100-00251MicroLab 30 - 40 User - S Guide Rev B

MicroLab 30/40 User's Guide
Doc. p/n 100-00251 Rev. B

September 2017
Spectro Scientific - An ISO 9001:2008 Company

One Executive Drive, Suite 101, Chelmsford, MA 01824 | Tel. (+1) 978 431 1120
www.spectrosci.com
Preface
Copyright Notice
© 2017 Spectro Scientific. All rights reserved.
The information and descriptions in this document are the sole property of Spectro Scientific and
may not be copied, reproduced, disseminated, or distributed without explicit written permission from
Spectro Scientific.
The statements, configurations, technical data, and recommendations in this document are believed
to be accurate and reliable at the time of this publication, but Spectro Scientific assumes no
responsibility or liability for any errors or inaccuracies that may appear in this document.
Spectro Scientific is not responsible for any infringement of patents or other rights of third parties
that may result from the use of this document. The content of this document is furnished for
informational purposes only, is subject to change without notice, and does not represent a
commitment or guaranty by Spectro Scientific.
Spectro Scientific makes no warranty, express or implied, with respect to the content of this
document. Spectro Scientific shall not be liable for any loss or damage, including consequential or
special damages, resulting from any use of this information, even if loss or damage is caused by
Spectro Scientific as a result of negligence or any other fault.
Warranty
Spectro Scientific warrants to the original purchaser that all Spectro Scientific instruments will be
free from defects in material or workmanship for a period of one year from date of invoice.
Spectro Scientific's sole obligation and your exclusive remedy under this Limited Warranty and, to
the extent permitted by law, any warranty or condition implied by law, shall be the repair or
replacement of parts, without charge, that are defective in material or workmanship and that have
not been misused, carelessly handled, abnormal conditions or operation, accidents or acts of God,
or misrepaired by persons other than Spectro Scientific or Authorized Service Provider.
To make a claim under this Limited Warranty, you must return the complete instrument,
transportation prepaid, to Spectro Scientific Factory Service Center or Authorized Service Location.
The determination of whether any product has been subject to misuse or abuse will be made solely
by Spectro Scientific. If a hardware defect arises and a valid claim is received within the limited
warranty period, at its option and to the extent permitted by law, Spectro Scientific will either:
(1) repair the hardware defect at no charge, using new parts or refurbished parts that are equivalent
to new in performance and reliability or
(2) exchange the product with a product that is new or refurbished that is equivalent to new in
performance and reliability and is at least functionally equivalent to the original product, or
(3) refund the purchase price of the product.
Spectro Scientific may request that you replace defective parts with user-installable new or
refurbished parts that Spectro Scientific provides in fulfillment of its warranty obligation. A
ii
replacement product or part, including a user-installable part that has been installed in
accordance with instructions provided by Spectro Scientific, assumes the remaining warranty of
the original product.
After an issue with the unit has been verified, the offending module where the issue originates
should be returned to the factory for repair by authorized Spectro personnel.
Patents
U.S.
9,500,658; 9,274,041; 9,234,829; 9,176,041; 8,867,034; 8,661,878; 8,384,895; 8,079,250;
7,518,720; 7,495,761; 7,385,694; 7,307,717; 7,237,431; 7,184,141; 7,019,834; 6,873,411;
6,707,043; 6,455,850; 6,452,179; 6,104,483; 2,640,059; 2,340,097.
Others
163,024; 141,344; P5707513; EP1105710B1; AU2003257512B2; AU199953978B2.
Spectro Scientific Phone Numbers
Main Number (U.S.) (+1) 978-486-0123
Technical Support: (U.S.) (+1) 978-431-1130
Main Number (China) - 8610-6785-7242
Safety Information
This device must be used by trained operators, according to the instructions presented in this
manual.
To reduce the risk of injury, do not open the instrument enclosure or remove access
panels.
There are no user serviceable parts inside. Refer servicing to qualified service personnel.
Improper use could cause physical harm or damage to the device. Pay attention to all warning
labels and messages.
This device incorporates a sensor which operates by means of a Class 3R laser diode
that has a visible beam.
The sensor unit should not be opened under any circumstances.
• Average Power: 4.2 mW inside the sensor

• Maximum Power: 5 mW
• Wavelength: 670 nm
This product is certified as a Class 1 laser product under U.S. Department of Health and Human
Services (DHHS) Radiation Performance Standard according to the Radiation Control for
Health and Safety Act of 1968. This means that the product does not produce hazardous laser
radiation.
iii
For United States users: This product is certified as a Class I laser product under the Regulation
Performance Standard according to the Food, Drug and Cosmetic Act of 1990. This means that the
device does not produce hazardous laser radiation. The label shown below indicates compliance
with the CDRH regulations:
The laser safety label is located inside the instrument on the laser sensor, visible when the rear ser-
vice panel has been removed by authorized service personnel
Since radiation emitted by the laser is completely confined within protective housings and external
covers, the laser beam cannot escape from the device during any phase of the user operation.
There is no possibility of danger from the laser provided that the equipment is operated according to
the instructions in this manual.
Do not attempt to bypass the spark door locks. High voltages exist inside the spark chamber
when a test is running.
The plasma created is extremely hot. Allow a minimum of 20 seconds for the electrodes to
cool before working anywhere around them.
Use in a well-ventilated area. The device produces ozone when high voltage is arcing across the
electrodes
For United States users:
US OSHA regulations state that 0.100 ppm is the maximum allowable ozone concentration in
industrial working areas: permissible human exposure – 8 hours per day, 6 days a week
The MicroLab 30/40 was tested for ozone emissions in a closed office space of 73 cubic meters (864
cubic feet) with low air ventilation and with the analyzer in full operational mode. The resulting ozone
emission is < 0.045 ppm measured directly at the exhaust vent.
Avoid fluid contact with the skin and eyes
Wear appropriate safety equipment such as gloves, an apron and safety goggles
Never use the MicroLab 30/40 to test anti-freeze, water, brake fluid, Phosphate Ester-
based hydraulic fluids, Skydrol, or Blow-Out Preventer fluids as these fluids will cause
irreparable damage.
Test used fluids from diesel and gasoline engines, gearboxes, hydraulics and trans-
missions only. Do not attempt to test flammable liquids such as gasoline, kerosene, or
diesel fuel.
Do not allow fluids to enter groundwater or sewers. In the event of a spill,

1. Apply an absorbent material to the spill
2. Place the material in an appropriate chemical waste container
3. Follow local, state, and federal regulations for disposal
iv
Document Conventions
There are three types of special instructions that appear in this manual. They are there to protect
the user and the device and also to emphasize key points or instructions.
An operating procedure or practice that may cause damage to the device, injury to the
user, or have a catastrophic impact on testing fluids or analyzing results if ignored.
An operating procedure or practice that may have a serious impact on testing fluids or
analyzing results if ignored.
An item of special interest, like a time-saving tip.
v
Document Revision History
Revision Date Description
A April 2016 Initial public release
B September 2017 Patents list updated.

Test result output page updated.
Reset button on the side connector panel has been
removed as it is no longer needed.
The battery backup/UPS has been replaced with a line
conditioner/surge protector.
Blank report paper is no longer provided.
The Epson printer is now an available option
An End-User License Agreement has been added.
An extended flush sequence has been added.
Users are able to replace certain report data with data
from external analyzers like the FerroCheck.
Recommendation to keep the MicroLab powered up
whenever possible.
Caution to keep the area below the spark stand clear
of debris to avoid blocking the filter.
Warnings have been added in several places to allow
electrodes to cool before working around them.
Manager-level admin settings have been added
describing accessible screens in the Admin Tab.
Instructions have been added to create and export
data as a .csv file.
Instructions for loading printer drivers have changed.
vi
End User License Agreement (EULA)
1. Definitions
"Software” means computer programs provided to Licensee by SPECTRO SCIENTIFIC directly
or indirectly, and any related materials, including, but not limited to, Documentation related
thereto, and any subsequent revisions, improvements or updates.
"Documentation" means any information which is provided to Licensee in writing or fixed in other
tangible form, including, but not limited to, logic diagrams, manuals, lists, schematics, drawings
and marketing, development, maintenance, pricing and/or product information.
2. Scope of Authorized Use
2.1: Software is furnished under a personal, non-transferable, non-exclusive license solely for
Licensee's own use only on the Spectro Single unit ("Unit") on which Software is first installed.
2.2: Licensee shall not copy nor permit any party to copy Software. If Licensee is unable to
operate Software on the Unit due to an equipment malfunction, the Software may be used
temporarily on another Unit or Configuration during the period of equipment malfunction.
Licensee shall not sub-license, transfer or otherwise make software available to any third party.
Licensee shall not modify, de-compile, disassemble or otherwise reverse engineer Software.
2.3: Licensee shall allow SPECTRO SCIENTIFIC reasonable access to its premises to audit
Licensee's compliance with this Agreement.
2.4: Licensee agrees that any Software coming into Licensee’s possession shall be subject to this
Agreement, and Licensee shall pay applicable license fees, if any, including any Monthly License
Fees, to SPECTRO SCIENTIFIC for the use of such Software.
3. Title and Ownership: Confidentiality
Title to, ownership of, and all patent, copyright, trade secrets and other intellectual property rights
in the Unit, Software or any of it parts shall at all times remain with SPECTRO SCIENTIFIC.
Software is confidential and proprietary and Licensee shall observe the proprietary nature
thereof.
Licensee shall not disclose, provide or otherwise make available Software or any part or copies
thereof to any third party. Licensee shall take action by instruction or agreement with its
employees who are permitted access to Software, to protect the confidentiality of the Software.
Licensee shall keep Software and such material secure, and prevent unauthorized access,
copying, or use thereof. Licensee agrees to notify SPECTRO SCIENTIFIC immediately of any
unauthorized knowledge, possession, or use of Software or any such materials by any person or
entity.
4. Payment, Shipment, and Risk of Loss
Licensee shall pay invoiced license fees, including tax on the license fee, for use of the Software,
within thirty (30) days after shipment.
vii
5. Limited Warranty; Warranty Disclaimer
SPECTRO SCIENTIFIC warrants that all Software will substantially conform, for a period of thirty
(30) days from shipment, to SPECTRO SCIENTIFIC's specifications at shipment.
SPECTRO SCIENTIFIC does not warrant Software will be error free or that all errors will be
remedied. SPECTRO SCIENTIFIC's entire liability and Licensee's exclusive remedy under this
warranty shall be for SPECTRO SCIENTIFIC to make reasonable efforts to remedy, in a manner
deemed suitable to SPECTRO SCIENTIFIC, any non-conformance reported in writing within the
warranty period.
NEITHER SPECTRO SCIENTIFIC NOR ITS THIRD PARTY VENDOR (IF ANY) MAKE OR
GIVE ANY OTHER REPRESENTATION OR WARRANTY REGARDING THE SOFTWARE,
INCLUDING EXPRESS OR IMPLIED WARRANTIES OF MERCHANTABILITY AND FITNESS
FOR A PARTICULAR PURPOSE.
6. Limitation of Remedies
IN NO EVENT SHALL SPECTRO SCIENTIFIC OR ITS THIRD PARTY VENDOR (IF ANY) BE
LIABLE FOR SPECIAL, INDIRECT, INCIDENTAL OR CONSEQUENTIAL DAMAGES ARISING
OUT OF OR IN CONNECTION WITH THE USE OR PERFORMANCE OF SOFTWARE OR
UNITS.
LICENSEE ACKNOWLEDGES AND AGREES THAT THE SOFTWARE AND UNIT IT
OPERATES ON ARE BEING PROVIDED HEREUNDER FOR OIL ANALYZING ACTIVITIES
ONLY AND SPECTRO SCIENTIFIC HAS NO LIABILITY OR RESPONSIBILITY TO PROVIDE
INFORMATION OR DATA RELATED TO THE OPERATION OR CONDITION OF EQUIPMENT
OR MACHINERY BEING OPERATED.
7. Infringement Indemnity
SPECTRO SCIENTIFIC disclaims all liability for copyright, patent or other infringement, including
any incidental or consequential damages.
8. Termination
8.1: Licenses shall become effective upon Software shipment and terminate at such time as
Licensee discontinues use of Software on the Unit or Configuration, or upon sale, lease or transfer
by operation of law or otherwise, of the Unit.
8.2: If Licensee fails to cure any breach of this Agreement, including failure to pay any required
initial, monthly, or other license fees, within (10) days after receipt of written notice of such breach,
the license(s) for the Software related to such breach shall be terminated.
8.3: Upon termination of any license, Licensee shall immediately terminate use of such Software
and immediately return or destroy at SPECTRO SCIENTIFIC’s direction all copies of such
Software and other proprietary materials and certify in writing as to such destruction or return.
Sections 3, 5, 6, and 7 shall survive termination of this Agreement.
viii
9. Miscellaneous
9.1: This Agreement shall be governed by the laws of the Commonwealth of Massachusetts,
excluding choice of law provisions. This Agreement states the entire understanding between the
parties as to Software licensed hereunder.
9.2: Licensee agrees not to export Software, or re-export or resell Software from or in country of
installation, without first complying with all applicable export laws and regulations.
ix
Certificate of Conformity
x
Table of Contents
Preface ii
Copyright Notice ii
Warranty ii
Patents iii
U.S. iii
Others iii
Spectro Scientific Phone Numbers iii
Safety Information iii
Document Conventions v
Document Revision History vi
End User License Agreement (EULA) vii
1. Definitions vii
2. Scope of Authorized Use vii
3. Title and Ownership: Confidentiality vii
4. Payment, Shipment, and Risk of Loss vii
5. Limited Warranty; Warranty Disclaimer viii
6. Limitation of Remedies viii
7. Infringement Indemnity viii
8. Termination viii
9. Miscellaneous ix
Certificate of Conformity x
1 MicroLab Fully Automated Oil Analyzer 1
Chemistry 1
Viscosity 1
Elemental Analysis 2
Particle Counter 2
2 Unpacking, Installing and Configuring the MicroLab 30/40 3
Unpacking Cautions and Best Practices 3
Packing List and Parts/Test Supplies Ordering Information 4
MicroLab 30/40 External Features 5
Installing the MicroLab 6
Electrical Requirements 7
Connecting a USB Printer 8
Loading Printer Drivers 8
Completing the Setup 8
Powering Up the MicroLab 10
Powering Down the MicroLab Correctly 10
xi
Login Access 10
Manager-Level Administrator Settings 11
Software Defaults 11
Report Defaults 12
Oil and Capacity Defaults 13
3 Analyzing Used Fluid Samples 15
Daily Set-Up Procedures 16
Empty the Waste Bottle 16
Check the CheckFlush Bottle Fluid Level 16
Check the Printer Paper 16
Clean the Sipper Screen Filter 17
Clean the Collimator Lens 19
Run a Manual Flush 20
Run a Check Base Line Test 21
Collecting a Used Fluid Sample 23
Required Sample Fluid Volumes 23
Filling the Sample Bottle 23
Preparing Samples 24
MicroLab 30 Sample Preparation 24
MicroLab 40 Sample Preparation 24
Testing a Fluid Sample 25
Select a Testing Option Screen 30
Select a Component Screen 30
The Analysis Cycle 36
Extended Flushing Routines 37
High Metals Detected 37
High Soot Detected 38
High Particle Counts Detected 38
Adjusting the Extended Flushing Settings 38
Generating MicroLab Reports 38
Manual Parameter Entry 39
Example Full Report 40
4 Weekly Tasks 41
Measure the Electrode Gap 41
Check the Lower Electrode Height 41
Run an IR Night Flush 42
5 Maintaining the Electrodes 43
Description 43
Cleaning the Electrodes 44
xii
Measuring the Electrode Gap 46
Resetting the Electrode Gap 47
Monitoring the Lower Electrode Height 47
Replacing the Electrodes 48
6 Standardization Procedures 50
Check Base Line 51
Test Requirements 51
Procedure 51
Verify Metals 52
Procedure 52
Standardize Metals 55
Procedure 55
Extended Metals Option 56
Standardizing the Viscometer 57
7 Over-Pressure Sampling 59
8 Clean Oil Sampling 62
9 Manual Flushing Options 67
Viscometer Flush 67
Short Flush 67
Medium Flush 67
Long Flush 67
IR Night Flush 68
10 Printing Historical Reports 69
View Customers/Units/Components 69
11 Troubleshooting 72
Contacting the Support Team 72
Will Not Pass the Standardization 72
Will Not Pass Base Line or Verify Metals 73
High Elements Detected at the End of the Sample 74
Wear Metals Results are in Question 75
Viscometer Issues 75
A Understanding Your Reports 77
Engines 77
Transmissions 78
B Replacing the Spark Box Air Filter 79
C Exporting Data as a .CSV File 81
xiii
1 MicroLab Fully Automated Oil
Analyzer
The MicroLab combines automation and artificial intelligence to provide a simplified oil analysis tool.
The user inputs the sample information on the integrated touchscreen and then an automated flu-
idics system seamlessly takes the sample through the multi-component analysis and self-cleaning
process. The embedded expert system then provides a complete data analysis with color-coded
alarm limits along with diagnostic statements and maintenance recommendations.
Chemistry
The MicroLab infrared spectrometer measures six key parameters which indicate potential oil
degradation and contamination.
Both the MicroLab 30 and 40 provide:
• Oil degradation: Oxidation, Nitration, TBN
• Oil contamination: soot, water, glycol
Viscosity
The MicroLab Dual Temperature Viscometer (DTV) provides kinematic viscosity analysis which can
help identify potential oil degradation or contamination.
Both the MicroLab 30 and 40 provide:
• Kinematic viscosity at 40C and 100C
• Viscosity Index (VI)
1
Elemental Analysis
The MicroLab Optical Emission Spectrometer quantifies wear metals caused from mechanical
components, as well as other elements from oil additives or sources of contamination.
• MicroLab 40 analyzes 20 elements including wear, contamination and additives
• MicroLab 30 analyzes 10 elements (wear and contamination) and is upgradable to
include all 20 elements
Basic Metals Extended Metals

Aluminum (Al) Barium (Ba)
Chromium (Cr) Boron (B)
Copper (Cu) Calcium (Ca)
Iron (Fr) Magnesium (Mg)
Lead (Pb) Manganese (Mn)
Molybdenum (Mo) Nickel (Ni)
Potassium (K) Phosphorus (P)
Silicon (Si) Titanium (Ti)
Sodium (Na) Vanadium (V)
Tin (Sn) Zinc (Zn)
Particle Counter
The MicroLab 40 model is equipped with a particle counter to measure particle contamination
which is crucial for maintaining hydraulic systems, compressors and turbines.
The MicroLab 40 measures:
• Gross particle count distribution
• ISO particle size
2
2 Unpacking, Installing and Configuring
the MicroLab 30/40
This section covers the following topics:
Unpacking Cautions and Best Practices on page 3
Packing List and Parts/Test Supplies Ordering Information on page 4
MicroLab 30/40 External Features on page 5
Installing the MicroLab on page 6
Electrical Requirements on page 7
Connecting a USB Printer on page 8
Completing the Setup on page 8
Powering Up the MicroLab on page 10
Powering Down the MicroLab Correctly on page 10
Login Access on page 10
Manager-Level Administrator Settings on page 11
Unpacking Cautions and Best Practices

Note the dimensions of the shipping container before moving it to its final
location to ensure that you have adequate clearance through doors and
passages.
Always remove the waste container and CheckFlush bottle and
CheckFlush bracket prior to lifting or moving the MicroLab.
Use of a pallet jack or fork lift is strongly recommended.
Always use two or more people to lift or move the device as it is heavy
and weight distribution is uneven. Serious injury can result from trying to
move the MicroLab alone or from unsteady handling.
Do not lift using the rear panel edge or using the keyboard.
Lift by grasping the handle with one hand and the bottom of the chassis
with the other, and lifting with your legs.
3
Packing List and Parts/Test Supplies Ordering Information
Check the contents of the packing crate against the packing list and the following table. Use the
part numbers in the table to order replacement parts and consumable testing items.
Part Number Description QTY

200-00222 Line Conditioner - 120 VAC option
or 1
Line Conditioner - 230 VAC option
200-00223
P-11153 Universal Cable Kit 1
100-00234 MicroLab Best Practices Poster 1
100-00251 User Manual 1
22194-00 Filter Screen, 1.27 cm (1/2") Dia, #60 X 60 MESH, 304 SS 25
24086-00 Stainless Steel Brush for Electrodes 1
26338-00 Power Cord Adapter for Color Printers, 1.8 m (6 ft) 1
27230-00 USB Cable, 1.8 m (6 ft) 1
29002-05-ABS 150 ml (5 fl oz) ABS High Temp Sample Bottle W/38 ct Cap 300
29015-00 Hex Key, 3.96 mm (5/32") Plastic Handle Ball Dr 1
29021-00 MicroLab Input Form, 14 cm x 21.5 cm (5-1/2" x 8-1/2") 2
29033-00 Cleaning Swabs (Bag of 100) 15
29034-00 LDPE Tubing, 4.76 mm OD x 3 mm ID (3/16" x 0.118") 7
29036-00 Pump, Sample Extractor 1
29087-01 Test Standard, 0.94 L (32 fl oz) Bottle 1
29088-01 CheckFlush 3.7 L (1 gal) 8
29089-01 Low Viscosity Standard Fluid, 0.94 L (32 fl oz) Bottle 1
29090-01 High Viscosity Standard Fluid, 0.94 L (32 fl oz) Bottle 1
29422-00 Optional Epson Stylus C88+ Inkjet Printer - 110 VAC - 220 VAC 1
Extended Low Standard Fluid, 0.94 L (32 fl oz) Bottle. Not supplied with
29530-00 1
the MicroLab 30 Base Metals kit
Extended High Standard Fluid, 0.94 L (32 fl oz) Bottle. Not supplied with
29531-00 1
the MicroLab 30 Base Metals kit
29611-00 Waste Bottle, 1.89 L (64 fl oz) 1
29612-00 Adapter Kit, Remote Drain Port 1
29816-00 Hex Key, 1.27 mm (0.05") Lower Electrode Set Screw 1
29823-00 Long Sample Intake Straw, 350 Package, 142 mm (5.6") 1
29824-00 Kim Wipes, 11.4 cm x 21.5 cm (4.5" x 8.5") Box of 280 1
Ultrasonic Cleaner, B200 117VAC 50/60 Hz Branson 200. Supplied with
M97101A 1
MicroLab 40 Starter Kit, Extended Metals kit only
4
MicroLab 30/40 External Features
• Keyboard: Used for all data entry. The keyboard will drop flat when not in use.
• Touch-screen display. Used to select function buttons in the user interface.
• Sample stand. Remove the drip tray when using samples with the pressure cap on.
• Sipper nozzle. The sample bottle flow tube connection.
• Fluid filter housing. Contains a replaceable filter to strain impurities from the sample.
• Spark door. The spark stand and electrodes are located behind this door.
• Flush bottle bracket. Holds a container of fluid used to clean the fluid path after a test.
• USB connectors for a USB printer and/or a USB mouse to control menus (not supplied).
• On/off switch for the main power supply.
• Waste door. Access to a waste bottle that must be emptied every day and regularly
thereafter before it gets full.
5
Installing the MicroLab
The procedures described in this section are in accordance with the following specifications:
Physical Properties
Dimensions 74 cm x 66 cm x 66 cm (29 in x 26 in x 26 in)
Weight 54 Kg (120 lb)
Power Requirement
230 VAC / 5A / 50 Hz
Input
115 VAC / 9A / 50 - 60 Hz
Sample Size
Required 150 ml ( 5 fl oz )
Data Output
1 LCD Display
2 USB Printer port
3 Ethernet port
Environmental
Operational 4o C to 25o C (40o F to 77o F)
Storage 4o C to 50o C (40o F to 112o F )
Make sure your proposed location can accommodate the MicroLab. The device is designed to fit
on a counter-top or an optional cart and requires additional space for a printer.
You can use any USB printer with the MicroLab. An Epson Stylus C88 InkJet printer
is a suitable option available from Spectro Scientific - part number 29422-00.
Contact your sales professional for further information.
We recommend 0.5 m2 (5 ft2) of floor space leaving sufficient operating room around the sides.
Do not install the device closer than 15 cm (6") to any wall and do not obstruct the airflow through
the device.
The device is recommended for temperature-controlled indoor use only. Ideally, the temperature
inside the room should not vary more than 6o C over one hour and should not exceed 85%
humidity for prolonged periods.
Do not install the device in direct sunlight to avoid internal temperature extremes and/or possible
damage to the LCD screen.
6
Electrical Requirements
This section is for approved and qualified technicians only. Electricity can cause
injury or death.
1. Locate the Spectro Scientific label on the back of the Microlab to confirm you have a device
that matches the local power supply (115 VAC or 230 VAC):
2. A line conditioner/surge protector is supplied with the MicroLab for the correct utility voltage
in your country. Locate an appropriate utility power source as follows:
The system requires 3-wire (Hot, Neutral, Ground) single-phase input power of 230 VAC
+/- 10 VAC or 115 VAC +/- 5 VAC.
The minimum power requirement is 1100 W with the capability of handling spikes up to
1700 W per circuit.
Do not use extension cords.
Additional power conditioning should be utilized to maintain a clean power supply if you are
in a remote area that experiences frequent power surges or brown-outs or if you are
operating from generator power.
You can purchase a separate Uninterrupted Power Supply (UPS) which is rated for more
power stabilization and includes a battery backup feature which provides a short amount of
battery run-time for the analyzer so you can properly shut it down in the event of a power
outage.
This UPS is available from Spectro (PN: 26359-00 for 120v and PN: 26349-00 for 230v).
3. Determine the phase from the utility supply to the line conditioner by measuring the voltage
on each supply leg as follows:
The system requires single-phase power.

If the power is determined to be multi-phase, either the utility supply connector to the line
conditioner must be re-wired to single phase, or a converter must be used.
7
Phase Hot Neutral Ground
230 +/- 10 VAC <10 VAC <10 VAC
Single
115 +/- 5 VAC <5 VAC <5 VAC
120 +/- 5 VAC 120 +/- 5 VAC <10 VAC
Multi
60 +/- 5 VAC 60 +/- 5 VAC <5 VAC
Connecting a USB Printer

You can connect any USB printer to the MicroLab. A suitable Epson Stylus C88 InkJet
printer is available as an option from Spectro Scientific - part number 29422-00. Contact
your sales professional for further information.
1. Unpack the printer and install it in a suitable location.

2. Plug the power cord into any suitable electrical outlet
3. Connect a suitable USB cable between the printer and the USB connector on the back of
the MicroLab marked PRINTER:
4. Complete the printer setup in accordance with the manufacturer's instructions.

Loading Printer Drivers
When you connect the printer to the MicroLab and the analyzer is powered on with an internet
connection, the system will automatically search the internet for the appropriate print driver for
your printer or you can download the print driver on a separate computer to a thumbdrive and
load it into the MicroLab that way as well.
If you are using the Epson Stylus C88 printer there is an icon on the desktop for the print driver
which you can launch from there.
Completing the Setup
1. Ensure that all internal cables and plumbing are secure after shipping.
2. Install the CheckFlush bracket to the right side panel and connect the tube to the
CheckFlush bottle.
8
3. Place the waste container behind the door in the front panel under the waste outlet. There is
an external port equipped with a female 9.5 mm (3/8") -18 NPT connector that can be set up
by an approved engineer to allow for larger waste containers. A special tube is inserted
inside the waste door and this port then becomes active.
4. Check the electrode gap and make adjustments if necessary. See Maintaining the
Electrodes on page 43 for instructions.
5. MicroLab 40 only - unpack the ultrasonic bath and plug it into a suitable power outlet.
Fill the ultrasonic bath with fluid to a depth of at least 25 mm (1 in) before you power it on
otherwise damage may result.
6. Connect an internet cable (not supplied) between the MicroLab connector marked
NETWORK and an active Internet connection.
7. Connect the MicroLab INPUT POWER connector to the line conditioner.
The power cable must be a 3-conductor cable with an IEC320-C13 plug to match the
MicroLab input power connector.
Before you measure any used samples, a Standardize Metals procedure must be
performed. If you choose to have the installation carried out by a Spectro field
technician, this step will be done for you. Otherwise, you will need to perform this
step yourself.
See Standardize Metals on page 55 for instructions.
8. Power up as described below and test for internet access.
9
Powering Up the MicroLab
1. Locate the panel on the right side of the MicroLab housing the System Power switch:
2. Set the Power switch to ON. The switch will light up, and the computer will begin the boot
process.
Powering Down the MicroLab Correctly
Do not power down by simply shutting the System Power switch off. Follow these
steps instead.
1. Press the Shutdown button in the top right corner:
2. When the screen goes dark, flip the system power switch to OFF.
Login Access
There are 3 levels of login access from the Admin tab:
User Level Access: This is used for all operation functions and user maintenance of the
MicroLab. This provides access to the Data and Maintenance tabs on the Main Menu.
Manager Level Access: This allows access to several administrator settings in the Admin Tab
from the Main Menu.
Technician Level Access: This allows access to only factory trained technicians used for
support, repair, and advanced settings.
10
Manager-Level Administrator Settings
Click the Admin Tab on the Main Menu and enter your manager login credentials to access the
Administrator Settings screen:
Software Defaults
Software Defaults allows you to:
• Change the language of the MicroLab text
• Add a customer logo to show up on the home screen and the report
• Change the “WELCOME TO” message to list your company or department
• Enter your company contact info that will show up on a report
11
Report Defaults
Report Defaults allows you to:
• Change the image on the report to your company logo
• Set a time for the report to remain on the screen before closing
• Choose whether the report should always show historic sample info
• Auto print the report
• Choose the options you have to get the report – print only; print and export; print,
export and email
• These options are shown at the top of the screen when the report is displayed
• Choose the Modes to show on the Main Menu so you can hide any modes that do not
pertain to your equipment. For instance, if you are a vehicle maintenance shop you
might want to eliminate Railroad, Marine, Generator, and Industrial if you will never
have that type of equipment
• Report with limits will show the typical viscosity limits for the type of oil you tested in
addition to showing the actual result
12
Oil and Capacity Defaults
Oil and Capacity Defaults allows you to
• Set up default oil info for equipment categories. The user can still change them if
necessary at the oil input screens
13
Click the Add Oil button to open the following screen to add a new oil to the database:
14
3 Analyzing Used Fluid Samples
Daily Set-Up Procedures on page 16
Collecting a Used Fluid Sample on page 23
Preparing Samples on page 24
Testing a Fluid Sample on page 25
Extended Flushing Routines on page 37
Generating MicroLab Reports on page 38
Adding Results From External Devices on page 39
The MicroLab screen should be open at the Main Menu, like this:
There is no reason to shut the MicroLab down other than for maintenance or
storage. If you have to restart the MicroLab, you must perform two sample burns on
any clean or used oil sample to warm up and stabilize the device.
15
Daily Set-Up Procedures
As best practice, the following tasks should be completed at the beginning of each day before
you test any samples.
There are also some important maintenance tasks that must be performed regularly -
see Weekly Tasks on page 41 for details.
Empty the Waste Bottle

The waste fluid bottle is behind the door in the cabinet front. Empty the bottle every morning and
check the waste bottle occasionally throughout the day. If the bottle gets full the Waste indicator
in the System Status panel will change from green to red:
If the indicator is red, you will not be able to run any more samples until you empty the
waste bottle and the indicator has reset to green.
Check the CheckFlush Bottle Fluid Level

Make sure the CheckFlush bottle in the bracket on the right side of the MicroLab is full of
CheckFlush fluid. Cross-contamination can occur if the level gets too low.
Check the Printer Paper
Fill the printer if the paper is getting low.
16
Clean the Sipper Screen Filter
The filter needs to be cleaned or replaced every morning and after testing heavily
contaminated fluids.
You will need the following items from the parts kit:
• A sample bottle with 12 mm (1/2 in ) of CheckFlush fluid.
• A sample bottle with 12 mm (1/2 in) of clean oil
• A cotton swab
• Package of new filter screens
The fluid filter is inside a metal fitting known as the Fluid Filter Housing:
1. Unlock the fluid filter housing (below, left) by turning it one-quarter turn anti-clockwise (to the
left), then slide it off the housing fitting (below, right):
17
2. Use the blunt end of a swab to push the filter out, like this:
3. Drop the filter into the CheckFlush fluid bottle and shake it gently.
If there is debris in the filter that cannot be removed in this way, or if the screen is
damaged, then replace it with a new filter screen.
4. Drop the clean filter inside the fluid filter housing and press it into place using the swab
stick:
5. Dip a clean cotton swab into the container of clean oil and wipe inside the fluid filter
housing to lubricate along the threads.
6. Push the filter housing firmly back over the housing fitting and lock it by turning it
one-quarter turn clockwise (to the right).
18
Clean the Collimator Lens
You will need a box of KimWipes from the accessories kit for this procedure.
The collimator is a small glass lens to the left of the electrode stand:
Use a clean, dry KimWipe (supplied) and wipe the lens gently.
Do not apply pressure to the lens as it might accidentally move and disturb the alignment. If
this happens, contact Technical Support for assistance.
You can also wrap the wipe around the cotton end of a swab to apply gentle pressure. Do
not use a swab alone to clean the lens.
19
Run a Manual Flush
You will need the following supplies from the accessories kit:
• A clean 150 ml (5 fl oz) standard sample bottle
• The bottle of CheckFlush fluid
• A clean sipper straw
1. From the Main Menu click the Maintenance button in the top right corner.
The Maintenance Menu will open:
2. Click Flush. This will open the Flush Option menu:
3. Click Short. A Method Confirmation message will display similar to this one:
20
Whenever you see a Method Confirmation box like this pop up during a procedure, you
need to follow the step(s) described, like this:
4. Fill the sample bottle with 100 ml (3 fl oz) of CheckFlush fluid.

5. Put the long end of a clean straw into the sample bottle.
6. Set the bottle on the sample stand and slide the short end over the nozzle, like this:
7. Click OK to start the flush. The computer will manage the entire process. When it is done,
the Main Menu will appear again.
Run a Check Base Line Test
This test is required to check for any residual contamination.
You will need the following supplies from the parts kit:
• A 150 ml (5 fl oz) sample bottle
• Bottle of CheckFlush fluid
• 3 cotton swabs
Procedure
1. Fill the sample bottle with CheckFlush fluid and set it aside.
2. From the Main Menu, click the Maintenance button in the upper right corner:
3. From the Maintenance Menu, click the Standardization link.

4. From the Standardize Options Menu, click the Check Base Line link.
21
Follow the instructions in the confirmation message:
See Cleaning the Electrodes on page 44 for instructions if necessary. Then continue
with the steps in the Confirmation Message, as follows:
1. Fill the sample bottle with CheckFlush fluid, insert a clean straw, and connect the straw to
the sipper nozzle.
2. Click OK to start the Base Line test.
3. After the test, you should see the message confirming the base line test passed:
4. If the test fails, run the test again with fresh CheckFlush fluid.
If it still fails, refer to Will Not Pass Base Line or Verify Metals on page 73 for details.
22
Collecting a Used Fluid Sample
Never use the MicroLab 30/40 to test anti-freeze, water, brake fluid, Blow-Out Pre-
venter fluids or Phosphate Ester-based hydraulic fluids like Skydrol or FyrQuel as
these fluids will cause irreparable damage.
Do not test flammable liquids such as gasoline, kerosene, or diesel fuel.
Test used lubricants from diesel and gasoline engines, gearboxes, hydraulic sys-
tems and transmissions only.
Sample bottles should be used once only. Dispose of used sample bottles in
accordance with local, state and Federal guidelines.
Severe burns may occur when drawing fluids from a hot fluid reservoir. We
recommend you wait at least 30 minutes for the fluid to cool.
Only trained personnel should take fluid samples from equipment. Always follow
local or manufacturer guidelines to draw the most representative oil sample with the
proper tools and safety equipment.
Required Sample Fluid Volumes

The following sample volumes apply depending on the tests to be performed:
Metals and IR properties only 60 ml (2 fl oz)

Metals, IR properties and measured viscosity 120 ml (4 fl oz)
Metals, IR properties, measured viscosity and particle count 150 ml (5 fl oz)
Filling the Sample Bottle

Use the supplied sample extraction pump and tubing to collect the sample in accordance with local
training.
1. Take a sample bottle and screw it into the pump housing.
2. Cut a suitable length of plastic hose.
3. Loosen the hose clamp on the top of the pump and insert the plastic tube:
4. Finger-tighten the hose clamp and pull back on the plunger to fill the bottle
23
Preparing Samples
Preparation depends on whether you have a MicroLab 30 or a MicroLab 40.
MicroLab 30 Sample Preparation
1. Screw the sample bottle lid on tightly and shake the sample well - 30 seconds minimum
for fresh samples; longer for particularly heavy oils and greases and for older samples
that have been standing or have been in transit for a long period.
2. Start testing the sample immediately to avoid settling.

MicroLab 40 Sample Preparation
You will need 150 ml (5 fl oz) of used fluid (1 full sample bottle).
1. Screw the sample bottle lid on tightly and shake the sample well - 30 seconds minimum
for fresh samples; longer for particularly heavy oils and greases and for older samples
that have been standing or have been in transit for a long period.
Fill the ultrasonic bath with a minimum of 25 mm (1") of water before you switch it on or
damage may occur.
2. Turn on the heater and set the timer for two minutes so the bath can warm up.
3. Place the sample bottle in the bath and set the timer for 30 seconds minimum or until no
more surfacing bubbles are observed. Be prepared to run the bath for 2 minutes or
longer to degass heavy oils and greases.
4. Start testing the sample immediately to avoid settling.
24
Testing a Fluid Sample
Fluids should be at room temperature (19o C to 25o C (65o F - 75o F) when they are being
tested.
The MicroLab requires the user to enter basic information about the equipment, the component and
the oil that is being tested. The following screens describe how to enter this information.
To begin, make sure your screen shows the Main Menu, like this:
Either,
If you have previously measured a sample from this particular vehicle, you will have a Vehicle ID for
it. You can enter the Vehicle ID in the box above the Start button and press the green arrow:
Then skip to Select a Testing Option Screen on page 30 to continue.
25
Or,
If you do not have a vehicle ID or if this is the first time this vehicle is being tested, you will need to
select a mode in the Main Menu. The modes are listed on the left side of the Main Menu.
When you select a mode it will change to green and the mode name will appear in the Start but-
ton like this:
The available modes are:

ON-ROAD TRUCK (which includes Buses, RVs, and Trucks)
AUTO
OFF-ROAD
MARINE
INDUSTRIAL
RAILROAD
COMMERCIAL GENSET
You must ensure you are in the proper application mode before continuing because it
will directly impact the following:
1. Which databases will be used for equipment selection, and
2. Rules and Evaluation statements used on the reports.
26
For this example you will use the On-Road Truck mode.
1. Click On-Road Truck. The button will turn green.
2. Click the Start Button.
3. The Select Customer/Unit screen opens similar to this example:
4. Select the customer you wish to use and press the Select button. You can sort the customer
list by selecting one of the 4 categories in the top right of the screen – Last Name (or the
Customer Name), First Name, Vehicle ID, or City.
If your customer is not listed, press the New Customer button to open the following screen:
27
5. Company or Last Name is the only required field. Fill out as much information as possible
to ensure that the proper customer is aligned with the correct unit information.
6. Press the Save button when data entry is completed to add the new customer.
7. Click the Select button to choose your customer.
Note that you can change any Customer and/or Vehicle information in any of the
following screens by clicking the ‘Change’ button to the right of the selection.
The example below was sorted by the Vehicle ID. This allows you to see all the vehicles in the
system and the applicable customer name:
8. Select the Vehicle ID you wish to use and press the Select button. The example above
uses Vehicle ID AB123456 belonging to customer ABC Trucking.
Either accept a vehicle already listed or set up a new vehicle by pressing the New Vehicle
button to open this screen:
28
9. Fill out the screens as completely as possible for the vehicle by selecting the drop down
arrow and selecting the proper make and model. The red asterisk indicates a required field.
If the make and/or model you require is not listed, select ‘Custom’ from the drop down lists and add
the details. You will then be asked to save this custom make and model at the end of the data
selection.
There are extra fields to add Jobsite and Description if needed.
10. Once the screen is complete, press Save to add the vehicle.
11. Highlight the vehicle you want to use and press the Select button to open the Select a
Testing Option dialog box.
These options appear because you are in the On-Road Truck Mode. Other modes will
display different options.
29
Select a Testing Option Screen
Choose the testing option from the choices in this screen:
Different modes may display different options. For this example, click Diesel Engine.
The Select a Component screen opens similar to this example:
Select a Component Screen
If you had chosen an incorrect customer or vehicle, you can go back and make
a change by pressing the Change button(s).
For this example, click Diesel Engine to select it.
30
The On-Road Diesel Component Information screen opens similar to this example:
You can edit any of the fields in this screen. Fields with the red asterisk are required. Once you have
have completed all of the required fields, the Oil Info button will become active.
In this example, only the Miles Since New or Overhaul required field is blank. Enter 6000 and click
the Oil Info button to proceed.
31
The Oil and Analysis Information screen opens similar to this example:
Fields marked with a red asterisk are required. Entries for Oil Brand, Oil Type and Oil Weight are
selected by clicking the down arrow and selecting from the drop-down lists.
It is extremely important that you enter the correct oil weight.
Oil Brand - Click the down arrow and scroll to your brand. For this example, select Shell.
Oil Type - Click the down arrow and scroll to your type. For this example, select Rotella.
32
Oil Weight Selection and Oil Weight - All Weights is selected by default. You can click Common
Weights if you are using a popular commercial brand. This will reduce the number of oil weights in
the Oil Weight field for you to scroll through.
You can also start typing your oil weight into the field to bring up a list of relevant options
For this example, select 15W-40.

Date Taken - The default is to today's date.
Synthetic - Select Yes or No as appropriate.
Miles/Hours/Kilometers on Oil - This is since the last change.
If you can't find your brand or oil type, scroll down to "Custom," select it, then complete the Custom
Information screen.
Press the Analyze button to continue.
33
The Oil Analysis Activation screen opens similar to this example:
This is the last opportunity to check the customer and vehicle information. You can edit
any entries by pressing the Change button.
You can edit the oil selections by pressing the Back button.
34
At this point you can choose what test(s) to run. You can click the check-box in the lower left corner
to set your selection as a default.
• The Extended Metals option will only display if you have purchased the Extended Metals
package.
• If you want to run the Viscometer, click Measured (40C and 100C)
• If you do not want to run the Viscometer, click Calculated and the viscosity will be
estimated instead.
If you have the MicroLab 40, the particle counter will be active for hydraulic or transmission
fluids only.
You can also choose which type of report you need, whether or not to print an ‘Understanding your
Report’ and also whether the report prints automatically at the end of the sample run.
Press the GO button to start analyzing the sample.
Either,
If your oil sample weight is less than ISO-320, the following confirmation message box will open:
Follow the prompts and click OK.

Click OK to start the analysis cycle; see The Analysis Cycle on page 36 for details.
35
Or,
If your oil sample weight is ISO-320 or greater, the following method confirmation box will open
automatically:
Do not test used oils with a viscosity greater than ISO 320 in a regular sample
bottle to avoid the possibility of personal injury. Refer to Over-Pressure Sampling
on page 59 to complete the instructions in this dialog box.
The Analysis Cycle

The analysis takes about 10 - 12 minutes to complete (based on the tests you have chosen to
run) after all data entry and manual tasks have been performed. A timer indicates progress as the
sample is processed.
If you want to stop the analysis, press the STOP button. The stop process takes 15-30 seconds
after which you will be returned to the Main Menu.
For a typical sample, the analysis will complete and the MicroLab flushing will automatically start
to clean the instrument for the next sample.
36
Extended Flushing Routines
Samples that contain high concentrations of metals, high soot levels or high particle counts can be
difficult to clean from the system. Samples like this can cross contaminate future samples and
impact results. For this reason the MicroLab automatically monitors these conditions and will
automatically prompt you to perform additional flushing when needed to prevent cross
contamination. These prompts are described in this section.
High Metals Detected
If high metals are detected the following message is displayed:
The user should follow the steps and select OK to continue. The high metals flush routine will send
CheckFlush to the OES to clean the system and then it will spark the CheckFlush to recheck the con-
tamination level.
If it is determined that the OES requires more cleaning it will prompt the user to repeat the extra
cleaning steps; otherwise the system will exit the cleaning routine. The extended cleaning can be
repeated up to three times for the system to try to achieve the desired level of cleanliness. If the sys-
tem still measures carryover contamination after the additional cleaning it will recommend that the
operator conducts a standardization.
This recommendation is designed to ensure the best results, but it is not a required
step until the sample counter at the bottom of the screen indicates that a
standardization is required.
See Standardization Procedures on page 50 for more information.
37
High Soot Detected
If high soot levels are detected the following message is displayed:
The user should follow the instructions on the screen to provide additional cleaning to the IR.
High Particle Counts Detected
If high particle counts are detected the following message is displayed;
In this case it is recommended that the user performs a viscometer/particle counter flush which is
found in the Maintenance Tab on the Main Menu. This should be done prior to running the next
sample. See Viscometer Flush on page 67 for more details.
Adjusting the Extended Flushing Settings
For some customers the time to complete a sample and move to the next one is more critical than
preventing low levels of carryover which can involve multiple rounds of extended flushing. Cus-
tomer Support can assist in adjusting the settings that trigger the extended flush routines. This
involves setting the thresholds of various elements that trigger the flush routines or turning off the
extended flush that is associated with certain elements if they are not important to a customer’s
application.
Generating MicroLab Reports

The parameters in the report depend on whether you have a MicroLab 30 or MicroLab 40 and typ-
ically indicate oil condition, contamination, wear metals, additive elements, cleanliness in
accordance with ISO Code 4406. The current report plus up to 3 historical reports are included.
Diagnostics are provided for the current sample which suggest possible problem sources and
recommend service options. See Example Full Report on page 40.
38
Adding Results From External Devices
The MicroLab has the option to add a measurement result from an external instrument for Fuel Dilu-
tion, Water Content, Total Acid Number (TAN), and Total Ferrous to have them included in the
MicroLab report. These are enabled/disabled through the Admin menu and will require support from
Service since this is a locked menu.
When enabled, the user will be prompted for the external value, after the MicroLab has performed
its normal sample measurements and before the final report is generated.
This is an example of the dialog box for Total Ferrous:
If a value is entered it will appear at the bottom of the MicroLab report similar to this example:
An example of a full report is shown below:
39
Example Full Report
40
4 Weekly Tasks
The following tasks need to be completed weekly to maintain top performance:
Measure the Electrode Gap on page 41
Check the Lower Electrode Height on page 41
Run an IR Night Flush on page 42
Measure the Electrode Gap

The electrode gap is the distance between the upper and lower electrodes and it should be no more
than 3.9 mm (5/32").
As samples are run, the gap between electrodes will increase. The flat end of the white electrode
gap tool (supplied) is used as a gauge for measuring the electrode gap as follows:
Insert the flat end of the gapping tool between the electrodes. There should be a slight drag on the
tool as you slide it into and out of the gap.
If the gapping tool is too loose between the electrodes, or if the gap is too small to allow the flat end
of the gapping tool between them, then you need to reset the gap.
See Resetting the Electrode Gap on page 47.
Check the Lower Electrode Height
The lower electrode will erode with use over time. We recommend you routinely check the electrode
height depending on usage. Typically you should check the electrode height weekly, as follows:
Place the U-shaped end of the gapping tool around the bottom electrode. It should stand higher
than the gapping tool, like this:
41
If the electrode is lower than the gapping tool, it needs to be replaced:
See Replacing the Electrodes on page 48.
If you replace the electrodes, you must do Standardize Metals procedure.
Run an IR Night Flush

This type of extended flush is used to soak the IR module cell windows and ensure they stay
clean from soot buildup.
The process takes approximately 7 hours, and we recommend running it overnight.
The flush needs to be done at a minimum of once a week. Run it more often when
testing very sooty fluid samples.
Follow these steps to start the process:

1. Click the Maintenance button.
2. Click Flush.
3. Click IR Night Flush.
4. The process checks the number of sooty samples run during the previous week. If there
were any run, and the cell is contaminated, the on-screen instructions will prompt you
through an automated process.
Otherwise, you will see a message that the IR cell is not contaminated and you will be
prompted to click Yes to continue, or No to cancel the procedure.
42
5 Maintaining the Electrodes
Description on page 43
Cleaning the Electrodes on page 44
Measuring the Electrode Gap on page 46
Resetting the Electrode Gap on page 47
Monitoring the Lower Electrode Height on page 47
Replacing the Electrodes on page 48
The plasma generated in the spark gap is extremely hot. To avoid severe burns, allow at
least 20 seconds for the electrodes to cool down before working around them.
Take care to avoid the sharp needle behind the upper electrode holder.
Description
The electrodes are on a stand behind the spark door located to the right of the LCD screen.
They are positioned vertically with a 3.9 mm (5/32") gap between them (arrowed):
43
Cleaning the Electrodes
You will be prompted by a dialog box whenever you need to clean the electrodes.
Use a minimum of 4 cotton swabs to clean the electrodes.

Not all types of swabs will fit and some contain contaminants that will affect the
instrument results, so use only the swabs supplied with the MicroLab.
Do not touch the cotton tip to avoid contamination. Do not store the swabs in an open
container.
You will need the following consumables from the parts kit:
• 4 swabs
• Stainless steel wire brush
If the electrodes seem burned or heavily contaminated, you can use the stainless steel wire brush
to clean them before you use the swabs.
When cleaning with the wire brush, hold a clean wipe over the collimator lens to
protect it from possible contamination by flying debris.
44
1. Clean the inside of the upper electrode by inserting a swab down through the hole in the top
of the electrode holder.
Force the swab down into the center of the electrode until the tip appears in the spark gap
and spin it counter-clockwise (to the left):
If you break the tip off a swab while cleaning, be sure to remove all debris from the
electrodes and around the electrode stage.
Swab debris in the electrodes can cause a fire and can also clog the drain below the
electrode stage.
2. Repeat Step 1 with a clean swab.

3. Take a clean swab and clean all around the outside of the bottom electrode:
Do not allow the tip to touch the electrode stage as this is frequently contaminated. If you
do, you must discard the swab.
45
4. Insert a clean swab between the electrodes and clean the flat surfaces:
Measuring the Electrode Gap

You need to check the electrode gap weekly before you begin testing samples.
The electrode gap is the distance between the upper and lower electrodes and it should be no
more than 3.9 mm (5/32"). The flat end of the white electrode gap tool (supplied) is used as a
gauge for measuring the electrode gap .
As samples are run, the gap between electrodes will increase.
Insert the flat end of the gapping tool between the electrodes. There should be a slight drag on
the tool as you slide it into and out of the gap.
If the gapping tool is too loose between the electrodes, or if the gap is too small to accept the flat
end of the gapping tool, then you need to reset the gap.
46
Resetting the Electrode Gap
If you adjust the electrode gap, then you must Standardize the device when you are done.
See Standardize Metals on page 55 for more details.
1. Loosen the upper electrode holder screw using a 3.9 mm (5/32") hex key:
2. Allow the upper electrode to slide down until it is flush with the top of the gapping tool.
3. Apply light finger pressure to the top of the electrode to hold the gapping tool in place and re-
tighten the upper electrode holder screw.
Monitoring the Lower Electrode Height

The lower electrode will erode with use over time. We recommend you routinely check the electrode
height depending on usage.
Checking the electrode height is one of the required weekly tasks.

You must also check it before a Standardization procedure.
47
1. Place the U-shaped end of the gapping tool around the bottom electrode. It should stand
higher than the gapping tool, like this:
2. If the electrode is lower than the gapping tool like this, it needs to be replaced:
Replacing the Electrodes

If you are replacing the lower electrode, flip or replace the upper electrode regardless of
its age or condition.
There is a sharp needle on the back of the upper electrode holder; use caution when
replacing the upper electrode to avoid injury.
The upper electrode is reversible, so you can flip it over to the unused end and fit it
back in the holder. Once both ends are used, it needs to be replaced.
48
1. Loosen the set screw holding the lower electrode with a 1.27 mm (0.05") hex key:
2. Turn the electrode counter-clockwise (to the left) to remove.

3. Screw the new electrode in place by turning it clockwise (to the right).
4. Tighten the set screw to hold it in place.
5. Remove the upper electrode cap screw using a 3.9 mm (5/32") hex key:
6. Allow the upper electrode to drop out of the electrode holder.

7. If the other end of the electrode has not been used, you can flip it over and use the other end.
Otherwise, it needs to be replaced. Slide the electrode up into the holder so that about 9.5
mm (3/8") - roughly the thickness of the U-shaped end of the gapping tool - protrudes below
the holder.
8. Replace the upper electrode screw, but do not tighten it as you need to set the gap.
9. Re-gap the electrodes.
The socket head cap screws should be finger tight plus ¼ turn with the wrench.
Over-tightening the screws may cause stress to and/or the cracking of the holder.
10. Tighten the upper electrode holder screw.
49
6 Standardization Procedures

Check Base Line on page 51
Verify Metals on page 52
Standardize Metals on page 55
Standardizing the Viscometer on page 57
Occasionally, it is necessary to standardize the MicroLab in order to compensate for minor
changes affecting calibration.
There are three distinct Standardization processes. You can run any of them at any time you
believe your results are particularly abnormal, but generally they are set to a schedule based on
the number of samples run.
The Standardization schedule is shown at the bottom of the Main Menu similar to this example:
This tells you the maximum number of samples you can test before you must re-run one or more
of the Standardization procedures.
By default, the number of samples necessary between procedures are Base Line = 20,
Verify Metals = 35 and Standardize Metals = 50.
These defaults can be changed but you will need to contact Technical Support for
help.
Procedure counters will change to yellow when procedures are due within 5 samples,
and then to red when they are at 0 (zero).
If any counters are at 0 (zero) you will not be allowed to run any more samples
until the expired procedure has been run. This will reset the counter and allow you
to run samples again.
You must start and complete the Standardization process in the same day, otherwise
the schedule counter will not reset.
50
Check Base Line
The Check Base Line Test is used to determine if there is contamination in the flow system or on the
electrodes of the Analyzer. It should be performed at the beginning of each day, or any time you
wish to confirm that the Auto Flush cycle has sufficiently cleaned the internal lines and electrodes
after running a highly contaminated sample.
You must perform this procedure if the Check Base Line Due counter at the bottom of the
Main Menu is at zero.
As a best practice, we recommend you perform the procedure at the beginning of each
workday.
You may run the procedure at any time, especially if the counter is near zero.
Test Requirements
Locate the following items from the consumables kit that came with the device:
• Bottle of CheckFlush fluid
• 3 cotton swabs
Procedure
1. Make sure the CheckFlush bottle is full.
2. Fill the sample bottle with CheckFlush fluid and set it aside.
3. From the Main Menu, click the Maintenance button.
5. From the Standardize Options Menu, click the Check Base Line link.
6. Follow the instructions in the on-screen checklist:
7. Click OK to start the test.

8. When the sample test is done, you should see a message confirming the test passed. Click
OK to return to the Main menu.
51
If the test fails, run it again with a fresh fluid sample.
If it still fails, see Will Not Pass Base Line or Verify Metals on page 73.
Verify Metals
The Verify Metals procedure is performed to verify that the OES is still calibrated properly.
You must perform this procedure if the Verify Metals Due counter at the bottom of the
Main Menu is at zero after every 35 samples run.
You may perform the procedure at any time if you think your test results are particularly
abnormal or if the sample counter is approaching zero.
Test Requirements
• Bottle of blue standard fluid
• Clean sipper straws
• 3 Cotton swabs
If you have the Extended Metals package, you also need
• 2 more sample bottles
• Bottle of yellow Low Concentration Scale (LCS) standard fluid
• Bottle of brown High Concentration Scale (HCS) standard fluid
Procedure
Shake each bottle of standard for at least 30 seconds, or longer if they have been
standing or in transit for a week or longer.
1. Take a 150 ml (5 fl oz) bottle and fill it with the blue standard fluid.
2. If you have the Extended Metals package, take a 150 ml (5 fl oz) bottle and fill it with
yellow Low Concentration Scale fluid (LCS) and fill another with brown High
Concentration Scale fluid (HCS).
3. From the Main Menu, click the Maintenance button.
52
5. From the Standardize Options Menu, click the Verify Metals link. A dialog box will pop up
asking you to confirm you really want to run a Verification test and not a Standardization test:
6. Click Yes, then follow the instructions in the check-list:
7. A message should display to confirm the Basic Metal test passed.
8. If the test does not pass first time, try running a fresh fluid sample.
If it still does not pass, see Will Not Pass Base Line or Verify Metals on page 73.
9. Click OK.
If you have the Basic Metals only option, the test is complete. You will be returned to the Main Menu.
The following section is for users with the Extended Metals option.
10. Follow the instructions in the following check-list to test the LCS standard (yellow) fluid:
53
11. At the end of the test, you should see a message that the LCS test was successful:
12. If you do not see this message, run the test again with fresh LCS fluid.
If it still does not pass, refer to the Troubleshooting Guide: Will Not Pass Base Line
or Verify Metals on page 73.
13. Press OK and follow these instructions to test the HCS standard (brown) fluid:
14. At the end of the test, you should see a message that the test was successful:
15. If you do not see this message, run the test again with fresh HCS fluid.
If it still does not pass, refer to the Troubleshooting Guide: Will Not Pass Base Line or
Verify Metals on page 73.
16. Click OK to return to the Main Menu.
54
Standardize Metals
The Standardize Metals procedure calibrates the Optical Emission Spectrometer (OES).
You must standardize if you have replaced the electrodes or adjusted the electrode
gap.
You must standardize when the counter reaches 0 after each 50 samples.
As a best practice, we recommend that you run a manual Long Flush before per-
forming the Standardization.
You may standardize if the sample counter is approaching zero.
You may standardize if you question the analyzer's performance.
Test Requirements
• Bottle of blue standard fluid
• Clean sipper straws
• Clean cotton swabs
If you have the Extended Metals package, you will also need the following:
• 2 more sample bottles
• Bottle of yellow Low Concentration Scale (LCS) fluid
• Bottle of brown High Concentration Scale (HCS) fluid
Procedure
Shake each bottle of standard for at least 30 seconds, or longer if they have been standing
or in transit for a week or longer.
1. Take a 150 ml (5 fl oz) bottle and fill it with the blue standard fluid.
2. If you have the Extended Metals package, take a 150 ml (5 fl oz) bottle and fill it with yellow
Low Concentration Scale standard (LCS) and fill another with brown High Concentration
Scale standard (HCS).
3. From the Main Menu, click the Maintenance button:
4. Click the Standardization link.
5. Click the Standardize Metals link.
You will be asked about the cleanliness of the device:
55
Optional - Cancel the Standardization and run a long flush as described in Manual
Flushing Options on page 67.
6. Click OK to continue the test and follow the prompts in the following check-list:
This process will take about 10 minutes and you should see a dialog box confirming the basic
metal standardization is complete:
If the test fails, retest with a fresh sample.

If it fails again, refer to the Troubleshooting Guide: Will Not Pass the Standardization on
page 72 for information.
If you have the Basic Metals package only, the process is complete. Click OK to return to the
Main Menu.
Otherwise, continue to the next section.
Extended Metals Option
If you have the Extended Metals option, click OK and follow the prompts to test the LCS fluid.
This process will take about 10 minutes until you see a dialog box confirming the LCS
measurement is complete:
• If the test fails, retest with fresh LCS fluid.
56
•If it fails again, refer to the Troubleshooting Guide: Will Not Pass the Standardization on
page 72 for instructions.
7. Click OK and follow the prompts to test the brown HCS fluid.
This process will take about 10 minutes until you see a dialog box confirming the HCS measurement
is complete.
• If it fails, press Cancel and retest with fresh HCS fluid.

• If it fails again, refer to the Troubleshooting Guide: Will Not Pass the Standardization on
page 72.
8. Click OK to return to the Main Menu.
Standardizing the Viscometer
The Viscometer is standardized at the factory and it has no set number of samples before it is stand-
ardized in the field. If your viscosity results are in question, refer to Viscometer Issues on page 75 for
information.
Follow these procedures to standardize the viscometer only if you have been instructed by
Technical Support to do so.
Test Requirements
Shake the standards bottle for at least 30 seconds, or longer if they have been standing or
in transit for a week or longer.
You will require the following:

• A 150 ml (5 fl oz) sample bottle of Low Viscosity Standard (pink fluid)
• A 150 ml (5 fl oz) sample bottle of High Viscosity Standard (green fluid)
Procedure
1. From the Main Menu, press the Maintenance button then press Visc Standardization.
2. Enter your username (default is 1) and password (default is 1) and press the Login button.
3. You will be prompted for the viscometer measurements at 40C and 100C for both Low and
High Viscosities; these numbers are printed on the bottle label.
57
For this example ONLY, enter the following values:
High Visc at 40C = 142.4 High Visc at 100C = 15.0
Low Visc at 40C = 46.7 Low Visc at 100C = 6.9
Your numbers could be different from the ones above; please refer to your high and low
viscosity fluid bottles to find your numbers.
4. After entering the numbers on the analyzer, follow the prompts on the screen. You will
enter the low viscosity fluid first and then the high viscosity.
5. Once the viscometer standardization is complete, it will either display the Viscometer
Standardization Completed message, or it will simply go back to the Main Menu.
At this point, you will need to run samples to verify that the viscometer standardization
was good.
6. While in Measured Mode, run 2 consecutive samples in a row of the Low Viscosity fluid.
Enter the Low Viscosity Fluid as a Custom Oil. When prompted to enter the oil weight, for
this procedure you should select SAE20.
7. While in Measured Mode, run 2 consecutive samples of the High Viscosity fluid.
Enter the High Viscosity Fluid as a Custom Oil. When prompted to enter the oil weight, for
this procedure you should select SAE40.
8. To determine if the viscosity standardization was successful, compare the results from
the report to the numbers for V40 and V100 for both the low and high viscosity fluids. The
results should be within the accepted tolerance to the numbers on the bottles, as follows:
Tolerance for V40 results: +/- 7.0 cSt.
Tolerance for V100 results: +/- 1.0 cSt.
9. If the results are outside the accepted tolerance then repeat the standardization process,
and repeat the verification samples.
10. If the results are still not acceptable, contact Technical Support for assistance.
58
7 Over-Pressure Sampling
This section applies only to instruments equipped with the over-pressure kit.
When high viscosity oil samples are to be measured (> ISO 320), the analyzer will prompt you to use
the sample bottle over-pressure cap module, as shown below:
Do NOT dilute the sample.

Eye protection is highly recommended. When the over-pressure cap is in use the oil is
under pressure. Removing the straw from the nozzle before the sample test is complete
may cause the sample to spray.
1. Remove the grill plate over the sample well. This will allow the extra clearance required for
bottles with the pressure cap.
2. Use a clean wipe to clean the inside of the pressure cap, including threads and o-ring.
3. Use a clean cotton swab to clean the straw port from the bottom of the cap.
4. Remove the fitting nut and clean the straw port from the top of the cap.
5. Screw the pressure cap TIGHTLY on the sample bottle.
The sample bottle cap MUST be on tight

A loose fit will result in an air leak preventing instrument from achieving proper air pressure
within the sample bottle
59
6. Unscrew the straw clamp and insert the straw. Tighten the clamp finger-tight only so you
don't crush the straw.
7. Make sure the pressure tube is firmly connected to the pressure cap fitting.
8. Make sure the pressure tube is firmly connected to the bulkhead fitting, then click OK:
60
The Analysis in Progress dialog box opens similar to this example:
The analysis takes about 10 - 12 minutes to complete based on the required tests. The status bar
indicates processing percentage progress.
For a typical sample, the analysis will complete and the MicroLab flushing will automatically start
to clean the instrument for the next sample.
61
8 Clean Oil Sampling
There are times when you might want to analyze incoming fresh oil supplies; for example,
• Before you put the oil into a machine or vehicle
• Baseline Testing
There is no vehicle information involved; otherwise the method is the same as for a used fluid.
In the lower right corner of the Main Menu is a check-box marked Fresh Oil:
1. Click the check-box to open the Oil And Analysis Information screen:
2. Select entries for Oil Brand, Oil Type and Oil Weight by clicking the down arrow and
selecting from the drop-down list.
It is extremely important that you enter the correct oil weight.
62
Common Weights include most commercial engine and other oils. The system defaults to
All Weights. You can start typing your oil weight into the field to bring up a list of relevant
choices.
If your oil brand and/or oil type are not listed, select Custom and enter as much detail as pos-
sible, then confirm all your entries.
3. Indicate if this is a synthetic or not.
4. Optional - enter a Sample ID and/or operator information.
5. Place a clean straw in the sample bottle and slide the straw over the sample nozzle.
6. Press the Analyze button to open the Oil Analysis Activation screen. Fields available here
depend on what metals package was purchased:
Analyze Section:
• Check the Physical Properties (IR) box .
• Check the Metals (OES) box. If you have the Extended Metals package, select
Extended Metals. Otherwise Base Metals Only will be the default option.
Viscosity Mode:
• Select Calculated to have the IR module estimate the viscosity of the sample instead of
the Viscometer measuring it.
• Select Measured (40C and 100C) to report the measured viscosity at both 40C and
100C.
• 40C Only. Click this option to report viscosity results at 40oC only.
• 100C Only. Click this option to report estimated viscosity results at 100oC only
The following fields are optional:
Print Understanding Your Report - Click Yes if you want to print out a primer on how to interpret
the test result report. Default is No.
Report Style - Click either Numeric or Numeric History.
Auto-Print Report - Default is Yes.
63
Set my Selection as Default - This is a check-box in the lower left corner. Check this box if you
want to save your current selections as defaults any time you test oil from this source in the
future.
7. Press the Go button to start the analysis.
8. Clean the electrodes.
9. Click OK to start the measurement. The completion percentage is displayed as a timer:
When the measurement is complete, the analysis report opens similar to the example below.
64
On the left side of the report, instead of an owner or company it simply says NEWOIL:
The sample analysis appears on the right side of the report similar to this example:
65
66
9 Manual Flushing Options
You can start a manual system flush whenever you think one is appropriate; for example, after
testing a particularly sooty diesel oil sample.
When doing a Short, Medium or Long Flush, the screen will prompt you for a clean sample bottle
with 90 ml (3 fl oz ) of CheckFlush fluid. The IR Night Flush requires 150 ml (5 fl oz).
1. From the Main Menu click the Maintenance button.
2. From the Maintenance menu, click the Flush link to open the Flush Options Menu:
Viscometer Flush
The Viscometer and Particle Counter Flush (if installed) allows the user to perform additional
cleanings directly to the Viscometer and the Particle Counter to eliminate sample carry over and
contamination contained within these two components.
Short Flush
The short flush applies an extra flush to the system when light contamination is encountered.
Medium Flush
The medium flush applies an extra flush to the system when mid-range contamination is
encountered.
Long Flush
The long flush applies an extra flush to the system when heavy contamination is encountered.
67
IR Night Flush
This type of extended flush is used to soak the IR module cell windows and ensure they stay free
from soot buildup.
The flush needs to be done at a minimum of once a week. Run it more often when
testing very sooty fluid samples regularly.
The process takes approximately 7 hours, and we recommend running it overnight.
Follow these steps to start the process:

1. Click the Maintenance button.
2. Click Flush.
3. Click IR Night Flush
4. The process checks the number of sooty samples run during the previous week. If there
were any run, and the cell is contaminated, the on-screen instructions will prompt you
through an automated process.
Otherwise, you will see a message that the IR cell is not contaminated.
5. Either click Yes to continue the flush or click No to exit.
68
10 Printing Historical Reports
Follow these steps to print the test history for any vehicle.
You must make sure you select the same analysis mode in the Main Menu that was the
active mode when you measured the sample.
This will display all the records for tests done under that mode in the Analysis Mode
column.
1. Click the DATA button on the Main Menu, then select Reports – View / Print / Export from
the Data Settings menu to open the report similar to this one:
You can sort the report by selecting one of the three options in the top corner: Vehicle ID,
Component ID or Company/Last Name.
You can also sort by clicking the top of each column.
In this example, there are 4 test records for Vehicle ID 90914.
2. Click a row to highlight it and press the Select button to open the report.
View Customers/Units/Components
This report is View Information only - just click the row you want to report on to highlight it.
There are 4 sorting options in the drop-down menu: Components, Customers, Sample Information,
and Units.
69
Component View
Customers View
Sample Information View
70
Units View
71
11 Troubleshooting
Contacting the Support Team
Before calling or emailing the support team:
• Note the Serial Number
• Leave the Microlab powered up and connected to the internet
• Place a 150 ml (5 fl oz) sample of Blue test standard fluid under the sipper and
connect the straw to the sipper nozzle
• Take pictures of the electrodes
Email us at support@spectrosci.com or call (+1) 978-431-1130 to open a support ticket.
Will Not Pass the Standardization
Possible solutions:
1. Spark box maintenance is required. Run a Short Flush; see Short Flush on page 67 for
details. Open the spark box and watch the flow between the electrodes. You should not
see fluid splashing between the electrodes (should be pulsating like a heartbeat). If you
have CheckFlush splashing or the fluid is touching the upper electrode, please let the
support team know.
2. Run a sample of High Viscosity Standard (Part number 29090-01) through the analyzer.
Use SAE40 as the oil weight, and select Metals Only. This will help remove the
contamination and clean the analyzer.
3. Check the lower electrode height - Check the life of the lower electrode (Part number
23076-00). Use the Gapping tool (Part number 555-440-144) to see if you still have life
left on the lower electrode. See Monitoring the Lower Electrode Height on page 47 for
details.
Replace the electrode if needed. Any time you replace the lower electrode, you should
turn the upper electrode (Part number 23042-00) upside down and re-use it. If both ends
of the upper electrode are used, replace it.
Any time you replace the upper or lower electrodes, you must re-standardize the
analyzer. (Base Line or Verify Metals will not pass if the electrodes were replaced). See
Standardization Procedures on page 50.
4. Check that the gap between the lower and upper electrodes is still within the 3.9 mm
(5/32") tolerance.
72
The thin end of the gapping tool should fit between the electrodes with a “drag”. If it is too
tight to accept the tool, or if it is too loose, adjust the gap. See Resetting the Electrode Gap
on page 47 for details.
After you adjust the gap, you must re-standardize the analyzer. (Base Line or Verify
Metals will not pass if the gap is changed). See Standardization Procedures on page
50.
5. Clean the spark box with a clean dry paper towel. Make sure the spark box is free of debris
and broken cotton swabs.
There is a sharp needle behind the upper electrode holder. Be careful when cleaning the
electrodes.
6. Cover the Collimator lens with a clean wipe or tissue to protect the lens, then clean the
electrodes thoroughly. See Cleaning the Electrodes on page 44 for details.
7. Clean the Collimator lens with a lint free Kim wipe (Part number 29824-00).
8. Clean or replace the fluid intake filter (Part number 29033-00).
9. Use a new clean straw (Part number 29823-00).
10. Use a new clean sample bottle (Part number 29002-05) and pour in new blue test Standard
fluid (Part number 29087-01). Shake the sample for 30 seconds before use.
11. Re-run the full Standardization process and follow the on-screen prompts.
Will Not Pass Base Line or Verify Metals
Possible solutions:
1. Spark Box maintenance required. Run a Short Flush. Open the spark box and watch the
flow between the electrodes. You should not see fluid splashing between the electrodes
(should be pulsating like a heartbeat). If you have CheckFlush splashing or the fluid is
touching the upper electrode – please let the support team know.
2. Run a sample of High Viscosity Standard (Part number 29090-01) through the analyzer. Oil
weight is SAE40. Metals only. This will help remove the contamination and clean the
machine.
3. Electrode gap – Check that the gap between the lower and upper electrodes is still within
the 3.9 mm (5/32") tolerance. The thin part of the gapping tool should fit between the
electrodes with a “drag”. If it is loose, you will need to make an adjustment.
After you adjust the gap, you must re-standardize the analyzer. (Base Line or Verify
Metals will not pass if the gap is changed). See Standardization Procedures on page
50 for details.
73
4. Clean the spark box with a clean dry paper towel. Make sure the spark box is free of
debris and broken cotton swabs.
There is a sharp needle behind the upper electrode holder. Be careful when cleaning the
spark box.
5. Cover the collimator lens with a clean wipe or tissue to protect it, then clean the
electrodes thoroughly with the cotton swabs (Part number 29033-00).
6. Scrub the lower and upper electrodes with the Stainless Steel wire brush (Part number
24086-00) if the electrodes seem burnt or very contaminated.
7. Clean the Collimator lens with a lint-free Kim wipe (Part number 29824-00).
9. Use a new sipper straw (Part number 29823-00).
10. Use a new clean sample bottle (Part number 29002-05) and pour in new Standard
depending on the test you are running:
CheckFlush for Base Line or Test Standard for Verify Metals.
11. Shake the sample for 30 seconds.
12. Re-run the test that was failing and follow the screen prompts.
13. If the test fails again, flush the analyzer again with clean fluids and then re-standardize it
instead of running the Base Line or Verify Metals tests.
High Elements Detected at the End of the Sample
Uncertainty as to whether the analyzer is clean after running a contaminated sample with abnor-
mal readings.
Possible solution:
1. Spark Box maintenance required. Cover the collimator lens with a clean tissue to protect
it, then clean the electrodes thoroughly with a minimum of 4 cotton swabs (Part number
29033-00). Scrub with the stainless wire brush (Part number 24086-00) if the electrodes
seem burnt or heavily contaminated.
2. Clean the Collimator lens with a lint free Kim wipe (Part number 29824-00).
3. Clean or replace the fluid intake filter ( Part number 29033-00).
4. Run a sample of High Viscosity Standard (Part number 29090-01) through the analyzer 2
times back to back for Metals, IR and Viscometer (DTV). For this procedure, when
prompted for the oil weight enter SAE40. This will help remove the contamination and
ensure the analyzer is clean.
5. Place a 150 ml (5 fl oz) sample of clean CheckFlush fluid (Part number 29088-01) under
the sipper and run a Base Line test. There is either a Pass or a Fail notification:
a. If the Base Line test passed, start running samples again.
b. If the Base Line test failed, the analyzer is still contaminated. Follow steps 1-5 twice; if
the Base Line test still fails, please contact the support team.
74
Wear Metals Results are in Question
Possible solution:
1. Immediately after the sample that you are questioning, run a sample of the blue Standard
calibration fluid (Part number 29087-01).
The Standard contains 50 ppm +/- 10, so the expected range is between 40 ppm and 60
ppm for the regular wear metals.
If the metals test within range, the sample results are valid.
If the metals test out of range, follow the instructions to re-standardize the MicroLab; see
Standardization Procedures on page 50 for details.
2. Once the MicroLab is re-standardized, re-run the sample.
Viscometer Issues
Possible solutions:
1. Check the temperature on the Viscometer temperature controller in the back of the
analyzer.
Remove the 2 screws holding a small viewing port on the back of the MicroLab and remove the port
to see the display
Do not attempt to remove the entire back panel. The temperature display is easily visible
through the viewing port.
There are no user-serviceable parts inside - do not attempt to replace the temperature
controller or any other parts. If you suspect the controller or the display is faulty, contact
Technical Support for assistance.
The red numbers should read 100 (Top) and 40 (Bottom) degrees C. The tolerance is +/- 0.6 C, so
measurements between 99.4 – 100.6 (top) and 39.4 – 40.6 (bottom) are required in order to run the
test.
75
a. If the temperature is not within range, click the Shutdown button on the Main Menu to
turn off the software correctly - do not simply power down with the System Power
switch.
b. Once the analyzer screen goes dark, flip the System Power switch on the right side of
the analyzer to the OFF position.
c. Leave the device powered down for 10 minutes so the temperature controller will reset.
d. Turn the analyzer back on using the System Power switch. The temperatures should
come into the correct range within approximately 5 minutes of powering up. Run the
sample when the temperature is within range.
e. If the red temperature alarm is blinking, please contact the support team.
3. Use a clean sipper straw (Part number 29823-00).
4. Use a clean150 ml (5 fl oz) sample bottle (Part number 29002-05) and pour in new High
Viscosity Standard.
5. Standardize the Viscometer - every 6 months or any time test results appear in question.
6. Using a clean 150 ml (5 fl oz) sample bottle (Part number 29002-05), run a sample of
High Viscosity Standard (Part number 29090-01) through the analyzer 2 times back to
back selecting just the Viscometer test. When prompted for the oil weight for this
procedure, use SAE40.
The Viscometer requires 150 ml (5 fl oz) of fluid.

The oil weight is also a key piece of information in determining for how long to pump the
oil. This will ensure the viscometer is working correctly. Expected results are printed on
the bottle label.
If the results are within tolerance (V40C is +/- 7 cSt and V100C is +/- 1 cSt), then run the
samples.
If the results are not within tolerance, please contact the support team for further assistance.
76
A Understanding Your Reports
You don't need to be an expert. The built-in diagnostics do it for you!
Engines
77
Transmissions
You don't need to be an expert. The built-in diagnostics do it for you!
78
B Replacing the Spark Box Air Filter
The air filter should be replaced every 6 months in a shop environment or every 12 months in a lab
environment.
1. Locate the air filter cover on the right side of the MicroLab and loosen the screw:
2. Remove the filter cover to expose the air filter:
79
3. Use the screwdriver blade to help slide the filter out of the housing:
Instead of using a screwdriver, you could use a strip of electrical or duct tape to stick to
the filter and use that as a makeshift handle to pull the filter out.
4. Insert a clean filter.
Make sure the arrow stamped on the filter points toward the back of the MicroLab.
5. Put the cover back in place by inserting the bottom tab first, then tightening the screw.
80
C Exporting Data as a .CSV File
This section describes how to create and export a .csv file.

1. From the Main Menu, in the DATA Tab click Create CSV to open this dialog box:
2. Click the down arrow to open a list of data sorting options:
3. Select your required sorting option and click OK.

4. Browse to where you want to save your file. For example, you can insert a thumbdrive into
the MicroLab and save your file so you can open it on any computer:
5. Click the Generate button to create the file.

6. Click Exit.
81

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Spectro Scientific - An ISO 9001:2008 Company

• Average Power: 4.2 mW inside the sensor

Do not allow fluids to enter groundwater or sewers. In the event of a spill,

An item of special interest, like a time-saving tip.

Revision Date Description

A April 2016 Initial public release

B September 2017 Patents list updated.

Basic Metals Extended Metals

Unpacking Cautions and Best Practices

Part Number Description QTY

Operational 4o C to 25o C (40o F to 77o F)

Storage 4o C to 50o C (40o F to 112o F )

The system requires single-phase power.

Connecting a USB Printer

1. Unpack the printer and install it in a suitable location.

4. Complete the printer setup in accordance with the manufacturer's instructions.

7. Connect the MicroLab INPUT POWER connector to the line conditioner.

8. Power up as described below and test for internet access.

1. Press the Shutdown button in the top right corner:

Empty the Waste Bottle

Check the CheckFlush Bottle Fluid Level

The Maintenance Menu will open:

2. Click Flush. This will open the Flush Option menu:

4. Fill the sample bottle with 100 ml (3 fl oz) of CheckFlush fluid.

3. From the Maintenance Menu, click the Standardization link.

Required Sample Fluid Volumes

Metals and IR properties only 60 ml (2 fl oz)

Filling the Sample Bottle

2. Start testing the sample immediately to avoid settling.

Then skip to Select a Testing Option Screen on page 30 to continue.

The available modes are:

For this example, click Diesel Engine to select it.

It is extremely important that you enter the correct oil weight.

For this example, select 15W-40.

Follow the prompts and click OK.

The Analysis Cycle

Generating MicroLab Reports

An example of a full report is shown below:

Measure the Electrode Gap

See Replacing the Electrodes on page 48.

If you replace the electrodes, you must do Standardize Metals procedure.

Run an IR Night Flush

Follow these steps to start the process:

Use a minimum of 4 cotton swabs to clean the electrodes.

2. Repeat Step 1 with a clean swab.

Measuring the Electrode Gap

Monitoring the Lower Electrode Height

Checking the electrode height is one of the required weekly tasks.

Replacing the Electrodes

2. Turn the electrode counter-clockwise (to the left) to remove.

6. Allow the upper electrode to drop out of the electrode holder.

10. Tighten the upper electrode holder screw.

This section covers the following topics:

7. Click OK to start the test.

6. Click Yes, then follow the instructions in the check-list:

7. A message should display to confirm the Basic Metal test passed.

If the test fails, retest with a fresh sample.

• If the test fails, retest with fresh LCS fluid.

• If it fails, press Cancel and retest with fresh HCS fluid.

You will require the following:

High Visc at 40C = 142.4 High Visc at 100C = 15.0