UOP 539 ppm(v) 500 <0.5
Page 52 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-LZ-110B-I/L Propylene Dryer 20/09/2023 0:00 COS UOP 539 ppm(v) 0.02 <0.02
I/L
Arsine UOP 539 ppm(v) 0.03 <0.03
Phosphine UOP 539 ppm(v) 0.03 <0.03
Moisture Content ASTM D 1142 ppm(w) 1 0.40
513-S-331A Reactor1 20/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 3.50
Xylene Solubility ASTM D 5492 Wt% 3.22
Xylene Solubility by NMR Default % 3.44
513-S-331B Reactor2 20/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 3.39
Xylene Solubility ASTM D 5492 Wt% 3.24
Xylene Solubility by NMR Default % 3.44
513-S-415 Reactor 3 20/09/2023 0:00 Melt Flow Rate ASTM D 1238 g/10min 3.49
Xylene Solubility ASTM D 5492 Wt% 3.44
Xylene Solubility by NMR Default % 3.71
R03RR PP Pellet 20/09/2023 0:00 Irg 1010 ASTM D 6247 ppm 380 520 380
I 168 ASTM D 6247 ppm 750 1050 895
DHT 4A ASTM D 6247 ppm 250 350 380
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.21
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 14
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 34

Page 53 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 20/09/2023 0:00 Under Size Default Wt% 0.2 0.0
Over Size Default Wt% 1 3.5
Size Default Wt% 98 96.5
Fines Default Wt% 0 0.0
Yellowness Index ASTM E 313 0 -4.38
513-S-331A Reactor1 20/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.34
513-S-331B Reactor2 20/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.40
513-S-415 Reactor 3 20/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.61
R03RR PP Pellet 20/09/2023 2:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.20
513-S-331A Reactor1 20/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.48
Xylene Solubility by NMR Default % 3.27
513-S-331B Reactor2 20/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.42
Xylene Solubility by NMR Default % 3.31
513-S-415 Reactor 3 20/09/2023 4:00 Melt Flow Rate ASTM D 1238 g/10min 3.76
Xylene Solubility by NMR Default % 3.79
R03RR PP Pellet 20/09/2023 4:00 I 168 ASTM D 6247 ppm 750 1050 900
DHT 4A ASTM D 6247 ppm 250 350 255
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.22
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 12
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0

Page 54 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

513-PP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
R03RR PP Pellet 20/09/2023 4:00 Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
513-S-331A Reactor1 20/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.66
513-S-331B Reactor2 20/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.44
513-S-415 Reactor 3 20/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.73
R03RR PP Pellet 20/09/2023 6:00 Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.20

# of Samples in Unit: 60
# of Analytes in Unit: 244

Page 55 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-C-101 O/L RFG feed to DCU 19/09/2023 10:00 Methane UOP 539 Vol % 57.17
Ethane UOP 539 Vol % 19.24
Ethylene UOP 539 Vol % 2.94
Propane UOP 539 Vol % 1.41
Propylene UOP 539 Vol % 0.42
Iso Butane UOP 539 Vol % 0.40
N Butane UOP 539 Vol % 2.61
C4 Unsaturated UOP 539 Vol % 0.7
Iso Pentane UOP 539 Vol % 0.17
n-Pentane UOP 539 Vol % 0.16
C5 Unsaturated UOP 539 Vol % 0.2
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.05
Oxygen UOP 539 Vol % 0.11
Nitrogen UOP 539 Vol % 0.87
Carbon Monoxide UOP 539 Vol % 0.34
Hydrogen UOP 539 Vol % 13.19
Hydrogen Sulfide UOP 539 ppm(v) <0.5
COS UOP 539 ppm(v) <0.5
Gross Calorific Value ASTM D 5865 Kcal/kg 12749
Net Calorific Value ASTM D 3588 Kcal/kg 11573
Total Mercaptans ASTM D 6228 ppm(v) 6.0
Molecular Weight Default 19.76
Methyl Mercaptan ASTM D 5504 vol. ppm 4.00

Page 56 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-C-101 O/L RFG feed to DCU 19/09/2023 10:00 Ethyl Mercaptan ASTM D 6228 vol. ppm <0.5
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
514-SC4-2101 LP Fuel Gas 19/09/2023 14:00 Methane UOP 539 Vol % 63.07
Ethane UOP 539 Vol % 5.42
Ethylene UOP 539 Vol % 6.26
Propane UOP 539 Vol % 0.64
Propylene UOP 539 Vol % 0.52
Iso Butane UOP 539 Vol % 0.15
N Butane UOP 539 Vol % 0.51
C4 Unsaturated UOP 539 Vol % 0.3
Iso Pentane UOP 539 Vol % 0.05
n-Pentane UOP 539 Vol % 0.05
C5 Unsaturated UOP 539 Vol % 0.0
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.08
Oxygen UOP 539 Vol % 0.05
Nitrogen UOP 539 Vol % 7.58
Carbon Monoxide UOP 539 Vol % 0.62
Hydrogen UOP 539 Vol % 14.73
Hydrogen Sulfide UOP 539 Vol % 0.0100 0.0004
Molecular Weight UOP 539 17.27
Net Calorific Value UOP 539 Kcal/kg 10450.00
Gross Calorific Value UOP 539 Kcal/kg 11550.00

Page 57 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

514-FGU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
514-SC4-2102 HP Fuel Gas 19/09/2023 14:00 Methane UOP 539 Vol % 68.16
Ethane UOP 539 Vol % 8.47
Ethylene UOP 539 Vol % 10.85
Propane UOP 539 Vol % 0.69
Propylene UOP 539 Vol % 0.41
Iso Butane UOP 539 Vol % 0.16
N Butane UOP 539 Vol % 0.5 0.57
C4 Unsaturated UOP 539 Vol % 0.25
Iso Pentane UOP 539 Vol % 0.05
n-Pentane UOP 539 Vol % 0.04
C5 Unsaturated UOP 539 Vol % 0.02
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.62
Oxygen UOP 539 Vol % 0.04
Nitrogen UOP 539 Vol % 3.04
Carbon Monoxide UOP 539 Vol % 0.32
Hydrogen UOP 539 Vol % 6.29
Hydrogen Sulfide UOP 539 Vol % 0.0100 0.0006
Molecular Weight UOP 539 19.01
Net Calorific Value UOP 539 Kcal/kg 11056.00
Gross Calorific Value UOP 539 Kcal/kg 11000 12000 12168
# of Samples in Unit: 3
# of Analytes in Unit: 69

Page 58 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

515-Sr LPG TU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
515-SC4-1501 LPG to B/L 19/09/2023 6:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 500 10
515-SC4-1501 LPG to B/L 19/09/2023 14:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 500 10
Hydrogen Sulfide ASTM D 2420 ppm(v) Negative
515-SC4-1501 LPG to B/L 19/09/2023 22:00 Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
PHP Default Positive
Volatility:Evaporation Temp in°C for ASTM D 1837 °C -2 -1.2
95%v at760mm
# of Samples in Unit: 3
# of Analytes in Unit: 6

Page 59 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

516-Cr LPG TU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
516-E-102 U/S SR Reg.Inlet 19/09/2023 14:00 % Spent UOP 209 % 5 25 1.90
line caustic from
% strength UOP 209 % 5 20 15.5
516-E-102
Mercaptide UOP 209 ppm(w) 10000 220.0
Sulphide IS 3025:P 29 ppm(w) 55000 470
516-SC1-1104 Spent Caustic 19/09/2023 14:00 % strength UOP 209 % wt 3.6
from 516-C-101
Mercaptide UOP 209 ppm(w) 1256.0
Spent Caustic UOP 209 % wt 7.7
Sulphide IS 3025:P 29 ppm(w) 5139.0
516-SC1-1404 SR Reg.caustic 19/09/2023 14:00 % Spent UOP 209 % 5 25 3.90
from
% strength UOP 209 % 5 20 14.7
516-G-102A/B
Mercaptide UOP 209 ppm(w) 2000 8000 227.0
Sulphide IS 3025:P 29 ppm 3500 331.0
516-T-103 SR+CR) Spent 19/09/2023 14:00 % Spent UOP 209 Wt% 5 25 1.30
Caustic
% strength UOP 209 Wt% 5 20 15.80
Mercaptide UOP 209 ppm(w) 43695 650.0
Sulphide IS 3025:P 29 ppm 70000 2216.0
516-SC4-2601 LPG 19/09/2023 22:00 Total Volatile Sulphur ASTM D 3246 ppm(w) 100 20
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Hydrogen Sulfide ASTM D 2420 Negative
PHP Default Positive
Volatility:Evaporation Temp in°C for ASTM D 1837 °C -1.6
95%v at760mm
# of Samples in Unit: 5
# of Analytes in Unit: 21

Page 60 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-001 ATF Feed to 19/09/2023 6:00 Acidity Total IS 1448:P 113 mg 0.015 1.5 0.0260
Prewash KOH/g
Density at 15°C ASTM D 4052 kg/m³ 783 788.0
Initial Boling Point IS 1448:P 18 °C 160.5
Temperature at 5% Volume IS 1448:P 18 °C 168.0
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 169.2
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 174.5
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 181.7
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 193.0
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 216.9
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 236.3
Recovery
Final Boiling Point IS 1448:P 18 °C 247.2 239.5
Flash Point, Abel IS 1448:P 20 °C 40 45.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.224
Color -Saybolt ASTM D 156 20 26
Doctor Test IS 1448:P 19 Negative
Sulphur Mercaptan IS 1448:P 109 ppm(w) 350 190
519-SN-008 ATF After Clay 19/09/2023 6:00 Acidity Total IS 1448:P 113 mg 0.015 0.0019
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 787.9
Freezing Point IS 1448:P 11 °C -60 -63.6
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 21.0
Page 61 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-008 ATF After Clay 19/09/2023 6:00 Total Sulphur ASTM D 4294 Wt% 0.25 0.229
Filter
Color -Saybolt ASTM D 156 16 18
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative
Silver Strip Corrosion for 4hrs @ IP 227 0
50°C
Interface Rating IS 1448:P 42 1b
519-SN-001 ATF Feed to 19/09/2023 14:00 Density at 15°C ASTM D 4052 kg/m³ 783 786.2
Prewash
Flash Point, Abel IS 1448:P 20 °C 40 43.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.215
Color -Saybolt ASTM D 156 +26
Doctor Test IS 1448:P 19 Positive
519-SN-008 ATF After Clay 19/09/2023 14:00 Acidity Total IS 1448:P 113 mg 0.015 0.0012
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 787.8
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 17.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.229
Color -Saybolt ASTM D 156 16 21
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative
Silver Strip Corrosion for 4hrs @ IP 227 0
50°C
519-SN-001 ATF Feed to 19/09/2023 22:00 Density at 15°C ASTM D 4052 kg/m³ 783 784.9
Prewash
Flash Point, Abel IS 1448:P 20 °C 40 45.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.198
Page 62 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

519-ATF Merox
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
519-SN-001 ATF Feed to 19/09/2023 22:00 Color -Saybolt ASTM D 156 +26
Prewash
Doctor Test IS 1448:P 19 Positive
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 3a
50°C
519-SN-008 ATF After Clay 19/09/2023 22:00 Acidity Total IS 1448:P 113 mg 0.015 0.0018
Filter KOH/g
Density at 15°C IS 1448:P 16 kg/m³ 783 787.0
Mercaptan Sulfur IS 1448:P 109 ppm(w) 18 17.0
Total Sulphur ASTM D 4294 Wt% 0.25 0.221
Color -Saybolt ASTM D 156 16 19
Copper Strip Corrosion for 2 hrs @ IS 1448:P 15 1a
100°C
Doctor Test ASTM D 4952 Negative
Silver Strip Corrosion for 4hrs @ IP 227 0
50°C
# of Samples in Unit: 7
# of Analytes in Unit: 53

Page 63 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

520-SWU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
520-SC-1202 Stripped water 19/09/2023 22:00 Ammonia IS 3025:P 34 ppm 50 50.0
H2S IS 3025:P 29 ppm 50 6.7
pH IS 3025:P 11 7 9 9.2
# of Samples in Unit: 1
# of Analytes in Unit: 3

Page 64 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

521-SWU-II
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
521-SC-1202 Stripped water 19/09/2023 22:00 Ammonia IS 3025:P 34 ppm 50 18.00
H2S IS 3025:P 29 ppm 50 6.3
pH ASTM D 1293 5.5 8.9
# of Samples in Unit: 1
# of Analytes in Unit: 3

Page 65 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

522-ARU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
522-E-105 Cooling water 19/09/2023 18:00 H2S IS 3025:P 29 ppm 204.0
return from lean
amine water cooler
522-E-205 522-E-205 19/09/2023 18:00 H2S IS 3025:P 29 ppm 187.0
522-SC-1302 Lean Amine 19/09/2023 18:00 H2S IS 3025:P 29 ppm(w) 1500 198.0
MDEA Concentration Default Wt% 38.0 40.5
# of Samples in Unit: 3
# of Analytes in Unit: 4

Page 66 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

524-SRU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
524-SC.B-2002 MP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 8.00
Conductivity IS 3025:P 14 µS/cm 32 0.50
Iron Content ASTM D 1068 mg/l 0.29
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 mg/l <0.02
pH IS 3025:P 11 9.2 9.8 7.8
524-SC.B-2201 LP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 6.00
Conductivity IS 3025:P 14 µS/cm 32 2.49
Iron Content ASTM D 1068 mg/l 0.2 3.6 0.35
Phosphate APHA 4500 mg/l <0.5
P.D
Silica ASTM D 859 mg/l <0.02
pH IS 3025:P 11 9.2 9.8 8.50
524-SC.B-2401 LP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 4.00
Conductivity IS 3025:P 14 µS/cm 32 4.60
Iron Content ASTM D 1068 mg/l 0.36
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 mg/l <0.02
pH IS 3025:P 11 9.2 9.8 9.6
524-SC.B-2601 MP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 10.00
Conductivity IS 3025:P 14 µS/cm 32 51.00
Iron Content ASTM D 1068 ppm(w) 0.39
Phosphate APHA 4500 mg/l 0.2 3.6 8.96
P.D
Page 67 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

524-SRU-I
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
524-SC.B-2601 MP Blow down 19/09/2023 6:00 Silica ASTM D 859 ppm 0.10
pH IS 3025:P 11 9.2 9.8 9.9
524-SC.B-3001 HP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 8.00
Conductivity IS 3025:P 14 µS/cm 0 32 2.49
Iron Content ASTM D 1068 ppm(w) 0.30
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 ppm <0.02
pH IS 3025:P 11 9.2 9.8 9.0
524-SC.B-3402 LP Blow down 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 14.00
Iron Content ASTM D 1068 mg/l 0.32
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 mg/l <0.02
TDS IS 3025:P 16 mg/l 1
pH IS 3025:P 11 9.2 9.8 8.80
524-SC-6301 BFW 19/09/2023 6:00 Conductivity ASTM D 1125 µS/cm 1.72
pH ASTM D 1293 9.1
524-SC.H-4401 TGTU (Lean 19/09/2023 18:00 H2S IS 3025:P 29 ppm 241.0
Amine)
TSS IS 3025:P 17 ppm 32
MDEA Concentration Default Wt% 46.30
# of Samples in Unit: 8
# of Analytes in Unit: 41

Page 68 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

525-SRU-II
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
525-SC.B-2002 LP blowdown 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 20 6.00
Conductivity IS 3025:P 14 µS/cm 32 1.80
Iron Content ASTM D 1068 mg/l 2 0.30
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 mg/l 20 <0.02
pH IS 3025:P 11 9.2 9.8 8.6
525-SC.B-2201 LP blowdown 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 20 8.00
Conductivity IS 3025:P 14 µS/cm 32 1.00
Iron Content ASTM D 1068 mg/l 2 0.26
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 mg/l 20 <0.02
pH IS 3025:P 11 9.2 9.8 7.5
525-SC.B-2401 LP blowdown 19/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 10.00
Conductivity IS 3025:P 14 µS/cm 32 2.10
Iron Content ASTM D 1068 ppm(w) 0.35
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 ppm <0.02
pH IS 3025:P 11 9.2 9.8 8.9
525-SC.B-2601 MP blowdown 19/09/2023 6:00 Conductivity IS 3025:P 14 µS/cm 32 11.76 alkalinity -
6mg/l
Phosphate APHA 4500 mg/l 0.2 3.6 3.96 SILICA -
P.D 0.12mg/l
pH IS 3025:P 11 9.2 9.8 9.5 Fe-0.39mg/l

Page 69 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

525-SRU-II
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
525-SC.B-3001 HP blowdown 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 20 6.00
Conductivity IS 3025:P 14 µS/cm 32 9.24
Iron Content ASTM D 1068 mg/l 2 0.40
Phosphate APHA 4500 mg/l 0.2 3.6 3.71
P.D
Silica ASTM D 859 mg/l 20 0.08
pH IS 3025:P 11 9.2 9.8 9.9
525-SC.B-3402 LP blowdown 19/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 6.00
Conductivity IS 3025:P 14 µS/cm 32 0.76
Iron Content ASTM D 1068 ppm(w) 0.42
Phosphate APHA 4500 mg/l 0.2 3.6 <0.5
P.D
Silica ASTM D 859 ppm <0.02
pH IS 3025:P 11 9.2 9.8 7.9
525-SC.H-3601 Quench water to 19/09/2023 6:00 H2S IS 3025:P 29 mg/l 53.0
quench tower
pH IS 3025:P 11 NULL 6.8 8.5 8.5
(524-C-101)
# of Samples in Unit: 7
# of Analytes in Unit: 35

Page 70 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

530-BBU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
530-SC-2001. Reactor O/L 19/09/2023 1:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 2882
530-SC-2001. Reactor O/L 19/09/2023 4:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 4064
Viscosity ratio at 60°C (Residue of IS 1206:P 2 5.4
RTFOT)
530-SC-2903 Scrubber Wash 19/09/2023 6:00 pH IS 3025:P 11 8.4
Water
530-SC-2001. Reactor O/L 19/09/2023 7:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 4562
Penetration @ 25°C, 100g, 5Sec, IS 1203 mm 49.0
1/10mm
Softening Point (R & B) IS 1205 °C 52.5
530-SC-2001. Reactor O/L 19/09/2023 10:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3363
Viscosity ratio at 60°C (Residue of IS 1206:P 2 5.3
RTFOT)
530-SC-2001. Reactor O/L 19/09/2023 13:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 2958
530-SC-2903 Scrubber Wash 19/09/2023 14:00 pH IS 3025:P 11 8.0
Water
530-SC-2001. Reactor O/L 19/09/2023 16:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3270
Viscosity ratio at 60°C (Residue of IS 1206:P 2 5.0
RTFOT)
530-SC-2001. Reactor O/L 19/09/2023 19:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3231
530-SC-2001. Reactor O/L 19/09/2023 22:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3325
Viscosity ratio at 60°C (Residue of IS 1206:P 2 5.3
RTFOT)
530-SC-2903 Scrubber Wash 19/09/2023 22:00 pH IS 3025:P 11 8.0
Water
530-SC-2001. Reactor O/L 20/09/2023 1:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3431
530-SC-2001. Reactor O/L 20/09/2023 4:00 Absolute Viscosity @ 60°C IS 1206:P 2 Poise 3147

Page 71 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

530-BBU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 13
# of Analytes in Unit: 19

Page 72 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

551-Crude Tanks
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
CRT Line 551-Crude Oil 19/09/2023 1:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 882.7 451761256
CRT Line 551-Crude Oil 19/09/2023 9:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 881.6 451761256
551-T-01C 551-Crude Oil 19/09/2023 12:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 882 903 879.9 Composite
CRT Line 551-Crude Oil 19/09/2023 17:00 BS&W ASTM D 4007 Vol % 0.10
Tanks
Density at 15°C ASTM D 1298 kg/m3 879.9 B. No.
451780163
CRT Line 551-Crude Oil 20/09/2023 1:00 BS&W ASTM D 4007 Vol % 0.10 451780163
Tanks
Density at 15°C ASTM D 1298 kg/m3 879.4
# of Samples in Unit: 5
# of Analytes in Unit: 10

Page 73 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

553-LPG Spheres
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
553-MB-01G LPG Storage 19/09/2023 8:00 Ethane ASTM D 2163 Vol % 1.18
Bullet
Propane ASTM D 2163 Vol % 24.69
Propylene ASTM D 2163 Vol % 2.89
Iso Butane ASTM D 2163 Vol % 14.63
N Butane ASTM D 2163 Vol % 12.15
trans-2-Butene ASTM D 2163 Vol % 9.37
1-Butene ASTM D 2163 Vol % 8.87
Iso Butylene ASTM D 2163 Vol % 18.20
cis-2-Butene ASTM D 2163 Vol % 6.93
Iso Pentane ASTM D 2163 Vol % 0.40
n-Pentane ASTM D 2163 Vol % 0.07
1,3 Butadiene ASTM D 2163 Vol % 0.24
Trance-2-Pentene ASTM D 2163 Vol % 0.31
2 Methyl 2 Butene ASTM D 2163 Vol % 0.02
1 Pentene ASTM D 2163 Vol % 0.03
C5 Hydrocarbons and Heavier ASTM D 2163 Vol % 0.83
COS ASTM D 2163 ppm(v) <0.02
Ethyle Mercapton ASTM D 2163 ppm <0.5
Moisture ASTM D 2163 ppm(v) 24.0
Total Volatile Sulphur ASTM D 3246 ppm(w) 10
Hydrogen Sulfide ASTM D 2420 Pass
# of Samples in Unit: 1
# of Analytes in Unit: 21

Page 74 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

556-Coke handling
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
Coke_ Dispatch Coke_ Dispatch 19/09/2023 3:56 Moisture Content: As received IS 1448:P 132 Mass% 4.20 PB11BF7385
Pet Coke Pet Coke 19/09/2023 9:30 Moisture Content: As received IS 1448:P 132 Mass% 3.90
BeltNo.12 Silo-2 BeltNo.12 Silo-2
Coke_ Dispatch Coke_ Dispatch 19/09/2023 10:45 Moisture Content: As received IS 1448:P 132 Mass% 3.44 PB10EH749
1
# of Samples in Unit: 3
# of Analytes in Unit: 3

Page 75 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0101 Spent caustic 19/09/2023 6:00 Sulphide IS 3025:P 29 ppm 25000 299.0
storage tank I/L
558-SC-0102 Treated Spent 19/09/2023 6:00 Sulphide IS 3025:P 29 ppm 20 18.0
Caustic
558-SC-0105 OWS SUMP 19/09/2023 6:00 Free Oil Visual Vol % 1.5 SLUDGE
OIL
PRESENT
558-SC-0106 Desalter Inlet 19/09/2023 6:00 Free Oil Visual Vol % 0.6 SLUDGE
OIL
PRESENT
558-SC-0107 Sour Water 19/09/2023 6:00 Alkalinity APHA 2320 D ppm 58.00
COD APHA 5220 C ppm 309
Nitrates APHA 4500 ppm 57.5
NO3-
TDS IS 3025:P 16 ppm 84
pH IS 3025:P 11 9.2
Sulphide IS 3025:P 29 ppm 7.4
558-SC-0201 API I/L 19/09/2023 6:00 Free Oil Visual Vol % 1.2 SLUDGE
OIL
PRESENT
558-SC-0202 TPI I/L 19/09/2023 6:00 Free Oil Visual Vol % NO FREE
OIL
TSS IS 3025:P 17 ppm 25 56
558-SC-0203 Outlet of TPI I/L of 19/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 525 <4
DAF super cell
TSS IS 3025:P 17 ppm 20 38
558-SC-0204 DAF outlet A 19/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 10 <4
TSS IS 3025:P 17 ppm 10 22
558-SC-0205 DAF outlet-B 19/09/2023 6:00 Oil & Grease IS 3025:P 39 ppm 4 10 <4

Page 76 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0205 DAF outlet-B 19/09/2023 6:00 TSS IS 3025:P 17 ppm 10 18
558-SC-0206 SBR I/L 19/09/2023 6:00 Alkalinity IS 3025:P 23 ppm 77.00
Ammonia IS 3025:P 34 ppm 50 59.00
BOD(3days at 27° C) IS 3025:P 44 ppm 600 39 16/09/2023
COD APHA 5220 C ppm 1000 268
Nitrite Default ppm 55
Ortho phosphate APHA 4500 P ppm 25.00
Phenol APHA 5530 C ppm 100 8.000
Sulphide IS 3025:P 29 ppm 50 6.70
TSS APHA 2540 C ppm 20 32
pH IS 3025:P 11 7 8 7.4
558-SC-0301 MBR Inlet 19/09/2023 6:00 Alkalinity APHA 2320 D ppm 85.00
Ammonia IS 3025:P 34 ppm 40 43.00
BOD(3days at 27° C) IS 3025:P 44 ppm 250 37 16/09/23
COD APHA 5220 C ppm 500 185
Nitrates APHA 4500 ppm 57.2
NO3-
Ortho phosphate APHA 4500 P ppm 0.69
Sulphide IS 3025:P 29 ppm 7
TSS IS 3025:P 17 ppm 30 37
pH IS 3025:P 11 7 8 7.3
558-SC-0302 Treated Effluent 19/09/2023 6:00 Alkalinity IS 3025:P 23 mg/l 88.0
Pump Discharge
Ammonia IS 3025:P 34 mg/l 1.17
BOD(3days at 27° C) IS 3025:P 44 mg/l 5.0 16/09/2023
COD APHA 5220 C mg/l 49.0
Page 77 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

558-ETP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
558-SC-0302 Treated Effluent 19/09/2023 6:00 Conductivity IS 3025:P 14 uS/cm 704.00
Pump Discharge
Oil & Grease IS 3025:P 39 mg/l <4
Phenol APHA 5530 C mg/l <0.1
Phosphate APHA 4500 mg/l <0.5
P.D
Sulphide IS 3025:P 29 mg/l <0.5
TDS APHA 2540 D mg/l 457.0
TSS IS 3025:P 17 mg/l 5.0
pH IS 3025:P 11 7.8
558-SC-0803 CRW System DMF 19/09/2023 6:00 COD APHA 5220 C mg/l 66
Outlet
Oil & Grease IS 3025:P 39 mg/l 4 <4
Sulphide IS 3025:P 29 mg/l <0.5
TDS APHA 2540 D mg/l 633
TSS APHA 2540 C mg/l 16
pH ASTM D 1293 7.1
558-SC-0102 Treated Spent 19/09/2023 14:00 Sulphide IS 3025:P 29 ppm 20 29.0
Caustic
558-SC-0102 Treated Spent 19/09/2023 22:00 Sulphide IS 3025:P 29 ppm 20 30.0
Caustic
558-SC-0107 Sour Water 19/09/2023 22:00 Ammonia IS 3025:P 34 ppm 47.00

# of Samples in Unit: 18
# of Analytes in Unit: 59

Page 78 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1401 MS-VI Blending 19/09/2023 2:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 19/09/2023 2:00 Cetane Number ASTM D 613 No 51.5 51.10
(BS VI) Station
Total Sulphur ASTM D 5453 mg/kg 10 7.5
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 6:00 Benzene Content ASTM D 3606 Vol % 0.95 0.95
(BS VI) station
Aromatics ASTM D 1319 Vol % 35.0 30.0
Olefines ASTM D 1319 Vol % 12.5
Saturates ASTM D 1319 Vol % 57.5
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 741.9
Initial Boling Point ASTM D 86 °C 34.1
Final Boiling Point ASTM D 86 °C 195 193.8
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 35.4
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 55.7
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 87.4
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 56.5
Total Sulphur ASTM D 5453 mg/kg 10 6.5
Doctor Test ASTM D 4952 Negative
Research Octane Number (RON) ASTM D 2699 92.0 91.5
561-SC-1901 HSD-VI Blending 19/09/2023 6:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C
Density at 15°C ASTM D 4052 kg/m³ 827.6
Initial Boling Point ASTM D 86 °C 119.0

Page 79 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 19/09/2023 6:00 Temperature at 95% Volume ASTM D 86 °C 360 352.3
(BS VI) Station Recovery
Final Boiling Point ASTM D 86 °C 362.0
Flash Point, Abel IS 1448:P 20 °C 37 34.5
Total Sulphur ASTM D 5453 mg/kg 10 7.0
Cetane Index ASTM D 4737 51.8
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 10:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 19/09/2023 10:00 Total Sulphur ASTM D 5453 mg/kg 10 7.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 14:00 Benzene Content ASTM D 3606 Vol % 0.95 0.89
(BS VI) station
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 741.7
Initial Boling Point ASTM D 86 °C 34.3
Final Boiling Point ASTM D 86 °C 195 196.3
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 36.6
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 55.8
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 87.0
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 55.9
Total Sulphur ASTM D 5453 mg/kg 10 6.5
Doctor Test ASTM D 4952 Negative
561-SC-1901 HSD-VI Blending 19/09/2023 14:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C
Density at 15°C ASTM D 4052 kg/m³ 827.8

Page 80 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 19/09/2023 14:00 Initial Boling Point ASTM D 86 °C 116.0
(BS VI) Station
Temperature at 95% Volume ASTM D 86 °C 360 349.9
Recovery
Final Boiling Point ASTM D 86 °C 364.8
Flash Point, Abel IS 1448:P 20 °C 37 33.0
Total Sulphur ASTM D 5453 mg/kg 10 7.0
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 19/09/2023 18:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 19/09/2023 18:00 Total Sulphur ASTM D 5453 mg/kg 10 7.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
Flash Point, Abel IS 1448:P 20 °C 37 38.0
561-SC-1401 MS-VI Blending 19/09/2023 22:00 Benzene Content ASTM D 3606 Vol % 0.95 0.79
(BS VI) station
Copper Strip Corrosion for 3 hrs @ ASTM D 130 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 744.7
Initial Boling Point ASTM D 86 °C 33.9
Final Boiling Point ASTM D 86 °C 195 195.1
Recovery up to 70°C (E70) ASTM D 86 Vol % 10 45 32.7
Recovery up to 100°C (E100) ASTM D 86 Vol % 40 70 52.4
Recovery up to 150°C (E150) ASTM D 86 Vol % 75 86.0
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 58 55.2
Total Sulphur ASTM D 5453 mg/kg 10 6.5
Doctor Test ASTM D 4952 Negative
561-SC-1901 HSD-VI Blending 19/09/2023 22:00 Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
(BS VI) Station 50°C

Page 81 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

561-Process Blending
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
561-SC-1901 HSD-VI Blending 19/09/2023 22:00 Density at 15°C ASTM D 4052 kg/m³ 827.6
(BS VI) Station
Initial Boling Point ASTM D 86 °C 121.0
Temperature at 95% Volume ASTM D 86 °C 360 347.8
Recovery
Final Boiling Point ASTM D 86 °C 360.3
Flash Point, Abel IS 1448:P 20 °C 37 36.0
Total Sulphur ASTM D 5453 mg/kg 10 7.0
Doctor Test ASTM D 4952 Negative
561-SC-1401 MS-VI Blending 20/09/2023 2:00 Doctor Test ASTM D 4952 Negative
(BS VI) station
561-SC-1901 HSD-VI Blending 20/09/2023 2:00 Total Sulphur ASTM D 5453 mg/kg 10 6.5
(BS VI) Station
Doctor Test ASTM D 4952 Negative
# of Samples in Unit: 15
# of Analytes in Unit: 76

Page 82 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

575-CPP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
575-SC-3511 Makeup Water 19/09/2023 10:00 Iron Content ASTM D 1068 ppm(w) <0.02
TSS APHA 2540 C ppm 1
575-SC-3512 Cooling Water 19/09/2023 10:00 Iron Content ASTM D 1068 ppm 0.03
TSS APHA 2540 C ppm 2.0
575-SC-4221 Fuel Gas 19/09/2023 11:00 Methane UOP 539 Vol % 38.006 78.29
Ethane UOP 539 Vol % 16.483 6.46
Ethylene UOP 539 Vol % 19.889 6.72
Propane UOP 539 Vol % 0.435 0.66
Propylene UOP 539 Vol % 1.664 0.21
Iso Butane UOP 539 Vol % 0.026 0.16
N Butane UOP 539 Vol % 0.1 0.41
C4 Unsaturated UOP 539 Vol % 0.10
Iso Pentane UOP 539 Vol % 0.04
n-Pentane UOP 539 Vol % 0.02
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 0.05
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 2.52
Carbon Monoxide UOP 539 Vol % 0.09
Hydrogen UOP 539 Vol % 4.17
Gross Calorific Value ASTM D 3588 Kcal/kg 12517.00
Net Calorific Value ASTM D 3588 Kcal/kg 11338.00
Hydrogen Sulfide Dragger Vol % 0.0006
Molecular Weight Default 18.42 21.42 18.08

Page 83 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

575-CPP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
# of Samples in Unit: 3
# of Analytes in Unit: 24

Page 84 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

576-CPU
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
576 SC-0103 Surface 19/09/2023 22:00 Silica ASTM D 859 ppm <0.02
Condansate
TOC ASTM D 5310 ppm 0.1
576-SC-0102 Pure Condensate 19/09/2023 22:00 Silica ASTM D 859 ppm 0.02 <0.02
TOC ASTM D 5310 ppm 0.1
576-SC-0201 Unpolished 19/09/2023 22:00 TOC ASTM D 5310 ppm 0.4
Condansate
Pump Discharge
576-SC-0406 Polished 19/09/2023 22:00 TOC ASTM D 5310 ppm 1 0.1
Condensate Pump
Discharge
576-SC-CMO CPU MB Outlet 19/09/2023 22:00 Silica ASTM D 859 ppm 18 <0.02

# of Samples in Unit: 5
# of Analytes in Unit: 7

Page 85 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

577-RODM
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
577-SC-0901 Degasser outlet to 19/09/2023 22:00 Alkalinity ASTM D 1067 ND
RO-I feed tank
outlet
577-SC-1503 DM Water pump 19/09/2023 22:00 Conductivity IS 3025:P 14 µS/cm 0.2 0.20
discharge
Iron Content ASTM D 1068 ppm 0.01 <0.02
Silica ASTM D 859 ppm 0.01 <0.02
TOC ASTM D 5310 ppm 0.6 6.9
pH IS 3025:P 11 6.7 7.3 6.9
# of Samples in Unit: 2
# of Analytes in Unit: 6

Page 86 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

578-RWTP
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
578-SC-0210 RGSF Common 19/09/2023 22:00 TSS IS 3025:P 17 mg/l 1 2
Outlet
578-SC-0402 Drinking water 19/09/2023 22:00 Iron Content ASTM D 1068 ppm(w) 0.1 <0.02
pump discharge
TSS IS 3025:P 17 mg/l 1 1
Turbidity IS 3025:P 10 NTU 1 <1
pH IS 3025:P 11 7 8 7.7
# of Samples in Unit: 2
# of Analytes in Unit: 5

Page 87 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 19/09/2023 9:00 Methane UOP 539 Vol % 9.24
HEADER
Ethane UOP 539 Vol % 0.61
Ethylene UOP 539 Vol % 0.41
Propane UOP 539 Vol % 0.68
Propylene UOP 539 Vol % 2.21
Iso Butane UOP 539 Vol % 0.24
N Butane UOP 539 Vol % 0.22
C4 Unsaturated UOP 539 Vol % 0.6
Iso Pentane UOP 539 Vol % 0.08
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.03
Carbon Dioxide UOP 539 Vol % 1.48
Oxygen UOP 539 Vol % 3.03
Nitrogen UOP 539 Vol % 27.48
Carbon Monoxide UOP 539 Vol % 0.23
Hydrogen UOP 539 Vol % 53.45
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0020
Total Hydrocarbon UOP 539 Vol % 14.34
Molecular Weight UOP 539 14.18
Net Calorific Value UOP 539 Kcal/kg 5168.00
Gross Calorific Value UOP 539 Kcal/kg 5838.00
589-SC-1701 OFFSITE FLARE 19/09/2023 19:00 Methane UOP 539 Vol % 7.22
HEADER
Ethane UOP 539 Vol % 0.57
Ethylene UOP 539 Vol % 0.44

Page 88 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 19/09/2023 19:00 Propane UOP 539 Vol % 0.55
HEADER
Propylene UOP 539 Vol % 2.72
Iso Butane UOP 539 Vol % 0.30
N Butane UOP 539 Vol % 0.20
C4 Unsaturated UOP 539 Vol % 0.7
Iso Pentane UOP 539 Vol % 0.06
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.02
Carbon Dioxide UOP 539 Vol % 1.22
Oxygen UOP 539 Vol % 1.30
Nitrogen UOP 539 Vol % 39.72
Carbon Monoxide UOP 539 Vol % 0.15
Hydrogen UOP 539 Vol % 44.76
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0010
Total Hydrocarbon UOP 539 Vol % 12.86
Molecular Weight UOP 539 16.66
Net Calorific Value UOP 539 Kcal/kg 4022.00
Gross Calorific Value UOP 539 Kcal/kg 4521.00
589-SC-1701 OFFSITE FLARE 20/09/2023 1:00 Methane UOP 539 Vol % 7.55
HEADER
Ethane UOP 539 Vol % 0.61
Ethylene UOP 539 Vol % 0.47
Propane UOP 539 Vol % 0.77
Propylene UOP 539 Vol % 2.56
Iso Butane UOP 539 Vol % 0.86

Page 89 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

589 OFF SITE

Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
589-SC-1701 OFFSITE FLARE 20/09/2023 1:00 N Butane UOP 539 Vol % 0.36
HEADER
C4 Unsaturated UOP 539 Vol % 1.2
Iso Pentane UOP 539 Vol % 0.08
n-Pentane UOP 539 Vol % 0.04
C6+ heaviers UOP 539 Vol % 0.07
Carbon Dioxide UOP 539 Vol % 1.35
Oxygen UOP 539 Vol % 2.69
Nitrogen UOP 539 Vol % 35.47
Carbon Monoxide UOP 539 Vol % 0.15
Hydrogen UOP 539 Vol % 45.76
Hydrogen Sulfide UOP 539 Vol % 1.0000 0.0100
Total Hydrocarbon UOP 539 Vol % 14.58
Molecular Weight UOP 539 16.84
Net Calorific Value UOP 539 Kcal/kg 4560.00
Gross Calorific Value UOP 539 Kcal/kg 5105.00
# of Samples in Unit: 3
# of Analytes in Unit: 63

Page 90 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

607-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
607-SC3-1601 Combined Hot 19/09/2023 6:00 Bromine Number ASTM D 1159 gm/100g 10.6
Feed (FSD outlet) m
Density at 15°C ASTM D 4052 kg/m³ 859 847.1
Initial Boling Point IS 1448:P 18 °C 73.7
Temperature at 5% Volume IS 1448:P 18 °C 154.5
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 188.0
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 243.6
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 278.6
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 311.1
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 348.8
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 364.1
Recovery
Final Boiling Point IS 1448:P 18 °C 374.6
Nitrogen ASTM D 4629 ppm(w) 244.0
Total Sulphur ISO 8754 ppm 1.61
Cetane Index ASTM D 4737 48.8
Bromine Number ASTM D 1159 gm/100g 10.4 10.6
m
Density at 15°C ASTM D 4052 kg/m³ 859 847.1
Nitrogen ASTM D 4629 mg/kg 384 244
Total Sulphur ISO 8754 Mass% 1.71 1.61
607-SC3-3001 Stripper bottom 19/09/2023 6:00 Moisture Content ISO 12937 ppm(w) 300
Diesel
Doctor Test ASTM D 4952 Negative
Page 91 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

607-DHDT
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
607-SC5-4901 Naphtha Product 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 770 722.0
Nitrogen Content ASTM D 4629 mg/kg 0.1
Total Sulphur ASTM D 5453 mg/kg 4 0.8
607-SC6-4101 Diesel product 19/09/2023 6:00 Density at 15°C ASTM D 4052 kg/m³ 820 859 829.2
Total Sulphur ASTM D 5453 mg/kg 8 4.5
607-SC4-3601 Treated Fuel Gas 19/09/2023 14:00 H2S DRAEGER Vol % 20 0.0006
TUBE
607-SC6-4101 Diesel product 19/09/2023 14:00 Total Sulphur ASTM D 5453 mg/kg 8 4.0
607-SC6-4101 Diesel product 19/09/2023 22:00 Total Sulphur ASTM D 5453 mg/kg 8 3.5

# of Samples in Unit: 8
# of Analytes in Unit: 28

Page 92 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

912-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
912-S-21302 DGA Samples 19/09/2023 10:00 Ammonia IS 3025:P 34 mg/l 21544.000
Conductivity IS 3025:P 14 mS/cm 135.60
Iron Content APHA 3500 D ppm(w) 0.29
Oil Content Default mg/l <4
912-S-21602 DGA Samples 19/09/2023 10:00 CO2 Vendor wt.% ND
Method
H2S Default ppm(w) 176.000
DGA Strength Vendor's wt.% 41.800
Method
# of Samples in Unit: 2
# of Analytes in Unit: 7

Page 93 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

917-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
917-CC-1102 Refinery Off Gas 19/09/2023 10:00 Methane UOP 539 Vol % 33.57
O/L
Ethane UOP 539 Vol % 12.59
Ethylene UOP 539 Vol % 17.24
Propane UOP 539 Vol % 0.56
Propylene UOP 539 Vol % 0.76
Iso Butane UOP 539 Vol % 0.18
N Butane UOP 539 Vol % 0.95
C4 Unsaturated UOP 539 Vol % 0.53
Iso Pentane UOP 539 Vol % 0.08
n-Pentane UOP 539 Vol % 0.06
C5 Unsaturated UOP 539 Vol % 0.09
C6+ UOP 539 Vol % 0.49
Carbon Dioxide UOP 539 Vol % <0.0050
Oxygen UOP 539 Vol % 0.08
Nitrogen UOP 539 Vol % 10.58
Carbon Monoxide UOP 539 Vol % 0.74
Hydrogen UOP 539 Vol % 21.50
Hydrogen Sulfide UOP 539 ppm(v) <0.5
Molecular Weight UOP 539 Default 19.75
Net Calorific Value UOP 539 Kcal/kg 10013
Gross Calorific Value UOP 539 Kcal/kg 10969
COS UOP 539 ppm(v) <0.5
Total Mercaptans ASTM D 6228 ppm vol. <2
917-S-11101 Rich UCARSOL 19/09/2023 10:00 CO2 Vendor's ppm 77 ND
from Refinery B/L Method
Page 94 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

917-ROG
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
917-S-11101 Rich UCARSOL 19/09/2023 10:00 H2S Default ppm 36 146.0
from Refinery B/L
TSS IS 3025:P 17 ppm 21.0
Oil Content Default ppm <4
UCARSOL Strength Vendor's % wt 75 70.2
Method
917-S-11201 Lean UCARSOL to 19/09/2023 10:00 CO2 Vendor wt. ppm 47 ND
Treater Method
H2S Default wt. ppm 26 ND
Heat Stable Salt Vendor % 0.1
Method
UCARSOL Strength Vendor's % wt 75 69.80
Method
917-CC-1102 Refinery Off Gas 19/09/2023 22:00 Hydrogen Sulfide UOP 539 ppm(v) <0.5
O/L
COS UOP 539 ppm(v) <0.5
Total Mercaptans ASTM D 6228 ppm vol. <2.0
Propyl Mercaptan ASTM D 6228 vol. ppm <0.5
Butyl Mercaptan ASTM D 6228 vol. ppm <0.5
Ethyl Mercaptan ASTM D 6228 vol. ppm <0.5
Methyl Mercaptan ASTM D 6228 vol. ppm <0.5
# of Samples in Unit: 4
# of Analytes in Unit: 39

Page 95 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
553-MB-01D LIQUEFIED 19/09/2023 1:45 C2 Hydrocarbon ASTM D 2163 Vol % 1.10
PETROLEUM
C3 Hydrocarbon ASTM D 2163 Vol % 26.12
GAS-COQ
C4 Hydrocarbon ASTM D 2163 Vol % 71.85
C5 Hydrocarbon ASTM D 2163 Vol % 2.5 0.93
Density at 15°C IP 432 -2000 kg/m3 571.5
Total Volatile Sulphur ASTM D 3246 ppm(w) 140 25
Vapour Pressure at 40°C IP 432 -2000 kPa 520 1050 639
Caustic test IS 4576:2018 Pass
Note 10
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Free Water Content Visual None
Hydrogen Sulfide ASTM D 2420 Pass
Odour IS 4576:2018 Adequate
Note:12
Volatility:Evaporation Temp in°C for IS 1448:P 72 °C 2.2 0.8
95%v at760mm
554-T-08B HIGH SPEED 19/09/2023 2:00 Acidity Total ASTM D 974 mg 0.2 0.05
DIESEL KOH/g
(BS-VI)-COQ Ash Content IS 1448:P 4 Mass% 0.01 0.006
Carbon Residue (Ramsbottom) on IS 1448:P 8 Mass% 0.3 0.14
10 percent residue
Cetane Number IS 1448:P 9 51 51.4
Cold Filter Plugging Point ASTM D 6371 °C 18 -7
Total Contamination EN 12662 mg/kg 24 13
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
50°C
Density at 15°C ASTM D 4052 kg/m³ 810 845 829.4
Page 96 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-08B HIGH SPEED 19/09/2023 2:00 Temperature at 95% Volume IS 1448:P 18 °C 360 352.7
DIESEL Recovery
(BS-VI)-COQ Flash Point, Abel IS 1448:P 20 °C 35 37.0
Kinematic Viscosity @ 40°C IS 1448:P 25 cSt 2 4.5 2.456
Lubricity:wear scar diameter (wsd ISO 12156-1 µm 460 420
1.4) at 60°C
Oxidation Stability ASTM D 2274 g/m³ 25 15
Pour Point IS 1448:P 10 °C 15 -9
Total Sulphur ASTM D 5453 mg/kg 10 8.0
Water Content ISO 12937 mg/kg 200 110
Acidity-Inorganic ISO 6618 Nil
Appearance Visual Clear,bright,
and free
from
sediments,s
uspended
matter and
undissolved
water at
normal
ambient fuel
temperature
Cetane Index ASTM D 4737 46 52.8
FAME content Default N/A-Bio
Diesel Not
Added
Polycyclic Aromatic Hydrocarbons IP 391 Mass% 8 2.87
(PAH)
513-S-710 F Poly Propylene 19/09/2023 2:00 Irg 1010 ASTM D 6247 ppm 380 520 445
I 168 ASTM D 6247 ppm 750 1050 710

Page 97 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 F Poly Propylene 19/09/2023 2:00 DHT 4A ASTM D 6247 ppm 250 350 280
Small ( 0.20 to 0.49mm2) Default No/1520 30 28
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.26 H23I1089
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 40
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.54
Volatile Matter Licensor ppm 500 260
Method
Yellowness Index ASTM E 313 0 -4.09
513-S-710 A Poly Propylene 19/09/2023 8:00 Irg 1010 ASTM D 6247 ppm 380 520 420
I 168 ASTM D 6247 ppm 750 1050 870
DHT 4A ASTM D 6247 ppm 250 350 300
Small ( 0.20 to 0.49mm2) Default No/1520 30 29
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.63 H23I1090
Loos-Forign/ Brown / Black & Others Default no/5kg 1 3

Page 98 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 A Poly Propylene 19/09/2023 8:00 Fused Pellet Default no/5kg 1 25
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.35
Volatile Matter Licensor ppm 500 225
Method
Yellowness Index ASTM E 313 0 -4.37
513-S-710 E Poly Propylene 19/09/2023 13:00 Irg 1010 ASTM D 6247 ppm 380 520 425
I 168 ASTM D 6247 ppm 750 1050 880
DHT 4A ASTM D 6247 ppm 250 350 270
Small ( 0.20 to 0.49mm2) Default No/1520 30 29
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.54 LOT
NO.H23I109
1
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 2 Elongate
Fused Pellet Default no/5kg 1 26
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36

Page 99 of 104
 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 E Poly Propylene 19/09/2023 13:00 Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.48
Volatile Matter Licensor ppm 500 235
Method
Yellowness Index ASTM E 313 0 -4.08
554-T-05B SUPERIOR 19/09/2023 13:30 Density at 15°C ASTM D 4052 kg/m3 788.4
KEROSENE
Initial Boling Point IS 1448:P 18 °C 160.3
(GRADE-A)-COQ
Percent Recovered below 200°C IS 1448:P 18 Vol % 78.0
Final Boiling Point IS 1448:P 18 °C 237.1
Temperature at 5% Volume IS 1448:P 18 °C 168.2
Recovery
Temperature at 10% Volume IS 1448:P 18 °C 169.1
Recovery
Temperature at 30% Volume IS 1448:P 18 °C 174.7
Recovery
Temperature at 50% Volume IS 1448:P 18 °C 181.9
Recovery
Temperature at 70% Volume IS 1448:P 18 °C 192.7
Recovery
Temperature at 90% Volume IS 1448:P 18 °C 214.9
Recovery
Temperature at 95% Volume IS 1448:P 18 °C 228.9
Recovery
Mercaptan Sulfur ASTM D 3227 mg/kg 99.00
Total Sulphur ASTM D 5453 ppm(w) 2200.0

Page 100 of 104

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-05B SUPERIOR 19/09/2023 13:30 Appearance Visual Clear and
KEROSENE bright.Free
(GRADE-A)-COQ from
un-dissolve
d
water,foreig
n matter
and other
visible
impurities
Color -Saybolt IS 1448:P 14 +20
553-MB-01E LIQUEFIED 19/09/2023 17:45 C2 Hydrocarbon ASTM D 2163 Vol % 1.17
PETROLEUM
C3 Hydrocarbon ASTM D 2163 Vol % 25.54
GAS-COQ
C4 Hydrocarbon ASTM D 2163 Vol % 72.23
C5 Hydrocarbon ASTM D 2163 Vol % 2.5 1.06
Density at 15°C IP 432 -2000 kg/m3 572.1
Total Volatile Sulphur ASTM D 3246 ppm(w) 140 25
Vapour Pressure at 40°C IP 432 -2000 kPa 520 1050 636
Caustic test IS 4576:2018 Pass
Note 10
Copper Strip Corrosion for 1 hrs @ ASTM D 1838 1b
38°C
Free Water Content Visual None
Hydrogen Sulfide ASTM D 2420 Pass
Odour IS 4576:2018 Adequate
Note:12
Volatility:Evaporation Temp in°C for IS 1448:P 72 °C 2.2 0.6
95%v at760mm
513-S-710 B Poly Propylene 19/09/2023 19:00 Irg 1010 ASTM D 6247 ppm 380 520 405

Page 101 of 104

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 B Poly Propylene 19/09/2023 19:00 I 168 ASTM D 6247 ppm 750 1050 910
DHT 4A ASTM D 6247 ppm 250 350 305
Small ( 0.20 to 0.49mm2) Default No/1520 30 30
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.24
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 4 Triplet fused
Fused Pellet Default no/5kg 1 30
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 36
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.44
Volatile Matter Licensor ppm 500 240
Method
Yellowness Index ASTM E 313 0 -4.03
554-T-04B MOTOR 19/09/2023 21:50 Aromatic Content IS 1448:P 23 Vol % 35 30.3
GASOLINE
Benzene Content ASTM D 3606 Vol % 1 0.96
(BS-VI)-COQ
Copper Strip Corrosion for 3 hrs @ IS 1448:P 15 Rating 1b
50°C
Density at 15°C ISO 12185 kg/m3 720 775 743.3
Percent evaporated at 70°C (E 70°C) ASTM D 86 Vol % 10 45 34.2
Percent evaporated at 100°C (E ASTM D 86 Vol % 40 70 54.6
100°C)

Page 102 of 104

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
554-T-04B MOTOR 19/09/2023 21:50 Percent evaporated at 150°C (E ASTM D 86 Vol % 75 87.2
GASOLINE 150°C)
(BS-VI)-COQ Final Boiling Point ASTM D 86 °C 210 194.3
Residue ASTM D 86 Vol % 2 1.0
Lead Content (Pb) ASTM D 5059 g Pb/l 0.005 <0.005
Olefin Content IS 1448:P 23 Vol % 21 13.0
Oxidation Stability IS 1448:P 28 min 360 >360
Oxygen content ASTM D 4815 Wt% 3.7 0.15
Ether containing five or more C ASTM D 4815 Vol % 15 0.65
atoms per molecule
Reid Vapour Pressure @ 38°C ASTM D 5191 kPa 60 56.7
Total Sulphur ASTM D 5453 mg/kg 10 6.5
Appearance Visual Clear and
bright.Free
from
un-dissolve
d
water,foreig
n matter
and other
visible
impurities
Engine intake system cleanliness IS 2796:Note MFA Used
5
Motor Octane Number (MON) ASTM D 2700 81 82.4
Research Octane Number (RON) ASTM D 2699 91 91.8
Vapour Lock Index (VLI) Calculation 950 806.4
Color Visual Orange
Gum Content (Solvent washed) IS 1448:P 29 g/m³ 40 12.0

Page 103 of 104

 HPCL-MITTAL ENERGY LIMITED
DAILY EXECUTIVE REPORT

Reporting Period: From 00:41 hrs on 19-Sep-23 to 08:41 hrs on 20-Sep-23 Report Date: 20-Sep-23 8:41 hrs

Refinery Product
Sampling Name of Draw Date/ Test Specification Observed
Parameters UOM
Point Sample Time Method Results Comments
Min Max
513-S-710 F Poly Propylene 20/09/2023 0:00 Irg 1010 ASTM D 6247 ppm 380 520 410
I 168 ASTM D 6247 ppm 750 1050 925
DHT 4A ASTM D 6247 ppm 250 350 285
Small ( 0.20 to 0.49mm2) Default No/1520 30 29
CM2
Medium ( 0.5 to 1.50mm2) Default No/1520 2 2
CM2
Melt Flow Rate ASTM D 1238 g/10min 3.10 3.70 3.21
Fines Default Not Present
Loos-Forign/ Brown / Black & Others Default no/5kg 1 0
Fused Pellet Default no/5kg 1 31
Tails Default no/5kg 3 0
Fine Embedded BP(0.1-0.5mm) Default no/5kg 1 0
Big Embedded BP(>0.5mm) Default no/5kg 0 0
pellet Count Default No/Gm 34 42 34
Xylene Solubility ASTM D 5492 Wt% 3.0 4.0 3.48
Volatile Matter Licensor ppm 500 230
Method
Yellowness Index ASTM E 313 0 -4.25
# of Samples in Unit: 10
# of Analytes in Unit: 164

Total # of Samples: 315

Total # of Analytes: 1,786

Page 104 of 104