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  • Typical Column Profiles

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    Hector Chamate
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    Distillation practices involve separating mixtures based on differences in boiling points. The key steps are: 1) A mixture is fed into the column and vaporizes, with heavier components collecting near the bottom and lighter ones rising to the top. 2) Vapors from the top are condensed and returned as reflux to refine the separation. Liquid from the bottom is boiled as reboiled to drive the process. 3) Concentration and temperature profiles show components separating as the mixture travels up or down the column during distillation or fractionation of binary, complex, or multi-component mixtures.

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    Distillation practices involve separating mixtures based on differences in boiling points. The key steps are: 1) A mixture is fed into the column and vaporizes, with heavier components collecting near the bottom and lighter ones rising to the top. 2) Vapors from the top are condensed and returned as reflux to refine the separation. Liquid from the bottom is boiled as reboiled to drive the process. 3) Concentration and temperature profiles show components separating as the mixture travels up or down the column during distillation or fractionation of binary, complex, or multi-component mixtures.

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    4 views10 pages

    Typical Column Profiles

    Uploaded by

    Hector Chamate
    Distillation practices involve separating mixtures based on differences in boiling points. The key steps are: 1) A mixture is fed into the column and vaporizes, with heavier components collecting near the bottom and lighter ones rising to the top. 2) Vapors from the top are condensed and returned as reflux to refine the separation. Liquid from the bottom is boiled as reboiled to drive the process. 3) Concentration and temperature profiles show components separating as the mixture travels up or down the column during distillation or fractionation of binary, complex, or multi-component mixtures.

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    DISTILLATION PRACTICES

    FLOW RATE PROFILES


    DISTILLATION PRACTICES
    L0 V0 + VFeed
    CONDENSER D
    EXTERNAL
    DISTILLATION REFLUX
    COLUMN
    L0

    REFLUX DRUM L0

    Vapor
    LFeed V0 + VFeed
    FEED FEED L0 + LFeed
    LFeed VFeed VFeed
    Liquid D
    V0
    V0
    M

    R
    REBOILER

    V0 L0 + LFeed
    R FLOW RATE
    DISTILLATION PRACTICES

    CONCENTRATIONS
    AND TEMPERATURE PROFILES
    BINARY DISTILLATION
    DISTILLATION PRACTICES
    CONCENTRATIONS TEMPERATURE

    CONDENSER

    DISTILLATION
    EXTERNAL
    REFLUX L0
    COLUMN
    L0

    REFLUX DRUM

    A
    Vapor
    BINARY
    MIXTURE
    Liquid A
    A B 100%

    B
    M

    R
    REBOILER

    100% 0 1 TBOILING A TBOILING B


    B
    DISTILLATION PRACTICES
    CONCENTRATIONS TEMPERATURE

    CONDENSER

    EXTERNAL
    DISTILLATION REFLUX
    COLUMN
    L0

    Column Stage

    Column Stage
    REFLUX DRUM

    A
    Vapor
    BINARY
    MIXTURE
    Liquid A
    A B 100%
    Sidedraw
    B
    M

    REBOILER

    0 1
    100% xA xB Tsidedraw
    B
    DISTILLATION PRACTICES

    CONCENTRATIONS PROFILES
    COMPLEX MIXTURES
    DISTILLATION PRACTICES

    TOVHD TBTM

    COLUMN TEMPERATURE

    TEMPERATURE

    BPA BPB BPC BPD BPE

    LIGHT HEAVY
    KEY KEY

    BP : Boiling Point
    COMPLEX MIXTURES
    DISTILLATION PRACTICES
    MOLAR FRACTION

    CONDENSER LIGHT
    KEY
    EXTERNAL A C
    DISTILLATION REFLUX
    COLUMN
    L0

    RECTIFICATION
    REFLUX DRUM
    BPC

    Vapor
    A, B, C
    FEED
    D, E E
    Liquid A, B, C

    BPD

    STRIPPING
    D
    M

    HEAVY
    KEY
    REBOILER

    0 1
    D, E
    DISTILLATION PRACTICES

    TEMPERATURE PROFILE :
    COMPLEX MIXTURES
    DISTILLATION PRACTICES
    OVERHEAD
    CONDENSER
    PRODUCT
    EXTERNAL DEW POINT
    REFLUX
    1 1

    16 16
    REFLUX DRUM

    24 24
    Vapor

    FEED 25 25

    Liquid DISTILLATE
    34 34

    42 42
    M

    REBOILER BTM PRODUCT


    BUBBLE POINT
    TEMP
    RESIDUE

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