UNIVERSIDAD NACIONAL DE COLOMBIA INFORME:

FACULTAD DE CIENCIAS
DIRECCION CURRICULAR DE QUIMICA **23RQ-223
LABORATORIO DE SERVICIOS A ESTUDIANTES DE POSGRADO (LASAP) (LAB.233)
ID MUESTRA:
DM1 (OSCAR)
Distancia Focal (10x)
Fri Sep 22 16:27:18 2023 (GMT-05:00) Collection time: Tue Sep 19 13:47:34 2023 (GMT-05:00)
14

13

12

82.14
11

1471.12

225.94
10

525.96
9
Raman Intensity (cps)

104.75
8

647.63
7
3363.98

1445.90
6

912.26
1636.21
5

583.77
2448.12

3500 3000 2500 2000 1500 1000 500

Raman shift (cm-1)
EXPERIMENT INFORMATION: Exposure time: 60.00 sec
Experiment filename: C:\My Documents\Omnic\VRParam\dxr_rm_default.exp Number of exposures: 2
Experiment title: Default - DXR Raman Microscope Number of background exposures: 512
Experiment accessory: Microscope
Laser: 532 nm
SPECTRAL QUALITY RESULTS: Grating: 900 lines/mm
CCD overflow test passed Spectrograph aperture: 50 µm pinhole
The spectrum is weak Laser power level: 1.0 mW
Fluorescence test passed
Photobleaching was detected in the spectrum
Spectrum appears to have sample heating
Sample burning test passed

Collect Sample
Background collected: Fri Dec 09 11:39:58 2022 (GMT-05:00)
Final format: Shifted spectrum (cm-1)
Calibrated: Tue Sep 19 10:28:06 2023 (GMT-05:00)
Resolution: 1.9285 Raman shift (cm-1) from 63.6406 to 3426.8867
Camera temperature: -50 C
White light corrected
Fluorescence corrected:
Polynomial order: 5
Cosmic ray threshold: Medium
Smart background used
Auto exposure used
SYSTEM STATUS
Instrument Status Pass Date Tested: Tue, Sep 19 2023
Scheduled Maintenance Disabled

EL PRESENTE INFORME SOLO ES APLICABLE A LA MUESTRA ENTREGADA PARA ANALISIS Y NO CONSTITUYE

UN CONCEPTO TECNICO DE LA MISMA.

ANALISIS:
WALTER ALIRIO MEDINA MARTINEZ
QUIMICO UN
MATRICULA PROFESIONAL: PQ2862