ATTACHMENT 1

ANNEX I
TO
CONTRACT SPECIFICATION APPENDIX XIII
LABORATORY CHEMICAL TESTING REQUIREMENTS

1. SOIL
Sample Report
Parameter Constituent Instrument Used by ATS Method used by ATS
No. issued

pH pH in soil and waste pH Meter ISO10390 24168-001

Conductivity Specific Electrical Conductivity In soil (Salinity) E.C Meter ISO 11265 24168-001
Moisture Content Moiosture Content Gravimetric Analysis ASTM D 2216 29968-001
Density Dry Bulk Density Gravimetric Analysis ASTM D 7263-09 29968-001
Determination of unsaturated hydraulic conductivity Wall and stand pipe
Hydraulic Conductivity (permeability) and water-retention charactristic Wind's conductivity ASTM D6391 24171-001
Evaporation Method meter/permeameter
Particle Size
Determination of PSD in mineral soil material Set of ASTM/BS Sieved BS 1377-2 / ASTM D422 24687-002
Distribution
Total PHC n-Hexane Extractable Meterial (Oil & Grease) Automated Soxhlet US EPA 9071 B 28274-001. Rev1
TPH reported as Saturated, Aromatic, Resins & TLC FID PI-469, IP 143/IP-
TPH SARA NTS SARA 30496-003
asphsltenes 368
Total Carbon Total Organic and Inorganic Carbon (TOC, TIC) TOC / TN Analyser ISO 10694:1995 29545-001
Extractable Aliphatics C10-C16, C16-C35, >C35 GC-FID US EPA 8015 C 29645-001
Polynuclear Aromatic Hydrocarbon (EPA 16:
Acenapthene, Acenaphthylene, Anthracene, Pyrene,
Benzo (a)pyrene, Benzo (a)Anthracene, Phenanthrene,
Extractable Aromatics GC-MS US EPA 8015 C 29646-001
Chrysene,Fluorene, Benzo(b) Fluoranthene, Benzo(ghi)
perylene, Napthalene, Benzo(k)fluoranthene, Dibenzo
(a,h) anthracene, Fluoranthene, indeno (13-cd) pyrene)
Aluminium, antimony, Arsenic, Barium, Beylium, Boron,
Cadmium, Calcium, Chromium, Cobalt, Copper, Iron,
Lead, Lithium, Magnesium, Magnese, Mercury,
Metals ICP-OES EPA 3051A, EPA 6010D 221108-12
Molyndenum, Nickel, Phosphorus, Potasium, Silica,
Selenium, Silver, Sodium, Strontium, Thalium, Tin,
Titsnium, Tugsten, Vanadium, Zinc
Chloride DISCRETE ANALYSER ISO 15923-1 28537-001
Fluoride DISCRETE ANALYSER ISO 15923-1 28537-002
Nitrite-N DR 6000 HACH 8507 28537-002
Nitrate-N DISCRETE ANALYSER ISO 15923-1 28537-002
Inorganic Anions
o-Phosphate DISCRETE ANALYSER ISO 15923-1 28537-002
Sulfate DISCRETE ANALYSER ISO 15923-1 28537-001
Cyanide SFA US EPA 335.4 28537-002
Carbonate (CaCO3, Acid Soluble Carbonate) Manual BS 1377-3 29665-002
Total Nitrogen TOC / TN Analyser ASTM D5176-91 -
Phosphorus ICP-OES EPA 3051A, EPA 6010D 221108-12
Nutrients
Potasium ICP-OES US EPA 6010 B 221108-12
Sodium ICP-OES US EPA 6010 B 221108-12

2. WATER
Sample Report
Parameter Constituent Instrument Used by ATS Method used by ATS
No. issued
pH pH In Liquids pH Meter APHA 4500 H+ B 29201-002
Electrical Conductivity Specific Conductance (salinity) E.C Meter APHA-2510 B 29201-002
Color Spectrophotometeric DR 6000 (HACH) HACH 8025 26941-001
Temperature Thermometric Thermometer APHA 2550 A 26941-001
LDO101 User Manual,
Oxygen Desolved Oxygen (Membrane Electrode) Electrode 29201-002
HACH 10360
Turbidity Formazin Turbidity TL2300 turbidimeter Method 2130B 26941-001
TSS Total Suspended Solids Filtration apparatus + Oven APHA 2540 D 25578-001
 Total Dissolved solids by drying method Filtration apparatus + Oven APHA 2540 C 29201-002
TDS
Total Dissolved solid by electrode method Electrode HACH 8160 29201-002
COD Chemical Oxygen Demand COD digation reactor APHA 5220 D 25578-001
TOC Total Organic Carbon TOC / TN Analyser APHA 5310B 28033-001
DOC Dissolved Organic Carbon TOC / TN Analyser APHA 5310B 28033-001
Total PHC Oil & Grease Gravimetric Analysis ASTM D7678-11 25578-001
Aluminium, antimony, Arsenic, Barium, Beylium, Boron,
Cadmium, Calcium, Chromium, Cobalt, Copper, Iron,
Metals ICP-OES US EPA 6010 D 29201-002
Lead, Lithium, Magnesium, Magnese, Mercury,
Molyndenum, Nickel, Phosphorus, Potasium, Silica,
Nitrite-N APHA 4500 NO2-B 26941-001
Nitrate-N APHA 4500 NO3-F 26941-001
Bromide APHA 9221 B&C 29201-002
DISCRETE ANALYSER
Chloride APHA 4500 CL 29201-002
Fluoride APHA 4500F-D 26941-001
o-Phosphate-P APHA 4500 P-E 29201-002
Cyanide SFA ANALYSER APHA 4500 CN-F 29201-002
Inorganic Anions
Total Nitrogen TOC / TN Analyser DIN EN 12260 26742-001
Sulfate UV SPECTRO APHA 4500 SO4-E 29201-002
Sulfide UV SPECTRO APHA 4500 S2-F 25578-001
Sodium bicarbonate
Carbonate Autotitrater APHA 2320 B 29201-001
Calcium Carbonate Autotitrater APHA 2320 B 29201-001
Total Alkalinity Autotitrater APHA 2320 B 29201-001
Alkalinity Acid Binding Capacity Autotitrater APHA 2320 B 29201-001
Chlorine Total Residual Chlorine spectrophotometer APHA 4500-Cl G. 25578-001
BOD Biological Oxygen Demand BOD Track with Incubator APHA-5210 D 25578-002