Professional Documents
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Gem Ident LabManual
Gem Ident LabManual
AND TESTING
THE GEM
IDENTIFICATION
PROCESS
SEPARATING
RED, PINK, AND
PURPLE GEMS
SEPARATING
BLUE AND
VIOLET GEMS
SEPARATING
GREEN GEMS
SEPARATING
ORANGE, YELLOW,
AND BROWN GEMS
SEPARATING
COLORLESS AND
WHITE GEMS
SEPARATING
GRAY AND
BLACK GEMS
IDENTIFYING
IMITATIONS, ROUGH,
AND SYNTHETIC
CRYSTALS
GEM IDENTIFICATION
RI CHART
Table of Contents
Instrumentation and Testing 5
1
Acknowledgements
The Gemological Institute of America gratefully acknowledges the following people for
their participation in the preparation of this lab manual:
Technical Assistance
Abba Steinfeld, Alison Mader, Bill Herberts, Brenda Harwick, Brian Genstel, Brook Ellis,
Carl Chilstrom, Catherine Genstel, Christopher Smith, Dan Campbell, Dino DeGhionno,
Elizabeth Harvey, Eric Tollefson, Jim Shigley, Jim Viall, John Kearney, John Koivula,
Lisa Schoening, Louisa Turner, Mark Johnson, Martin Harmon, Mary Johnson,
Melissa Watson-Lafond, Michael Evans, Michael Wobby, Michele Daniels, Michelle DeVore,
Norine Honea, Phil York, Ric Taylor, Richard Hughes, Seung-Hae Moon, Sue Johnson,
Shane McClure, Tom Moses, Veronica Clark-Hudson
Photo Courtesies
The following people loaned us gem materials or otherwise assisted in gathering or
producing some of the images used in this manual:
Abe and Anisa Suleman; American Siba Corp. and Rima Investors Corp.; Andy Lucas;
Apollo Diamond Inc.; Arthur Skuratowicz; Benjamin Zucker; Bill Korst—World Gem
Resources, Ltd.; Bill Vance—Waldport, Oregon.; Brian Davenport; Charlie Eitzen—Larimar
Jewelry, St. Croix, U.S. Virgin Islands; Crystal Kingdom; Duncan Pay; DW Enterprises;
Elena Bologova—GemStones from Russia; Etienne Perret; Gary B. Wilson—Lapidary
Design Group; Gary Bowersox; Gordon Bleck; High Desert Gems; J.R. Dunn Jewelers;
Jayrock; JEOL USA, Inc.; Jonte Berlon; K&K International; Kyocera Corp.; LE MINERAL
BRMT; Marc Bielenberg; Marc Sarosi; Marisa Goebel; Mary Mathews; Mason-Kay Fine
Jade Jewelry; Meg Berry; Merilee Chapin; Michael Schramm Imports; Morion Company;
Mountain-Mark Trading Ltd.; Nafco Gems; Pala International; Revelations In Stone;
Robert Van Wagoner; Rod Griffin—Yowah, S.W.Q. Australia; Roxanne Kremer;
Steven Bookbinder; Temple Trading Company; The Gemesis Corporation; Top Geo Ltd.;
William Larson; Zareh Boyadjian
All spectra/illustrations by Peter Johnston, GIA Course Development Senior Illustrator
©
©2005 The Gemological Institute of America
All rights reserved: Protected under the Berne Convention.
No part of this work may be copied, reproduced, transferred, or
transmitted in any form or by any means whatsoever without the
express written permission of GIA.
Printed in the United States.
This manual owes its inspiration to past editions of the GIA Gem Identification Lab Manual and
Handbook of Gem Identification by Richard T. Liddicoat, Jr.
Cover photos by Eric Welch/GIA, Joel Beeson/GIA, John Koivula/GIA, Shane McClure/GIA,
Terri Weimer/GIA, and Vincent Cracco/GIA
Facing page: Gem identification is a fundamental part of the gem and jewelry business. You must
be able to identify a gem before you can grade it or place a value on it.
2
Joel Beeson/GIA
3
GEM IDENTIFICATION LAB MANUAL
RI chart—A chart that lists all the gem materials in the manual in descending RI
order. Each listing has page references to guide you to the proper entries in the
gem separation sections.
4
INSTRUMENTATION AND TESTING
General Observation 5
Color 7
Transparency 8
Cutting Style 8
Phenomena 8
Luster 10
Breaks in the Stone 11
Dispersion and Fire 11
Heft 11
Assembled Stones 12
Using Magnification 39
The Loupe 40
The Gemological Microscope 41
Fluorescence Testing 53
Procedure and Results 53
Precautions and Limitations 54
Additional Tests 55
Determining SG by Hydrostatic Weighing 55
Determining SG with Heavy Liquids 56
Using the Color Filter 59
Using a Thermal Conductivity Meter 60
Immersion 61
The Read-through Effect 62
Pavilion Flash 62
Thermal Reaction Tests 62
GENERAL OBSERVATION
During the general observation stage, you should look for characteristics that point to a gem’s most likely identity. This helps
you narrow your choices and often reduces the number of necessary tests.
GENERAL OBSERVATION
Before you start testing with instruments, you begin the gem identification process
with general observation. During this stage, you look for characteristics that point
to certain gem species and varieties and rule out others. Narrowing your choices
early helps reduce the steps needed to finally make an identification. An important
first step is to use a gemcloth to clean the gem you’re working with.
5
GEM IDENTIFICATION LAB MANUAL
Tino Hammid/GIA
General observation focuses on key attributes like color and transparency to narrow gem identification
possibilities.
6
GENERAL OBSERVATION
COLOR
Color is the combination of hue, tone, and saturation created by the various wave-
lengths of light that a stone absorbs, transmits, or reflects. Hue is the most impor-
tant factor to consider for gem identification. Tone and saturation can be useful,
but they’re generally more important for grading purposes.
To evaluate color:
1. Examine the stone under daylight-equivalent reflected light. Look at it face-up
against a white or light gray background from a distance of about 10 inches. If
you don’t have a daylight-equivalent light source, use an ordinary fluorescent
lamp. Incandescent light isn’t suitable because many stones, especially reddish
ones, look slightly different under incandescent light.
As a general rule, don’t shine light through a stone from behind to judge its
color. However, if a gem appears black in reflected light—which might occur
with a dark greenish blue sapphire or tourmaline, for example—you might have
to use transmitted light to determine the color.
2. Describe the hue, tone, and saturation of the stone. Determine the dominant and
modifying hues. When you record them, use a capital letter for the dominant
hue and lower case for the modifying hue. There’s a list of hue abbreviations in
the chart below.
Describe tone as very light, light, medium light, medium, medium dark, dark, or
very dark. Abbreviate the tone terms: for example, “vl” for very light.
Describe saturation as strong, moderate, or weak.
3. Record the presence of any unintended color zoning or banding (such as growth
zoning) as an inclusion in the magnification section of the worksheet.
4. Place the stone under incandescent light to check for color change. Record
color change only if it’s moderate or strong.
7
GEM IDENTIFICATION LAB MANUAL
TRANSPARENCY
Transparency is a material’s relative ability to transmit light. To check transparency,
shine a bright light, like a penlight or fiber-optic light, through the stone. Judge the
area where the stone’s transparency is greatest. Classify the stone’s transparency as:
Transparent (TP)—Capable of transmitting light with little or no distortion, so
objects appear clear and sharp
Semitransparent (STP)—Capable of transmitting light with some distortion, so an
object viewed through the material is indistinct
Translucent (TL)—Capable of transmitting and diffusing light so an object viewed
through the material cannot be distinguished
Semitranslucent (STL)—Capable of transmitting light only through thin areas,
usually at the edges
Opaque (O)—Incapable of transmitting light
CUTTING STYLE
Cutting style is the shape and fashioning pattern of a finished gemstone. Classify
the cutting style of the gemstone as:
Faceted (Fac)—Bound by flat, geometric, polished surfaces
Cabochon (Cab)—A curved, convex form. A single cabochon (S-cab) has a convex
top and flat base, while a double cabochon (D-cab) has a convex top and base
Buff-top (B-top)—Cabochon top and faceted bottom
Tablet (Tab)—Flat with parallel surfaces
Cameo (Cam)—A low-relief carving, often fashioned from material layered in
different colors, so the carving is raised above the underlying layer
Intaglio (Int)—A design engraved below the surface of the gem
Bead (Bd)—A gem of any shape with a drill-hole
Sphere (Sph)—Round shape with no drill-hole
Tumbled (Tum)—Polished and rounded in a mechanical tumbler and irregular
in shape
Rough (Ro)—A natural crystal or irregular shape with unpolished surfaces
Carving (Car)—Shaped into a three-dimensional form, sometimes abstract, but
often resembling an animal
PHENOMENA
Phenomena are optical effects that occur in some gem species. Phenomenal gems
are often fashioned as cabochons or tablets to display their phenomena. To look
for a phenomenon, move a strong, concentrated light source, such as a penlight or
fiber-optic light, above the stone. The types of phenomena are:
Asterism (A)—A star effect usually produced by light reflecting from minute,
precisely oriented, needle-like inclusions. In a cabochon, asterism looks like
several arms or rays of light radiating from a common center.
Adularescence (Ad)—A billowy light seen in moonstone varieties of feldspar.
Caused by diffraction, interference, and diffusion of light by minute concen-
trations within the stone of another feldspar with a refractive index (RI) slightly
different from the main mass.
Joel Beeson/GIA
Aventurescence (Av)—A colored spangle or glitter effect produced by light
The penlight is an important tool for reflecting from platelets. Seen in goldstone glass, aventurine quartz, and sunstone
detecting phenomena. feldspar.
8
GENERAL OBSERVATION
Maha Tannous/GIA
9
GEM IDENTIFICATION LAB MANUAL
LUSTER
Luster is the appearance of a material’s surface in reflected light. You judge luster
on the part of the gem where it’s highest, or where the gem has the best polish,
and you describe luster in terms of its quality and intensity. A gem’s luster can
also indicate its hardness or RI.
To determine luster:
1. Reflect light off the surface of the stone.
2. Look at all polished, rough, and fractured surfaces.
3. Classify the luster as high, medium, or low and indicate whether you’re describing
a fashioned or rough stone. Record the luster of polished surfaces under P.LUS
and the luster of fractured surfaces under FR.LUS.
Use these abbreviations on your worksheet:
HIGH LUSTER
Metallic (Metal)—The highest luster, with metal- or mirror-like reflections, as in
hematite.
Adamantine (Adam)—Reflections are sharp, as in well-polished diamond. The
highest luster possible for most transparent stones. Seen in some high-RI and OTL
materials.
Subadamantine (S-adam)—Reflections are sharp but not as sharp as adamantine.
Seen in high-RI and OTL materials such as zircon and demantoid garnet.
MEDIUM LUSTER
Vitreous (Vit)—Glass-like surface appearance. The most common luster for trans-
parent stones and glass.
Subvitreous (S-vit)—The surface might appear slightly greasy and not as glass-like
as vitreous.
LOW LUSTER
Greasy (Gre)—The surface appears coated with grease or oil, with bright but not
sharp reflections. Seen in nephrite and jadeite.
Resinous (Res)—Reflections are distinct, but neither sharp nor bright. Seen in
amber.
Waxy (Wx)—Reflections are dim and blurred, as in turquoise. The surface looks
like a wax candle or an unpolished fingernail.
Dull (Dl)—Reflections are very dim and blurred, as in poorly polished, unpolished,
or worn gems.
SHEEN
Sheen is a subcategory of luster that appears in some gems. It’s a reflection that
occurs just below the stone’s surface. If you see it, describe it using one of these
abbreviations:
Silky (Sky)—Bright but diffused reflections, similar to silk or satin fabric,
produced by a fibrous or patterned structure. Commonly seen in tiger’s-eye and
amazonite.
Pearly (Prl)—A sheen produced by structural characteristics, commonly seen in
pearl and rough moonstone.
10
GENERAL OBSERVATION
HEFT
Heft is the weight of an object compared to its size. You usually estimate it by feel,
and it gives an indication of a gemstone’s specific gravity (SG) or physical density.
It can help you separate materials with very low SG, like amber and plastic, and
very high SG, like hematite and GGG. Classify heft as high, moderate, or low.
11
GEM IDENTIFICATION LAB MANUAL
ASSEMBLED STONES
Garnet-and-glass Assembled stones consist of two or more separate
DoubletDoublet garnet pieces of material glued or fused together to form a
single piece. The most common assembled stones are
glass
doublets, with two parts, and triplets, with three
parts. The components of an assembled stone can
be natural or synthetic gems or a variety of other
colorless synthetic spinel manmade materials. Detecting them often requires
magnification, but you can sometimes see evidence
Synthetic Spinel Triplet colored of assembly during General Observation.
cement layer
Visible signs that suggest the specimen is an assem-
colorless synthetic
bled stone include:
spinel • A separation plane
Sapphire and
Synthetic Ruby • A luster difference on the crown, which
Doublet indicates a garnet-and-glass doublet
natural sapphire
• The red-ring effect, which indicates a garnet-
synthetic ruby
and-glass doublet
• A girdle plane that appears colorless when you
shine a penlight toward you, through the gem’s
girdle area, which indicates a triplet
Opal Doublet opal layer
12
USING THE REFRACTOMETER
cover
removable magnifier
polarizing filter
mirror
light portal
baffle
Peter Johnston/GIA
The refractometer provides essential gem identification information as long as the gem you’re
identifying has a testable polished surface.
13
GEM IDENTIFICATION LAB MANUAL
1.76 1.762
Peter Johnston/GIA
An RI reading taken with white light (left) is typically not as well defined as one taken with
monochromatic light (right).
14
USING THE REFRACTOMETER
FLAT-FACET TESTING
Use the following procedure to determine a gem’s RI with flat-facet testing:
1. Find the largest facet that also has the best polish.
2. Rub the facet on a piece of paper to remove dust or other material.
3. Begin with white light and no magnification (remove the eyepiece). Looking
first without magnification will help you avoid misinterpreting an OTL reading
or a vague reading.
4. Use the applicator to place a very small, pinhead-sized drop of RI liquid on the
metal stage, just behind the hemicylinder. You can remove excess RI liquid
from the applicator by touching it against the inside of the bottle first.
5. Using your fingers, place the stone on the drop of RI liquid. Slide the stone
gently from the far end, toward the center of the hemicylinder. If you’re testing
an oval, marquise, pear, or emerald cut, align the length of the stone with the
hemicylinder.
As an alternate to steps 4 and 5, you can touch the applicator a few times
against the metal stage of the refractometer, or against the lip of the RI bottle,
making increasingly smaller dots of liquid. When the last dot is about the size of
a pinhead, touch the applicator directly to the center of the hemicylinder. With
your fingers, place the stone directly on that final dot. Press very gently on the
stone to make sure it’s in contact with the hemicylinder and not floating on the
RI liquid.
If you suspect that you have too much contact liquid, pick up the stone, wipe the
hemicylinder with a tissue, and carefully replace the stone. Repeat either applica-
tion process until you have the correct amount of liquid.
6. Look at the scale on the refractometer from a distance of about 10 in. (25 cm).
Nod your head up and down and look for the facet’s outline on the scale where
the stone and hemicylinder meet. If you’re having trouble finding the outline,
slide the stone slightly forward and backward on the hemicylinder. For higher
RIs, the outline will appear as you slide the stone toward you. For lower RIs,
the outline will appear as you slide the stone away from you.
7. Find the green shade cutoff in the outline and note the approximate RI reading
at the bottom of the cutoff.
OTL stones show a shade cutoff or spectral color cutoff at approximately 1.80.
You can see this under white light with no magnification. If you’ve followed the
procedures correctly but the only reading you get is around 1.80 or 1.81—the RI
of the contact liquid—the stone is OTL and you’re finished with refractometer
testing.
8. Look at the scale under magnification to refine your reading. Place the eyepiece
on the refractometer when you see the green shade cutoff in the stone’s outline.
The green shade cutoff appears as a narrow blue-green band that covers about
two scale divisions. The RI is the highest numerical reading, which appears at
the bottom of the blue-green band. Round the RI to the nearest hundredth
(0.01).
If possible, switch to monochromatic light to sharpen the reading. The blue-green
band will change to a sharp gray line or cutoff. Read the RI at that location and
round it to the nearest thousandth (0.001).
15
GEM IDENTIFICATION LAB MANUAL
1 5
0° 1.621 1.641 120° 1.625 1.641
2 6
30° 1.624 1.641 150° 1.623 1.641
3 7
60° 1.627 1.641 180° 1.621 1.641
4
90° 1.641 1.641
Peter Johnston/GIA
To calculate a DR gem’s birefringence, rotate it 180° on the hemicylinder and note its maximum and minimum RIs every 30°. Birefringence is
the difference between the highest and lowest of all the readings. This tourmaline’s minimum RI reading is 1.621 and its maximum is 1.641. Its
birefringence is 0.020.
16
USING THE REFRACTOMETER
17
GEM IDENTIFICATION LAB MANUAL
Garnet-and-glass doublets can show the red-flag effect, which is a red reflection at
the bottom of the stone’s image. You might see this reflection when you use white
light and no magnification to take an RI reading on a stone’s table. If the garnet
cap is very thin, you might get a second, lower RI from the glass or you might see
only the RI of the glass.
Some aggregates and rocks—lapis lazuli, for example—have very poor polish, with
pitted or irregular surfaces. You can form a better seal and get a clearer reading if
you add a little extra RI liquid to fill the cavities.
If a facet isn’t perfectly flat or if there’s too much RI liquid, the facet might not be
parallel to the hemicylinder. This misalignment can cause readings to waver
between scale divisions, in an effect called parallax. Analyze another facet or
adjust the amount of RI liquid. Don’t mistake parallax for double refraction. If
parallax occurs while you’re determining birefringence, hold your head steady as
you turn the stone and polarizing filter.
If you don’t expect to use the refractometer for a month or so, coat the hemicylinder
with a thin film of petroleum jelly to prevent tarnishing. You can remove tarnish
from the hemicylinder by hand-polishing it with a paste of cerium oxide powder
moistened with water. This won’t remove scratches: If the hemicylinder becomes
too scratched or pitted, you’ll have to replace it.
CURVED-SURFACE TESTING
You have to use a method called spot reading to find the RI of a stone with curved
surfaces. The point of contact between the gem and the hemicylinder appears as a
round or oval spot on the scale. Its shape reflects the shape of the contact area.
Here’s how to take a spot reading:
1. Locate the curved area on the gem with the best polish and smoothest surface.
Since the top gets the most wear, one of the sides might be best.
2. Rub the area on a piece of paper or a gemcloth to remove dust or other material.
3. Use white light and no magnification (remove the eyepiece).
4. With the applicator, place a pinhead-sized drop of contact liquid on the metal
stage, just behind the hemicylinder.
5. Touch the curved surface of the stone to the contact liquid. To reduce the size of
the liquid drop on the stone, gently touch the stone against the metal stage on
the refractometer. With practice, you can judge the amount of contact liquid on
the stone by observing the size of the drop left behind on the metal stage.
6. Place or hold the stone gently on the hemicylinder, making sure the area with
the spot of RI liquid is in contact with the glass. If the curved surface is elon-
gated, place the stone so the long direction of the spot is parallel to the long
direction of the hemicylinder.
7. Look for the spot on the scale from approximately 10 in. (25 cm) away. The
spot should cover no more than two or three scale divisions.
The polish quality of the stone’s surface can make a difference in the appearance
of the spot. Its appearance determines the method you use to take the RI reading:
50/50, blink, or average.
With a 50/50 reading, read the stone’s RI at the point where the spot is exactly
half light and half dark. The dark or green shade is usually the bottom half of the
spot because the image of the curved surface is reversed. Well-polished stones
often give a 50/50 reading, and it’s typically the most accurate spot-RI reading.
With a blink reading, read the stone’s RI where the spot changes abruptly, or
blinks, from light to dark. This typically occurs on stones with low polish quality,
a slightly irregular surface, or sharp curves. The blink reading is usually less accu-
rate than the 50/50 reading.
18
USING THE REFRACTOMETER
Terri Weimer/GIA
Of the three types of spot readings, 50/50 readings are the most accurate (left). You read the
stone’s RI where the spot is exactly half light and half dark. With blink spot readings (center), you
read the stone’s RI at the point where the spot changes abruptly from light to dark. With average
readings (right), average the values of the last completely dark spot and the first completely light
spot on the scale.
Terri Weimer/GIA
If a cabochon or tumbled gem won’t rest on the hemicylinder, you can hold it gently in place to
take a reading.
With an average reading, the spot lightens gradually over a number of scale divisions.
To take the stone’s RI reading, average the last completely dark spot and the first
completely light spot (add them together and divide by two). This RI reading is the
least accurate spot reading, and it’s generally seen only on stones with poor polish.
19
GEM IDENTIFICATION LAB MANUAL
BIREFRINGENCE BLINK
Stones with low hardness often have poor polish, so spot and flat-facet methods
often don’t give you accurate RI readings on them. The birefringence blink method
works for stones with poor polish and high birefringence. To check for birefringence
blink, use white light and no magnification. Follow the steps for curved-surface spot
readings. The spot should be about two to three scale divisions in size.
1. Look for one of the typical spot reactions: 50/50, blink, or average.
2. After you see it, rotate the polarizing filter over the viewing lens at least 90°
and watch the spot closely.
3. If the stone has high birefringence, the spot might blink light to dark, or light green
to light red or pink, as you turn the filter back and forth. You’ll have to move your
head up and down a bit to see the blinking over the scale range. Birefringence
blink can resemble a regular spot blink, but a spot blink occurs at a specific point
on the scale, while birefringence blink occurs over a much larger area.
4. Take readings at the points where the blinking starts and stops. Estimate bire-
fringence by subtracting the low reading from the high reading.
Birefringence blink typically occurs on carbonates like azurite, azurmalachite,
calcite, calcareous coral, malachite, natural and cultured pearls, rhodochrosite, and
shell. These materials have birefringence ranging from 0.106 to 0.228, and they
might even show birefringence blink on flat-facet readings.
Spot readings on gems with moderate birefringence—like peridot and tourmaline—
sometimes show birefringence blink. Flat facets on materials with low hardness
and high birefringence, such as single crystal rhodochrosite or calcite, can also
show birefringence blink instead of a more precise reading.
1.66
birefringence = 0.17
Rhodochrosite
HIGH RI LOW RI
1.60
blinking
stops at
OTL
birefringence = 0.20
Peter Johnston/GIA
20
USING THE REFRACTOMETER
21
GEM IDENTIFICATION LAB MANUAL
VISUAL PLOTTING
Visual plotting provides seven possible results: uniaxial positive, uniaxial negative,
uniaxial with optic sign indeterminable, biaxial positive, biaxial negative, biaxial
without sign, and biaxial with optic sign indeterminable.
For visual plotting to be successful, the stone must have a flat, well-polished sur-
face and show clear RI readings. This is the visual plotting procedure:
1. Use monochromatic light and magnification.
2. Position the stone on the hemicylinder with its long direction parallel to the
length of the hemicylinder.
3. Rotate the polarizing filter over the eyepiece and look for two RI readings. You
might need to rotate the stone slightly to see both readings if you’re looking in
an optic axis direction. The readings appear as a dark gray and lighter gray cut-
off. Read the RIs at the bottom of these cutoffs and record both readings.
4. Turn the stone slowly 180° without readjusting the polarizing filter. You can
determine whether the stone is uniaxial or biaxial by observing the behavior of
the two numerical RI readings.
If one numerical RI remains constant and one varies, the stone is uniaxial. This
reflects the behavior of the ordinary ray, whose RI remains constant, and the
extraordinary ray, whose RI varies. In uniaxial stones, both RIs share a common
value. If both numerical RI readings vary, the stone is biaxial. Once you’ve deter-
mined optic character, you can take the next step, which is determining optic sign.
22
USING THE REFRACTOMETER
0o 180o
0o 180o
Biaxial
0o 180o
common
point common
point
common
Both shade point
cutoffs move
23
GEM IDENTIFICATION LAB MANUAL
24
USING THE REFRACTOMETER
Peter Johnston/GIA
1. Record the lowest value for the low numerical shade cutoff (alpha) and the
highest value for the high numerical shade cutoff (gamma).
2. Add the two values together and divide by two. This gives you the midpoint
between the two readings.
3. Record the lowest RI value for the high numerical shade cutoff and the highest
RI value for the low numerical shade cutoff. This allows you to determine the
common point (beta), which is the value that crosses the midpoint. It might be
the lowest RI value you record for the high numerical shade cutoff or the highest
RI value you record for the low numerical shade cutoff.
4. Determine whether the common point is closer to the low numerical shade cutoff
or closer to the high numerical shade cutoff. If the common point is less than the
value you calculated for the midpoint and closer to the low numerical shade cut-
off, the gem is biaxial positive. If the common point is greater than the midpoint
value and closer to the high numerical shade cutoff, the gem is biaxial negative.
If both the lowest RI for the high numerical shade cutoff and the highest RI for the
low numerical shade cutoff reach the midpoint—if the value of the common point
is exactly halfway between the high and low numerical shade cutoffs—the stone is
without optic sign.
If the high and low RI readings don’t share a common point—if neither passes
through the midpoint—you can try a different facet or use the polarizing filter to
find the intermediate RI, or common point. As you turn the filter parallel to the
refractometer scale’s horizontal divisions, one of the shade cutoffs will disappear.
The remaining shade cutoff is the common point. Once you know where the
common point is, you can work out the gem’s optic sign.
25
GEM IDENTIFICATION LAB MANUAL
1.670 1.670 1.671 1.671 1.672 1.673 1.673 1.675 1.678 1.679 1.678 1.677 1.670
1.679 1.680 1.681 1.681 1.689 1.691 1.697 1.698 1.695 1.689 1.680 1.680 1.680
Peter Johnston/GIA
26
USING THE REFRACTOMETER
1.60
1.70
1.80
1.60
1.70
1.80
1.60
1.70
1.80
Peter Johnston/GIA
CHARACTERISTIC PLOTS
These illustrations show examples of characteristic plots for uniaxial and biaxial
gems.
In uniaxial gems one shade cutoff typically remains constant during a 180° rotation
while the other moves. Gemologists sometimes call the shade cutoff that moves the
extraordinary ray. They refer to the constant shade cutoff as the ordinary ray.
If the low numerical shade cutoff remains constant during a 180° rotation and the
high numerical shade cutoff moves, the gem’s optic character is uniaxial positive.
Quartz is an example of a uniaxial positive gem.
If the high numerical shade cutoff remains constant during a 180° rotation and the
low numerical shade cutoff moves, the gem’s optic character is uniaxial negative.
Examples of uniaxial negative gems are corundum and tourmaline.
27
GEM IDENTIFICATION LAB MANUAL
1.50
Low numerical shade cutoff (alpha)
1.60
common point
(beta)
1.70
High numerical shade cutoff (gamma)
1.80
1.40
1.50
Low numerical shade cutoff (alpha)
1.60
common point
(beta)
1.70
High numerical shade cutoff (gamma)
1.80
1.50
Low numerical shade cutoff (alpha)
1.60
common point
1.70 (beta)
High numerical shade cutoff (gamma)
1.80
1.40
1.50
Low numerical shade cutoff (alpha)
1.60
common point
1.70 (beta)
High numerical shade cutoff (gamma)
1.80
28
USING THE REFRACTOMETER
1.40
1.50
Low numerical shade cutoff (alpha)
1.60
common point
(beta)
1.70
High numerical shade cutoff (gamma)
1.80
1.40
1.50
Low numerical shade cutoff (alpha)
1.60
common point
(beta)
1.70
High numerical shade cutoff (gamma)
1.80
29
GEM IDENTIFICATION LAB MANUAL
30
USING THE POLARISCOPE
GIA POLARISCOPE
analyzer
Eric Welch/GIA
power button
stoneholder attachment
light source
light portal
Peter Johnston/GIA
The polariscope has two polarizing filters: the polarizer at the bottom and the analyzer at the top.
You can move the analyzer back and forth to align the filters in the dark, or crossed, position or
the light, or uncrossed, position.
31
GEM IDENTIFICATION LAB MANUAL
A gem will give one of three reactions when you rotate it in the polariscope with the analyzer in the dark position. If the stone stays light during
rotation, it’s probably AGG (left). If it stays dark, it’s SR (center). If it blinks from light to dark and back again, it’s either DR or it’s SR with ADR (right)
and requires a confirmation test.
32
USING THE POLARISCOPE
During rotation under crossed polarizing filters, SR materials like this blue glass often show ADR
as moving bands of light and shadow. The bands are called snake-like bands, and they sometimes
merge to form a cross.
Rather than true blinking, SR materials with ADR might show moving bands of
light and shadow—often called snake-like bands—during rotation. The bands
sometimes intersect in a cross shape.
The crosshatch effect, a network of intersecting, shadowy lines that resembles
woven fabric, is typical of ADR materials like synthetic spinel.
If you see blinking, or if you think you recognize an ADR reaction, use the
confirmation test below to find out if the gem is truly DR, or if it’s SR with ADR.
CONFIRMATION TEST
There is a way to confirm double refraction with the polariscope if you see
blinking. These are the steps of that confirmation test:
1. Set the analyzer in the dark position. Shield the stone to block all light except
the light from the polariscope that’s passing through it. Use a piece of opaque
material with a small hole in it or surround the stone with your fingers.
2. Rotate the stone to the point where it appears lightest.
3. Keep looking at the lightest area of the stone as you quickly turn the analyzer
to the light position.
Both by Joel Beeson/GIA
If the gem gets noticeably lighter as you turn the analyzer, it’s SR with ADR.
If the material remains the same or appears darker as you turn the analyzer, To perform the confirmation test, set the polar-
iscope’s analyzer in the dark position and rotate
it’s DR. the gem to the position where it appears light-
est (top). Watch the lightest part of the stone
carefully as you rotate the polarizer to the light
PRECAUTIONS AND LIMITATIONS position. If the gem remains the same or gets
darker, it’s DR (bottom).
A gem must be transparent to translucent for testing with the polariscope. Don’t
test opaque and near-opaque stones with a polariscope.
The gem must be large enough for you to detect and interpret its reactions to
polarized light. If the stone is very small, try placing the magnifier from a refrac-
tometer on top of the polariscope’s analyzing filter. The magnifier can help you
see the reaction a little better.
Highly included SR or DR stones can give AGG reactions if they contain inclusions
that scatter light. Consider only the transparent areas of the stone you’re testing.
33
GEM IDENTIFICATION LAB MANUAL
All synthetic spinels and many red, orange, and purple garnets show strain, which
affects how light passes through a gem and can cause a false polariscope reading.
Gems like amber, glass, and opal, assembled stones, and OTL gems can also give
indefinite results with the polariscope. Some SR gems that are OTL can appear to
be DR. It’s best to confirm SR or DR in OTL stones by looking for the absence or
presence of doubling under magnification.
If you have a high-RI gem—especially a round brilliant cut—don’t place it face-
down because most of the light will reflect back into the polarizer from the gem’s
pavilion facets. Turn the gem on its side, and try that orientation instead.
If you get an SR reaction, examine stones in at least three different directions to
make sure you’re not analyzing an optic axis direction in a DR stone.
You must confirm any DR or ADR reaction, but you don’t need to confirm an SR
or AGG reaction.
Joel Beeson/GIA
34
USING THE POLARISCOPE
You won’t find interference colors on every gem you test. When The “double L” is a uniaxial The Airy’s spiral is a uniaxial
you don’t, you can look for a dark shadow—the brush—that optic figure that resembles a optic figure that’s unique to
sweeps across the stone as you move it. Touch the optic figure cross with distorted L-shaped quartz.
sphere to the narrowest part of the brush to find the gem’s optic arms. Make sure you don’t
figure. mistake it for a biaxial optic
figure.
A typical biaxial optic figure You might see this type of If the angle between a biaxial
resembles a bow-tie dividing biaxial optic figure if a biaxial gem’s optic axes is very small,
concentric circles. gem’s two optic axes are the brushes might appear to
close together. It resembles a intersect. This makes a figure
“figure 8” divided by a dark that’s very similar to a uniaxial
shadow. figure. Fortunately, stones with
this type of biaxial optic figure
are rare.
35
GEM IDENTIFICATION LAB MANUAL
CONFIRMATION TEST
Perform this test when you resolve only a partial optic figure, such as one-half of
a biaxial or one-fourth of a uniaxial figure. This might occur with a highly frac-
tured stone.
1. Find the partial optic figure under crossed polarizing filters.
2. Rotate the stone horizontally while you’re looking at it exactly in the optic axis
direction.
3. If the brush moves in the direction opposite the rotation, the stone is biaxial; if
the brush doesn’t move, the stone is uniaxial.
Partial optic figures are more difficult to identify than full ones. With the polariscope in the dark position, locate the partial optic figure, which
resembles a brush. If the brush doesn’t move as you turn the stone 180°, the figure is uniaxial (left). If the brush turns away from the direction of
rotation, the figure is biaxial (right).
36
USING THE DICHROSCOPE
Terri Weimer/GIA
You can use a dichroscope on rough or fashioned, loose or mounted, transparent or semitransparent
stones. If a stone is pleochroic, a dichroscope shows two colors in most viewing directions.
37
GEM IDENTIFICATION LAB MANUAL
5. Repeat the process until you’ve looked at the stone from at least three
PLEOCHROISM CONFIRMATION TEST
directions. If you examine a pleochroic stone in an optic axis direction, you
won’t see its different colors. If you look in only one direction, you might
mistake an optic axis view for a non-pleochroic result. If you look in at least
three directions and still see no color differences, the stone is not pleochroic.
If you see the same two colors from different viewing directions, the stone is
dichroic. The presence of two pleochroic colors proves the stone is DR, but
doesn’t tell you whether it’s uniaxial or biaxial. Continue checking the stone in
other directions for a third pleochroic color. If it’s present, it will be paired with
one of the other two colors. If this occurs, the stone is trichroic. The presence of
three pleochroic colors also proves the stone is biaxial.
38
USING MAGNIFICATION
Terri Weimer/GIA
Magnification is the most important tool for separating natural gems from their synthetic counter-
parts.
USING MAGNIFICATION
Magnification can help you determine if a gem is treated or if it contains internal
fractures, vulnerable cleavages, or other structural defects. It’s one of the most
important tools for separating natural gems from synthetics. This is a vital separation
because there’s such a large value difference between many synthetic gems and their
natural counterparts of equivalent quality.
39
GEM IDENTIFICATION LAB MANUAL
THE LOUPE
Loupes are portable, affordable, and versatile gem identification tools. By practicing
the techniques outlined below, you can master the loupe and maximize its effective-
ness in the gem identification process. Make sure you have a fully corrected 10X
triplet loupe.
40
USING MAGNIFICATION
GEMOLOGICAL MICROSCOPE
oculars
pod
zoom adjustment
objectives
overhead light
focus adjustment
light well
stage
base
Eric Welch/GIA
The microscope is a standard gem-testing instrument that’s highly sophisticated. Familiarize your-
self with its parts before you begin using it.
41
GEM IDENTIFICATION LAB MANUAL
42
USING MAGNIFICATION
To create darkfield illumination, close the baffle With the light well’s baffle open, brightfield
and turn on the well light. illumination transmits light up through a trans-
parent stone to your eye.
To create diffused illumination, open the baffle To produce reflected illumination, use the To create polarized illumination, open the
and place a tissue, a translucent white plastic microscope’s overhead light. Make sure you microscope’s baffle, place one polarizing filter
plate, or the white plastic cover from the micro- turn the well light off. over the light well, and hold another between
scope light over the well on the stage. the stone and the objectives. Rotate the hand-
held polarizing filter to cross the filters.
TYPES OF ILLUMINATION
A microscope offers many lighting options. Different types of lighting work best
for seeing different gem features. The most useful techniques are darkfield, bright-
field, diffused, reflected, and polarized lighting.
Darkfield illumination—View the stone against a black, non-reflective back-
ground (the baffle) and light it from the side by turning on the well light with the
baffle in place. Inclusions stand out as bright objects against a dark background.
This is the most common type of illumination in gemology.
Brightfield illumination—Open the baffle and light the stone directly from
below. Inclusions should stand out as dark objects against a bright background. All by Eric Welch/GIA
This method helps you find curved striae or other low-relief or structural To create pinpoint brightfield illumination, keep
inclusions. the baffle open and close the iris diaphragm
until its opening is smaller than the stone.
Diffused illumination—Open the baffle and place a diffuser plate, facial tissue, or
other translucent material over the light. Illuminate the stone from behind. The
light softens and scatters, helping you see color zoning and banding.
Reflected illumination—Light the stone from above and look for surface charac-
teristics in reflected light. Also called vertical overhead illumination.
Polarized illumination—Look at the stone in an illuminated field between
crossed polarizing lenses. This helps you see optic figures, pleochroism, strain,
and other effects normally seen in the polariscope.
Pinpoint brightfield illumination—Open the baffle and close the iris diaphragm
to restrict the light source to a small opening directly beneath the stone. This lets
you see curved striae and other structures more clearly.
43
GEM IDENTIFICATION LAB MANUAL
To create horizontal illumination, direct a fiber- To create oblique illumination, direct a fiber-
optic light at the gem from the side. optic light toward the gem at an angle between
horizontal and overhead.
44
USING MAGNIFICATION
Eric Welch/GIA
To use a standard immersion cell to examine a gem’s interior, place the cell on a diffused light
source like the microscope’s upturned fluorescent light. To use magnification, place a diffuser plate
or a facial tissue over the well light and place the immersion cell on top.
IMMERSION
Immersion makes it easier to see into the stone. This is the procedure:
1. Fill the immersion cell with methylene iodide, glycerin, mineral oil, or water to
reduce reflection and refraction.
2. Use brightfield illumination, and place a diffuser plate or facial tissue under the
immersion cell to diffuse the light.
45
GEM IDENTIFICATION LAB MANUAL
Taijin Lu/GIA
Doubling proves double refraction. It’s especially helpful for identifying OTL gems.
46
USING THE SPECTROSCOPE
Eric Welch/GIA
With the correct illumination, the spectroscope is one of the most useful gem-testing instruments. For best results, use a
concentrated light source.
47
GEM IDENTIFICATION LAB MANUAL
PRISM SPECTROSCOPE
slit control
drawtube
prisms
lens
A prism spectroscope usually has an adjustable slit to control the amount of light that enters the
instrument. A drawtube lets you focus on different parts of the spectrum.
DIFFRACTION-GRATING SPECTROSCOPE
lens
TYPES OF SPECTROSCOPES
There are two basic types of spectroscopes, the prism spectroscope and the
diffraction-grating spectroscope. Each one shows the spectrum in a different way.
• With a prism spectroscope, the hues in the spectrum don’t spread evenly.
They’re stretched out in the blue and violet end and compressed in the red
end. This makes it more difficult to see absorption in the red, but easier in the
violet. The spectrum itself is usually bright. Most desktop models are prism
spectroscopes.
48
USING THE SPECTROSCOPE
Diffraction-
grating type
TRANSMISSION METHOD
The transmission method is best for transparent to translucent stones. With this
method, you shine light directly through the gemstone from below. If the stone is
faceted, turn it table-down so there are fewer reflections to interfere with your
reading. You might have to try other orientations, too. Start with the light on a low
setting and bring the brightness up slowly so you don’t overwhelm the spectrum
and miss any fine lines that might be there.
With a desktop spectroscope, follow these steps:
1. Close the iris diaphragm in the instrument’s base and place the stone on it.
2. Adjust the iris opening to a size appropriate for the size of the stone. Only light
passing through the stone should enter the slit of the spectroscope.
3. Adjust the intensity of the light with the rheostat. Try a lower intensity for light-
colored stones and a higher intensity for dark or translucent stones.
4. Adjust the distance between the spectroscope and the stone until you see the
spectrum. You might need the stone to be as close as 0.5 inch or as far as 2
inches (about 1.25 cm to 5.00 cm) from the spectroscope.
5. Close the slit on the spectroscope completely, and then open it slowly until you
see the entire spectrum. The slit should be barely open when you look at a
transparent stone’s spectrum. Open the slit a little more when you work with
translucent stones, or to see absorption in the violet and blue regions. For best
results, look for an absorption spectrum just as the slit begins to open.
6. Start with the drawtube pulled all the way up and use it to focus the spectrum. Peter Johnston/GIA
If you push in or shorten the tube, absorption in the blue looks sharper. If you To use the transmission method to see a trans-
then pull the tube out slightly, absorption in the red looks sharper. parent-to-translucent gem’s absorption spec-
trum, you shine light directly through it from
7. Change the position of the stone until you find the maximum absorption. A below.
stoneholder can make handling the stone easier.
49
GEM IDENTIFICATION LAB MANUAL
With the internal reflection method, light enters the gem’s pavilion, reflects off its table, and exits
through its pavilion. The method works well with small, light-toned, transparent stones because it
forces the light to follow a longer path through the gem.
Use the external reflection method, which reflects light off the stone’s surface, only for opaque
stones.
50
USING THE SPECTROSCOPE
51
GEM IDENTIFICATION LAB MANUAL
cutoff
lines band
• Cut or shape: For best results, transmit light through the long direction of
light-colored, transparent stones and through the short direction of dark,
translucent stones.
• Dust or dirt in the slit: This can cause distracting dark, horizontal lines in the
spectrum.
• Heat: If the temperature is too high, this changes the spectrum or makes it
difficult to see.
If you don’t succeed at first, try a different lighting method. For example, if you
can’t see a spectrum with transmitted light, try reflected light.
Cooling a diamond in liquid nitrogen helps make its spectrum more visible.
Remember, not all types of stones have diagnostic absorption spectra, so the
instrument can’t be used with every stone. However, if a stone shows a consistently
distinctive absorption spectrum, that can help a lot in its identification.
Remember that some pleochroic gemstones show different spectra from different
directions, so examine a gem from more than one direction. In addition, it’s best to
examine the stone with a 10X loupe before using the spectroscope. This helps you
avoid misinterpreting the spectra of assembled stones.
RESULTS
A spectroscope shows absorption in nanometers (nm), which equal one millionth
of a millimeter. The types of absorption patterns include:
Lines—Narrow and sharply defined
Bands—Well defined and wider than lines
Cutoff—Complete absorption, extending from a distinct edge to the end of the
spectrum. Often found in the blue or violet area.
General absorption—Vaguely defined absorption that covers a large area of the
spectrum.
Emission lines—Bright, sharp, vertical lines seen in the red area of the absorption
spectra of some gems colored by chromium.
52
FLUORESCENCE TESTING
FLUORESCENCE TESTING
Characteristic reactions to ultraviolet (UV) radiation can help you separate certain
natural gems from their synthetic counterparts. It can also tell you if a stone is
assembled. A modern use of UV fluorescence testing is to detect emerald treat-
ments that use oils and manmade resins.
Eric Welch/GIA
You need a UV lamp and either a viewing cabinet or contrast-control spectacles to test gems for
fluorescence and phosphorescence.
53
GEM IDENTIFICATION LAB MANUAL
5. If the stone looks inert when it’s sitting beside the comparison stone, remove
the comparison stone. Strong fluorescence in the comparison stone can over-
whelm weak fluorescence in the tested stone.
Make sure the “fluorescence” is not simply light reflecting from the stone. Beware
of red, violet, or purple reflections that look like weak fluorescence. If you’re testing
with SW and you want to check for reflections, put a piece of window glass between
the lamp and the stone. If the effect remains, the reflections are not fluorescence.
SW does not pass through ordinary glass.
6. Record the energy source (LW or SW) and what you see. If there’s no fluores-
cence, write “inert.” If the stone fluoresces, describe both the strength and the
color.
Describe the strength of fluorescence as weak (barely visible), moderate (distinctly
visible), or strong (bright). You can abbreviate the strength description as W, M, or
S, or circle the appropriate letter on the worksheet. Also note if the fluorescence is
uneven, patchy, or zoned.
Fluorescent color is most often described by its hue. Occasionally, gemologists
use modifiers that refer to tone or saturation, such as “light” or “brownish.” You
might sometimes want to use descriptive terms like “chalky white” or “brick red.”
For some gems, fluorescent reactions differ When you judge a stone’s fluorescence, think about its transparency as well.
with the type of UV radiation. Under LWUV, the
natural ruby at left reacts with weak red fluores-
Fluorescence in translucent and opaque stones often looks like a glowing surface
cence, while the flame-fusion synthetic ruby at coating. In transparent stones, it looks like an internal glow combined with a
right glows a very strong orangy red (top). glowing surface.
Under SWUV, the natural ruby is almost inert,
but the synthetic ruby appears a moderate to 7. Turn the lamp off and watch for phosphorescence. Note how long it lasts if
strong orangy red (bottom). you’re making a separation that depends on that reaction and its duration.
8. Switch to the other UV light source. Look for fluorescence and record what
you see.
9. Turn the lamp off and watch for phosphorescence. Note how long it lasts if you
want to make a separation that depends on that reaction and its duration.
10. Make absolutely sure that the UV lamp is switched off. Then, if you used
contrast-control spectacles, you can take them off. If you used a viewing
cabinet, remove the stone from the cabinet.
54
ADDITIONAL TESTS
Eric Welch/GIA
To use an electronic scale for hydrostatic weighing, you need a special holder, a beaker, a wire stand, and a wire basket.
ADDITIONAL TESTS
The additional and advanced tests in this section are grouped separately because
the tests might be limited to specific separations, the test results—and conclusions
drawn from them—might vary widely depending on the type of specimen, and
some of the tests might be destructive.
55
GEM IDENTIFICATION LAB MANUAL
56
ADDITIONAL TESTS
You can use special calibrated liquids to determine a stone’s SG. The stone at left floats because its
SG is lower than the liquid’s. The stone in the center stays in position because its SG is about the
same as the liquid’s. The SG of the stone at right is higher than the SG of the liquid, so it sinks.
A typical set of SG liquids includes five liquids with SGs of 2.57, 2.62, 2.67, 3.05,
and 3.32. Because the liquids are toxic, each liquid comes in a small bottle with a
childproof screw cap.
The 2.57-SG liquid can often help separate feldspars like microcline (2.54 SG)
and orthoclase (2.58 SG) from chalcedony (2.60 SG). Chalcedony usually sinks
fairly quickly, while the feldspars float, remain suspended, or sink very slowly.
The 2.62 liquid can be useful for separating chalcedony (2.60 SG) from quartz
varieties with larger twin or single crystals and SGs around 2.65.
The 2.67 liquid was useful for separating natural emerald from some flux-grown
synthetic emeralds. Today, newer types of hydrothermal synthetic emeralds have SGs
within the range of natural emeralds, so it’s not as easy to use SG to separate them.
The 3.05 liquid can be useful for separating tourmaline, with an SG between 3.00
and 3.12, from the gems that resemble it, such as spodumene (3.18 SG) and topaz
(3.52 SG).
The 3.32 liquid can separate nephrite (2.90 to 3.02 SG) from jadeite (3.30 to 3.50 SG).
57
GEM IDENTIFICATION LAB MANUAL
CALIBRATION STONES
To maintain their accuracy, heavy liquids must be periodically checked and cali-
brated. To check a liquid’s SG, gemologists use comparison stones of known SG.
They’re also known as calibration stones or indicator stones.
• 2.57-SG liquid: top, microcline (SG = 2.56); bottom, chalcedony (SG = 2.60)
• 2.62-SG liquid: top, chalcedony (SG = 2.60); bottom, quartz (SG = 2.66)
• 2.67-SG liquid: top, synthetic emerald (SG = 2.66); bottom, calcite (SG = 2.70)
• 3.05-SG liquid: top, pink tourmaline (SG = 3.04); bottom, green tourmaline
(SG = 3.06)
• 3.32-SG liquid: bottom, jadeite (SG = 3.34), synthetic corundum (SG = 4.00),
CZ (SG = 5.80)
58
ADDITIONAL TESTS
Cobalt causes the blue color you see in synthetic blue spinel under incandescent light (left). Gems colored by cobalt transmit red light but absorb
yellowish green light, so they appear pink to red through a color filter (right).
59
GEM IDENTIFICATION LAB MANUAL
60
ADDITIONAL TESTS
61
GEM IDENTIFICATION LAB MANUAL
Eric Welch/GIA
Comparing read-through in round brilliants can help you separate diamond from its simulants. The
diamond at far left shows no read-through, while the YAG at far right shows extreme read-through.
PAVILION FLASH
Checking for pavilion flash might help you distinguish among certain OTL, SR,
colorless diamond simulants. You might want to use it in conjunction with the
read-through test, as it’s most useful for separating the three SR diamond simu-
lants that show some read-through when cut as well-proportioned round brilliants:
CZ, GGG, and YAG.
1. Hold the stone table-down and examine it under magnification. If you’re using a
microscope, darkfield lighting works well, although you can use reflected light.
2. Gently rock and tilt the stone until you see colors flash across the pavilion.
Don’t dip the stone into the well light because this can create unwanted reflections.
Diamond simulants show a broad monochromatic flash across some or all of the
pavilion.
• CZ usually shows a broad orange flash over most of its pavilion surface.
Both by Mike Havstad/GIA • GGG also shows an orange and blue pavilion flash, but it’s less extensive than CZ.
A round-brilliant GGG shows an orange and • YAG generally shows a blue and violet flash over about one half of its pavilion.
blue pavilion flash (top) while a similarly cut
YAG shows blue and violet (bottom).
62
ADDITIONAL TESTS
To use a hot point, touch or nearly touch the test specimen with the instrument in
an inconspicuous place and then smell or observe the results.
The TRT can detect oil- or polymer-filled fractures in transparent gems. It can
also help identify some organic gems by causing them to produce distinctive odors
when they’re brought close to the heated tester.
Testing with the TRT is generally destructive to the specimen. It should always be
done with great care and with permission from the stone’s owner. You should
never use destructive tests on the gems in GIA stone sets.
63
THE GEM IDENTIFICATION PROCESS
General Observation 66
Instrument Tests 67
Additional Tests 68
GENERAL OBSERVATION
Color, transparency, cut, phenomena, luster,
dispersion/fire, heft, assembly
10X MAGNIFICATION
Assembly, fracture, fracture luster,
doubling, cleavage
REFRACTOMETER
Refractive index, birefringence,
sr/dr
POLARISCOPE
Determine or confirm sr/dr, agg, DICHROSCOPE
sr/adr Confirm sr/dr (when
polariscope is not
recommended)
IDENTIFY STONE
Species, required treatments, variety, and group
as necessary
Successful gem identification depends on following a logical sequence of tests and observations.
65
GEM IDENTIFICATION LAB MANUAL
GENERAL OBSERVATION
Begin the gem identification process with general observation, first with your unaided
eye and then with a loupe. The characteristics you observe and record at this stage
help you narrow the possibilities. Place a dash (—) next to categories that don’t
apply to the gem you’re testing.
1. Start by observing the stone’s color. Look at the stone face-up against a neutral
white or light gray background, about 10 inches below a source of daylight-
equivalent light. At the COLOR position in the GENERAL OBSERVATION
column on the worksheet, record the stone’s tone, hue, and saturation.
2. Look for eye-visible pleochroism and color zoning or banding by turning the gem
in the light and looking at it from different angles. If you see eye-visible pleochro-
ism, wait until you’ve checked with the dichroscope before you mark the
PLEOCHROISM section on your worksheet.
3. Determine the gem’s transparency. After completing the color and transparency steps,
you’ll usually narrow your choices from dozens to just a few possibilities. Color and
transparency are key indicators that narrow your gem-identification options.
4. Examine the gem’s cutting style because it can sometimes provide clues to identity.
5. Check for the appearance of a phenomenon. It might also narrow the possible
identifications. To look for phenomena, move a strong, concentrated light like a
penlight or fiber-optic light back and forth above the stone. Also, check the gem
for color change by looking at it under daylight-equivalent light and then switching
to incandescent light.
6. Luster is another clue to a gem’s identity. Stones with higher RIs and hardness ratings
generally have better polish and luster. Poor polish, wear, and abrasions can mask a
gem’s luster, so you should judge luster on the area with the best polish.
7. Dispersion is a gem’s ability to separate white light into spectral colors. This property
can help you get closer to a gem’s identity because gems vary in their ability to dis-
perse white light and display the resulting flashes of color called fire. It’s most useful
with colorless OTL gems that simulate diamond. Based on the amount of fire you see,
record dispersion as weak, moderate, strong, or extreme.
8. Heft is a gemstone’s weight in relation to its size. Heft can help you separate
stones with low specific gravity (SG) from stones with high SG. You can’t test
mounted stones for heft.
9. Examine the stone as well as you can with your unaided eye and your loupe. Look for
signs that the gem might be assembled, like luster differences or separation planes.
10. Examine the stone for surface breaks with your loupe under reflected light. The
nature and luster of a break can provide clues to the stone’s identity. The three
types of breaks are cleavage, parting, and fracture. Pay close attention to vulnerable
areas like the girdle and culet.
66
THE GEM IDENTIFICATION PROCESS
Once you’ve completed the general observation stage, you should have a much narrower
list of possible identifications. Then you can move on to the instrument tests.
INSTRUMENT TESTS
You won’t be able to confirm a stone’s identity with general observation alone. There
are limits to what you can observe and conclude with just your eyes and a loupe. To
continue the identification process, you must use more sophisticated gem-testing
instruments. With careful use of these tools, you can identify most commercially
available gems. If you’re still in doubt about a gem’s identity after you perform all
required tests, send the gem to a reputable gemological laboratory—like the GIA
Gem Laboratory—for positive identification.
REFRACTOMETER
The refractometer is the most important primary instrument for gem identification.
With it, you can get an RI reading from the polished surface of all but the few stones
that are OTL. Because many RIs are specific to certain stones, they’re especially
valuable for making identifications.
1. Begin by testing under white light with no magnification. When you see the green
shade cutoff, you can refine your reading by looking at the scale under magnification
and switching to monochromatic light, if available. If the shade cutoff doesn’t
move, the gemstone might be SR. Test the gem in three different positions, rotating
the polarizing filter 90° each time. If the shade cutoff remains stationary, the gem
is probably SR. Enter the stone’s RI at the HI position in the RI/BIREFRINGENCE
column on your worksheet.
2. If the shade cutoff moves when you rotate the polarizing filter 90°, the gem is DR.
Rotate the stone 180°, stopping every 30° to check and record the highest and lowest
numerical RI readings. Subtract the lowest of the low numerical readings from the
highest of the high numerical readings to get the gem’s birefringence.
3. In the RI/BIREFRINGENCE column on your worksheet, record a DR stone’s RI
figures at HI, LO, and BIRE.
4. If you’re testing a curved surface with the spot method, write your results in the SPOT
position.
POLARISCOPE
The polariscope determines if a gem is SR, DR, SR/ADR, or AGG. You can also use
a polariscope to resolve a gem’s optic figure and to detect pleochroism.
1. If you get an SR reaction when you’re testing for SR/DR/ADR/AGG, test the
stone in three directions.
2. Use the confirmation test to distinguish between DR and SR/ADR.
3. Record your results in the worksheet’s OPTIC CHARACTER column.
4. If after consulting the lab manual, you find that optic character is a key separation
test, use your optic figure sphere to determine it.
Now that you’ve listed the gem’s characteristics under general observation and
recorded its RI, birefringence, and polariscope reactions, check this manual’s separa-
tion sections and RI chart. The separation sections of the manual list gems by color
and transparency in descending RI order and list key separation tests that will help
you make a final identification.
If you can’t narrow the possibilities using the color and transparency lists, you can refer
to the RI chart. The chart lists RIs in descending order to make it easier to search for
that property alone. Once you find the RI that matches the gem you’re testing, turn to
the page listed on the chart for key separation tests and more information.
67
GEM IDENTIFICATION LAB MANUAL
DICHROSCOPE
The dichroscope helps you detect characteristic pleochroism and confirm double
refraction. To determine if the dichroscope is a required test, refer to the relevant
separation section in this manual. Enter your results in the worksheet’s
PLEOCHROISM column.
MICROSCOPE OR LOUPE
Magnification is the next step. It’s the key tool for separating natural from synthetic
gems and for detecting treatments. Enter your results in the INCLUSIONS column
on your worksheet.
SPECTROSCOPE
The spectroscope reveals distinctive absorption in some gems. Refer to the relevant
separation section in this manual to determine when it’s a required test and which
absorption patterns to look for. If you see a recognizable spectrum, sketch the results
in the ABSORPTION SPECTRUM column.
ADDITIONAL TESTS
At this point, you might have to use one or more additional tests to identify the stone.
1. Although fluorescence rarely identifies a gemstone, it’s information that can
help separate one gem from another and confirm the results of other tests.
Record the strength and color of the stone’s reaction to both LWUV and
SWUV. If the stone doesn’t fluoresce, record it as inert.
2. Record the numerical estimate that results from any SG tests. Record an L if you
use heavy liquids to determine SG. Record an H if you use the hydrostatic SG
method.
3. If you use any other tests, like thermal conductivity or the color filter, record
their results.
Identification No. 1 The stone is transparent, dark bluish green, and faceted.
It has vitreous luster and no noticeable dispersion. There’s no evidence that it’s assembled,
and no sign of fracture or cleavage. The gem has moderate heft.
Step 1—GENERAL OBSERVATION: List the gem’s color, transparency, etc.
Step 2—RI/BIREFRINGENCE: Using monochromatic light, you get a maximum RI reading
Tucker Gems
of 1.644 and a minimum reading of 1.624 with the refractometer. Subtracting the low read-
Tourmaline
ing from the high reading gives you a birefringence of 0.020. As you rotate the gem, both
RIs meet at a common point, but only the shadow edge that marks the lower numerical read-
ing moves. This tells you that the gem is DR and uniaxial negative.
Step 3—LAB MANUAL: You consult the lab manual’s “transparent green” section to narrow
the stone’s possible identities and to determine key separation tests. The manual gives tour-
maline as the only choice and lists RI and birefringence as key tests. There’s no need for fur-
ther testing.
Step 4—VARIETY/SPECIES: Record the gem’s species as tourmaline. There’s no required
variety call for this gem.
69
GEM IDENTIFICATION LAB MANUAL
70
THE GEM IDENTIFICATION PROCESS
and determine single or double refraction. You see two pleochroic colors: greenish Zircon
blue and nearly colorless. This confirms the gem is DR.
Step 4—LAB MANUAL: You consult the lab manual’s “transparent blue” section to
narrow the stone’s possible identities and to determine key separation tests. The
manual lists zircon, with doubling and spectrum as the key tests.
Step 5—MAGNIFICATION/INCLUSIONS: You check with a loupe or a microscope
for doubling. You observe strong doubling and many tiny abrasions along the facet
junctions.
Step 6—ABSORPTION SPECTRUM: You see a typical zircon spectrum with the
spectroscope.
Step 7—VARIETY/SPECIES: Record the gem’s species as zircon. There’s no
required variety call for this gem. Magnification (doubling), absorption spectrum,
and dichroscope reaction were key tests.
71
GEM IDENTIFICATION LAB MANUAL
Opal triplet Step 2—RI/BIREFRINGENCE: Using white light, you get a spot-RI reading of 1.54 on
the stone’s top portion.
Step 3—LAB MANUAL: You consult the lab manual’s “assembled” section to narrow
the stone’s possible identities and to determine key separation tests. The manual lists
opal triplet and synthetic opal triplet as possibilities. The manual lists magnification as
a key test.
Step 5—MAGNIFICATION: Viewing the stone through its colorless top, you detect
play-of-color patches of varying size and color distribution. These are characteristic of
natural opal. There are no mosaic patches of color with a snakeskin or scale-like
structure that would be typical of synthetic opal. This confirms that the layer with
play-of-color is natural.
Step 6—VARIETY/SPECIES: Record the gem’s species as opal triplet. There’s no
required variety call for this gem. General observation and magnification were the key
tests.
72
THE GEM IDENTIFICATION PROCESS
GENERAL OBSERVATION
Start by judging the gem with your unaided eye. Use a 10X loupe to detect breaks
or evidence of assembly. Record your observations.
COLOR—Record the gem’s tone, hue, and saturation.
TP—Record the gem’s transparency.
CUT—Record whether the gem is faceted, a cabochon, a bead, etc. (It’s not
necessary to specify the cut in any detail.)
PH—Identify the phenomenon, if present.
P.LUS—Judge the gem’s polish luster where the polish is best.
DISP—Record the strength of dispersion, if fire is present.
HEFT—Record whether the gem feels heavy or light in relation to its size.
ASSEM—Record any sign of an assembled stone: red ring, separation plane, etc.
FR—Record the type of fracture, if present.
FR. LUS—Record the luster of the fracture surface, if present.
CL—Record the number of cleavage directions and the angle of intersection, if any.
RI AND BIREFRINGENCE
Test for RI—and birefringence on DR stones—and use this section to record your
results.
HI—Record the highest RI of a DR stone or the single RI of an SR stone.
LO—Record the lowest RI of a DR stone.
BIRE—Record a DR stone’s birefringence.
SPOT—Record a spot reading if a flat-facet reading isn’t possible.
MISC—Record any extra comments, such as poor polish, a red-flag effect on a
garnet-and-glass doublet, etc.
73
GEM IDENTIFICATION LAB MANUAL
If the stone is DR and transparent, you might look for a uniaxial or biaxial optic
figure when this information is necessary to identify the stone. If you find evidence
that the stone is uniaxial or biaxial, circle the U or B. If you observe a very specific
type of optic figure, like a bull’s-eye or Airy’s spiral, note it. You can also determine
optic character with the refractometer by using visual plotting.
U—Circle U for a uniaxial optic figure.
B—Circle B for a biaxial optic figure.
You might need to find optic sign for a few advanced separations. You can
generally determine it by plotting the refractometer readings. Record the results
of your test. Circle + (positive) or – (negative), or write in w/o (without) or i/d
(indeterminable).
At this point, consult the separation section or RI chart in this manual to refine
your list of possibilities. The manual will also tell you which key separation tests
are best for making a final identification.
PLEOCHROISM
Use a dichroscope if one is available. If not, use a polariscope. If you detect
pleochroism, note its strength by circling S (strong), M (moderate), or W (weak).
List the colors you see next to the numbers 1, 2, and 3. You might need to use this
test to check whether some gems—such as red garnet or ruby—are DR.
ABSORPTION SPECTRUM
If you see a recognizable absorption pattern, record it by drawing any lines, bands,
or cutoffs on the blank spectrum diagram.
ADDITIONAL TESTS
Indicate any additional tests you might have performed:
SG—If necessary, record an estimate of the stone’s SG. Circle L if you used SG
liquids or H if you used hydrostatic weighing.
CF—If necessary, record the stone’s reaction to the color filter.
LW—If necessary, record the stone’s reaction to LWUV.
SW—If necessary, record the stone’s reaction to SWUV.
74
THE GEM IDENTIFICATION PROCESS
WORKSHEET ABBREVIATIONS
Because space on the worksheet is limited, you might want to use the abbreviations
listed on the next pages. If no abbreviation is listed, write out the full word.
General Observation
Other
Hue C colorless Polish Luster (P.LUS)
P purple W white Metal metallic
rP reddish purple Gr gray Adam adamantine
RP/PR red-purple/purple-red Bl black S-adam subadamantine
stpR strongly purplish red Pi pink (light tones and low Vit vitreous
slpR slightly purplish red saturations of red or pur-
S-vit subvitreous
ple)
R red Gre greasy
Br brown (low saturations of
oR orangy red red, orange, and yellow) Res resinous
RO/OR red-orange/orange-red
Wx waxy
rO reddish orange
Transparency (TP) Dl dull
O orange
TP transparent Sky silky
yO yellowish orange
oY orangy yellow STP semitransparent Prl pearly
Y yellow TL translucent
gY greenish yellow STL semitranslucent
Dispersion (DISP)
YG/GY yellow-green/green-yellow O opaque
Ex extreme fire
styG strongly yellowish green St strong fire
yG yellowish green Cut Mod moderate fire
slyG slightly yellowish green Fac faceted Wk weak fire
G green Cab cabochon
vslbG very slightly bluish green Bd bead
bG bluish green Sph sphere Heft
vstbG very strongly bluish green Tab tablet Hi high
GB/BG green-blue/blue-green Cam cameo Mod moderate
vstgB very strongly greenish blue Int intaglio Lo low
gB greenish blue Car carving
vslgB very slightly greenish blue Tum tumbled
B blue Ro rough continued on next page....
75
GEM IDENTIFICATION LAB MANUAL
76
SEPARATING RED, PINK, AND PURPLE GEMS
Many important stones fall into the category of transparent red to purple gems. The list includes
corundum, garnet, quartz, and topaz.
77
GEM IDENTIFICATION LAB MANUAL
2.417 Naturally colored diamond Irradiated diamond, synthetic diamond, CZ, zircon, YAG
SR (Page 83)
2.417 Irradiated-color diamond Naturally colored diamond, synthetic diamond, CZ, zircon, YAG
SR (Page 84)
2.150 CZ (synthetic cubic zirconia) Diamond, irradiated diamond, synthetic diamond, zircon, YAG
SR (Page 86)
1.925 to 1.984 (high type) Zircon Diamond, irradiated diamond, synthetic diamond, CZ, YAG, spessar-
1.810 to 1.815 (low type) (Page 86) tite, almandite
DR
1.833 YAG (yttrium aluminum garnet) Diamond, irradiated diamond, synthetic diamond, CZ, zircon, spessar-
SR (Page 86) tite, almandite
Transparent Red, Pink, and Purple Gems with RIs between 1.70 and 1.80
RI and SR/DR/AGG Gem Material Commonly confused with:
1.780 to OTL range Almandite garnet Zircon, YAG, spessartite, ruby, synthetic ruby, pyrope-almandite, pyrope
SR (Page 87)
1.762 to 1.770 Corundum; ruby, fancy sapphire Almandite, synthetic corundum, pyrope-almandite, pyrope, synthetic
DR (Page 88) spinel, spinel
1.762 to 1.770 Synthetic corundum; synthetic ruby, Ruby, fancy sapphire, almandite, pyrope-almandite, pyrope, synthetic
DR synthetic fancy sapphire spinel, spinel
(Pages 90 to 92)
1.762 to OTL Corundum with synthetic ruby over- Ruby, lattice diffusion treated corundum, synthetic ruby
DR growth
(Page 94)
1.762 to 1.770 Corundum, color-change sapphire Synthetic color-change sapphire, color-change garnet, alexandrite
DR (Page 95) chrysoberyl, synthetic alexandrite chrysoberyl
1.762 to 1.770 Synthetic corundum, synthetic color- Color-change sapphire, color-change garnet, alexandrite chrysoberyl,
DR change sapphire synthetic alexandrite chrysoberyl
(Page 95)
1.750 to 1.780 range Pyrope-spessartite garnet (including Pyrope-almandite, pyrope, synthetic spinel, spinel, alexandrite
SR “malaya,” color-change) chrysoberyl, synthetic alexandrite chrysoberyl, color-change sapphire
(Page 96)
1.750 to 1.780 range Pyrope-almandite garnet (including Almandite, corundum, synthetic corundum, pyrope-spessartite, pyrope,
SR rhodolite) synthetic spinel, spinel
(Page 96)
continued on next page....
78
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
1.746 to 1.755 Synthetic alexandrite chrysoberyl Color-change sapphire, synthetic color-change sapphire, color-change
DR (Page 98) garnet, alexandrite chrysoberyl
1.730 to 1.750 range Pyrope garnet Almandite, corundum, synthetic corundum, pyrope-spessartite, pyrope-
SR (Page 99) almandite, synthetic spinel, spinel
1.722 (red) Flame-fusion synthetic spinel Corundum, synthetic corundum, pyrope-spessartite, pyrope-almandite,
1.728 (pink) (Page 100) pyrope, spinel
SR
79
GEM IDENTIFICATION LAB MANUAL
Transparent Red, Pink, and Purple Gems with RIs between 1.60 and 1.70
RI and SR/DR/AGG Gem Material Commonly confused with:
1.624 to 1.644 Tourmaline (including parti-colored) Tanzanite, kunzite spodumene, andalusite, apatite, danburite, topaz,
DR (Page 104) pezzottaite
1.470 to 1.700 range Glass Any red, pink, or purple transparent gem material
SR (Page 113)
1.460 to 1.700 range Plastic Any red, pink, or purple transparent gem material
SR (Page 113)
80
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Transparent Red, Pink, and Purple Gems with RIs between 1.50 and 1.60
RI and SR/DR/AGG Gem Material Commonly confused with:
1.583 to 1.590 Beryl, morganite Synthetic pink beryl, scapolite, synthetic pink quartz, labradorite
DR (Page 106)
1.571 to 1.578 Hydrothermal synthetic red and pink beryl Morganite, red beryl, synthetic pink quartz
DR (Page 106)
1.550 to 1.564 Scapolite Beryl, labradorite, amethyst, synthetic amethyst, synthetic pink
DR (Page 108) quartz
1.544 to 1.553 Synthetic pink quartz Beryl, synthetic beryl, scapolite, rose quartz
DR (Page 110)
1.470 to 1.700 range Glass Any red, pink, or purple transparent gem material
SR (Page 113)
1.460 to 1.700 range Plastic Any red, pink, or purple transparent gem material
SR (Page 113)
81
GEM IDENTIFICATION LAB MANUAL
Transparent Red, Pink, and Purple Gems with RIs below 1.50
RI and SR/DR/AGG Gem Material Commonly confused with:
1.470 to 1.700 range Glass Any red, pink, or purple transparent gem material
SR (Page 113)
1.460 to 1.700 range Plastic Any red, pink, or purple transparent gem material
SR (Page 113)
82
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Species Diamond
Prism
General observation Purple, purple-pink, purplish pink, pink to orangy pink, and brownish
pink, often with light tone and low saturation. Vivid red gems exist,
but they’re extremely rare. Under 10X, look for naturals, waxy to 415.5
Diffraction
directions. Polish lines never oriented the same way on adjacent facets.
Positive reaction to diamond tester.
415.5
Typical cutting style Faceted, often in radiant cuts to help intensify bodycolor. Girdle
often faceted or polished.
SR/DR/AGG SR (might show ADR and strain colors in a mosaic pattern under
crossed filters in the polariscope)
Pleochroism None
Spectrum Broad band centered on 563 nm and possibly a line at 415.5 nm. John Koivula/GIA
Some stones also display a line at 575 nm. (Cooling diamond with Naturally colored pink diamond often has
liquid nitrogen helps make its spectrum more visible.) unevenly distributed color, concentrated along
parallel bands.
Fluorescence Some stones show no reaction or a very faint reaction to UV, but
many show a medium to strong reaction under LW, most commonly
blue. Reaction to SW varies from inert to faint blue. Some Type II
stones might show medium to strong orange fluorescence under both
LW and SW.
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, OTL RI, SR nature, magnification,
positive reaction to diamond tester, and possibly spectrum.
Treatments such as irradiation and surface coating can be applied
to off-color diamonds to make them appear fancy-colored. Shane McClure/GIA
Treatments like fracture filling and laser drilling might be used Natural pink diamonds generally display
to improve the appearance and apparent clarity of fancy-colored strong strain patterns under magnification and
diamonds. Fancy-colored diamonds often require advanced testing polarized light.
at a gemological laboratory to determine origin of color.
83
GEM IDENTIFICATION LAB MANUAL
Species Diamond
Prism
General observation Evenly distributed pink to red color, with no colored graining or
linear color zones. Might show facet-related color zoning.
503 575 637
595 658
Dispersion 0.044 (moderate fire—might be masked by bodycolor)
Diffraction
RI OTL
Birefringence/doubling None
503 575 637
595 658
SR/DR/AGG SR (might show ADR)
84
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Prism
General observation Tend to occur as either light-toned pinks or dark reds. Pink to orangy
or brownish pink to purplish pink in weak to strong saturations and
light to medium tones. Red to orangy red to purplish red to purple in
moderate to strong saturations and medium to dark tones. Red and pink
Diffraction
colors produced by a combination of irradiation and annealing.
RI OTL
Birefringence/doubling None
IRRADIATED PINK TO RED SYNTHETIC DIAMOND
SR/DR/AGG SR
Magnification Darker red stones show distinct color zoning consisting of intersecting
Prism
square and cross-shaped yellow zones surrounded by larger areas of
red. Lighter-toned stones often show uneven coloration with alternating
pink and colorless, pink and yellow, or lighter and darker pink zones.
Elongated or rounded opaque inclusions of metallic flux often occur as
pinpoints and small groups of larger grains.
Diffraction
Spectrum Some stones show sharp lines at 637 nm and 658 nm and broad
absorption from 500 nm to 640 nm, increasing toward the violet.
Others show sharp lines at 575 nm, 595 nm, and 637 nm. (Cooling
diamond with liquid nitrogen helps make its spectrum more visible.)
Fluorescence Inert through moderate to strong orange or orange-red under LW and The spectrum of an irradiated pink to red
weak to moderate orange or orange-red under SW. Some red stones synthetic diamond might show sharp lines at
might show intense green cross-shaped, square, or hourglass-shaped 637 nm and 658 nm and broad absorption
areas over reddish orange areas that correspond to the color zoning. from 500 nm to 640 nm, followed by increasing
Green areas might phosphoresce for several seconds after the SWUV absorption toward the violet (top). Or it might
is turned off. show a series of sharp lines from the green
through the red of the spectrum, including lines
SG 3.52 (+/-0.10) at 503 nm, 527 nm, 553 nm, 575 nm, 595 nm,
637 nm, and 658 nm (bottom).
Comments Key tests are magnification and fluorescence, which can help with
detection of cross-shaped, square, or hourglass-shaped internal growth
patterns. Spectrum might also be helpful. If in doubt, submit diamond
to a gemological laboratory for advanced testing.
Metallic flux inclusions and The characteristic fluorescent This pink synthetic diamond’s The metallic inclusion in this
cross-shaped color zoning are pattern in irradiated red syn- color zoning consists of dis- synthetic pink diamond has a
characteristic of red synthetic thetic diamond is a strong tinct areas of purplish pink and brownish halo. It’s a tension
diamond. green cross surrounded by orangy pink. fracture that occurred when the
weak orange color. inclusion solidified.
85
GEM IDENTIFICATION LAB MANUAL
CZ ZIRCON YAG
General observation Commonly a light-toned pink, but can be Often dark brownish red. Facet Light to dark purplish red, pink.
strong ruby-like red or orangy red. edges might show chipping. Vitreous Vitreous to subadamantine
Subadamantine polish luster, conchoidal to subadamantine polish luster, con- polish luster, conchoidal to
fracture with subadamantine fracture choidal fracture with vitreous to uneven fracture with vitreous to
luster. Heft reveals that loose stones are subadamantine fracture luster. subadamantine fracture luster.
much heavier than diamonds of similar Negative reaction to diamond tester. Negative reaction to diamond
size. Negative reaction to diamond tester. tester.
Dispersion 0.060 (strong fire—might be masked by 0.038 (moderate fire—might be 0.028 (weak fire—might be
bodycolor) masked by bodycolor) masked by bodycolor)
SR/DR/AGG SR DR SR
Magnification Generally inclusion free, but might Natural inclusions, moderate to strong Might show gas bubbles
contain unmelted zirconium oxide particles doubling that might be eye-visible in
and gas bubbles. larger stones. Always check for dou-
bling in three directions.
Spectrum Variable, not diagnostic Key line at 653.5 nm, with several Not diagnostic
other lines possible (a few red
zircons might lack absorption lines)
Comments Key tests are OTL RI reading, lack of Key tests are OTL RI reading, Key tests are OTL RI reading,
doubling, negative reaction to diamond strong doubling, and spectrum. lack of doubling, negative reac-
tester, and SG. Conchoidal fracture tion to diamond tester, and SG.
distinguishes CZ from diamond. CZ is a YAG is a manmade material with
manmade material with no gem-quality no natural counterpart.
natural counterpart.
653.5
86
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
SPESSARTITE GARNET
SPESSARTITE GARNET ALMANDITE GARNET
Prism
Group Garnet Garnet
412 432
General observation Orange, brownish orange, Generally dark-toned brownish orange
424
yellowish orange, reddish to brownish red to purplish red hue
orange, red-orange (always with low saturation. Vitreous to sub-
Diffraction
has an orange component adamantine polish luster, conchoidal
and never shows any purple). fracture with greasy to vitreous
Vitreous to subadamantine fracture luster. Large sizes might be
412 432
polish luster, conchoidal especially dark, and large gems are 424
fracture with vitreous to sub- often cut shallow to compensate for
adamantine fracture luster. dark tone. Cabochons might be cut in
hollowback style for same reason. Bands in the violet at 412 nm, 424 nm, and
432 nm, along with bands at 505 nm, 527 nm,
Typical cutting style Faceted Faceted gems or cabochons and 575 nm in the green-yellow, are often pres-
ent in spessartite garnet’s spectrum.
RI 1.810 (+0.004/-0.020) 1.780 to OTL
Comments Key tests are RI, SR nature, Key tests are RI, SR nature, and
505 575
spectrum, and possibly spectrum. Color is also helpful. 527
color. Bands in the blue
area of spessartite garnet’s
spectrum help separate it from The main features of almandite’s spectrum are
almandite. three very strong bands at 505 nm, 527 nm,
and 575 nm in the yellow-green.
87
GEM IDENTIFICATION LAB MANUAL
Species Corundum
468 693 General observation Light pink through slightly orangy red to strong red, slightly to strongly
476
purplish red to purple. Ruby can be orangy red through strongly purplish
red, but the dominant color must be red. Vitreous to subadamantine
Diffraction
Typical cutting style Faceted gems or cabochons. Translucent or opaque material might be
468 693
476 carved.
Fluorescence Ruby—Weak to strong red under LW and SW, with best reaction
Joel Beeson/GIA under SW. Slightly weaker than synthetic ruby. Heat-treated rubies
Natural corundum occurs in a wide range might show chalky fluorescence.
of hues, including orangy reds through Pink sapphire—Strong orange-red to red under LW, faint to weak
purples. orange to red under SW
SG 4.00 (+0.10/-0.05)
Comments Key tests for separating natural corundum from other similarly colored
natural gems are RI, birefringence, pleochroism, magnification and
spectrum. Magnification is the key test for separating natural from
synthetic corundum.
88
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Species Corundum
General observation Purple to pink, reddish purple to purplish red, orangy red to red, Nicholas DelRe/GIA
medium to dark in tone. Face-up color might be uneven, giving the Color concentrations at facet
gem an unnatural, watery appearance. Some stones have an orange junctions in chromium lattice
color component because repolishing removes some of the treated diffusion treated corundum.
layer from yellow starting material.
Pleochroism Some stones show typical pleochroism, but others show a combination
of purplish pink to purplish red and brownish yellow. Individual
stones might show pairs of different pleochroic colors on adjacent
facets where repolishing removed some of the treated layer.
SG 4.00 (+0.10/-0.05)
Comments Key test is magnification with immersion. Higher than normal RIs,
along with a patchy response to SW and atypical pleochroism, can
indicate lattice diffusion treatment with chromium. Might require Lattice diffusion with beryllium
can result in fern-like recrystalliza-
advanced testing. tion of former zircon crystals within
discoid fractures.
89
GEM IDENTIFICATION LAB MANUAL
General observation Light pink through slightly orangy red to strong red, slightly to
strongly purplish red to purple. Synthetic ruby must show red as the
dominant color. Might show poor polish, with polishing marks on
most facets due to rapid polishing.
Typical cutting style Faceted gems or cabochons, often symmetrical and cut to precise
calibrated sizes. Often brilliant style, including scissors cut.
SR/DR/AGG DR
Pleochroism Same as natural, but might be visible directly through the table facet,
which is usually not the case with natural ruby
Magnification Curved growth (striae) often confused with polish marks, but curved
striae are internal and cross facet junctions. Strings of gas bubbles
might resemble needles. Twinning planes possible, but very rare or
difficult to observe. When present, they’re usually formed by rapid
cooling of the boule. These are known as Plato lines. They’re best seen
with magnification, polarized light, and immersion. The stone also
has to be viewed parallel to its optic axis. The twinning then appears
as sets of lines that intersect at 60°or 120° angles. Sometimes quench-
crackled and heated in the presence of a chemical—usually borax—
to create natural-looking fingerprints. This process might make the
striae less visible. (see photos, page 93)
SG 4.00 (+0.10/-0.05)
Comments The key test for separating flame-fusion synthetic corundum from
natural is magnification. Immersion might help with detection of faint
curved growth structures, especially in pink and purple gems.
90
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
General observation Light pink through slightly orangy red to strong Light pink through slightly orangy red to
red, slightly to strongly purplish red to purple. strong red, slightly to strongly purplish red to
Synthetic ruby must show red as the dominant purple. Synthetic ruby must show red as the
color. dominant color.
SR/DR/AGG DR DR
Magnification Often nearly inclusion free. Might contain faint Swirls of color and gas bubbles, sometimes
curved striae, gas bubbles, or smoke-like, swirling, distorted in shape
veil-like inclusions, especially in pulled synthetic
star ruby.
Fluorescence Ruby—Strong red under LW and SW, with best Strong to very strong red under LW, moderate
reaction under SW. Typically slightly stronger than to strong red under SW
natural ruby.
Pink sapphire colored by chromium—Moderate to
strong red under LW, weak orangy red to pinkish
violet under SW
Pink sapphire colored by titanium—Inert to LW,
characteristic chalky blue under SW
Comments Key test is magnification, but inclusion-free stones Key test is magnification, but inclusion-free
might need laboratory analysis. stones might need laboratory analysis.
91
GEM IDENTIFICATION LAB MANUAL
Variety Synthetic ruby, synthetic sapphire (designate by color) Synthetic ruby, synthetic sapphire
(designate by color)
General observation Light pink through slightly orangy red to strong red, slightly to Light pink through slightly orangy red to strong
strongly purplish red to purple. Synthetic ruby must show red as red, slightly to strongly purplish red to purple.
the dominant color. Synthetic ruby must show red as the dominant
color.
SR/DR/AGG DR DR
Pleochroism Same as natural, although Kashan flux-grown synthetics typically Same as natural
show more orange pleochroism than natural rubies
Magnification Flux inclusions are generally white and high-relief, but might Strong growth zoning possible. To avoid confus-
appear near-colorless, whitish, brownish, or yellow to orange. ing subparallel growth structures with those seen
Flux might also appear as two-phase, wispy veils that look like in natural gems, examine stones in several
natural fingerprints, or as coarse globules that might appear orientations and look for mosaic-type, chevron,
drippy, tubular, rod-like, or icicle-like, or as droplets or dashed or zigzag growth zoning. Sometimes two- or
lines or clouds of minute particles. Flux corundum can have three-phase inclusions in fingerprint patterns;
uniform, parallel growth planes. Sharp-edged triangular or small whitish inclusions; possibly tiny, flake-like
hexagonal platelets or stubby needle-like metallic inclusions copper crystals that show a metallic luster in
(usually platinum) strongly indicate synthetic. Platinum platelets fiber-optic lighting. (see photos, page 93)
show as bright metallic reflections in reflected light, but appear
black when backlit. Some types of flux-grown synthetic ruby
might contain remains of a seed crystal with natural inclusions,
but this is rare. (see photos, page 93)
Fluorescence Ruby—Strong red, possibly with a bluish overtone under LW. Weak to moderate red under LW, inert to weak
Might be slightly weaker under SW and often slightly stronger red under SW
than natural ruby.
Pink sapphire—Moderate to strong red, possibly chalky under
LW, moderate red to strong orangy red, possibly chalky under
SW. LW and SW reactions might have roughly the same intensity.
Comments The key test for separating natural from flux-grown synthetic The key test for separating natural from
corundum is magnification. hydrothermal synthetic corundum is magnifica-
tion.
92
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
INCLUSION PHOTOGRAPHS
Untreated natural Burmese ruby: Short Untreated natural Afghan ruby: Untreated natural Vietnamese ruby: Untreated natural ruby:
rutile needles and rounded mineral Included crystals of colorless, rounded Apatite crystals and blue color zoning. Negative crystal.
crystals. apatite and dark rutile.
Heat-treated natural Thai ruby: Melt Heat-treated natural ruby: Heat- Heat-treated natural ruby from Mong Heat-treated natural Mong Hsu
relic with “lacy” fingerprint. damaged crystals (snowballs) with Hsu, Myanmar: Faint hexagonal growth ruby: White hexagonal core.
tension cracks. banding and healed fractures.
Heat-treated natural ruby: Glass-filled Heat-treated natural ruby: Partially Flame-fusion synthetic ruby: Curved Flame-fusion synthetic ruby:
surface-reaching cavity. healed fracture with flux-like residue. striae. Cloud of gas bubbles.
Flame-fusion synthetic ruby: Curved Flame-fusion synthetic ruby: Partially Flux-grown synthetic ruby: Platinum Flux-grown synthetic ruby:
striae and gas bubbles. healed fractures resulting from quench inclusions. Fingerprint-like inclusion of flux
crackling and heat treating with borax. droplets.
Ramaura flux-grown synthetic ruby: Ramaura flux-grown synthetic ruby: Kashan flux-grown synthetic ruby: Hydrothermal synthetic ruby:
Irregular flux inclusions with trapped Wispy veils. “Comet tail” inclusion. Zigzag growth structures.
gas bubbles.
93
GEM IDENTIFICATION LAB MANUAL
General observation Color appears strongly saturated red face-up, but patchy table-down
on white paper. Color is actually confined to a thin layer of synthetic
ruby (0.1 to 0.3 mm thick) over an essentially colorless faceted natural
corundum seed. Repolishing removes areas of the overgrowth, leading
to uneven color distribution.
SR/DR/AGG DR
Magnification Fashioned stones might show areas of crystal growth that are smooth
and slightly wavy or stepped with a series of small, flat crystal
Both by Christopher P. Smith/Gübelin Gem Lab
surfaces. They might also show indentations or cavities with similarly
Looking at corundum with a synthetic over-
stepped sides that were missed in the repolishing process. There’s a
growth layer under magnification in darkfield
(top) and reflected light (bottom), you can see very sharp boundary between the red overgrowth layer and the color-
that the facet junctions of the core material and less seed, along with a high concentration of aligned, linear inclusions
the overgrowth layer don’t align. along the boundary between the synthetic ruby overgrowth and the
seed. These inclusions outline the seed’s original facets, which might
not match the repolished surface above. With immersion, you might
also see a “mottled” or “roiled” texture within the overgrowth layer.
This contrasts with the heat-treated natural inclusions visible in the
seed corundum.
SG 4.00 (+0.10/-0.05)
94
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Prism
Species Corundum Synthetic corundum
450 470
460
General observation Commonly pink-brown through Typically reddish purple or purple in
brownish pink and purple, very incandescent light, changing to gray-
Diffraction
rarely reddish brown in incan- ish blue in daylight and fluorescent
descent light, changing to lighting. Vitreous to subadamantine
yellowish brown, grayish violet, polish luster, conchoidal fracture
450 470
grayish blue, or very rarely with vitreous fracture luster. 460
green in daylight and fluores-
cent light. Vitreous to
subadamantine polish luster, Natural color-change corundum often shows
conchoidal fracture with vitre- chromium lines in the red with iron-related lines
ous fracture luster. at about 450 nm, 460 nm, and 470 nm.
SR/DR/AGG DR DR
Spectrum Typically combines features of Cutoff at about 460 nm, strong line
ruby and pink sapphire or band due to vanadium at 474 nm,
(chromium lines in the red) faint broad absorption between 550 474 690
with iron-related lines at about nm and 610 nm, and possibly a fluo-
450 nm, 460 nm, and 470 nm. rescent line in the red at 690 nm
Diffraction
95
GEM IDENTIFICATION LAB MANUAL
PYROPE-SPESSARTITE GARNET
PYROPE -SPESSARTITE PYROPE-ALMANDITE GARNET
GARNET
Variety Color change (if present) Rhodolite, only if the gem has a
Prism
General observation Usually light to dark, slightly Orangy red to brownish red, dark
410 430
420
pinkish orange, reddish red to purplish red to light reddish
orange, or orangy red to purple. Rhodolite variety must have
yellowish orange. Vitreous a purple color component. High-
Pyrope-spessartite garnet’s spectrum shows to subadamantine polish quality gems have medium to
strong bands at 410 nm, 420 nm, and 430 nm luster, conchoidal fracture medium-dark tone. Vitreous polish
in the blue-violet area of the spectrum and a with vitreous fracture luster. luster, conchoidal fracture with
combination of lines at 460 nm, 480 nm, 504 Might show color change. greasy to vitreous fracture luster.
nm, 520 nm, and 573 nm in the blue-green to
yellow area.
Typical cutting style Faceted gems or cabochons Faceted gems or cabochons
Pyrope-almandite and rhodolite spectra Spectrum Strong bands at 410 nm, 420 Same as almandite, with three
typically show very strong bands at 505 nm, nm, and 430 nm occasionally strong bands in the green and
527 nm, and 575 nm in the yellow-green area. merge to form a cutoff at yellow of the spectrum at 505 nm,
435 nm. Also often shows 527 nm, and 575 nm. Most red-
lines in the blue-to-green and garnet mixtures of pyrope and
yellow of the spectrum at almandite, including rhodolite,
460 nm, 480 nm, 504 nm, show this spectrum.
520 nm, and 573 nm.
Comments Key tests are color, RI, SR Key tests are RI, SR nature, and
nature, and spectrum. spectrum. Purple color component
Bands in the blue area of must be present for rhodolite
pyrope-spessartite garnet’s variety.
spectrum help separate it
from pyrope-almandite.
Sometimes sold as “malaya”
or “malaia” in the trade.
96
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Variety Alexandrite
Prism
Species Chrysoberyl
General observation Color change from yellowish, brownish, grayish, or bluish green in
daylight or fluorescent light to orangy or brownish red to purplish
red in incandescent light. Vitreous to subadamantine polish luster,
Diffraction
conchoidal fracture with greasy to vitreous fracture luster.
Pleochroism Strong green, orange, and purple-red trichroism ALEXANDRITE (GREEN DIRECTION)
Prism
liquid inclusions, needle-like inclusions, or twinning
Diffraction
between about 540 nm and 605 nm; weak lines in the blue at 468 nm,
473 nm, and 476.5 nm; and a cutoff in the violet
Green pleochroic direction—Strong lines in the red at 678 nm and
680.5 nm; weaker ones at 645 nm, 649 nm, 655 nm, and 665 nm; a
broad absorption between about 555 nm and 640 nm; and a cutoff in
the violet at about 470 nm
Orange pleochroic direction—No strong absorptions In the green pleochroic direction, alexandrite
shows strong lines in the red at 678 nm and
Fluorescence Inert to moderate red under LW and SW 680.5 nm; weaker ones at 645 nm, 649 nm,
655 nm, and 665 nm; a broad absorption
SG 3.73 (+/-0.02) between about 555 nm and 640 nm; and a
cutoff in the violet at about 470 nm.
Comments Key tests are appearance of color change, RI, pleochroism, and spectrum.
Magnification separates natural from synthetic alexandrite.
John Koivula/GIA
Natural alexandrite can
contain negative crystals (above),
angular fluorite crystals (top
right), and angular apatite crystals
(bottom right).
97
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC ALEXANDRITE
General observation Bluish green in daylight or fluorescent light, brownish red to purple-
red in incandescent light. Vitreous to subadamantine polish luster,
conchoidal fracture with greasy to vitreous fracture luster.
John Koivula/GIA
SR/DR/AGG DR
SG 3.73 (+/-0.02)
Comments Magnification is the key test for separating synthetic from natural
alexandrite. Strong red fluorescence indicates synthetic.
Shane McClure/GIA
98
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
RHODONITE5
SINGLE-CRYSTAL RHODONITE PYROPE GARNET
Prism
Group Not required Garnet
General observation Red, orangy red, pink. Vitreous Medium to dark reddish
to subvitreous polish luster, orange, red through slightly
conchoidal fracture with vitreous purplish red to pale pink,
Diffraction
fracture luster. Can show perfect colorless (rare). Vitreous
cleavage in two directions. Mohs polish luster, conchoidal frac-
5.5 to 6.5. ture with greasy to vitreous
fracture luster.
Typical cutting style Faceted mainly for collectors Faceted gems or cabochons Rhodonite shows a broad band centered on
548 nm with narrow bands at 408 nm, 412 nm,
RI 1.733 to 1.747 (+0.010/-0.013) 1.730 to a little over 1.750 455 nm, and 503 nm.
(Around 1.740 is normal,
although some rare light pink CHROME PYROPE
to colorless pyrope might drop
to 1.717)
Prism
Birefringence/doubling 0.010 to 0.014 None
Diffraction
Pleochroism Weak to moderate, orange-red None
and brownish red
around 490 nm
Comments Key tests are RI, birefringence, Key tests are RI and spectrum,
and spectrum. and possibly color and SR
nature. Some stones might
show a pyrope spectrum along
with an RI that’s slightly
above 1.750. If this occurs, Pyrope garnets that aren’t colored by
the spectrum positively identi- chromium show a cutoff around 490 nm and
just the 505-nm band.
fies the stone as pyrope.
99
GEM IDENTIFICATION LAB MANUAL
General observation Pale pink most common, red very Usually a vivid, medium dark,
rare slightly purplish red
Flux-grown synthetic spinel might have fewer SR/DR/AGG SR with strong ADR (crosshatch SR
lines in the red of its spectrum than its natural effect common)
counterpart.
Pleochroism None None
Comments Key tests are RI, SR/ADR Magnification is the key test
polariscope reaction, and magnifi- for separating flux-grown
cation. Triplets that imitate synthetic spinel from natural
John Koivula/GIA
amethyst (soudé amethyst) are spinel.
Tiny flux particles in flux-grown made using colorless synthetic
synthetic spinel. spinel joined by a dark purple
cement layer. If you get a 1.728 RI
on a gem resembling amethyst,
always check for a separation
plane.
John Koivula/GIA
100
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Prism
General observation Light pink through strongly Pink to red and purple (also
saturated reddish orange, orangy blue, violet, brown, and
red, pure red, and purplish red to colorless). Vitreous polish
purple. Vitreous to subadamantine luster, conchoidal fracture
polish luster, conchoidal fracture with vitreous fracture luster.
Diffraction
with vitreous fracture luster.
Comments Key tests are RI, SR nature, Key tests are RI, birefrin-
magnification, and spectrum. gence, and optic character.
Very rare.
101
GEM IDENTIFICATION LAB MANUAL
General observation Light to medium-dark bluish Pink to violet-pink, often light in Yellowish green to brownish green and orangy
purple and violetish blue to violet. tone. Vitreous polish luster, brown. Due to strong pleochroism, both green
Zoisite also occurs in light-toned uneven to splintery fracture with and orangy pleochroic colors might be visible
pink or parti-colored colorless and vitreous fracture luster. Perfect through the crown. Depending on cutting
pink. Vitreous polish luster, con- cleavage in two directions at orientation, might appear brownish red. Vitreous
choidal to uneven fracture with nearly 90° angles to one another. polish luster, uneven to conchoidal fracture with
vitreous fracture luster. Perfect vitreous fracture luster. Distinct cleavage in one
cleavage in one direction. direction.
Typical cutting style Faceted Faceted, often with deep pavilion Faceted
to help improve depth of color
Birefringence/doubling 0.008 to 0.013 0.014 to 0.016 0.007 to 0.013 (tends to be higher when RI
values are low)
SR/DR/AGG DR DR DR
Optic character Biaxial positive Biaxial positive (common point Biaxial negative
is 0.006 from the high RI)
Pleochroism Strong. Usually strong blue, Moderate to strong pink to light Very strong, generally light yellowish green
purplish red, and greenish yellow. purple and colorless, except in and dark brownish red
Sometimes strong blue, violet, light stones
and colorless.
Magnification Often inclusion free Growth tubes and liquid Needles (probably rutile) and crystals (probably
inclusions apatite)
Spectrum Not diagnostic, but you might see Not diagnostic Not diagnostic, but might show clusters of
bands at 595 nm, 528 nm, and fine lines around 485 nm to 518 nm and around
455 nm 550 nm
Fluorescence Generally inert Strong yellowish pink to orange Inert to LW. Might fluoresce weak to moderate
under LW, weaker under SW green to yellowish green under SW.
Comments Key tests are RI, birefringence, Key tests are RI, birefringence, Key tests are RI, birefringence, optic character,
optic character, and pleochroism. and fluorescence. and pleochroism.
Color usually a result of non-
detectable heat treatment.
102
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
General observation Pink to purple. Vitreous Transparent to translucent Pale pink to strong red, purplish red and reddish purple;
polish luster, conchoidal to colorless to light pink. Vitreous also fine medium orange-red (imperial). Vitreous polish
uneven fracture with vitre- to greasy polish luster, uneven luster, conchoidal fracture with vitreous fracture luster.
ous fracture luster. Surface to subconchoidal fracture with Perfect basal cleavage, possibly with iridescent cleavage
might show abrasions due vitreous to greasy fracture planes. The color of some red to pink topaz results from
to low hardness (Mohs 5). luster. treatment with a surface coating.
RI 1.634 to 1.638 1.630 to 1.636 (+/-0.003) 1.619 to 1.627 (+/-0.010); red, pink, and purple stones
(+0.012/-0.006) typically 1.629 to 1.637
SR/DR/AGG DR DR DR
Optic character Uniaxial negative (distorted Biaxial positive or negative Biaxial positive (common point is 0.001 from the low
optic figure possible—might (common point almost RI)
appear biaxial) halfway between low and high
RI)
Pleochroism Weak to very weak, in None Weak to moderate, light red and orangy red to yellow
tones of bodycolor
Magnification Natural inclusions Natural inclusions Two- and three-phase inclusions, and inclusions
containing two non-miscible (unmixed) liquids. Surface
treatment results in spotty color. Chips on facet
junctions might reveal colorless material underneath.
Spectrum Not diagnostic Some stones might show a Not diagnostic, but some pink, red, and purple stones
doublet at 580 nm due to might show chromium lines in the red.
traces of rare-earth elements.
Comments Key tests are RI, birefrin- Key tests are RI, birefringence, Key tests are RI, birefringence, and optic character.
gence, and optic character. optic character, and possibly SG is helpful if you can’t obtain birefringence.
Apatite’s low numerical SG. Magnification is a key identifier of surface-treated
RI is generally higher than topaz.
the low numerical RI of
tourmaline.
Fine-quality
purplish red
topaz is rare.
103
GEM IDENTIFICATION LAB MANUAL
General observation Light pink through strongly Strong color zoning in varying combi-
saturated orangy red, pure nations of green, blue, and red hues,
red, purplish red to purple. usually alternating with colorless zones.
Diffraction
Typical cutting style Faceted gems, cabochons, Faceted gems, cabochons, polished
or carvings crystal slices, or carvings
Red to pink tourmaline’s spectrum shows an
increasing absorption through the blue to the RI 1.624 to 1.644 1.624 to 1.644 (+0.011/-0.009)
violet, fine lines at 450 nm and 458 nm, and (+0.011/-0.009)
broad absorption centered on 525 nm with a
fine line at 537 nm. Birefringence/doubling Usually 0.018 to 0.020 Usually 0.018 to 0.020
SR/DR/AGG DR DR
Magnification Thread-like liquid and gas Color zoning, thread-like liquid and
inclusions (trichites), mirror- gas inclusions (trichites), mirror-like
Robert Weldon/GIA like gas-filled fractures, gas-filled fractures
color zoning, needles,
crystals, liquid inclusions,
and growth tubes
Comments Key tests are almost always Key tests are appearance and almost
Both by Maha Tannous/GIA RI and birefringence. If always RI and birefringence. If bire-
Parti-colored tourmalines are zoned with two birefringence isn’t obtain- fringence isn’t obtainable, uniaxial
or more colors (top). The category includes able, uniaxial optic figure, optic figure, pleochroism, and SG
watermelon tourmalines (center) and liddicoatite pleochroism, and SG can can be helpful. Watermelon tourmaline
(bottom). be helpful. Red and strong has a red or pink core with green
pink tourmaline is called overgrowth. Bicolor stones display
rubellite in the trade. two distinct colors.
104
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
General observation Purplish pink. Vitreous polish luster, conchoidal fracture Pink or pinkish orange to deep red. Vitreous to
with vitreous to resinous fracture luster. Faceted stones are subvitreous polish luster. Easy cleavage in three
typically small, with eye-visible inclusions. Often shows directions, doubling evident with unaided eye. Might
chatoyancy, making it closely resemble cat’s-eye tourmaline. show poor polish due to low hardness (Mohs 4).
Typical cutting style Faceted gems or cabochons, depending on clarity Faceted mainly for collectors
SR/DR/AGG DR DR
Optic character Uniaxial negative (might show strain under polariscope) Uniaxial negative
Pleochroism Moderate pinkish orange and purplish pink to pinkish purple Moderate to strong. Some material shows red and
brownish red (South Africa), while some shows light
yellowish orange and orange-pink (Colorado).
Magnification Liquid inclusions; growth tubes, which might be numerous Liquid and two-phase inclusions are often plentiful.
enough to cause chatoyancy; fingerprints and numerous Expect strong doubling due to high birefringence.
fractures
Spectrum Band between 485 nm and 500 nm, might show weak lines at Very dark band around 410 nm, weaker bands at 450
465 nm and 477 nm, and a weak band between 550 nm and nm and 545 nm
580 nm
Comments Key tests are RI, birefringence, optic character, and spectrum. Key tests are RI, birefringence, and spectrum.
Pezzottaite was originally considered to be a cesium-rich
variety of beryl, but was classified as a new mineral in late
2003. The original deposit is depleted and the gem has become
a high-priced rarity for collectors. Might be sold as “hot pink-
red beryl,” “red beryl,” “raspberyl,” or malagasite in the trade.
RHODOCHROSITE
Prism
Eric Welch/GIA
Diffraction
105
GEM IDENTIFICATION LAB MANUAL
SR/DR/AGG DR DR
106
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
General observation Purplish red to red to Oregon material (rare) ranges from pale
orange-red, darker and more pinkish orange and pink to moderate Robert Kane/GIA
saturated than morganite. and strongly saturated reddish orange, Hexagonal growth zoning in natural red beryl.
Vitreous polish luster, con- red-orange, and deep red. Red and green
choidal fracture with bicolor gems exist, but are extremely NATURAL RED BERYL
vitreous to resinous fracture rare. Often displays aventurescence.
luster. Vitreous polish luster, uneven to splintery
fracture with vitreous to pearly fracture
Prism
luster. Two cleavage directions. Parting
also common.
Diffraction
RI 1.566 to 1.572 1.559 to 1.568 (+/-0.005); Oregon
(+0.002/-0.003) material commonly 1.563 to 1.572
Comments Key tests are RI, birefrin- Key tests are RI, birefringence, optic
gence, and strength of color. character, and magnification.
Magnification is the key Labradorite from Oregon is commonly
test for separating natural called sunstone whether or not it
from synthetic beryl. displays aventurescence.
107
GEM IDENTIFICATION LAB MANUAL
SCAPOLITE AMETHYST
General observation Violet, purple, rarely red. Vitreous Purple through violetish purple. Vitreous
polish luster, conchoidal fracture with polish luster, conchoidal fracture with
Eric Welch/GIA vitreous fracture luster. Two cleavage vitreous fracture luster.
Purple scapolite can look like directions.
amethyst, and the RIs of the
two stones might also overlap. Typical cutting style Faceted Faceted gems, cabochons, or beads.
If they do, check for optic
Translucent material might be carved.
sign. Scapolite is uniaxial
negative, while amethyst is
uniaxial positive. RI 1.550 to 1.564 (+0.015/-0.014). 1.544 to 1.553 (very constant)
Purple-to-violet stones commonly
1.536 to 1.541.
SR/DR/AGG DR DR
Shane McClure/GIA
108
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Typical cutting style Faceted (often rectangular step cut) Faceted Synthetic amethyst might
contain the two-phase
spicule inclusions that are
RI 1.544 to 1.553 (very constant) 1.544 to 1.553 characteristic of hydrothermal
growth.
Birefringence/doubling 0.009 0.009
SR/DR/AGG DR DR
Magnification Color zoning, twinning, liquid, two- Often inclusion-free, but might contain
phase and three-phase inclusions, characteristics of hydrothermal growth like
and negative crystals breadcrumb inclusions, two-phase (liquid and
gas) spicule inclusions perpendicular to a seed
plate, color banding parallel to a seed plate,
and flame-like twinning (rather than Brazil-law
twinning).
Comments Key tests are appearance, RI, Many synthetic amethysts are virtually inclu-
birefringence, optic character, and sion-free and grown on twinned seed crystals,
optic figure. so they might show Brazil-law twinning like
natural amethyst. It might be impossible to
distinguish between these synthetics and
natural gems using conventional gem-testing
equipment. Advanced laboratory testing can
separate hydrothermal synthetic quartz from
natural stones.
109
GEM IDENTIFICATION LAB MANUAL
General observation Most properties same as natural Light to medium-light pink, often with distinct, eye-
visible bands that are darker than the background
SR/DR/AGG DR DR
Magnification Often inclusion-free, but might contain Often inclusion free, but might contain characteristics
characteristics of hydrothermal growth indicating hydrothermal growth: breadcrumb inclu-
like breadcrumb inclusions, two-phase sions, two-phase (liquid and gas) spicule inclusions
(liquid and gas) spicule inclusions perpendicular to a seed plate, color banding parallel to
perpendicular to a seed plate, color a seed plate, and flame-like twinning (rather than
banding parallel to a seed plate, and Brazil-law twinning).
flame-like twinning (rather than Brazil-
law twinning).
Comments Some synthetic quartz is virtually Much greater degree of transparency than rose
inclusion-free and grown on twinned quartz, might need advanced laboratory testing.
seed crystals, so it might show Brazil- Transparent pink quartz is rare in nature.
law twinning like natural material. It
might be impossible to distinguish
between these synthetics and natural
gems using conventional gem-testing
equipment. Advanced laboratory testing
can separate hydrothermal synthetic
quartz from natural quartz.
The colorless seed plates are easy You might see needle-like two-phase Manufacturers produce hydrothermal
to see in these synthetic ametrine inclusions in a synthetic ametrine. synthetic quartz in many colors, includ-
crystals. ing pink.
110
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
General observation Quench crackling (heating and then rapid Occurs in almost all colors. Transparent to semitranslucent yellow,
cooling) produces multiple fractures to Vitreous to greasy polish luster. red, orangy red, or orange. Red or
create iridescent effects or to allow dye Three cleavage directions. Strong orangy red stone sold as fire opal in
penetration. Most commonly green or red, eye-visible doubling. the trade. Might show play-of-color.
but any color is possible. Fractures make Vitreous to resinous polish luster,
stones more vulnerable to breakage. conchoidal to uneven fracture with
subvitreous to waxy fracture luster.
Typical cutting style Faceted Occasionally faceted for Faceted gems, cabochons, or freeforms
collectors.
SR/DR/AGG DR, but might show an AGG reaction DR SR, commonly with ADR due to strain
due to multiple fractures
Magnification Network of cracks, often in a honeycomb Not diagnostic Might show patches of play-of-color
pattern. Dye visible in fractures. or mineral inclusions.
Comments Combination of typical quartz properties Key tests are RI, birefringence Key tests are RI, SR/ADR nature, and
and unnatural color, along with magnifi- blink, doubling, cleavage, SG, possibly magnification, which can
cation, identify this type of treated quartz. and possibly appearance. separate natural from synthetic with
play-of-color. Fire opal is sometimes
called Mexican opal. SG can help
separate opal from plastic imitation
opal.
“Honeycomb” texture with dye concen- Natural fire opal comes in a range of red and orangy red hues.
trations in quench-crackled dyed
quartz.
111
GEM IDENTIFICATION LAB MANUAL
General observation Transparent to translucent pink to purple (also Semitransparent to semitranslucent orangy red to red or light to dark
blue to violet, green, orange, yellow, brown, pink, with play-of-color. Material with vivid bodycolor might be
and colorless). Might be parti-colored. polymer impregnated. Conchoidal to uneven fracture with subvitreous
Vitreous to subvitreous luster, conchoidal to fracture luster.
step-like fracture with vitreous to subvitreous
fracture luster. Perfect octahedral cleavage in
four directions. Might have numerous pits
and scratches due to low hardness (Mohs 4).
Typical cutting style Faceted gems, cabochons, carvings, or beads Cabochons, carvings, beads
Magnification Triangular (tetrahedral) negative crystals and Play-of-color in a mosaic pattern across the surface, with a cellular,
two-phase inclusions, liquid inclusions, “chicken wire,” “snakeskin,” or scale-like structure that’s visible with
strong color zoning magnification and overhead or backlighting. Might show columnar
structure when viewed from the side.
Spectrum Not diagnostic Polymer-impregnated synthetic opal might show a broad absorption in
the green or green-blue, sometimes accompanied by a band around
580 nm or 610 nm. Newer orange to orange-red untreated synthetics
might show general absorption to 500 nm followed by a band at 550 nm
and a line at 580 nm.
Fluorescence Very variable Red or pink polymer-impregnated synthetics show strong orange-pink
under LW, moderate orange-pink under SW. Newer untreated red to
orange synthetics show very weak red under both LW and SW, with a
slightly stronger reaction to SW. Phosphorescence is rare and weak if
present.
Comments Key tests are RI, SG, and possibly cleavage. Magnification is the key to separating synthetic from natural opal.
Fluorescence and phosphorescence might also be helpful. Synthetic
opal is often polymer impregnated to make it more stable, and it has a
considerably lower SG than most natural opal.
Eric Welch/GIA
112
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
GLASS PLASTIC
General observation Transparent to opaque, almost Transparent to opaque, almost any appear-
any appearance possible. ance possible. Look for mold marks,
Look for mold marks, orange- orange-peel effect, concave facets, rounded
peel effect, concave facets, facet junctions. Warmer to the touch than
rounded facet junctions. glass imitations and crystalline gemstones. Shane McClure/GIA
Warm to the touch compared Low heft (SG), dull to waxy polish luster,
Magnification reveals spherical gas
to crystalline gemstones. conchoidal fracture with waxy to vitreous bubbles and irregular pink and color-
Vitreous polish luster, con- fracture luster. Surface might show less banding in this glass bead.
choidal fracture with vitreous numerous scratches due to low hardness
fracture luster. (Mohs 1.5 to 3).
Typical cutting style All styles. Can be faceted or All styles. Can be molded to variety of
molded to a variety of shapes shapes and finishes.
and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR (strain
colors common)
Comments Key tests are RI and magnifi- Key tests are RI and magnification. Low
cation. Low thermal heft (SG) and low thermal conductivity
conductivity (warm to the (warm to the touch) might also be helpful.
touch) might also be helpful.
113
GEM IDENTIFICATION LAB MANUAL
Naturally colored diamond from irradiated- Color distribution, spectrum, advanced laboratory
color diamond testing
Natural and synthetic corundum from red RI, birefringence, DR vs SR nature, pleochroism,
garnet magnification, spectrum, fluorescence
Natural and synthetic corundum from red RI, birefringence, DR vs SR nature, pleochroism,
spinel magnification, spectrum
114
SEPARATING TRANSPARENT RED, PINK, AND PURPLE GEMS
Alexandrite from natural and synthetic color- RI, birefringence, optic character, magnification,
change sapphire spectrum
Spinel from flame-fusion synthetic spinel Magnification, possibly RI and polariscope reaction
Kunzite from tourmaline, topaz, apatite, or RI, possibly birefringence and optic character
danburite
Sunstone feldspar from natural and synthetic Optic character, possibly pleochroism and
red beryl magnification
Amethyst from purple scapolite RI, birefringence, optic sign, possibly spectrum and
fluorescence
Glass and plastic imitations from DR gems Magnification, SR vs DR nature, low thermal
conductivity, possibly SG (heft)
115
GEM IDENTIFICATION LAB MANUAL
1.666 to 1.680 Lavender jadeite Hydrogrossular, dyed jadeite, sugilite, dyed nephrite
AGG (Page 123)
1.607 to 1.610 Sugilite Jadeite, dyed jadeite, dyed nephrite, charoite, chalcedony
AGG (Page 124)
1.470 to 1.700 range Glass Any red, pink, or purple translucent-to-opaque gem
SR (Page 132) material
1.460 to 1.700 range Plastic Any red, pink, or purple translucent-to-opaque gem
SR (Page 132) material
116
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
1.530 to 1.685 Pearl Cultured pearl, calcareous concretions, shell, glass and plastic
Usually too opaque to test (Page 128) imitations
1.530 to 1.685 Cultured pearl Pearl, calcareous concretions, shell, glass and plastic imitations
Usually too opaque to test (Page 128)
1.530 to 1.685 Shell Coral, calcareous concretions, pearl, cultured pearl, glass, plastic
AGG (Page 129)
1.470 to 1.700 range Glass Any red, pink, or purple translucent-to-opaque gem material
SR (Page 132)
1.460 to 1.700 range Plastic Any red, pink, or purple translucent-to-opaque gem material
SR (Page 132)
117
GEM IDENTIFICATION LAB MANUAL
Translucent-to-opaque Red, Pink, and Purple Gems with RIs below 1.50
RI and SR/DR/AGG Gem Material Commonly confused with:
1.486 to 1.658 Calcareous coral Dyed howlite, Gilson imitation coral, calcareous concretions,
AGG (Page 130) shell, opal, glass, plastic
1.486 to 1.658 Calcite When dyed, can resemble rhodonite, rhodochrosite, rose
AGG (including onyx marble) quartz, coral
(Page 130)
1.470 to 1.700 range Glass Any red, pink, or purple translucent-to-opaque gem material
SR (Page 132)
1.460 to 1.700 range Plastic Any red, pink, or purple translucent-to-opaque gem material
SR (Page 132)
118
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
CZ
General observation Translucent, uniform pink in reflected light. Faintly banded or striped
appearance in strong transmitted light. Subadamantine polish luster,
conchoidal fracture with subadamantine fracture luster.
SR/DR/AGG AGG
Spectrum Fine lines at 440 nm, 449 nm, 541 nm, 543 nm, 546 nm, 644 nm,
646 nm, 650 nm, 653 nm, 655 nm, and 656 nm; wider bands at
486 nm, 515 nm, and 523 nm
SG 6.14 to 6.16
Comments Key tests are OTL RI reading and possibly spectrum and appearance.
CZ is a manmade material with no gem-quality natural counterpart.
119
GEM IDENTIFICATION LAB MANUAL
Species Ruby-in-zoisite
General observation Ornamental material consisting of purplish red ruby crystals, often
of hexagonal outline, in a green zoisite and black hornblende rock
matrix. Matrix displays uneven fracture with dull luster.
SR/DR/AGG AGG
120
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
RHODONITE
RHODONITE UNAKITE
Prism
General observation Opaque red, pink, brownish red to An opaque, granite-like rock
purplish red. Might contain veins with a characteristic mottled
or splotches of black, white, or appearance composed of green
metallic-looking manganese oxide. epidote, white to gray quartz,
Diffraction
Vitreous to subvitreous polish luster, and pink feldspar. Greasy to
conchoidal to uneven or granular vitreous polish luster, granular
fracture with dull to vitreous to uneven fracture with dull
fracture luster. Mohs 5.5 to 6.5. fracture luster.
Comments Key tests are spot RI and possibly The key to this stone’s identity
spectrum. Appearance is also is its appearance.
distinctive.
Eric Welch/GIA
121
GEM IDENTIFICATION LAB MANUAL
HYDROGROSSULAR GARNET
HYDROGROSSULAR THULITE
460
Group Garnet Not required
General observation Variations of pink or green, often Pink, often mottled or streaked
Diffraction
Comments Key tests are spot RI and possibly Key tests are spot RI and
spectrum and SG. Appearance is possibly SG. Appearance is
also distinctive. also distinctive.
Maha Tannous/GIA
Terri Weimer/GIA
122
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
JADEITE
LAVENDER JADEITE DYED JADEITE
Prism
General observation Semitransparent and translu- Semitransparent and translucent to
cent to opaque. Light to dark opaque light to dark purple-violet to 437.5
purple-violet to violetish violetish purple, often with uneven
purple, often with uneven coloration, mottling, or root-like
Diffraction
coloration, mottling, or root- markings. Vitreous to greasy polish
like markings. Vitreous to luster with a dimpled polished
greasy polish luster with a surface, granular to splintery fracture
dimpled polished surface, with dull or silky fracture luster. 437.5
granular to splintery fracture
with dull fracture luster.
Jadeite’s spectrum shows a key band at 437.5 nm
Typical cutting style Carvings, beads, cabochons Cabochons, carvings due to iron.
Fluorescence Light purple stones are inert to Some dyed stones might show a
weak white or weak brownish moderate to strong orange under
Prism
red under LW, generally inert LW and a weaker reaction under
to SW SW
Comments Key tests are spot RI, spectrum, Key tests are magnification, spectrum,
and SG. Appearance might and possibly LW fluorescence.
also be helpful. Might be heat- Might require advanced testing to
treated, polymer impregnated, detect presence of dye.
or dyed.
123
GEM IDENTIFICATION LAB MANUAL
SUGILITE
SUGILITE DYED NEPHRITE
Comments Key tests are RI, spectrum, Key tests are spot RI and SG.
and SG. Appearance might Dye spectrum indicates
also be helpful. treatment.
124
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
General observation Red, pink, light brownish red, Semitranslucent to opaque. Dyed pink Semitranslucent to opaque purple with
orangy red, orangy pink (might also to imitate coral or rhodonite. Undyed swirls and spots of black, gray, white,
be transparent, appear light brown material is white, often with dark gray and brownish orange. Fibrous appear-
in areas, or show agate-like banding or black vein-like matrix. Vitreous ance, vitreous to waxy polish luster,
called the bacon-strip effect). polish luster, granular fracture with splintery to granular fracture with dull
Vitreous to subvitreous polish dull fracture luster. Might be impreg- fracture luster.
luster, uneven to granular fracture nated with plastic to improve luster.
with dull to vitreous fracture luster.
Might show poor polish due to low
hardness (Mohs 3.5 to 4.5).
Typical cutting style Cabochons, carvings, decorative Cabochons, carvings Cabochons, carvings, decorative
objects objects
RI 1.597 to 1.817 (+/-0.003) 1.586 to 1.605 (+/-0.003) (1.59 spot 1.550 to 1.559 (+/-0.002). Usually
reading common) gives a 1.55 or 1.56 spot reading for
mineral charoite, while other compo-
nents might give different RIs
Birefringence/doubling 0.220 (use birefringence blink 0.019 (usually not detectable) Usually not detectable
method)
Spectrum Very dark band around 410 nm, Not diagnostic Not diagnostic
weaker bands centered around
450 nm and 545 nm
Fluorescence Inert to moderate pink under LW, Not diagnostic Inert to patchy weak red under LW
inert to weak pink under SW and SW
Comments Key tests are RI, birefringence, and Key tests are RI and fluorescence. Key tests are RI and possibly fluores-
possibly spectrum. Appearance is Appearance might also be helpful. cence. Appearance is very distinctive.
very distinctive. Actually a rock made up of the minerals
charoite, aegirine-augite, feldspar, and
tinaksite.
125
GEM IDENTIFICATION LAB MANUAL
General observation Semitranslucent to opaque pink or red. Semitransparent to translucent pink, Various colors, often dyed. A coarse
Subvitreous polish luster, granular often cloudy and fractured. crystalline aggregate of tightly packed
fracture with dull fracture luster. Conchoidal to uneven fracture with quartz grains.
vitreous fracture luster.
Typical cutting style Cabochons, carvings Cabochons, carvings (rarely trans- Carvings, beads
parent enough to facet)
Birefringence/doubling Weak, but sometimes detectable with 0.009 Usually not detectable
spot reading
Magnification Lacks the structure of genuine coral. Liquid and two-phase inclusions Dye visible in fractures
Fine, granular texture visible under
high magnification.
Spectrum Not diagnostic Not diagnostic Not diagnostic. Might show a band in
the orange due to presence of dye.
Fluorescence Variable under LW, inert to SW Inert to weak purple under SW Generally inert
Comments Key tests are spot RI and magnification. Key tests are RI, birefringence, SG, Key tests are appearance and magnifi-
and possibly fluorescence. cation to detect dye concentrations
between crystal grains. Record both
the required treatment call and the
variety on the variety line of your GIA
worksheet.
Fractures can cause cloudiness when rose Even without magnification, you can Magnification reveals dye concentra-
quartz rough is faceted. see the dye concentrations in this dyed tions in this dyed quartzite’s fractures.
quartzite bead.
126
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
CHALCEDONY
SR/DR/AGG AGG
Agate is a chalcedony with a layered appear-
Spectrum Not diagnostic ance consisting of curved or angular bands.
SG 2.60 (+0.10/-0.05)
Comments Key tests are spot RI, SG, and possibly fracture and appearance.
Purple to violetish purple material sold as “purple chalcedony” might
be dyed. Check for dye concentrations in fractures.
127
GEM IDENTIFICATION LAB MANUAL
General observation Might be almost any bodycolor, Colors same as natural (see descriptions below). Surface luster varies from
but usually white or light yellow, dull to nearly metallic, depending on nacre quality. Uneven fracture with dull
and bodycolor might be modified to pearly fracture luster.
by pink, green, or blue overtone.
Surface luster varies from dull to Akoya (bead nucleated)—Typical size range 2 mm to 11 mm. Mostly spherical,
nearly metallic, depending on but might be button, pear, oval, or baroque in shape. Color can range from
nacre quality. Uneven fracture neutral to near-neutral whites and creams with rosé or green overtones, but can
with dull to pearly fracture luster. sometimes be yellow, pink (sometimes dyed), or blue.
Tahitian (bead nucleated)—Typical size range 8 mm to 14 mm. Spherical,
oval, button, drop, or baroque in shape (sometimes circled). Color can range
from near-neutral silver, cream, or brown to black or gray, to blue, green,
yellowish green, or purple, with green, blue, or rosé overtone.
South Sea (bead nucleated)—Typical size range 10 mm to 15 mm. Spherical,
near-round, oval, button, drop, or semi-baroque (sometimes circled). Color can
range from near-neutral white, cream, or silver to yellow, yellowish orange, or
blue, with green, blue, or rosé overtone.
Freshwater (usually tissue nucleated)—Typical size range 2 mm to 13 mm.
Spherical, near-round, oval, button, drop, to heavily baroque (sometimes
circled). Color can range from neutral to near-neutral grays, whites, and creams
to yellows, pinks, and purples, with blue or green overtone and orient.
Birefringence/doubling 0.155 (use birefringence blink 0.155 (use birefringence blink method)
method)
Magnification Not diagnostic Not usually diagnostic, unless you can examine a drill-hole and detect the
bead under the nacre
Fluorescence Variable. Inert to strong light blue, Variable. Inert to strong light blue, yellow, green, or pink under LW and SW.
yellow, green, or pink under LW
and SW.
Comments Key tests are RI, birefringence Key tests are RI, birefringence blink, SG, and magnification. Feels gritty when
blink, and SG. Feels gritty when rubbed against a tooth, while plastic and glass imitations feel smooth. Heft can
rubbed against a tooth, while separate cultured pearl from plastic imitations. X-radiography separates cultured
plastic and glass imitations feel from natural pearl. Cultured pearls might be dyed, irradiated, or polymer-
smooth. Heft can separate natural impregnated. Dye might be detectable as concentrations in nacre, especially
pearl from plastic imitations. X- at the drill-hole. Some irradiated colors are very intense and unnatural.
radiography separates natural from Impregnation might be visible with magnification. Drill-hole might interfere
cultured pearl. Drill-hole might with accurate SG reading.
interfere with accurate SG reading.
128
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
General observation Pink, orange, yellow, and brown. Dull to Virtually any color, but usually white, gray, Typically white, often dyed.
vitreous polish luster, uneven fracture brown, yellow, orange, or pink, with layered Might be dyed pink to
with dull fracture luster. Tridacna or patterned coloring. Might also show orient resemble coral or rhodonite.
“pearls” have a yellowish to whitish, (mother-of-pearl). Helmet shells, which are Can also be gray, yellow,
porcelain-like appearance. commonly used for cameos, show layering or brown. Vitreous polish
in two colors, commonly white and brown or luster, granular to uneven
white and orange. Shell cameos usually have fracture with dull fracture
concave backs due to the curved contours of luster. (Mohs 3.5 to 5)
the shells they’re cut from. Greasy or pearly
polish luster, uneven to splintery fracture
with dull fracture luster.
Typical cutting style Baroque, oval, off-round Cameos, carvings, beads, cabochons, inlays Carvings, beads
Birefringence/doubling 0.155 (use birefringence blink method) 0.155 (use birefringence blink method) 0.191 (use birefringence
blink method)
Magnification Wavy, flame-like structure in conch and Helmet shell—Irregular fibrous structure Not diagnostic
melo “pearls” Conch shell—Flame-like structure
Comments Key tests are RI, birefringence blink, Key tests are RI, birefringence blink, and Key tests are possibly RI
magnification (structure), and appear- magnification. Appearance might also be and birefringence blink.
ance. These are basically non-nacreous helpful. Appearance might also be
concretions from various mollusks, helpful. Birefringence blink
including conch and Melo melo snails separates dyed magnesite
and the giant clam (Tridacna). from dyed howlite.
Conch “pearls” have characteristic flame Helmet shell displays irregular fibrous structure
structure. under magnification.
129
GEM IDENTIFICATION LAB MANUAL
Birefringence/doubling 0.172 (use birefringence blink 0.172 (use birefringence blink method)
method)
Spectrum Not diagnostic Not diagnostic. Any visible lines are caused by
impurities or dye.
Comments Key tests are RI, birefringence Key tests are RI, birefringence blink, SG, and
blink, magnification, and possibly possibly appearance. Marble is a granular
fluorescence. Appearance might aggregate, onyx marble is a banded marble.
also be helpful. Satinspar is a fibrous aggregate that’s often
chatoyant (the name is also used for a similar
variety of gypsum).
130
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
General observation Orangy red to red, light to dark pink. Vitreous to Semitransparent to semitranslucent
resinous polish luster, conchoidal to uneven orangy red to red or light to dark pink,
fracture with subvitreous to waxy fracture luster. with play-of-color. Material with vivid
Might or might not show play-of-color. In some bodycolor might be polymer impregnated.
natural opals, dehydration causes a network of Conchoidal to uneven fracture with sub-
fine cracks called crazing. vitreous fracture luster.
Comments Key test is RI. Lack of surface structure and Magnification is the key to separating
absence of birefringence blink distinguish non- synthetic from natural opal. Fluorescence
phenomenal opal from shell or coral. SG can help and phosphorescence might also be
separate opal from plastic (SG 1.05 to 1.55). helpful. Synthetic opal is often polymer
Some natural opal is polymer impregnated to impregnated to make it more stable, and
make it more stable or improve its appearance. it has a considerably lower SG than most
Magnification separates natural opal from natural opal.
synthetic opal with play-of-color.
131
GEM IDENTIFICATION LAB MANUAL
General observation Bluish violet to purple bands in a Transparent to opaque, almost any Transparent to opaque, almost any
reddish to colorless background. appearance possible. Look for mold appearance possible. Look for mold
Vitreous to subvitreous luster, marks, orange-peel effect, concave marks, orange-peel effect, concave
conchoidal to step-like fracture facets, rounded facet junctions. Warm facets, rounded facet junctions. Warmer
with vitreous to subvitreous fracture to the touch compared to crystalline to the touch than glass imitations and
luster. Massive. Might have gemstones. Vitreous polish luster, crystalline gemstones. Low heft (SG),
numerous pits and scratches due conchoidal fracture with vitreous dull to waxy polish luster, conchoidal
to low hardness (Mohs 4). fracture luster. fracture with waxy to vitreous fracture
luster. Surface might show numerous
scratches due to low hardness (Mohs
1.5 to 3).
Typical cutting style Cabochons, beads, or decorative All styles. Can be faceted or molded All styles. Can be molded to a variety
objects to a variety of shapes and finishes. of shapes and finishes.
RI 1.434 (+/-0.001) Usually between 1.470 and 1.700, but 1.460 to 1.700
can go to OTL
SR/DR/AGG SR or AGG SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Magnification Not diagnostic Gas bubbles, cavities on surface where Gas bubbles, flow lines
gas bubbles were polished through,
flow marks (swirls)
Fluorescence Very variable, often strong Variable, not diagnostic Variable, not diagnostic
Comments Key tests are RI, lack of doubling, Key tests are RI and magnification. Key tests are RI and magnification.
and appearance. Low thermal conductivity (warm to Low heft (SG) and low thermal
the touch) might also be helpful. conductivity (warm to the touch)
might also be helpful.
Shane McClure/GIA
Robert Weldon/GIA
132
SEPARATING TRANSLUCENT-TO-OPAQUE RED, PINK, AND PURPLE GEMS
Rose quartz from synthetic quartz Magnification, possibly color and transparency, advanced
laboratory testing
Purple chalcedony from rhodonite Color, appearance, fracture, SG, and possibly RI (quartz
impurities might give a 1.54 reading)
133
SEPARATING BLUE AND VIOLET GEMS
The category of transparent blue and violet gems includes popular stones like the sapphires
at the top and bottom and the tanzanite on the right. The fluorite on the left is more rarely seen
as a gemstone.
135
GEM IDENTIFICATION LAB MANUAL
2.417 Naturally colored diamond Irradiated diamond, synthetic diamond, CZ, GGG, zircon, YAG
SR (Page 139)
2.417 Irradiated-color diamond Naturally colored diamond, synthetic diamond, CZ, GGG, zircon, YAG
SR (Page 140)
2.417 Synthetic diamond Diamond, irradiated diamond, CZ, GGG, zircon, YAG
SR (Page 140)
2.150 CZ (synthetic cubic zirconia) Diamond, irradiated diamond, synthetic diamond, GGG, zircon, YAG
SR (Page 141)
1.970 GGG (gadolinium gallium garnet) Diamond, irradiated diamond, synthetic diamond, CZ, zircon, YAG
SR (Page 141)
1.925 to 1.984 Zircon Diamond, irradiated diamond, synthetic diamond, CZ, GGG, YAG
1.810 to 1.815 (Page 142)
DR
1.833 YAG (yttrium aluminum garnet) Diamond, irradiated diamond, synthetic diamond, CZ, GGG, zircon,
SR (Page 143) gahnite
Transparent Blue and Violet Gems with RIs between 1.70 and 1.80
RI and SR/DR/AGG Gem Material Commonly confused with:
1.762 to 1.770 Corundum: sapphire Synthetic sapphire, gahnospinel, benitoite, synthetic spinel, spinel,
DR (Page 144) kyanite
1.762 to 1.770 Synthetic corundum: synthetic sapphire Sapphire, gahnospinel, benitoite, synthetic spinel, spinel, kyanite
DR (Pages 145 and 146)
1.728 Flame-fusion synthetic spinel Sapphire, synthetic sapphire, gahnospinel, spinel, kyanite
SR (Page 149)
1.714 Flux-grown synthetic spinel Sapphire, synthetic sapphire, spinel, kyanite, gahnospinel
SR (Page 150)
136
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
Transparent Blue and Violet Gems with RIs between 1.60 and 1.70
RI and SR/DR/AGG Gem Material Commonly confused with:
1.624 to 1.644 Tourmaline (including parti-colored) Kunzite spodumene, euclase, synthetic forsterite, apatite, topaz,
DR (Page 155) lazulite
1.470 to 1.700 range Glass Any blue or violet transparent gem material
SR (Page 162)
1.460 to 1.700 range Plastic Any blue or violet transparent gem material
SR (Page 162)
137
GEM IDENTIFICATION LAB MANUAL
Transparent Blue and Violet Gems with RIs between 1.50 and 1.60
RI and SR/DR/AGG Gem Material Commonly confused with:
1.577 to 1.583 Beryl, aquamarine Synthetic aquamarine, Maxixe or Maxixe-type beryl, synthetic quartz
DR (Page 156)
1.577 to 1.583 Synthetic beryl, synthetic aquamarine Aquamarine, Maxixe or Maxixe-type beryl, synthetic quartz
DR (Page 157)
1.577 to 1.583 Maxixe beryl or Maxixe-type beryl Aquamarine, synthetic beryl, synthetic quartz
DR (Page 157)
1.544 to 1.553 Synthetic blue quartz Aquamarine, synthetic aquamarine, Maxixe or Maxixe-type beryl,
DR (Page 158) iolite, glass
1.470 to 1.700 range Glass Any blue or violet transparent gem material
SR (Page 162)
1.460 to 1.700 range Plastic Any blue or violet transparent gem material
SR (Page 162)
1.430 to 1.470 range Synthetic opal (visually distinctive—rarely confused with anything within this
SR (Page 161) color range)
1.470 to 1.700 range Glass Any blue or violet transparent gem material
SR (Page 162)
1.460 to 1.700 range Plastic Any blue or violet transparent gem material
SR (Page 162)
138
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
DIAMOND
Species Diamond
General observation Pale to deep blue, pale to deep green-blue, rarely blue to violet.
Vivid blue diamonds exist, but are extremely rare. Under 10X, look
for naturals, waxy to granular or faceted girdle surface, bearding,
sharp facet junctions. Adamantine polish luster, step-like fracture. Naturally colored blue diamonds range from
Perfect cleavage in four directions. Polish lines never oriented the deep to pale blue.
same way on adjacent facets. Positive reaction to diamond tester.
Type IIb diamonds are electrically conductive.
Typical cutting style Faceted, often in radiant cuts to help intensify bodycolor. Girdle
often faceted or polished.
RI OTL
Birefringence/doubling None
Stephen Hofer/GIA
SR/DR/AGG SR (weak to strong ADR, sometimes with parallel or cross-hatched Naturally colored blue diamonds might have
patterns) color zoning. At 10X magnification, this
diamond shows alternating blue and colorless
Pleochroism None bands.
Magnification Color distribution is often even, but can be uneven with alternating TYPE IA OR IIA BLUE DIAMOND
blue and colorless zones. Other characteristics vary according to
diamond type.
Type IIb—Usually free of mineral inclusions, but opaque black
Prism
inclusions are sometimes present. Whitish, transparent, or reflective
graining, fractures, and cleavages are sometimes present.
Type Ia or IIa—Color zoning might be located near surface radia- 595
tion stains. Mineral inclusions, pinpoints, clouds, and colored or
whitish graining might also be present.
Diffraction
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, OTL RI, SR nature, magnification,
positive reaction to diamond tester, and possibly spectrum.
Treatments such as irradiation and surface coating can be applied to
off-color diamonds to make them appear fancy-colored. Treatments
like fracture filling and laser drilling might be used to improve the
appearance and apparent clarity of fancy-colored diamonds. Fancy-
colored diamonds often require advanced testing at a gemological
laboratory to determine origin of color.
139
GEM IDENTIFICATION LAB MANUAL
General observation Pale to deep blue, pale to deep green-blue. Blue or grayish blue, with moderate to strong
Might show facet-related color zoning. saturation and medium to dark tone. Synthetic blue
Type IIb diamonds are electrically conductive and
John Koivula/GIA
might be attracted to a magnet due to inclusions of
metallic (nickel-iron) flux.
Diamonds with irradi-
ated blue color might
show zoning around Dispersion 0.044 (moderate fire—might be masked 0.044 (moderate fire—might be masked by body-
the culet. by bodycolor) color)
RI OTL OTL
Spectrum Treated Type Ia or IIa diamonds some- No sharp lines or bands, with absorption increas-
times show weak to strong bands at ing toward the red end of the spectrum
415.5 nm, 478 nm, 496 nm, and 504 nm,
and a 595-nm line due to laboratory
irradiation (see page 139). (Cooling
James Shigley/GIA diamond with liquid nitrogen helps make
Chatham synthetic its spectrum more visible.)
blue diamonds often
have distinctive blue Fluorescence Treated Type Ia or IIa diamonds some- Often unevenly distributed and related to internal
and colorless zoning
times show weak to strong blue, greenish growth structures, with some sectors showing no
patterns.
blue, green, yellow, or orange fluores- reaction. Often displays a cross-shaped, square, or
cence, and no phosphorescence hourglass-shaped pattern. Usually inert to weak
orange under LW; weak to moderate green, yellow,
or orange under SW. Phosphorescence might be
long-lasting, moderate to strong blue or yellow.
Comments Key tests for separation of irradiated Key tests are magnification and fluorescence,
from naturally colored blue to blue-gray which can help with detection of cross-shaped,
Shane McClure/GIA
diamonds are magnification and fluores- square, or hourglass-shaped internal growth
Sometimes, the only cence. Irradiated diamonds often require patterns. If in doubt, submit diamond to a
inclusions present in
advanced testing at a gemological labora- gemological laboratory for advanced testing.
a Chatham synthetic
diamond are clouds tory to determine origin of color.
of pinpoints.
Synthetic diamonds often display uneven, hourglass-shaped internal growth zoning (left) and
metallic flux inclusions (center and right).
140
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
CZ GGG
General observation Light-toned grayish blue to Light to dark blue. Vitreous to subadaman-
strong, dark blue. tine polish luster, conchoidal fracture with
Subadamantine polish luster, vitreous to subadamantine fracture luster.
conchoidal fracture with Well-proportioned round brilliants might
subadamantine fracture show moderate see-through. Heft reveals
luster. Heft reveals that loose that loose stones are much heavier than Eric Welch/GIA
stones are much heavier diamonds of similar size and proportions Blue CZ comes in a light-toned grayish
than diamonds of similar (a 6-mm round brilliant GGG weighs about blue to dark blue color range. It’s often
size. Negative reaction to twice as much as an equivalent diameter used to imitate fancy blue diamond,
diamond tester. diamond). Negative reaction to diamond but its facet junctions are slightly
tester. rounded rather than sharp, and it lacks
natural inclusions. A diamond tester
readily identifies it as “not diamond.”
Typical cutting style Faceted Faceted
RI OTL OTL
SR/DR/AGG SR SR
Comments Key tests are negative Key tests are negative reaction to diamond
reaction to diamond tester, tester, OTL RI reading, fluorescence, and
OTL RI reading, lack of SG. GGG is a manmade material with no
doubling, and SG. natural counterpart.
Conchoidal fracture distin-
guishes CZ from diamond.
CZ is a manmade material
with no gem-quality natural
counterpart.
141
GEM IDENTIFICATION LAB MANUAL
ZIRCON
ZIRCON
Species Zircon
Prism
General observation Very strongly blue through green-blue (usually has green color
component). Facet edges might show chipping. Vitreous to sub-
653.5 adamantine polish luster, conchoidal fracture with vitreous to
subadamantine fracture luster. Negative reaction to diamond tester.
Diffraction
Spectrum Usually a key line at 653.5 nm. Might also have up to 40 fine lines
through rest of spectrum.
653.5
Fluorescence Inert to moderate light blue under LW
Robert Weldon/GIA
142
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
GAHNITE
YAG GAHNITE
Prism
General observation Medium to dark blue. Vitreous Transparent to translucent. Very
to subadamantine polish luster, dark blue or green to black.
conchoidal to uneven fracture Vitreous polish luster, conchoidal 459 480
with vitreous to subadamantine fracture with vitreous fracture
fracture luster. Negative reaction luster.
Diffraction
to diamond tester.
Comments Key tests are negative reaction to Key tests are dark color, lack of
diamond tester, OTL RI reading, doubling, SG, and possibly OTL
lack of doubling, and SG. YAG RI and spectrum. Gahnite marks
is a manmade material with no one end of an isomorphous series
natural counterpart. with spinel (page 150). Gem with
intermediate properties is called
gahnospinel (page 148). Rare.
143
GEM IDENTIFICATION LAB MANUAL
SAPPHIRE
SAPPHIRE
Species Corundum
450 471 General observation Light to dark violet, bluish violet, pure blue to strongly greenish
460
blue. Vitreous to subadamantine polish luster, conchoidal fracture
with vitreous fracture luster.
Diffraction
Typical cutting style Faceted gems or cabochons. Translucent or opaque material might be
carved.
450 471
460
RI 1.762 to 1.770 (+0.009/-0.005)
Spectrum Natural blue and violet sapphires might show a distinctive iron
absorption spectrum with strong bands in the violet-blue of the
spectrum at 450 nm, 460 nm, and 471 nm. The 450-nm band is usually
the strongest. Some heat-treated material might show only the 450-nm
band, and some heated stones might show no bands at all.
Shane McClure/GIA
This sapphire treated by lattice diffusion Fluorescence Generally inert. Might fluoresce red to orange under LW. Weak
with beryllium displays a near-colorless chalky blue or yellowish green under SW might indicate heat
zone at its surface. treatment.
SG 4.00 (+0.10/-0.05)
Comments Key tests for separating natural corundum from other similarly
colored natural gems are RI, birefringence, pleochroism,
magnification and spectrum. Magnification is the key test for
separating natural from synthetic corundum.
Joel Beeson/GIA
144
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
General observation Light to dark violet, bluish violet, pure blue to strongly Light violet-blue through blue to strongly greenish
greenish blue. Might have an unnatural, “watery” appearance. blue. Might show poor polish, with polishing marks
on most facets due to rapid polishing. Might show
obvious face-up color zoning with blue and colorless
areas as a result of uneven color distribution within
the boule.
Typical cutting style Faceted gems or cabochons Faceted gems or cabochons, often symmetrical and
cut to precise calibrated sizes. Often cut in brilliant
style, including scissors cut.
SR/DR/AGG DR DR
Pleochroism Moderate to strong violetish blue and greenish blue Same as natural, but might be visible directly
dichroism through table facet
Magnification Lattice diffusion with heavy elements like titanium produces Curved color banding and strings of gas bubbles that
color concentrations along facet junctions and girdle edge and might resemble needles. Twinning planes possible,
localized or blotchy color that bleeds into pits and surface- but very rare or difficult to observe. When present,
reaching fractures. These indications are best seen through a they’re usually formed by rapid cooling of the boule.
gem’s pavilion under immersion and diffused light. Facet These are known as Plato lines. They’re best seen
junctions and girdle outline stand out in high relief. (see with magnification, polarized light, and immersion.
photos, page 147) The stone also has to be viewed parallel to its optic
Lattice diffusion with beryllium in an oxygen-rich atmosphere axis. The twinning then appears as sets of lines that
removes or lightens blue color in overly dark sapphires. This intersect at 60° or 120° angles. Sometimes quench-
might produce yellow color in the stone’s interior. Subsequent crackled and heated in the presence of a chemical—
heat treatment removes the yellow color and might increase usually borax—to create natural-looking fingerprints.
the saturation of the stone’s remaining blue color, making it This process might make the curved color banding
more marketable. Magnification and immersion might reveal less visible. (see photos, page 147)
a colorless zone around the outside of an otherwise blue
stone. This surface-related zone overlies the gem’s natural
blue color zoning. (see photos, page 147)
Fluorescence Patchy fluorescence to SW, in locations where treated-color Inert to LW, commonly weak to moderate chalky
layer is removed by repolishing blue to blue-green to yellowish green under SW
Comments Key test is magnification with immersion. Fluorescence The key test for separating the flame-fusion synthetic
might also be helpful. Might require advanced testing. from natural corundum is magnification. Immersion
might help with detection of faint curved growth
structures.
145
GEM IDENTIFICATION LAB MANUAL
Variety Synthetic sapphire (designate violet by color) Synthetic sapphire (designate violet by color)
General observation Violet through greenish blue Violet through bluish violet to blue and blue-green
SR/DR/AGG DR DR
Pleochroism Same as natural Moderate to strong. Blue stones can show reddish violet and
blue-green, bluish violet stones might be violetish red and
bluish violet, violet stones might be violetish red and violet.
Hydrothermal synthetics owe their color to nickel and
chromium rather than titanium and iron, so their pleochroic
colors might be noticeably different from those of natural gems.
Magnification Flux inclusions are generally white and high relief, Strong growth zoning possible. To avoid confusing
but might appear near-colorless, whitish, brownish, or subparallel growth structures with those seen in natural gems,
yellow to orange. Flux might also appear as two-phase, examine stones in several orientations and look for mosaic-
wispy veils that look like natural fingerprints, or as type, chevron, or zigzag growth zoning. Sometimes two- or
coarse globules that might appear drippy, tubular, three-phase inclusions in fingerprint patterns; small whitish
rod-like, or icicle-like, or as droplets or dashed lines or inclusions; possibly tiny, flake-like copper crystals that show
clouds of minute particles. Flux corundum can have a metallic luster in fiber-optic lighting. (see photos, page 147)
uniform, parallel growth planes. Sharp-edged triangular
or hexagonal platelets or stubby needle-like metallic
inclusions (usually platinum) strongly indicate
synthetic. Platinum platelets appear bright and metallic
in reflected light, but black when backlit. (see photos,
page 147)
Spectrum Might show a faint line around 450 nm Lacks the 450-nm, 460-nm, and 471-nm lines characteristic
of natural blue to greenish blue sapphires. Stones that contain
chromium might show a similar spectrum to ruby, with
chromium lines at 469 nm, 475 nm, and around 690 nm, plus
a broad absorption at 510 nm to 620 nm.
Fluorescence Inert to LW, commonly weak to moderate chalky blue Depends strongly on the stone’s chromium content. Many
to blue-green to yellowish green under SW greenish blue to violet hydrothermal synthetic sapphires
contain chromium, so they fluoresce red under both LW and
SW (weaker under SW). Greenish blue to blue hydrothermal
synthetic sapphires that contain only nickel are inert to both
LW and SW.
Comments The key test for separating natural from flux-grown Key tests for separating natural from hydrothermal synthetic
synthetic corundum is magnification. corundum are magnification and possibly pleochroism and
spectrum.
146
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
INCLUSION PHOTOGRAPHS
Untreated natural sapphire: Negative Untreated natural sapphire: Mineral Untreated natural sapphire: Apatite Untreated natural sapphire:
crystal and intersecting needles. crystals. and calcite inclusions. Intersecting rutile needles.
Untreated natural sapphire: Fingerprint Untreated natural sapphire: Hexagonal Heat-treated natural sapphire: Discoid Heat-treated natural sapphire:
and negative crystals. zoning and negative crystals. fracture. Glass-filled cavity with gas
bubble.
Heat-treated natural sapphire: Sintered Heat-treated natural sapphire: Internal Heat-treated natural sapphire: Broken, Titanium lattice diffusion treated
area near girdle. color diffusion around rutile inclusions. or “dotted,” silk. natural sapphire: Bleeding
color around fractures.
Flame-fusion synthetic sapphire: Curved Flame-fusion synthetic sapphire: Curved Treated synthetic sapphire: Borax Flux-grown synthetic sapphire:
color banding and gas bubbles. color banding. induced fingerprint-like inclusion. Wispy flux inclusions.
Flux-grown synthetic sapphire: Flux-grown synthetic sapphire: Needles Flux-grown synthetic sapphire: Large Hydrothermal synthetic sapphire:
Platinum inclusions. and platinum platelets. flux inclusions. Chevron-type growth zoning.
147
GEM IDENTIFICATION LAB MANUAL
GAHNOSPINEL
GAHNOSPINEL BENITOITE
SR/DR/AGG SR DR
Comments Key tests are dark color, RI, Key tests are RI, birefringence,
lack of doubling, spectrum, and optic character, pleochroism, and
SG. Gahnospinel belongs to an possibly fluorescence. Rare.
isomorphous series between
gahnite (page 143) and spinel
(page 150). Its properties fall
between the two. Rare.
148
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
Prism
General observation Light-toned blue resembling aquamarine; greenish blue resembling
tourmaline; and vivid, dark, slightly greenish blue resembling
sapphire. Richly colored stones often show red flashes in transmitted 540 635
580
light due to cobalt content. Vitreous to subadamantine polish luster,
conchoidal fracture with vitreous fracture luster.
Diffraction
Typical cutting style Faceted
540 635
RI 1.728 (+0.012/-0.008) 580
Birefringence/doubling None
In its spectrum, dark blue flame-fusion synthetic
SR/DR/AGG SR with strong ADR, crosshatch effect common (see photo, page spinel shows bands at 540 nm, 580 nm, and
151) 635 nm, together with a weak absorption at
460 nm that increases through the violet.
Pleochroism None
LIGHT BLUE FLAME-FUSION SYNTHETIC SPINEL
Magnification Might contain gas bubbles (might be thread-like or, rarely, angular)
(see photo, page 151)
Prism
Spectrum Strong bands at 540 nm, 580 nm, and 635 nm dominate the green to
orange area of the spectrum. Strongest in stones with saturated blue
color. Unlike natural spinel of the same color, there are no lines or 540 635
580
bands in the blue of the spectrum. Blue-green synthetics often show
a mixture of manganese and cobalt absorption features.
Diffraction
Fluorescence Depends on stone’s depth of color.
Light blue—Weak to moderate orange under LW, chalky blue under
540 580 635
SW
Medium blue—Strong red under LW, strong bluish white under SW
Strong blue—Strong red under LW, strong mottled blue under SW
423 448.5
Diffraction
423 448.5
Light blue flame-fusion synthetic spinel is orange under LW (left) and Flame-fusion synthetic blue-green spinel often
chalky blue under SW (right). shows a mixture of manganese and cobalt absorp-
tion features in its spectrum. Look for bands in the
violet at 423 nm and 448.5 nm and faint, broader
bands centered on 540 nm, 575 nm, and 610 nm
in the green to orange area of the spectrum.
149
GEM IDENTIFICATION LAB MANUAL
General observation Bluish violet through greenish blue, often of low saturation. Many Usually a saturated, medium dark to dark,
natural spinels have a lavender color, and there are some rare vibrant very slightly violetish blue. Might show
blue stones. Vitreous to subadamantine polish luster, conchoidal red flashes when rocked under a light
fracture with vitreous fracture luster. source.
RI 1.718 (+0.017/-0.008) (often in the high range for blue and red colors) 1.714 (+/-0.003)
Magnification Minute octahedra or negative crystals, alone or in fingerprint patterns; Orangy brown to black flux inclusions,
included crystals, iron oxide staining (see photos, page 151) alone or in a fingerprint pattern. Also look
for metallic platelets. (see photos, page
151)
Spectrum Naturally colored dark blue spinel spectrum shows a strong, broad band Strong bands between 535 nm and
in the blue, centered on 459 nm, and a strong but much narrower band, 550 nm, 560 nm and 590 nm, and 615 nm
also in the blue, at 480 nm. Bands centered on 553 nm, 593 nm, and and 635 nm, plus a weak absorption at
632 nm can be near the positions of bands seen in synthetic blue spinel, 430 nm that increases through the violet
but their appearance is more diffuse and their widths are more variable.
Fluorescence Can vary. Many natural spinels owe their color to iron, but some rare Weak to moderate slightly chalky red to
examples contain cobalt, which affects their fluorescence. reddish purple, strongest under LW
Iron type—Inert
Cobalt type—Weak to moderate red under LW, inert to SW
Comments Key tests are RI, SR nature, magnification, and spectrum. Key tests are magnification, spectrum,
and possibly RI.
NATURAL BLUE SPINEL COLORED BY IRON NATURAL BLUE SPINEL COLORED BY COBALT
Prism
Prism
Diffraction
Natural blue spinel colored by iron shows bands in the blue Although some natural spinels show cobalt-related absorp-
at 459 nm and 480 nm. Bands at 553 nm, 593 nm, and tion bands in the green to orange area of the spectrum,
632 nm are not as sharp. two iron bands at 459 nm and 480 nm readily separate
them from synthetic stones.
150
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
INCLUSION PHOTOGRAPHS
Natural spinel: Included mineral crystals. Natural spinel: Fingerprint inclusion. Natural spinel: Negative crystals filled with
carbonate minerals.
Flux-grown synthetic spinel: Flux inclusions with Flux-grown synthetic spinel: Metallic platelet.
trapped gas bubbles.
151
GEM IDENTIFICATION LAB MANUAL
KYANITE
KYANITE TANZANITE
SR/DR/AGG DR DR
Comments Key tests are RI, birefringence, Key tests are RI, birefringence,
and optic character. Banded optic character, and pleochroism.
appearance might also be helpful. Color usually a result of non-
detectable heat treatment.
152
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
General observation Pink to violet-pink, often light in Blue to greenish blue, usually light in Usually blue to greenish blue (can also
tone. Vitreous polish luster, tone. Might be color zoned. Vitreous be pale yellow). Often color zoned or
uneven to splintery fracture with polish luster, conchoidal fracture with banded, with wide and narrow bluish bands
vitreous fracture luster. Perfect vitreous fracture luster. Perfect cleavage against a near-colorless background. Might
cleavage in two directions at in one direction with pearly luster on even be parti-colored. Usually light in tone,
nearly 90° angles to one another. cleavage surfaces. with vitreous polish luster.
Typical cutting style Faceted, often with deep pavil- Faceted Faceted, usually step cut
ion to help improve depth of
color
SR/DR/AGG DR DR DR
Optic character Biaxial positive (common point Biaxial positive Seems to be related to crystal growth.
is 0.006 from the high RI) Most fashioned stones are uniaxial nega-
tive. Most crystals have uniaxial negative
cores and biaxial rims, but some have
biaxial cores and uniaxial rims.
Pleochroism Moderate to strong pink to light Blue gems show weak bluish gray and Distinct blue and near-colorless (yellow
purple and colorless, except in light blue stones show weak light yellow and near-
light stones colorless)
Magnification Growth tubes and liquid inclu- Natural inclusions (red or blue plate- Natural inclusions, healing feathers,
sions like inclusions are common) occasional step-like growth zoning that
resembles lightning
Spectrum Not diagnostic Vague bands at 455 nm and 468 nm, Not diagnostic
occasional chrome lines around
690 nm
Comments Key tests are RI, birefringence, Key tests are RI, birefringence, optic Key tests are RI, birefringence, and
and fluorescence. character, and pleochroism. possibly optic character. Very rare.
EUCLASE
Euclase sometimes Jeremejevite
shows vague bands at is a rare gem
455 nm and 468 nm that’s prized
in its spectrum. by collectors.
Occasionally, there It might show
Prism
153
GEM IDENTIFICATION LAB MANUAL
General observation Violet to bluish violet, with Pale light blue and violet to intense
strong pleochroism. Vitreous violet-blue to blue. Vitreous polish
polish luster, conchoidal luster, conchoidal to uneven fracture
fracture with vitreous to with vitreous fracture luster. Surface
Diffraction
Pleochroism Strong blue and purplish pink Strong. Blue and yellow to color-
less.
Eric Welch/GIA
Magnification Indistinct white inclusions Natural inclusions
Synthetic forsterite’s that resemble dust particles,
eye-visible pleochroism makes
it a highly effective tanzanite
pinpoint inclusions that might
imitation. be gas bubbles, tiny needles,
and stringers
Tino Hammid/GIA Fluorescence Moderately chalky, very weak Blue—Blue to light blue under LW
Apatite comes in a orangy yellow under LW and and SW
slightly greenish blue hue weak greenish yellow under Violet—Greenish yellow under LW,
that imitates tourmaline’s SW light purple under SW
Paraíba color.
SG 3.23 (+0.01) 3.18 (+/-0.05)
Comments Key tests are RI, birefringence, Key tests are RI, birefringence,
and possibly pleochroism. A pleochroism, and possibly spectrum.
synthetic material produced as Paraíba-tourmaline-like hues
a tanzanite imitation, but with marketed as “neon” apatite.
a chemical composition similar Apatite’s low numerical RI is
to peridot. Distinguished from generally higher than the low
tanzanite by lower RI and numerical RI of tourmaline.
much greater birefringence.
154
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
TOURMALINE
TOURMALINE PARTI -COLORED
TOURMALINE
Prism
Species Tourmaline Tourmaline
General observation Dark-toned inky blue and Strong color zoning, in varying
strongly greenish blue to combinations of green, blue, and
Diffraction
intense, highly saturated, pure red hues, usually alternating with
blue, bluish violet, and violet. colorless. Vitreous polish luster,
Vitreous polish luster, conchoidal conchoidal fracture with vitreous
fracture with vitreous fracture fracture luster.
luster.
SR/DR/AGG DR DR
Robert Weldon/GIA
155
GEM IDENTIFICATION LAB MANUAL
General observation Light-toned blue and slightly greenish Medium to dark greenish Greenish blue to blue-green, generally
blue to dark-toned strongly greenish blue to violetish blue. Vitreous light in tone. Vitreous polish luster,
blue. Vitreous polish luster, conchoidal polish luster, uneven fracture conchoidal fracture with vitreous to
fracture with vitreous fracture luster. with vitreous fracture luster. resinous fracture luster.
Perfect basal cleavage, possibly with
iridescent cleavage planes. Most blue
topaz results from a combination of
irradiation and heat treatment. Some dark
topaz is treated with a surface coating.
Typical cutting style Faceted or cabochon Faceted or cabochon Faceted gems or cabochons. Included
material with good color might be carved.
RI 1.619 to 1.627 (+/-0.010); blue stones 1.612 to 1.643 (+/-0.005) 1.577 to 1.583 (+/-0.017). Aquamarine is
typically 1.609 to 1.617 typically toward the lower end of this
range, at 1.569 to 1.575.
SR/DR/AGG DR DR DR
Optic character Biaxial positive (common point is Biaxial negative Uniaxial negative
0.001 from the low RI)
Pleochroism Generally weak blue and colorless. Strong. Dark violetish blue Weak to moderate blue and greenish blue
Might be stronger in larger stones. and colorless to light blue. or different tones of blue (lighter color in
optic axis direction)
Magnification Two- and three-phase inclusions, liquid Not diagnostic Liquid-filled inclusions, fingerprints, two-
inclusions in planes. Surface treatment phase and three-phase inclusions, hollow
results in spotty color, with blue color or liquid-filled parallel tubes
concentrations in fractures. Chips on
facet junctions might reveal colorless
material underneath.
Spectrum Not diagnostic. Surface-treated topaz Not diagnostic Generally not diagnostic. In strongly
might show bands at 545 nm, 585 nm, saturated stones, you might see indistinct
and 640 nm due to cobalt. lines at 456 nm and 537 nm plus a strong
line at 527 nm.
Color filter Not diagnostic. Some surface-treated Not diagnostic Green (vs flame-fusion synthetic spinel
topaz might show pink to red. imitations of aquamarine, which are red
under the filter)
Comments Key tests are RI, birefringence, and Key tests are RI, birefrin- Key tests are RI, birefringence, optic
optic character. SG is helpful if you gence, optic character, and character, and possibly magnification.
can’t obtain birefringence. possibly pleochroism. Color usually a result of non-detectable
Magnification and unnatural color are heat treatment.
key identifiers of surface-treated topaz.
156
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
General observation Greenish blue to blue-green, Medium to dark blue. Vitreous polish luster, Purple to violet-blue. Vitreous
generally light in tone. Vitreous conchoidal fracture with vitreous to resinous polish luster, conchoidal fracture
polish luster, conchoidal fracture fracture luster. Color fades when exposed to with vitreous fracture luster. Two
with vitreous to resinous fracture light. cleavage directions.
luster.
SR/DR/AGG DR DR DR
Pleochroism Weak to moderate blue and Weak to moderate blue and light blue (darker Moderate to strong blue and
greenish blue, or different tones color in optic axis direction) bluish purple in pink, purple, and
of blue (lighter color in optic axis violet stones
direction)
Magnification Undulating growth, chevron Liquid-filled inclusions, fingerprints, two-phase Natural inclusions
growth zoning. Liquid and two- and three-phase inclusions, hollow or liquid-
phase inclusions might also be filled parallel tubes
present.
Spectrum Not diagnostic Bands centered around 560 nm, 587 nm, Not diagnostic, except in pink
624 nm, and 688 nm stones, which might show lines
at 652 nm and 663 nm
Comments The key test for separating Key tests are RI, birefringence, optic character, Key tests are RI, birefringence,
synthetic from natural aqua- pleochroism, and spectrum. Initial darker color optic character, and sometimes
marine is magnification. might also help separate Maxixe beryl from fluorescence. When scapolite’s
aquamarine. “Maxixe-type” beryl is laboratory- RI is as high as beryl’s and
irradiated beryl. Like the natural material, it labradorite’s, it has much higher
fades with exposure to UV radiation. In birefringence than either gem.
Maxixe-type beryl, the darker pleochroic color Visual plotting might be necessary
appears perpendicular to the optic axis. to separate scapolite from
amethyst.
157
GEM IDENTIFICATION LAB MANUAL
General observation Thin metal coating (typically Light to medium blue to green-
gold) gives colorless quartz a blue. Vitreous polish luster,
Diffraction
SR/DR/AGG DR DR
Optic character Uniaxial positive. Might show a Uniaxial positive. Might show a
bull’s-eye or Airy’s spiral optic bull’s-eye or Airy’s spiral optic
figure and Brazil-law twinning figure.
under crossed polarizing filters.
SG 2.66 2.66
158
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
General observation Purple through violetish purple. Most properties same as natural Eric Welch/GIA
Vitreous polish luster, con-
One of amethyst’s attractive hues is a
choidal fracture with vitreous light grayish purple.
fracture luster.
SR/DR/AGG DR DR
Many amethysts contain parallel liquid
Optic character Uniaxial positive. Might show a Uniaxial positive inclusions that gemologists call “soap
bull’s-eye or Airy’s spiral optic scum” or “zebra stripes.” They result
figure and Brazil-law twinning from disturbances during growth.
under crossed polarizing filters.
Magnification Color zoning, liquid, two-phase, Often inclusion-free, but might contain
and three-phase inclusions, neg- characteristics of hydrothermal growth
ative crystals like breadcrumb inclusions, two-phase
(liquid and gas) spicule inclusions
perpendicular to a seed plate, color John Koivula/GIA
banding parallel to a seed plate, and Some amethysts contain needles com-
flame-like twinning (rather than Brazil- posed of hematite.
law twinning).
Comments Key tests are RI, birefringence, Many synthetic amethysts are virtually
optic character, and optic figure. inclusion-free and grown on twinned
Visual plotting might be neces- seed crystals, so they might show Brazil- Shane McClure/GIA
sary to separate amethyst from law twinning like natural amethyst. It An amethyst might display twinning
scapolite. Presence of Brazil- might be impossible to distinguish when viewed under crossed polarizing
law twinning separates amethyst between these synthetics and natural filters.
from scapolite with similar gems using conventional gem-testing
properties. equipment. Advanced laboratory testing
can separate hydrothermal synthetic
Prism
159
GEM IDENTIFICATION LAB MANUAL
IOLITE
IOLITE CALCITE
General observation Violet through slightly violetish Occurs in almost all colors.
blue, with strong eye-visible Vitreous to greasy polish luster.
pleochroism. Small stones gener- Three cleavage directions. Strong
ally look grayish. Vitreous polish eye-visible doubling.
luster, uneven to conchoidal frac-
Diffraction
Comments Key tests are visible pleochroism, Key tests are cleavage, eye-visible
RI, birefringence, and optic doubling, RI, birefringence blink,
character. SG, and possibly appearance.
Eric Welch/GIA
160
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
Typical cutting style Faceted gems, cabochons, carv- Cabochons, carvings, beads
ings, or beads
Magnification Triangular (tetrahedral) negative Play-of-color in a mosaic pattern across the surface,
crystals and two-phase inclusions, with a cellular, “chicken wire,” “snakeskin,” or
liquid inclusions, strong color scale-like structure that’s visible with magnifica-
zoning tion and overhead or backlighting. Might show
columnar structure when viewed from the side.
Comments Key tests are RI, SG, and possibly Magnification is the key to separating synthetic
cleavage. from natural opal. Fluorescence and phosphores-
cence might also be helpful. Synthetic opal is
often polymer impregnated to make it more stable,
and it has a considerably lower SG than most
natural opal.
161
GEM IDENTIFICATION LAB MANUAL
BLUE GLASS
GLASS PLASTIC
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Comments Key tests are RI, possible Key tests are RI and magnification.
SR/ADR polariscope reac- Low heft (SG) and low thermal
tion, and magnification. conductivity (warm to the touch)
Low thermal conductivity might also be helpful.
(warm to the touch) might
also be helpful.
162
SEPARATING TRANSPARENT BLUE AND VIOLET GEMS
Diamond from synthetic diamond Magnification (growth zoning, inclusions), spectrum, fluorescence
(color and pattern), phosphorescence, advanced laboratory testing,
possibly magnetism
Naturally colored diamond from Color zoning, possibly fluorescence. Often requires advanced
irradiated diamond laboratory testing.
Diamond from CZ, YAG, and GGG Diamond tester, magnification, SG, possibly fluorescence
Sapphire from synthetic sapphire Magnification, possibly pleochroism and spectrum (to separate
hydrothermal from other synthetics and natural)
Sapphire from lattice diffusion treated Magnification with immersion and diffused light
sapphire
Spinel from flame-fusion synthetic RI, polariscope reaction, magnification, spectrum, fluorescence,
spinel color filter reaction
163
GEM IDENTIFICATION LAB MANUAL
Translucent-to-opaque Blue and Violet Gems with RIs between 1.70 and OTL
RI and SR/DR/AGG Gem Material Commonly confused with:
1.730 to 1.836 Azurite Azurmalachite when very little malachite is present, lapis lazuli
AGG (Page 167)
Translucent-to-opaque Blue and Violet Gems with RIs between 1.60 and 1.70
RI and SR/DR/AGG Gem Material Commonly confused with:
1.670—Sometimes around 1.500 due Lapis lazuli Azurmalachite, azurite, lazulite, dyed howlite, dyed blue jasper, imitation
to calcite or diopside inclusions (Page 175) lapis lazuli, dyed magnesite, dyed calcite
This gem is a rock, so readings can
differ depending on where you test.
1.610 to 1.650 Turquoise Jadeite, synthetic turquoise, pectolite, dyed howlite, amazonite, dyed
1.61 spot RI (Page 169) magnesite
AGG
1.610 to 1.650 Synthetic turquoise Jadeite, turquoise, pectolite, dyed howlite, amazonite, dyed magnesite
1.61 spot RI (Page 170)
AGG
1.470 to 1.700 range Glass Any blue or violet translucent-to-opaque gem material
SR (Page 179)
1.460 to 1.700 range Plastic Any blue or violet translucent-to-opaque gem material
SR (Page 179)
164
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
Translucent-to-opaque Blue and Violet Gems with RIs between 1.50 and 1.60
RI and SR/DR/AGG Gem Material Commonly confused with:
1.599 to 1.628 Pectolite Turquoise, synthetic turquoise, dyed howlite, dyed magnesite
1.60 spot RI (Page 171)
AGG
1.586 to 1.605 Dyed howlite Lapis lazuli, turquoise, synthetic turquoise, pectolite, imitation lapis
AGG (Page 171) lazuli, dyed magnesite
1.535 to 1.539 Dyed jasper chalcedony Lapis lazuli, imitation lapis lazuli, quartz, sodalite
1.53 or 1.54 spot RI (Page 173)
AGG
1.530 to 1.550 Imitation lapis lazuli (Gilson) Lapis lazuli, dyed howlite, dyed jasper chalcedony, dyed magnesite,
Too opaque to test (Page 174) sodalite
1.509 to 1.700 Dyed magnesite Lapis lazuli, turquoise, synthetic turquoise, pectolite, dyed howlite,
AGG (Page 175) imitation lapis lazuli
1.500—Can be around 1.670 Lapis lazuli Dyed howlite, dyed jasper chalcedony, imitation lapis lazuli, dyed
due to calcite or diopside (Page 175) magnesite, dyed calcite, sodalite
inclusions
This gem is a rock, so
readings can differ depending
on where you test.
1.470 to 1.700 range Glass Any blue or violet translucent-to-opaque gem material
SR (Page 179)
1.460 to 1.700 range Plastic Any blue or violet translucent-to-opaque gem material
SR (Page 179)
165
GEM IDENTIFICATION LAB MANUAL
1.470 to 1.700 range Glass Any blue or violet translucent-to-opaque gem material
SR (Page 179)
1.460 to 1.700 range Plastic Any blue or violet translucent-to-opaque gem material
SR (Page 179)
166
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
AZURMALACHITE AZURITE
Comments Key tests are distinctive appear- Key tests are RI and birefringence
ance, RI, and birefringence blink. Appearance might also be
blink. Stabilized azurite- helpful. Terri Weimer/GIA
malachite is widely available Stabilized azurite-malachite is made from
in the trade. It’s made from compressed and bonded nodules of azurite
chalky nodules of azurite and and malachite.
malachite that are compressed
together and bonded with a
polymer. The process is similar
to the one used to produce
stabilized turquoise.
167
GEM IDENTIFICATION LAB MANUAL
JADEITE
JADEITE LAZULITE
168
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
TURQUOISE
TURQUOISE
Species Turquoise
Prism
General observation Semitranslucent to opaque. Light to medium blue, greenish blue to
green. Often mottled, and might show dark patches or veins of
matrix, often recessed below the polished surface. Conchoidal or 420 432 460
granular fracture, depending on gem’s porosity, with waxy or dull
fracture luster.
Diffraction
Typical cutting style Cabochons, carvings, beads
SG 2.74 (+0.14/-0.36)
Comments Key tests are appearance, spot RI, spectrum, and possibly
Terri Weimer/GIA
fluorescence.
Veins of matrix are common in natural turquoise.
Because it’s softer than the surrounding
material, the matrix is often recessed below
the polished surface.
169
GEM IDENTIFICATION LAB MANUAL
Shane McClure/GIA
A hot point held close to wax- or plastic- Typical cutting style Cabochons, carvings, beads Cabochons, carvings, beads
impregnated turquoise produces a sweating
effect. RI 1.60 or 1.61 spot reading (with 1.610 to 1.650 (usually a 1.61
heavy treatment, can be as low as spot reading)
1.56)
Terri Weimer/GIA
Spectrum Occasionally shows weak to Lacks the 432-nm band
medium bands at 420 nm and 432 sometimes seen in natural
Unlike natural turquoise,
Gilson synthetic turquoise may nm (the 432-nm band is the turquoise
have matrix lines that are even stronger of the two). Might also
with its surface. Its character- show a weak band at 460 nm.
istic texture consists of tiny
blue microspheres in a lighter- Fluorescence Inert to weak greenish yellow under Same as natural
colored background. LW, inert to SW
170
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
Comments Key tests are appearance, spot RI, Key tests are RI, fluorescence,
and SG. Magnification and fluores- and color filter. Appearance
cence might also be helpful. might also be helpful.
171
GEM IDENTIFICATION LAB MANUAL
Comments Key tests are RI and magnifica- Key tests are color, spot RI,
Dyed blue chalcedony’s spectrum shows bands tion. Appearance and fracture spectrum, and color filter
around 540 nm, 585 nm, and 645 nm due to
might also be helpful. reaction.
cobalt.
Eric Welch/GIA
172
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
General observation Opaque dark blue to violetish blue. Translucent to semitranslucent. Blue
Conchoidal fracture with dull or waxy to green-blue. Might be unevenly
fracture luster. Lacks the pyrite and colored or resemble fine turquoise.
calcite often seen in natural lapis. Conchoidal fracture with dull to waxy
fracture luster.
RI 1.535 to 1.539 (1.53 or 1.54 spot 1.535 to 1.539 (1.53 or 1.54 spot
reading) reading)
Comments Key tests are spot RI, spectrum, and Key tests are color, RI, SG, and possibly
color filter reaction. Usually has higher appearance.
spot RI and polish luster than lapis and
imitation lapis.
173
GEM IDENTIFICATION LAB MANUAL
Eric Welch/GIA General observation Opaque. Intense violet to medium-dark Light green to greenish blue, with mot-
The inclusions in Gilson blue. Waxy to vitreous polish luster, tled green and white grid-like patterns
imitation lapis lazuli are granular to uneven fracture with dull caused by two intersecting cleavage
typically much more regularly fracture luster. directions. Uneven to splintery fracture.
distributed than the inclusions
in natural lapis. Typical cutting style Cabochons, tablets, beads Cabochons, beads
Magnification Even coloration with very little pyrite, Mottled coloring with grid-like patterns
Gilson imitation lapis shows which tends to be distributed in small
dark blue patches in reflected grains. Lacks darker blue ring around
light and no blue rings around pyrite inclusions. Surface shows many
pyrite crystals.
small, angular, dark violet particles in
reflected light.
174
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
General observation Typically white, often Semitranslucent to opaque. Medium to dark slightly
dyed. Can also be gray, greenish blue to violetish blue. Might be mottled in
yellow, or brown. Often various intensities of blue and contain white patches
shows gray veining like of calcite and scattered irregular specks or veins of
howlite. Vitreous polish brassy-colored pyrite. Waxy to vitreous polish luster, Eric Welch/GIA
luster, granular to uneven granular to uneven fracture with dull fracture luster.
Magnesite can be dyed to a
fracture with dull fracture variety of blue and turquoise
luster. Mohs hardness 3.5 colors.
to 5.
Typical cutting style Cabochons, carvings, Cabochons, carvings, beads, tablets, decorative objects
beads
Magnification Not diagnostic Pyrite and calcite inclusions, with pyrite grains
typically larger and more visible than in imitation
lapis. Pyrite grains are usually unevenly distributed
and have irregular outlines, commonly with darker
blue rings around them.
Fluorescence Generally inert Weak to moderate green or yellowish green under SW. Terri Weimer/GIA
Calcite inclusions might fluoresce pink under LW.
The appearance of natural
lapis lazuli can vary with its
Color filter Not diagnostic Dull, reddish brown mineral content.
Comments Key tests are possibly RI Key tests are distinctive appearance, RI, magnification,
and birefringence blink. and possibly fluorescence. Might be dyed, waxed, or
Appearance might also be impregnated.
helpful. Birefringence
blink separates dyed mag- Terri Weimer/GIA
175
GEM IDENTIFICATION LAB MANUAL
Typical cutting style Cabochons, carvings, beads Beads, cabochons, carvings, and
decorative objects
Comments Key characteristic is variegated, mottled Key tests are RI, birefringence blink,
appearance. Material is named for reputed SG, and possibly appearance. Marble
source (King Solomon’s copper mines) is a granular aggregate, onyx marble
near Red Sea port of Eilat, Israel. Might be is a banded marble. Satinspar is a
misrepresented as azurmalachite in the fibrous aggregate that’s often chatoy-
trade. Similar material comes from Peru. ant (the name is also used for a
Requires advanced testing to determine similar variety of gypsum).
exact composition.
176
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
SODALITE OPAL
Magnification Often veined with white inclu- Possible play-of-color patterns include very
sions (similar in appearance to small patches or dots (pinfire); large areas that
lower-quality lapis lazuli) flash predominately one color as the gem is
moved (flash); or even, distinct patches with a
“brush-stroke” appearance (harlequin). There
might also be areas that lack play-of-color or
that contain mineral inclusions or patches of
rock matrix. (Play-of-color in synthetic opal
tends to be much more regular.)
Fluorescence Might fluoresce patchy orange Inert to white to moderate light blue, green, or
or red under LW and SW yellow under LW and SW. Might phosphoresce.
Comments Key tests are appearance, RI, Key test is RI. SG can help separate opal from
SG, and possibly fluorescence. plastic (SG 1.05 to 1.55). Some natural opal is
polymer-impregnated to make it more stable or
improve its appearance. Magnification separates
natural opal from synthetic opal with play-of-
color.
177
GEM IDENTIFICATION LAB MANUAL
This carving shows bluejohn Typical cutting style Cabochons, beads, or decora- Cabochons, carvings, beads
fluorite’s attractive color
tive objects
banding.
RI 1.434 (+/-0.001) 1.430 to 1.470
Comments Key tests are appearance, RI, Magnification is the key to separating synthetic
and SG. from natural opal. Fluorescence and phosphores-
cence might also be helpful. Synthetic opal is
often polymer impregnated to make it more
stable, and it has a considerably lower SG than
most natural opal.
178
SEPARATING TRANSLUCENT-TO-OPAQUE BLUE AND VIOLET GEMS
BLUE GLASS
GLASS PLASTIC
Prism
General observation Transparent to opaque, almost Transparent to opaque, almost any
any appearance possible. Look appearance possible. Look for
for mold marks, orange-peel mold marks, orange-peel effect, 535 590 635
effect, concave facets, rounded concave facets, rounded facet
facet junctions. Warm to the junctions. Warmer to the touch
Diffraction
touch compared to crystalline than glass imitations and crys-
gemstones. Vitreous polish talline gemstones. Low heft (SG),
luster, conchoidal fracture with dull to waxy polish luster, con-
vitreous fracture luster. choidal fracture with waxy to 535 590 635
vitreous fracture luster. Surface
might show numerous scratches
due to low hardness (Mohs 1.5
to 3). Blue glass colored by cobalt shows bands at
535 nm, 590 nm, and 635 nm. The central
band at 590 nm is thinner than the two outer
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a ones. This is the reverse of synthetic blue
molded to a variety of shapes variety of shapes and finishes. spinel colored by cobalt.
and finishes.
Comments Key tests are RI and magnifica- Key tests are RI and magnifica-
tion. Low thermal conductivity tion. Low heft (SG) and low
(warm to the touch) might also thermal conductivity (warm to
be helpful. the touch) might also be helpful.
179
GEM IDENTIFICATION LAB MANUAL
Lapis lazuli from dyed blue jasper Appearance, fracture, possibly RI and SG
Lapis lazuli from imitation lapis lazuli Color, appearance, RI, magnification, SG
Lapis lazuli from sodalite Appearance, RI, magnification, SG, possibly transparency
Sodalite from dyed blue jasper Fracture, RI, SG, possibly transparency
180
SEPARATING GREEN GEMS
Transparent green gems include emerald, tourmaline, peridot, corundum, diopside, and zircon, with glass and plastic as
possible imitations.
181
GEM IDENTIFICATION LAB MANUAL
2.417 Diamond (natural and irradiated color) HPHT-treated diamond, synthetic diamond, green CZ, sphene,
SR (Page 186) zircon, demantoid, green YAG
2.417 Synthetic diamond Diamond, green CZ, sphene, zircon, demantoid, green YAG
SR (Page 188)
2.150 CZ (synthetic cubic zirconia) Diamond, synthetic diamond, sphene, zircon, demantoid, green
SR (Page 189) YAG
1.925 to 1.984 (high type) Zircon Diamond, synthetic diamond, green CZ, sphene, demantoid, green
1.810 to 1.815 (low type) (Page 189) YAG
DR or amorphous/SR
1.900 to 2.034 Sphene Diamond, synthetic diamond, green CZ, zircon, demantoid, green
DR (Page 190) YAG
1.888 Demantoid garnet Diamond, synthetic diamond, green CZ, sphene, zircon, green YAG,
SR (Page 190) grossularite-andradite
1.833 YAG (yttrium aluminum garnet) Diamond, synthetic diamond, green CZ, sphene, zircon,
SR (Page 191) demantoid
182
SEPARATING TRANSPARENT GREEN GEMS
1.762 to 1.770 Corundum, green sapphire Synthetic green sapphire, grossularite-andradite, chrysoberyl, synthetic
DR (Page 192) chrysoberyl
1.762 to 1.770 Synthetic corundum, synthetic green Green sapphire, chrysoberyl, synthetic chrysoberyl
DR sapphire
(Page 193)
1.762 to 1.770 Corundum; color-change sapphire Natural and synthetic alexandrite chrysoberyl
DR (Page 194)
1.752 to 1.769 range Grossularite-andradite garnet Demantoid, green sapphire, chrysoberyl, synthetic chrysoberyl,
SR (Page 195) tsavorite, synthetic spinel
1.746 to 1.755 Natural and synthetic alexandrite Natural and synthetic color-change corundum
DR chrysoberyl
(Pages 196 and 197)
1.740 Grossularite garnet, including tsavorite Tsavorite: grossularite-andradite, synthetic spinel (triplet), zoisite,
SR (Page 199) chrome diopside
Lighter green grossularite: chrysoberyl, synthetic chrysoberyl,
synthetic spinel
183
GEM IDENTIFICATION LAB MANUAL
1.691 to 1.700 Zoisite Tsavorite, diopside, kornerupine, apatite, tourmaline, green beryl
DR (Page 201)
1.675 to 1.701 Diopside Tsavorite, zoisite, kornerupine, enstatite, spodumene, peridot, euclase,
DR (Page 201) apatite, tourmaline, treated green topaz
1.634 to 1.638 Apatite Zoisite, diopside, spodumene, peridot, euclase, andalusite, tourmaline,
DR (Page 205) treated green topaz, brazilianite
1.624 to 1.644 Tourmaline (including parti-colored) Zoisite, diopside, kornerupine, enstatite, spodumene, peridot, euclase,
DR (Pages 205 and 206) andalusite, apatite, treated green topaz, brazilianite
184
SEPARATING TRANSPARENT GREEN GEMS
1.577 to 1.583 Emerald Green beryl, synthetic emerald, quench-crackled dyed quartz
DR (Pages 208 and 209)
1.544 to 1.553 Quartz (including praseolite) Green beryl, labradorite feldspar, scapolite
DR (Page 214)
1.430 to 1.470 Synthetic opal (visually distinctive—rarely confused with anything within this
SR (Page 216) color range)
185
GEM IDENTIFICATION LAB MANUAL
GREEN DIAMOND
NATURALLY COLORED AND IRRADIATED-COLOR DIAMOND
Species Diamond
Prism
General observation Light yellowish green to dark bluish green, often with low saturation.
Under 10X, look for naturals, waxy to granular or faceted girdle
415.5 surface, bearding, sharp facet junctions. Adamantine polish luster,
step-like fracture. Perfect cleavage in four directions. Polish lines
never oriented the same way on adjacent facets. Positive reaction to
Diffraction
diamond tester.
Pleochroism None
Fluorescence Some treated stones show very weak to strong yellowish green under
LW and very weak to weak green under SW.
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, OTL RI, SR nature, magnification, posi-
tive reaction to diamond tester, and possibly spectrum. Determining
John Koivula/GIA
whether a green diamond’s color is the result of natural radiation,
This irradiated green diamond laboratory irradiation, or high pressure high temperature (HPHT)
shows a distinct color zone
treatment is a challenge, and the origin of color in many green
at its culet. This means the
diamond was treated in a diamonds can’t be determined. If in doubt, submit a green diamond
cyclotron. to a reputable laboratory for advanced testing. Some stones treated
by early irradiation methods might be radioactive.
Eric Welch/GIA
186
SEPARATING TRANSPARENT GREEN GEMS
Species Diamond
Prism
General observation Strongly saturated greenish yellow to yellowish green
Diffraction
RI OTL
Birefringence/doubling None
Spectrum Might show a strong line at 503 nm, a dark band between
480 nm and 500 nm, a line at 415 nm, and sometimes emission lines
at 505 nm and 515 nm. (Cooling diamond with liquid nitrogen helps
make its spectrum more visible.)
SG 3.52 (+/-0.10)
187
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC DIAMOND
General observation Yellowish green to green or bluish green with weak to moderate or
strong saturation in light to dark tones. The alternating pattern of
blue and yellow zones causes the face-up green color in untreated
material. Laboratory irradiation produces green color in treated
stones. Gems might be attracted to a magnet due to inclusions of
metallic (nickel-iron) flux.
Shane McClure/GIA
Birefringence/doubling None
Magnification Untreated material shows uneven coloration due to alternating blue and
yellow zones, which might form a cross-shaped, square, or hourglass-
shaped pattern. Graining might mark the boundaries of the color zoning.
Coloration in treated stones might be evenly or unevenly distributed.
Elongated or rounded opaque inclusions of metallic flux often occur as
pinpoints and small groups of larger grains.
SG 3.52 (+/-0.10)
Comments Key tests are magnification and fluorescence, which can help
with detection of cross-shaped, square, or hourglass-shaped
internal growth patterns. If in doubt, submit diamond to a reputable
laboratory for advanced testing.
188
SEPARATING TRANSPARENT GREEN GEMS
CZ ZIRCON
General observation Yellowish green “peridot” color through Blue-green to slightly yellowish green through yellow-green. Facet
bluish green “emerald” color, light to dark in edges might show chipping. Vitreous to subadamantine polish luster,
tone. Subadamantine polish luster, con- conchoidal fracture with vitreous to subadamantine fracture luster.
choidal fracture with subadamantine fracture (Low-type green stones have lower luster and polish.) Negative reaction
luster. Heft reveals that loose stones are to diamond tester.
much heavier than diamonds of similar size.
Negative reaction to diamond tester.
Dispersion 0.060 (strong fire—might be masked by 0.038 (moderate fire—might be masked by bodycolor)
bodycolor)
RI OTL OTL
Birefringence/doubling None Can range from almost none up to 0.059 (strong). Not present or weak
in low-type zircon.
Optic character Not applicable Uniaxial positive (might not be detectable in low-type zircon)
Magnification Generally inclusion free, but might contain Natural inclusions, moderate to strong doubling that might be eye-visible
unmelted zirconium oxide particles and gas in larger stones. Always check for doubling in three directions. Low type
bubbles. usually shows very strong zoning that gives the stone a milky appearance
at some illumination angles; skeletal, angular inclusions are also common.
Spectrum Variable, not diagnostic Key line at 653.5 nm. Some green stones might show as many as 40 lines in
their spectra. Lines might be fuzzy and ill-defined in low-type green gems.
SG 5.60 to 6.00 3.90 to 4.73 (gradual increase from low to high types)
Comments Key tests are negative reaction to diamond Many green stones are low-property types. Key tests are less conclusive
tester, OTL RI reading, lack of doubling, with these stones because doubling and absorption spectra might be less
and SG. Conchoidal fracture distinguishes apparent. Key tests for high-type zircons are OTL RI reading, strong
CZ from diamond. CZ is a manmade material doubling, and spectrum. Low-type stones might show an OTL RI reading,
with no gem-quality natural counterpart. little or no doubling, a faint spectrum, and strong parallel zoning.
ZIRCON
Prism
653.5
Diffraction
653.5
Eric Welch/GIA
Zircon’s color range includes The 653.5-nm line in this spectrum positively identifies the gem
a yellowish green hue. as zircon.
189
GEM IDENTIFICATION LAB MANUAL
SPHENE
SPHENE DEMANTOID
Comments Key tests are OTL RI reading, Key tests are OTL RI reading, lack
very strong doubling (almost of doubling, magnification, and
twice that of zircon), and pos- spectrum.
sibly spectrum.
190
SEPARATING TRANSPARENT GREEN GEMS
YAG UVAROVITE
General observation Medium to dark bluish green through Light to dark green through yellow-green
yellowish green. Vitreous to sub- to brownish green. Occurs as irregular
adamantine polish luster, conchoidal aggregates of small, closely packed crystals on
to uneven fracture with vitreous to a rock matrix. Crystals are usually too small
Eric Welch/GIA
subadamantine fracture luster. Green to facet and can range in size from micro-
stones might show red flashes with scopic to no more than 4 mm in diameter. This green YAG is a product
of the pulling process.
transmitted light. Negative reaction to Best-quality specimens have uniform surface
diamond tester. coverage of crystals with no exposed matrix.
Typical cutting style Faceted Small slabs of tiny, unpolished crystals with
rock matrix backing
Fluorescence May show strong red under LW, weak Not diagnostic
red under SW
Comments Key tests are negative reaction to dia- Key test is appearance, called drusy, which
mond tester, OTL RI reading, lack of means it consists of small, tightly packed
doubling, and SG. YAG is a manmade crystals. Small slabs of uvarovite are often
material with no natural counterpart. used in designer jewelry.
Robert Weldon
191
GEM IDENTIFICATION LAB MANUAL
Species Corundum
450 471 General observation Strongly bluish green to yellowish green, usually dark in tone with
460
distinct color zoning. Vitreous to subadamantine polish luster,
conchoidal fracture with vitreous fracture luster.
Diffraction
Typical cutting style Faceted gems or cabochons. Translucent or opaque material might
be carved.
450 471
460
RI 1.762 to 1.770 (+0.009/-0.005)
The spectrum of natural green sapphire usually shows Birefringence/doubling 0.008 to 0.010
strong bands at 450 nm, 460 nm, and 471 nm. The
450-nm band is the strongest. SR/DR/AGG DR
Spectrum Green stones usually show a distinctive iron absorption spectrum with
three strong lines in the violet-blue at 450 nm, 460 nm, and 471 nm.
The 450-nm band is usually the strongest. In some stones, it might be
so strong that it overwhelms the other bands. Heat-treated stones might
Anthony de Goutière not show any absorption bands.
Heat treatment of natural sapphire often causes
an existing inclusion to expand into the Fluorescence Inert
surrounding gem, resulting in a discoid fracture.
SG 4.00 (+0.10/-0.05)
Comments Key tests for separating natural corundum from other similarly
colored natural gems are RI, birefringence, pleochroism, magnifica-
tion, and spectrum. Magnification is the key test for separating
natural from synthetic corundum. Green color can result from lattice
diffusion with beryllium.
Maha Tannous/GIA
192
SEPARATING TRANSPARENT GREEN GEMS
Typical cutting style Faceted gems or cabochons, often Faceted The typical pleochroic colors
of natural green corundum
symmetrical and to precise calibrated
(left) are different from
sizes. Often brilliant style, including those of some hydrothermal
scissors cut. synthetic corundum (right).
Some synthetics show
unusual reddish orange and
RI 1.762 to 1.770 (+0.009/-0.005) 1.762 to 1.770 (+0.009/-0.005) yellowish green pleochroic
colors.
Birefringence/doubling 0.008 to 0.010 0.008 to 0.010
SR/DR/AGG DR DR
Pleochroism Strong green and yellow-green Might duplicate natural. Some show moder-
ate to strong reddish orange to yellowish
orange and bluish green to yellowish green.
These stones are colored by a combination
of nickel and iron, so their pleochroic colors
might differ from natural stones.
Eric Welch/GIA
Magnification Curved color banding and strings of gas Strong growth zoning possible. To avoid
Magnification is the key test
bubbles that might resemble needles. confusing subparallel growth structures
for separating the natural
Twinning planes possible, but very rare with those seen in natural gems, examine green sapphire at left from the
or difficult to observe. When present, stones in several orientations and look for synthetic green sapphire at
they’re usually formed by rapid cooling mosaic-type, chevron, or zigzag growth right.
of the boule. These are known as Plato zoning. Sometimes two- or three-phase
lines. They’re best seen with magnifica- inclusions in fingerprint patterns; small
tion, polarized light, and immersion. whitish inclusions; possibly tiny, flake-like
The stone also has to be viewed parallel copper crystals that show a metallic luster
to its optic axis. The twinning then in fiber-optic lighting.
appears as sets of lines that intersect at
60º or 120° angles.
Fluorescence Weak orange under LW, dull brownish Generally inert, but some stones that contain
red under SW chromium might fluoresce purplish red
under both LW and SW.
Comments The key test for separating flame- The key test for separating natural from
fusion synthetic corundum from hydrothermal synthetic corundum is
natural is magnification. Immersion magnification. Pleochroism might also
might help with detection of faint be helpful.
curved growth structures.
193
GEM IDENTIFICATION LAB MANUAL
COLOR-CHANGE CORUNDUM
COLOR-CHANGE SAPPHIRE
Species Corundum
General observation Commonly pink-brown through brownish pink and purple, very
rarely reddish brown in incandescent light, changing to yellowish
brown, grayish violet, grayish blue, or very rarely green in daylight
Diffraction
SR/DR/AGG DR
Comments Key tests are detection of color change, RI, birefringence, and
magnification.
194
SEPARATING TRANSPARENT GREEN GEMS
Species Grossularite-andradite
Prism
Group Garnet
General observation Slightly greenish yellow to yellowish green and intense green,
typically of medium tone. Vitreous to subadamantine polish luster,
conchoidal to uneven fracture with greasy to vitreous fracture luster.
Diffraction
Typical cutting style Faceted
Fluorescence Inert
Comments Key tests are RI, SR nature, and possibly spectrum. Sold as “Mali”
or “grandite” garnet in the trade.
Tino Hammid/GIA
195
GEM IDENTIFICATION LAB MANUAL
Variety Alexandrite
Prism
Species Chrysoberyl
General observation Color change from yellowish, brownish, grayish, or bluish green in
daylight or fluorescent light to orangy or brownish red to purplish
red in incandescent light. Vitreous to subadamantine polish luster,
Diffraction
Natural alexandrites show a color change from Natural alexandrite might Negative crystals are among The angular apatite crystals in
bluish green in fluorescent light (left) to purplish contain angular fluorite crys- the clarity characteristics this alexandrite identify it as
red in incandescent light (right). tals that can help you separate found in natural alexandrite. natural.
it from synthetic material.
196
SEPARATING TRANSPARENT GREEN GEMS
SYNTHETIC ALEXANDRITE
General observation Bluish green in daylight or fluorescent light, brownish red to purple-
red in incandescent light. Vitreous to subadamantine polish luster,
conchoidal fracture with greasy to vitreous fracture luster. John Koivula/GIA
SR/DR/AGG DR
SG 3.73 (+/-0.02)
Comments Magnification is the key test for separating synthetic from natural
alexandrite. Strong red fluorescence indicates synthetic.
The large brown flux inclusion proves
that this alexandrite is a flux-grown
synthetic.
Shane McClure/GIA
197
GEM IDENTIFICATION LAB MANUAL
General observation Non-phenomenal yellow through strongly yellowish green, Non-phenomenal intense bluish green due to vanadium.
intense bluish green due to vanadium or chromium or both, Vitreous to subadamantine polish luster, conchoidal
to greenish brown. Vitreous to subadamantine polish luster, fracture with greasy to vitreous fracture luster.
conchoidal fracture with greasy to vitreous fracture luster.
SR/DR/AGG DR DR
Pleochroism Weak to moderate, usually different tones of the bodycolor Weak to moderate, usually different tones of the
bodycolor
Magnification Might show fingerprints, angular included crystals, liquid Might contain needle-like inclusions, curved striae, gas
inclusions, needle-like inclusions, and twinning. bubbles
Spectrum Natural yellowish green to greenish brown stones colored by Not diagnostic
iron show a strong band at 444 nm. Intense bluish “mint”
green stones might also show additional bands and lines,
with a band between 590 nm and 665 nm and an emission
line at 670 nm.
Fluorescence Yellowish and yellowish green stones are generally inert to Generally inert to both LW and SW, but a few stones
yellowish green under SW. Other colors are generally inert. might show faint red under LW
Bluish green “mint” chrysoberyl might be strong red under
LW due to high chromium content.
Comments Key tests are RI, birefringence, pleochroism, and spectrum. Magnification is the key test for separating natural
from synthetic chrysoberyl. Synthetic chrysoberyl is
produced by both pulling and modified floating zone
methods.
CHRYSOBERYL
Prism
444
Diffraction
444
Eric Welch/GIA
Chrysoberyl’s spectrum reveals a diagnostic band at 444 nm. Non-phenomenal chrysoberyl can occur in an attractive
mint green hue. The larger stone weighs 11.74 cts.
198
SEPARATING TRANSPARENT GREEN GEMS
Comments Key tests are RI, SR nature, Key tests are RI, birefringence, optic
and possibly magnification and character, spectrum, and possibly
fluorescence. pleochroism.
EPIDOTE
Prism
Peter Johnston/GIA
199
GEM IDENTIFICATION LAB MANUAL
IDOCRASE
Spectrum Generally faint absorption bands at Line at 464 nm, weak line at
423 nm in the violet and 448.5 nm 528.5 nm
464
in the blue.
Diffraction
Comments Key tests are RI, SR/ADR polar- Key tests are RI, birefringence,
iscope reaction, and magnification. optic character (test carefully),
Triplets that imitate peridot (soudé and spectrum. Sometimes
peridot) are made using colorless called vesuvianite in the trade.
synthetic spinel joined by a dark
yellowish green cement layer. If
you get a 1.728 RI on a gem
Maha Tannous/GIA
resembling peridot, always check
for a separation plane.
Idocrase occurs in brownish and yellowish
green and has vitreous to greasy polish luster.
200
SEPARATING TRANSPARENT GREEN GEMS
DIOPSIDE
ZOISITE DIOPSIDE
Prism
General observation Light to dark bluish green to Bluish green to yellowish green.
yellowish green. Vitreous Chrome diopside is intense green.
polish luster, conchoidal to Vitreous polish luster, conchoidal to 505
Diffraction
in one direction. cleavage in two directions at nearly
90° angles to one another.
505
Typical cutting style Faceted Faceted
RI 1.691 to 1.700 (+/-0.005) 1.675 to 1.701 (+0.029/-0.010) Diopside’s spectrum shows bands at 456 nm,
493 nm, and 505 nm. The 505-nm band is
Birefringence/doubling 0.008 to 0.013 0.024 to 0.030 diagnostic for the gem.
Prism
Pleochroism Strong greenish yellow to Weak to strong light and dark green
greenish brown, yellowish
green, and bluish green to 505
508
brownish green
Diffraction
Magnification Two- and three-phase inclu- Not diagnostic
sions, fingerprints, needles,
growth tubes, and solid
505
mineral inclusions
508
Spectrum Broad absorption of the violet Ordinary green—Diagnostic band Chrome diopside’s spectrum shows lines at
and most of the blue portion at 505 nm, with bands also at 505 nm, 508 nm, 635 nm, 655 nm, and 670 nm,
of the spectrum and weak to 456 nm and 493 nm and a cutoff in the blue area of the spectrum
distinct bands at 660 nm and Chrome-type—Lines at 505 nm, around 450 nm.
680 nm 508 nm, 635 nm, 655 nm, and
670 nm, and a cutoff in the blue
area around 450 nm
Comments Key tests are RI, birefringence, Key tests are RI, birefringence,
optic character, and pleochro- optic character, and spectrum.
ism. There is a chatoyant green Diopside’s low-RI reading is
zoisite that resembles cat’s-eye always higher than the low-RI
Eric Welch/GIA
tourmaline, but it’s extremely reading in peridot. Some yellowish
rare. green material is marketed as Diopside can be a bluish
“Tashmarine.” to yellowish green.
201
GEM IDENTIFICATION LAB MANUAL
KORNERUPINE
KORNERUPINE ENSTATITE
SR/DR/AGG DR DR
Spectrum Bands at 446 nm and 503 nm, Lines at 505 nm and 550 nm. Might
faint lines at 430 nm, 463 nm, show gradual cutoff below 470 nm.
and 540 nm (best observed in
the green pleochroic direction)
ENSTATITE Comments Keys tests are RI, birefrin- Key tests are RI, birefringence,
gence, optic character, optic character, and spectrum.
pleochroism, and possibly
spectrum and fluorescence.
Prism
505 550
Diffraction
505 550
202
SEPARATING TRANSPARENT GREEN GEMS
HIDDENITE SPODUMENE
SPODUMENE PERIDOT
Prism
General observation Yellow-green to medium green. Yellowish green to greenish yellow
Rare hiddenite is very slightly to brownish green. Moderate
bluish green through yellowish doubling due to birefringence.
green. Vitreous polish luster, Vitreous polish luster, conchoidal
uneven to splintery fracture with fracture with vitreous to sub-
Diffraction
vitreous fracture luster. Perfect vitreous fracture luster.
cleavage in two directions at
nearly 90º angles to one another.
Optic character Biaxial positive (common point Biaxial positive or negative PERIDOT
Prism
Pleochroism Moderate bluish green and Weak yellow-green and green,
yellowish green noticeable only in dark stones
453 497
Magnification Growth tubes and liquid inclusions Disk-like liquid and gas inclusions 477
Diffraction
chromite inclusions
Spectrum In yellow-green stones, look for Strong, narrow bands at 453 nm,
lines near 433 nm and 438 nm in 477 nm, and 497 nm 453 497
the blue area. Hiddenite shows a 477
Comments Key tests are RI, birefringence, Keys tests are RI, birefringence,
and spectrum. optic character, spectrum, and
possibly magnification. Peridot’s
low-RI reading is always lower
than the low-RI reading in
diopside.
Alan Jobbins
Magnification revealed a char- This peridot contains several The liquid and gas inclusion
acteristic chromite inclusion in dark, high-relief chromite in this peridot is called a
this peridot. crystals. “lily pad.”
203
GEM IDENTIFICATION LAB MANUAL
EUCLASE
EUCLASE ANDALUSITE
SR/DR/AGG DR DR
Comments Key tests are RI, birefringence, Key tests are RI, birefringence,
optic character, and pleochroism. optic character, and pleochroism.
204
SEPARATING TRANSPARENT GREEN GEMS
APATITE
APATITE TOURMALINE
Prism
General observation Yellowish green, brownish Light to dark green-blue to strongly
green, and green. Vitreous greenish blue to yellowish green
polish luster, conchoidal to (chrome tourmaline is intense
uneven fracture with vitreous green). Vitreous polish luster,
fracture luster. Surface might conchoidal fracture with vitreous
Diffraction
show abrasions due to low fracture luster.
hardness (Mohs 5).
Prism
optic figure possible—might
appear biaxial)
Diffraction
Magnification Natural inclusions Thread-like liquid and gas inclusions
(trichites), mirror-like gas-filled
fractures, color zoning
Spectrum Group of lines at 580 nm Usually not diagnostic, but some The spectra of green to blue tourmalines
stones might show faint bands at sometimes show faint bands at 462 nm,
462 nm, strong bands at 497 nm, strong bands at 497 nm, and weaker bands
and weaker bands at 560 nm. at 560 nm.
Comments Key tests are RI, birefringence, Key tests are almost always RI and
and optic character. Apatite’s birefringence. If birefringence isn’t
low numerical RI is generally obtainable, uniaxial optic figure and
higher than the low numerical SG can be helpful.
RI of tourmaline.
Robert Weldon/GIA
205
GEM IDENTIFICATION LAB MANUAL
PARTI-COLORED TOURMALINE
Variety Parti-colored
Species Tourmaline
General observation Strong color zoning, in varying combinations of green, blue, and
red hues, usually alternating with colorless. Vitreous polish luster,
conchoidal fracture with vitreous fracture luster.
Terri Weimer/GIA
Birefringence/doubling Usually 0.018 to 0.020
Parti-colored tourmalines include some gems
with green and red “watermelon” color zoning. SR/DR/AGG DR
Pleochroism Usually medium to strong, but might vary depending on which area
of the stone you examine
Magnification Color zoning, thread-like liquid and gas inclusions (trichites), mirror-
like gas-filled fractures
Robert Weldon/GIA
206
SEPARATING TRANSPARENT GREEN GEMS
General observation Vitreous polish luster, conchoidal fracture with vitreous Transparent to translucent. Usually light-toned, weakly
fracture luster. Basal cleavage, possibly with iridescent Yellowish green to greenish to moderately saturated,
cleavage planes. There are two types of treated green yellow, colorless (rare). slightly yellowish green.
topaz on the market: Vitreous polish luster, con- Vitreous polish luster,
Surface-treated topaz—Bluish green to greenish blue choidal fracture with vitreous conchoidal fracture with
Irradiated green topaz—Light to medium yellowish fracture luster. Perfect cleavage vitreous to resinous fracture
green or brownish green to a saturated green to blue-green. in one direction. luster.
Fades rapidly to a typical blue topaz color with exposure to
sunlight in under a day. Might be measurably radioactive.
RI 1.609 to 1.617 typical for surface-treated topaz 1.602 to 1.621 (+/-0.003) 1.577 to 1.583 (+/-0.017)
1.619 to 1.627 (+/-0.010) full topaz range
SR/DR/AGG DR DR DR
Optic character Biaxial positive (common point is 0.001 from the low RI) Biaxial positive Uniaxial negative
Pleochroism Surface-treated topaz—Weak, green to bluish green Weak, in tones of bodycolor Weak to moderate bluish
Irradiated green topaz—Not diagnostic green and green or two
tones of green
Spectrum Surface-treated topaz—Three bands at 545 nm, 585 nm, Not diagnostic Not diagnostic
and 640 nm due to cobalt
Irradiated green topaz—Not diagnostic
Comments Key tests are RI, birefringence, optic character, and Key tests are RI, birefringence, Key tests are RI, birefrin-
magnification. and optic character. gence, and optic character.
Brazilianite’s low numerical Green beryl is generally
RI is always lower than lighter in tone and lower in
tourmaline’s low numerical RI. saturation than emerald.
207
GEM IDENTIFICATION LAB MANUAL
EMERALD
EMERALD TRAPICHE EMERALD
Birefringence/doubling 0.005 to 0.009 (higher than most 0.006 to 0.007 (often not
flux-grown synthetics) detectable)
Pleochroism Moderate to strong green and bluish Weaker than normal emerald
green
Joel Beeson/GIA
Emerald’s tone range is from Magnification Liquid-filled inclusions, fingerprints, Not diagnostic. Transparent
medium-light to dark. Its green two-phase and three-phase inclusions, portion might contain natural
hues might be slightly angular growth zoning, tube-like and emerald inclusions.
yellowish or bluish.
needle-like inclusions; mineral inclu-
sions including pyrite crystals, calcite
inclusions along fractures, and biotite
flakes (see photos, page 212)
Comments Key tests are RI, birefringence, optic Key tests are appearance and
character, pleochroism, spectrum, spot RI.
and possibly magnification.
208
SEPARATING TRANSPARENT GREEN GEMS
FRACTURE-FILLED EMERALD
Variety Emerald
Species Beryl
General observation Surface-reaching fractures filled with various types of materials to All by John Koivula/GIA
reduce their visibility and improve the apparent clarity of emeralds. This fracture-filled emerald shows an
Fillers include oil, plastic, and resin. Treaters can improve the orange to pinkish purple flash effect.
apparent color of low-quality emeralds by adding colored dye to
the filler.
Magnification Look for surface-reaching breaks in reflected light. They might show
very slight outlining. Switch to darkfield lighting and look for the
flash effect. Filler might also “sweat out” from surface fractures, or
move within filled fractures, when the stone is exposed to a temperature
increase (hot point). Oils might have a slightly yellowish or brownish
color. Be careful not to confuse this color with oxide staining in
fractures. Decomposed oils might leave whitish or yellowish branch-
like patterns. You might also see trapped bubbles in the filling material,
flow structure, or whitish, textured, cloudy areas. (see photos, page This fracture-filled emerald shows a blue
212) flash effect.
Fluorescence Some oils might fluoresce chalky yellowish green to greenish yellow
under LW. Effect is weaker to inert under SW. Plastic and polymer
fillers are generally inert to UV, but some might respond a weak,
chalky white to white-blue under LW.
209
GEM IDENTIFICATION LAB MANUAL
General observation Medium to medium-dark green to very slightly bluish green Overgrowth type usually consists of a colorless faceted
beryl with a hydrothermally grown synthetic emerald
overgrowth layer. Sandwich type consists of multiple
layers of hydrothermal synthetic emerald grown on a
central seed plate.
SR/DR/AGG DR DR
Magnification Fingerprints, veils, “nailhead” or spicule inclusions, large or Overgrowth—Oriented strain cracks on surface, typical
small two-phase inclusions, phenakite or chrysoberyl crystals, beryl inclusions in natural core. Poor polish (the over-
gold rods and platelets, white particles randomly scattered or growth is seldom polished to avoid wearing away the
forming “comet tails” or stringers, seed plates in Biron mate- thin green layer). Often a dust-like foggy area in the
rial; numerous tiny red-brown and white particles, opaque contact zone between the core and the synthetic over-
black hexagonal plates and phenakite crystals in Russian growth. (see photo, page 212)
product; seed plates, nailhead spicules, and chevron-type Sandwich—Same inclusions as hydrothermal synthetic
growth zoning in Chinese and Russian products. (see photos, emerald. You might also detect a seed plate with
page 212) spicules pointing in the direction of growth.
Comments Magnification is the key test for separating synthetic from Magnification is the key test for identifying these
natural emeralds. synthetic emerald types. Immersion might help you
detect the overgrowth or the sandwich-type structure of
thin green and colorless areas. Be careful not to mistake
either type for an assembled stone. These are also
known as Lechleitner synthetics.
210
SEPARATING TRANSPARENT GREEN GEMS
SR/DR/AGG DR
Comments Magnification is the key test for separating synthetic from natural
emeralds.
211
GEM IDENTIFICATION LAB MANUAL
INCLUSION PHOTOGRAPHS
Natural emerald: Three-phase Natural emerald: Three-phase inclusion. Natural emerald: Calcite inclusions. Natural emerald: tube-shaped inclu-
inclusion. sions.
Natural emerald: Included Natural emerald: Bamboo-like mineral Natural Sandawana emerald: Growth Flux-grown synthetic emerald: Venetian
pyrite crystals. inclusions. tubes. blind effect.
Flux-grown synthetic emerald: Flux-grown synthetic emerald: Flux-grown synthetic emerald: Coarse Hydrothermal synthetic emerald:
Wispy flux inclusions. Interconnected flux channels. flux inclusions. Layered nailhead spicules parallel to
the seed plate.
Hydrothermal synthetic emer- Hydrothermal synthetic emerald: Liquid Hydrothermal synthetic emerald: Hydrothermal synthetic emerald: Gold
ald: Nailhead spicule. and two-phase inclusions and finger- Synthetic phenakite crystals. inclusions.
print-like pattern.
Hydrothermal synthetic emer- Hydrothermal synthetic emerald: “Overgrowth” synthetic emerald: Over- Lechleitner synthetic emerald: Rough.
ald: Wavy growth planes. Chevron growth pattern. growth layer over natural white beryl.
212
SEPARATING TRANSPARENT GREEN GEMS
LABRADORITE SCAPOLITE
General observation Green to yellowish green, usually light in Yellow to green (rare). Vitreous polish
tone. Oregon material (rare) can range from luster, conchoidal fracture with vitreous Tino Hammid/GIA
near-colorless to moderate or strongly fracture luster. Two cleavage directions.
Oregon sunstone is rare,
saturated green. Green and red bicolor gems
especially in green hues
exist, but are extremely rare. Often displays like this one.
aventurescence. Vitreous polish luster, uneven
to splintery fracture with vitreous to pearly
fracture luster. Two cleavage directions.
Parting also common.
SR/DR/AGG DR DR
Optic character Biaxial positive (often shows twinning in the Uniaxial negative
polariscope)
Pleochroism Yellowish green stones might show colorless Weak to moderate, in tones of
and light yellowish green dichroism. Oregon bodycolor
material might show very strong red and
green pleochroism. If properly oriented, a
faceted gem might appear uniformly red
when viewed from one side and green when
examined from the other.
Fluorescence Inert to weak under LW; Oregon material Inert to strong pink, orange, or
typically inert yellow
Comments Key tests are RI, birefringence, optic Key tests are RI, birefringence, and
character, and magnification. Labradorite optic character. When scapolite’s RI is
from Oregon is commonly called sunstone as high as beryl’s and labradorite’s, it
whether or not it displays aventurescence. has much higher birefringence than
either gem.
213
GEM IDENTIFICATION LAB MANUAL
General observation Green to yellowish green, typically Quench crackling (heating and then rapid Transparent to translucent.
with light tone and low saturation. cooling) produces multiple fractures to Medium to dark yellowish to
Vitreous polish luster, conchoidal create iridescent effects or to allow dye grayish green, generally low in
fracture with vitreous fracture penetration. Most commonly green or red, saturation. Vitreous polish luster,
luster. but any color is possible. Fractures make conchoidal fracture with vitreous
stones more vulnerable to breakage. fracture luster.
SR/DR/AGG DR DR, but might show an AGG reaction due to SR, commonly with ADR
multiple fractures
Optic character Uniaxial positive. Might show a Uniaxial positive Not applicable
bull’s-eye or Airy’s spiral optic
figure and Brazil-law twinning
under crossed polarizing filters.
Magnification Natural inclusions might be pres- Network of cracks, often in a honeycomb Round and elongated gas bubbles,
ent, but are not diagnostic. pattern. Dye visible in fractures. flow lines, roiled effect
Spectrum Not diagnostic Might reveal the presence of chromium- Not diagnostic
based dyes
Comments Key tests are RI, birefringence, Combination of typical quartz properties and Key tests are RI, SR nature,
optic character, optic figure, and unnatural color, along with magnification, magnification, and SG. Color
SG. Rarely found naturally, praseo- identify this type of treated quartz. might also be helpful. Moldavite
lite is usually produced through is a type of natural glass.
heat treatment of amethyst and
sometimes described as “greened”
amethyst.
Dye concentrations form a characteristic honey- Moldavite is a type of natural Natural moldavite glass commonly contains
comb pattern in quench-crackled and dyed glass. Transparent specimens round, high-relief gas bubbles.
green quartz. are often faceted.
214
SEPARATING TRANSPARENT GREEN GEMS
Typical cutting style Occasionally faceted for Faceted gems, cabochons, carvings,
collectors. or beads
SR/DR/AGG DR SR
Comments Key tests are cleavage, Key tests are RI, SG, and possibly
RI, birefringence blink, cleavage.
doubling, SG, and possibly
appearance.
215
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC OPAL
RI 1.430 to 1.470
Birefringence/doubling None
216
SEPARATING TRANSPARENT GREEN GEMS
GLASS PLASTIC
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a variety of
molded to a variety of shapes and finishes.
shapes and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR (strain
colors common)
Comments Key tests are RI and magni- Key tests are RI and magnification. Low
fication. Low thermal heft (SG) and low thermal conductivity
conductivity (warm to the (warm to the touch) might also be helpful.
touch) might also be helpful.
217
GEM IDENTIFICATION LAB MANUAL
Naturally colored diamond from irradiated Color zoning, possibly fluorescence. Often requires
diamond advanced laboratory testing.
Diamond from green CZ and green YAG Diamond tester, magnification, fluorescence, SG
Diamond from green zircon and sphene Diamond tester, SR vs DR nature, magnification,
spectrum, SG, possibly fluorescence
Green CZ from green YAG Fluorescence, SG, possibly see-through and fire
Zircon and sphene from green YAG Magnification and possibly doubling, pleochroism, and
spectrum
Sapphire from natural and synthetic RI, birefringence, optic character, spectrum
chrysoberyl
Grossularite from light green chrysoberyl Birefringence, optic character, spectrum, possibly
magnification
218
SEPARATING TRANSPARENT GREEN GEMS
Emerald from flux-grown synthetic emerald Magnification and possibly RI, birefringence,
fluorescence, and SG
Emerald from hydrothermal synthetic emerald Magnification and possibly RI, birefringence,
fluorescence, and SG
219
GEM IDENTIFICATION LAB MANUAL
Mason-Kay
Some of the world’s most beautiful jewelry is made from jadeite. It’s one of the most popular
translucent-to-opaque green gems.
220
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
1.729 to 1.768 Unakite (visually distinctive—rarely confused with anything within this
AGG (Page 224) color range)
221
GEM IDENTIFICATION LAB MANUAL
1.666 to 1.680 Dyed green jadeite Hydrogrossular, idocrase, jadeite, turquoise, nephrite, dyed calcite
AGG (Page 228)
1.610 to 1.650 Natural and synthetic turquoise Jadeite, dyed green jadeite, variscite
AGG (Pages 229 and 230)
1.606 to 1.632 Nephrite Maw-sit-sit, jadeite, dyed green jadeite, prehnite, variscite,
AGG (Page 230) serpentine, talc
1.560 to 1.570 Serpentine Saussurite, nephrite, variscite, talc, chrysoprase, chalcedony, maw-sit-sit
AGG (Page 231)
1.540 to 1.590 (1.54 spot RI) Talc (soapstone) Nephrite, serpentine, chalcedony
AGG (Page 232)
222
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
1.486 to 1.658 Calcite (including onyx marble) Can resemble malachite or jadeite when dyed
AGG (Page 235)
223
GEM IDENTIFICATION LAB MANUAL
General observation Opaque rock composed of the minerals Generally opaque. Vivid bluish A granite-like rock with a characteristic
azurite and malachite, patterned in bands green to green, usually banded in mottled appearance composed of green
of blue and green. Might show circular two or more tones of green. epidote, white to gray quartz, and pink
color banding and botryoidal growth. Might have a sheen. feldspar. Greasy to vitreous polish
luster, granular to uneven fracture
with dull fracture luster.
Typical cutting style Cabochons, carvings, beads Carvings, beads, cabochons, Carvings, beads, cabochons, tumbled
tablets, inlays specimens
RI Depending on where you test, you might 1.655 to OTL (1.909) 1.729 to 1.768 (spot readings possible
get readings typical of either mineral that around 1.74 to 1.76 or 1.52 to 1.54,
makes up this rock. depending on where you test)
Azurite—1.730 to 1.836 (+/-0.010)
Malachite—1.655 to 1.909
Birefringence/doubling Depends on where you test (use birefrin- 0.254 (use birefringence blink None
gence blink technique—both blink to technique)
OTL)
Azurite—0.106
Malachite—0.254
Comments Key tests are distinctive appearance, Key tests are RI and birefrin- The key to this stone’s identity is its
RI, and birefringence blink. Stabilized gence blink. Appearance is also appearance.
azurite-malachite is widely available in distinctive, with curved or angu-
the trade. It’s made from chalky nodules lar banding. Might have radial
of azurite and malachite that are com- fibrous structure and sheen, and
pressed together and bonded with a might be botryoidal.
polymer. The process is similar to the one
used to produce stabilized turquoise.
Azurmalachite shows a pattern of Stabilized azurite-malachite is made This malachite cabochon Unakite is often used for carvings like this
blue and green hues, circular color from compressed and bonded displays a distinctive banded elephant.
banding, and botryoidal growth. nodules of azurite and malachite. appearance.
224
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
MAW-SIT-SIT HYDROGROSSULAR
General observation An opaque saturated green Green to bluish green. Might show
rock with characteristic dark black inclusions. Vitreous polish
green to black veining or luster, uneven, granular, or splintery
mottling. Waxy to vitreous fracture with greasy to vitreous
polish luster, granular fracture fracture luster.
with dull fracture luster. Eric Welch/GIA
Prism
Birefringence/doubling None None
Diffraction
spots (concentrations of the inclusions
mineral kosmochlor)
460
Spectrum Not diagnostic Darker green material often shows a
cutoff below 460 nm.
Hydrogrossular’s spectrum usually shows a
Fluorescence Inert Inert cutoff at 460 nm.
Comments Key tests are appearance and Key tests are spot RI and possibly
magnification. spectrum and SG. Appearance is
also distinctive. Because hydro-
grossular is often mixed with
idocrase, it might be impossible to
separate the two species.
Eric Welch/GIA
225
GEM IDENTIFICATION LAB MANUAL
IDOCRASE
IDOCRASE RUBY -IN -ZOISITE
Spectrum Line at 464 nm, weak line at Zoisite matrix might show a band
528.5 nm at 455 nm. Ruby crystals should
give a typical ruby spectrum using
Maha Tannous/GIA
the reflected light technique.
Idocrase occurs in brownish and yellowish
Fluorescence Inert Generally inert
green and has vitreous to greasy polish luster.
SG 3.40 (+0.10/-0.15) Approximately 3.10 to 3.40,
depending on the ratio of ruby
inclusions to matrix
Comments Key tests are RI, spectrum, SG, Key test is very distinctive appear-
and possibly appearance. ance. Sometimes called “anyolite”
Sometimes called vesuvianite in the trade.
in the trade. Jadeite-like
idocrase is often mixed with
hydrogrossular, so it might be
impossible to separate the two
species.
Eric Welch/GIA
226
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
NON-CHROME JADEITE
SAUSSURITE JADEITE
Prism
General observation Grayish to yellowish green Semitransparent to opaque. Light to
rock composed of white dark green, often with uneven
feldspar and zoisite. Often has coloration, mottling, or root-like 437.5
mottled appearance. Vitreous markings. Vitreous to greasy polish
to greasy polish luster, granular luster with a dimpled polished sur-
Diffraction
to uneven fracture with dull face, granular to splintery fracture
fracture luster. with dull fracture luster.
RI Spot readings around 1.56 and 1.666 to 1.680 (+/-0.008) (1.66 spot Non-chrome jadeite shows a key line at
1.70, depending on area tested reading common) 437.5 nm due to iron.
JADEITE
Birefringence/doubling None Usually not detectable
Prism
Magnification Not diagnostic Often unevenly colored, with root-
like mottling 437.5 630 691
655
Spectrum Weak 460-nm band Generally a line at 437.5 nm. Jadeite
Diffraction
colored by chromium might also
show lines at 630 nm, 655 nm, and
691 nm.
437.5 630 691
Fluorescence Inert to moderate red under Light green stones inert to weak 655
Comments Key tests are appearance, RI, Key tests are appearance, RI,
spectrum, and fluorescence. spectrum, and SG. Type A jadeite
is enhanced solely with a surface
coating of wax.
Alan Jobbins
Eric Welch/GIA
227
GEM IDENTIFICATION LAB MANUAL
Species Jadeite
Prism
General observation Semitransparent and translucent to opaque. Light to dark green, often
with uneven coloration, mottling, or root-like markings. Vitreous to
greasy polish luster with a dimpled surface, granular to splintery
Diffraction
Spectrum Dyed green stones might have a single broad band in the red-orange
area. Naturally colored green jadeite has three lines in the same area.
SG 3.34 (+0.06/-0.09)
Shane McClure/GIA Comments Key tests are appearance, RI, spectrum, SG, and possibly magnification.
The dye concentrations in dyed and Might require advanced testing to detect presence of dye.
polymer-filled jadeite might resemble the
streaks in naturally colored jadeite.
Species Jadeite
Comments Dye can be detected with a microscope and a spectroscope, but these
Shane McClure/GIA
devices won’t reveal the presence of polymer. In Type C jadeite, the
Acid-bleached jadeite shows characteristic dye concentrates in the jadeite’s surface cracks. In most cases, the dye
etched boundaries between the gem’s is added to the polymer filler, but it can also be applied separately.
individual crystal grains.
Detection of polymer treatment often requires infrared spectroscopy,
usually in a gemological laboratory.
228
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
PREHNITE TURQUOISE
Typical cutting style Carvings, beads, cabochons Cabochons, carvings, beads TURQUOISE
Prism
1.63)
Birefringence/doubling 0.020 to 0.033 (base of cabo- Usually not detectable 420 460
432
chon might give a reading with
birefringence blink technique)
Diffraction
SR/DR/AGG DR (usually gives AGG polar- AGG
iscope reaction)
420 460
432
Magnification Not diagnostic If present, matrix is often recessed
below polished surface
When you read a turquoise spectrum under
Spectrum Might show a weak line at Occasionally shows weak to reflected light, it might show weak to medium
438 nm medium bands at 420 nm and bands at 420 nm and 432 nm. There’s some-
times also a weak band at 460 nm.
432 nm (the 432-nm band is
stronger). Might also show a weak
band at 460 nm.
Eric Welch/GIA
229
GEM IDENTIFICATION LAB MANUAL
General observation Semitranslucent to opaque, greenish blue Light to dark grayish green, Light to medium yellowish green to
to bluish green. When present, the spider- possibly with lighter or darker bluish green, often mottled or veined
web matrix is always even with the mottling. Vitreous to greasy polish with yellow to brown matrix. Waxy to
polished surface. luster, splintery to granular vitreous polish luster, granular to
fracture with dull fracture luster. uneven fracture with dull fracture luster.
Typical cutting style Cabochons, carvings, beads Carvings, beads, cabochons Cabochons, carvings
RI 1.610 to 1.650 (usually a 1.61 spot 1.606 to 1.632 (+0.009/-0.006) 1.560 to 1.590 (+0.003/-0.006) (spot
reading) (1.61 spot reading common) reading usually about 1.57)
Birefringence/doubling Usually not detectable Usually not detectable Usually not detectable
Spectrum Lacks the 432-nm band sometimes seen Rarely shows absorption lines. Strong band at 688 nm, weaker one at
in natural turquoise In exceptional-quality stones, you 650 nm
might see a vague line at 500 nm
or vague lines at the red end of
the spectrum.
Comments Key tests for separating synthetic from Key tests are appearance, RI, and Key tests are appearance, RI,
natural turquoise are magnification, SG. Bright green nephrite from spectrum, color filter, and SG.
spectrum, and possibly appearance. Canada is often sold as “polar
jade.”
Synthetic turquoise is often Nephrite is an attractive green Polar jade is a bright green nephrite Variscite is often fashioned into a
cut as a bead or cabochon. gem that’s often cabochon- that comes from Canada. cabochon. It generally has a mottled or
cut. veined appearance.
230
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
SERPENTINE
SERPENTINE
Species Serpentine
Prism
General observation Semitransparent to opaque, usually yellowish green, green, or greenish
yellow. Waxy to greasy polish luster, granular to uneven fracture with
dull to waxy fracture luster. Might show scratches and pits due to low
hardness (Mohs 2.5 to 6). Bowenite variety is harder, takes a better
polish, and is an effective jade substitute.
Diffraction
Typical cutting style Carvings, beads, cabochons
Spectrum Bright green stones might show a gradual cutoff at about 480 nm, a
band at 500 nm, and lines in the red at around 640 nm and 660 nm.
Translucent dark green stones might show a cutoff at about 480 nm,
a line at 500 nm, and increasing absorption in the red beyond 660 nm.
Dyed stones show a broad band between 630 nm and 675 nm and a
cutoff at 520 nm.
231
GEM IDENTIFICATION LAB MANUAL
General observation Green (from inclusions) with Various colors, often dyed. A Light to dark green, white, gray, or brown,
aventurescence. Vitreous polish coarse crystalline aggregate of often veined or mottled. Waxy to greasy polish
luster, granular to conchoidal tightly packed quartz grains. luster, uneven fracture with dull to waxy
fracture with vitreous fracture luster. fracture luster. Might show surface damage
due to very low hardness (Mohs 1). Can often
be scratched with a fingernail.
Typical cutting style Carvings, beads, cabochons Carvings, beads Ornamental carvings, decorative objects
Birefringence/doubling Might not be detectable in AGG Usually not detectable 0.050 (usually difficult to detect)
material
Magnification Tiny, randomly distributed, green Dye visible in fractures. Not diagnostic
disk-like chrome mica (fuchsite)
flakes or platelets
Spectrum Bands at approximately 649 nm Not diagnostic. Might show a Not diagnostic
and 682 nm, probably due to mica band in the orange due to
inclusions presence of dye.
Fluorescence Inert to weak grayish green or red- Generally inert Inert to weak pink under LW
dish under LW and SW
Comments Key tests are appearance, RI, and Key tests are appearance and Key tests are poor surface quality, RI, and SG.
magnification. magnification to detect dye Also known in the trade as steatite or, more
concentrations between crystal commonly, “soapstone.”
grains. Record both the
required treatment call and the
variety on the variety line of
your GIA worksheet.
This aventurine quartz cabo- Magnification reveals bright green mica The areas of dye concentration are
chon shows a typical speckled inclusions in this aventurine quartz. obvious in these dyed quartzite beads.
appearance.
232
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
General observation Translucent and generally evenly Translucent to semitranslucent. Blue to Semitransparent to translucent, light
colored. Slightly bluish green. green-blue. Might be unevenly colored to medium-dark yellowish green
Might show curved or irregular or resemble fine turquoise. Conchoidal (natural color). Greasy to vitreous
banding in various colors. fracture with dull to waxy fracture luster. polish luster, conchoidal fracture
Conchoidal fracture with dull to with dull to waxy fracture luster.
waxy fracture luster.
Typical cutting style Cabochons, carvings, beads Cabochons, carvings, beads Carvings, beads, cabochons
RI 1.535 to 1.539 (1.53 or 1.54 spot 1.535 to 1.539 (1.53 to 1.54 spot reading) 1.535 to 1.539 (1.53 to 1.54 spot
reading) reading)
Birefringence/doubling Usually not detectable Usually not detectable Usually not detectable
Spectrum Vague lines at 645 nm and 670 nm Not diagnostic Not diagnostic, but might show a
660-nm to 700-nm cutoff
Color filter Light grayish to reddish or pinkish Not diagnostic Not diagnostic
Comments Key tests are fracture, RI, spectrum, Keys tests are RI, SG, and possibly Key tests are fracture, RI, and SG.
and SG. Might be difficult to sepa- appearance.
rate from chrome chalcedony. A
color filter can help separate dyed
green chalcedony from chrysoprase.
645 670
Diffraction
Eric Welch/GIA
233
GEM IDENTIFICATION LAB MANUAL
CHROME CHALCEDONY
CHROME CHALCEDONY CHALCEDONY
Both by Eric Welch/GIA Spectrum Bands around 684 nm and 645 Not diagnostic
This green jasper Moss agate has dark nm and an ill-defined broad
cabochon displays inclusions that resem- absorption centered on 600 nm
characteristic mottling ble moss.
and banding. Fluorescence Inert Generally inert
Comments Key tests are fracture, RI, SG, Key tests are spot RI, SG, and
and possibly spectrum. Might possibly appearance and fracture.
be difficult to separate from
dyed green chalcedony.
234
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
AMAZONITE CALCITE
Comments Key tests are appearance, RI, Key tests are RI, birefringence
magnification, SG, and possibly blink, SG, and possibly appearance.
fluorescence. Marble is a granular aggregate,
onyx marble is a banded marble.
Satinspar is a fibrous aggregate
that’s often chatoyant (the name is
also used for a similar variety of
gypsum).
235
GEM IDENTIFICATION LAB MANUAL
SR/DR/AGG SR, commonly with ADR due SR with weak to strong ADR
to strain
Spectrum Cutoffs at 470 nm and 660 nm Some gems show bands at 550 nm
and 580 nm
236
SEPARATING TRANSLUCENT-TO-OPAQUE GREEN GEMS
GLASS PLASTIC
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a
molded to a variety of shapes variety of shapes and finishes.
and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR Both by Maha Tannous/GIA
(strain colors common) This pipe bowl looks like jade, but it’s
actually meta-jade, an imitation com-
Magnification Gas bubbles, cavities on Gas bubbles, flow lines posed of partially devitrified glass.
surface where gas bubbles
were polished through, flow
marks (swirls)
Comments Key tests are RI and magnifica- Key tests are RI and magnification. Under magnification, meta-jade
tion. Low thermal conductivity Low heft (SG) and low thermal displays gas bubbles and fibrous
(warm to the touch) might also conductivity (warm to the touch) inclusions.
be helpful. Meta-jade is a might also be helpful.
partially devitrified glass that’s
sold as a jade imitation. Its
partially crystallized structure
gives it a fern-like texture.
237
GEM IDENTIFICATION LAB MANUAL
Idocrase from green hydrogrossular RI, spectrum, SG, and possibly appearance
Dyed green chalcedony from dyed green Appearance, magnification, possibly fracture and RI
quartz
Chrysoprase from chrome chalcedony Color, spectrum, color filter, possibly magnification
Chrysoprase from glass RI, magnification, SG, and possibly fracture and fracture
luster
238
SEPARATING ORANGE, YELLOW, AND BROWN GEMS
These beautiful fancy-colored sapphires are among the identification choices for transparent
orange, yellow, and brown gems.
239
GEM IDENTIFICATION LAB MANUAL
2.150 CZ (synthetic cubic zirconia) Diamond, synthetic diamond, GGG, zircon, sphene, andradite,
SR (Page 250) YAG, spessartite
1.970 GGG (gadolinium gallium garnet) Diamond, synthetic diamond, CZ, YAG
SR (Page 250)
1.925 to 1.984 Zircon Diamond, synthetic diamond, CZ, sphene, andradite, YAG,
1.810 to 1.815 (Page 251) spessartite
DR
1.888 Yellow andradite garnet Diamond, synthetic diamond, CZ, zircon, sphene, YAG
SR (Page 252)
1.833 YAG (yttrium aluminum garnet) Diamond, synthetic diamond, CZ, GGG, zircon, andradite
SR (Page 253)
Transparent Orange, Yellow, and Brown Gems with RIs between 1.70 and 1.80
RI and SR/DR/AGG Gem Material Commonly confused with:
1.773 to 1.779 range Grossularite-andradite garnet (“Mali”) Spessartite, sapphire, synthetic sapphire, pyrope-spessartite,
SR (Page 254) chrysoberyl, grossularite
1.762 to 1.770 Synthetic corundum, synthetic yellow sapphire Grossularite-andradite, sapphire, pyrope-spessartite,
DR (Pages 257 and 258) chrysoberyl, grossularite
1.750 to 1.780 range Pyrope-spessartite garnet (including “malaya”) Spessartite, grossularite-andradite, sapphire, synthetic sapphire,
SR (Page 260) chrysoberyl, grossularite
240
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Transparent Orange, Yellow, and Brown Gems with RIs between 1.60 and 1.70
RI and SR/DR/AGG Gem Material Commonly confused with:
1.470 to 1.700 range Glass Any orange, yellow, or brown transparent gem material
SR (Page 275)
1.460 to 1.700 range Plastic Any orange, yellow, or brown transparent gem material
SR (Page 275)
241
GEM IDENTIFICATION LAB MANUAL
Transparent Orange, Yellow, and Brown Gems with RIs between 1.50 and 1.60
RI and SR/DR/AGG Gem Material Commonly confused with:
1.577 to 1.583 Yellow beryl, heliodor Synthetic beryl, brazilianite, labradorite, scapolite, quartz, synthetic quartz
DR (Page 268)
1.544 to 1.553 Synthetic quartz, synthetic citrine Beryl, labradorite, scapolite, quartz, orthoclase
DR (Page 270)
1.470 to 1.700 range Glass Any orange, yellow, or brown transparent gem material
SR (Page 275)
1.460 to 1.700 range Plastic Any orange, yellow, or brown transparent gem material
SR (Page 275)
Transparent Orange, Yellow, and Brown Gems with RIs below 1.50
RI and SR/DR/AGG Gem Material Commonly confused with:
1.470 to 1.700 range Glass Any orange, yellow, or brown transparent gem material
SR (Page 275)
1.460 to 1.700 range Plastic Any orange, yellow, or brown transparent gem material
SR (Page 275)
242
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Species Diamond
Prism
General observation Yellows, brownish yellows, and browns, often with light tone and
low saturation. Vivid “canary” yellow, orange, and fancy brown gems
exist, but they’re rare. Color sometimes evenly distributed, but some 415.5
gems show uneven color with irregular, “blotchy” zones or darker
yellow zones at their center. Under 10X, look for naturals, waxy to
Diffraction
granular or faceted girdle surface, bearding, sharp facet junctions.
Adamantine polish luster, step-like fracture. Perfect cleavage in four
directions. Polish lines never oriented the same way on adjacent
facets. Positive reaction to diamond tester. 415.5
Typical cutting style Faceted, often in radiant cuts to help intensify bodycolor. Girdle often
faceted or polished. Naturally colored yellow to near-colorless diamonds
often show a band in the violet at 415.5 nm. There
might also be some combination of fainter bands at
Dispersion 0.044 (moderate fire—might be masked by bodycolor) 423 nm, 435 nm, 451 nm, 478 nm, 496 nm, and
503 nm. In general, the deeper the diamond’s
RI OTL color, the stronger the lines will be.
SR/DR/AGG SR (might show strain colors in a mosaic pattern under crossed filters
in the polariscope)
Prism
Pleochroism None
Magnification Angular mineral inclusions (see photos, page 249), fractures and
cleavages, surface and internal graining, sometimes yellow or brown,
parallel to octahedral crystal faces. Internal graining might form a
Diffraction
cross-hatch or “tatami” pattern.
Spectrum Some yellow “cape” diamonds might show a line in the violet at 415.5
nm, with weaker bands at 423 nm, 435 nm, 451 nm, 478 nm, 496 nm,
and 503 nm. In general, the deeper the color, the more distinct the bands.
(Cooling diamond with liquid nitrogen helps make its spectrum more Naturally colored grayish to brownish yellow
visible.) Irradiated yellow diamonds might show a distinctive band at diamonds might show bands at 415.5 nm, 423 nm,
595 nm in the yellow. 433 nm, 452 nm, 465 nm, and 478 nm. They might
also show weak 496-nm and 503-nm bands.
Fluorescence Some stones show no reaction or a very faint reaction to UV, but
many show a medium to strong reaction under LW, most commonly
blue. Reaction to SW varies from inert to faint blue.
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, OTL RI, SR nature, magnification, positive
reaction to diamond tester, and possibly spectrum. Treatments such as
irradiation and surface coating can be applied to off-color diamonds to
make them appear fancy-colored. Treatments like fracture filling and
laser drilling might be used to improve the appearance and apparent Eric Welch/GIA
clarity of fancy-colored diamonds. Fancy-colored diamonds often Advanced laboratory testing deter-
require advanced testing at a gemological laboratory to determine mined that the color of this yellow cape
origin of color. diamond is natural.
243
GEM IDENTIFICATION LAB MANUAL
Species Diamond
Prism
General observation Typically light to dark brownish orange to yellow. Might show
treatment-related color zoning that follows the faceted shape of the cut
stone, but color is usually evenly distributed. Cyclotron-irradiated
gems often show an umbrella-shaped zone around the culet (see
photo, page 249).
Diffraction
Spectrum Irradiated yellow diamonds might show a diagnostic band at 595 nm.
Unfortunately, it’s eliminated by controlled heating, making detection of
An irradiated yellow diamond spectrum might
show a diagnostic band at 595 nm. laboratory irradiation more difficult. Irradiated orangy to brownish yellow
Unfortunately, it’s eliminated by controlled and yellow Type Ia diamonds typically show bands at 496 nm, 503 nm,
heating, making positive detection of this and 595 nm in their spectra. There’s sometimes also a 415.5-nm cape
treatment more difficult. line. Irradiated Type Ib stones might show some additional sharp bands
at 575 nm, 615 nm, 625 nm, and 637 nm. (Cooling diamond with liquid
nitrogen helps make its spectrum more visible.)
Fluorescence Irradiated Type Ia stones: Weak to strong yellow to green under LW,
weak to strong yellow to green under SW. LW reaction typically
stronger than SW.
Irradiated Type Ib stones: Weak to very strong orange, often with
wedge-shaped green zones under both LW and SW. LW reaction
might be stronger than or equal to SW reaction.
Comments Key tests are magnification and spectrum. Fluorescence might also be
helpful. Irradiated diamonds often require advanced testing at a gemo-
Robert Weldon/GIA logical laboratory to determine origin of color.
The yellow color of these natural diamonds is
the result of irradiation treatment.
difficult.
244
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Species Diamond
Prism
General observation HPHT treatment of brown nitrogen-containing Type Ia diamonds
produces strongly saturated greenish yellow, yellowish green, yellow,
or brownish yellow colors.
Magnification Etched or pitted naturals or feathers, tension fractures that often contain
Diffraction
graphite around crystalline inclusions. Some surface areas might show
etching and pitting if not completely repolished.
Spectrum Might show a strong line at 503 nm, a dark band between 480 nm
and 500 nm, a line at 415 nm, and sometimes emission lines at
505 nm and 515 nm. (Cooling diamond with liquid nitrogen helps
make its spectrum more visible.) The spectrum of an HPHT-treated yellow-green
diamond might show a dark band between
480 nm and 500 nm, a line at 503 nm, and
Fluorescence Chalky greenish yellow to yellowish green fluorescence under LW sometimes a line at 415.5 nm. There might also
and SW be emission lines at 505 nm and 515 nm.
Maha Tannous/GIA
245
GEM IDENTIFICATION LAB MANUAL
General observation Color is typically more saturated and darker than natural gems. Might
show vague zoning of lighter and darker yellow. Might be attracted to
a magnet due to inclusions of metallic flux. Virtually all are grown by
conventional high pressure high temperature (HPHT) techniques.
Color of untreated (as grown) synthetics can be modified by a combi-
Diffraction
nation of irradiation and heat treatment. Orange to pink and even red
colors are possible from yellow starting material.
RI OTL
The spectra of synthetic yellow to greenish to
orangy to brownish yellow and brown diamonds
usually don’t show any sharp absorption bands. Birefringence/doubling None
Cooling might reveal a 658-nm band.
SR/DR/AGG SR (might show weak ADR, sometimes in a cross-shaped pattern)
GREENISH TO ORANGY TO BROWNISH YELLOW
SYNTHETIC DIAMOND Magnification Uneven color zoning related to internal growth sectors might form a
cross-shaped or hourglass-shaped pattern. Graining might mark the
boundaries of the color zoning. Elongated or rounded opaque inclu-
Prism
the diamond is cooled with liquid nitrogen. Others (when cooled to low
temperatures) show a series of sharp bands between 600 nm and
700 nm, which gemologists believe result from flux that contains nickel.
Treated synthetics—Some yellow, greenish yellow, and yellowish
green synthetics might show a series of sharp bands between 473 nm
and 553 nm in their spectra. Others might show sharp bands at 503 nm,
Some greenish, orangy, and brownish yellow
synthetic diamonds might show sharp bands 527 nm, 553 nm, 575 nm, 595 nm, 617 nm, 637 nm, and 658 nm
between 600 nm and 700 nm when cooled to when cooled to low temperatures.
low temperatures. Gemologists believe these
bands result from nickel flux. Fluorescence Often unevenly distributed in a cross-shaped, square, or hourglass-
shaped pattern.
TREATED YELLOW TO GREENISH YELLOW TO Untreated synthetics—Usually inert under LW, weak to moderate
YELLOWISH GREEN SYNTHETIC DIAMOND green-yellow, yellow-green, green, or inert to SW. SW response
typically stronger than LW. Occasional weak yellow or greenish
yellow phosphorescence.
Prism
3.52 (+/-0.10)
Diffraction
SG
Comments Key tests are magnification and fluorescence, which can help with
detection of cross-shaped or hourglass-shaped internal growth patterns.
Spectrum might also be helpful. If in doubt, submit diamond to a
gemological laboratory for advanced testing.
If cooled to low temperatures, treated yellow,
greenish yellow, and yellowish green synthetic
diamonds might show a series of sharp bands
between 473 nm and 553 nm in their spectra.
246
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
John Koivula/GIA
Gemesis synthetic diamonds are typically yellow, with Synthetic diamonds often have intense, vivid colors.
more saturated color than natural diamonds. They can These were produced by Gemesis.
be found in a wide range of cuts, including baguettes.
Elizabeth Schrader/GIA
247
GEM IDENTIFICATION LAB MANUAL
General observation Grown by chemical vapor deposition (CVD) rather than conventional
HPHT techniques. Faint to dark brown or brownish yellow. Fashioned
gems are typically shallow because they’re cut from tabular crystals.
Might be grown on a conventional synthetic diamond or natural
diamond seed, so fashioned gems might include portions of either one.
Birefringence/doubling None
SR/DR/AGG SR
SG 3.52 (+/-0.10)
248
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
INCLUSION PHOTOGRAPHS
Vincent Cracco/GIA
Natural, untreated diamond: Included Natural, untreated diamond: Included Natural, untreated diamond: Contorted
crystals. crystal. etch channel.
Treated natural diamond: Laser drill- Cyclotron-irradiated natural diamond: Sumitomo synthetic diamond:
hole. Umbrella-shaped color zone around Hourglass-shaped graining.
the culet.
Gemesis synthetic diamond: Gemesis synthetic diamond: Gemesis synthetic diamond: Metallic
Concentrations of tiny pinpoint inclu- Characteristic colorless zone. flux inclusion.
sions.
Gemesis synthetic diamond: Metallic Sumitomo synthetic diamond: HPHT synthetic diamond from Russia:
flux inclusion. Cross-shaped pattern under polarized Uneven LW fluorescence with a cross
lighting. shape surrounding a central square or
octagon.
CVD synthetic diamond: Small, opaque CVD synthetic diamond: Brown graining
inclusions, possibly graphite. parallel to the table facet.
249
GEM IDENTIFICATION LAB MANUAL
CZ GGG
General observation Pale to strong yellow, orangy yellow Usually colorless to light brown or
to orange, and reddish orange. yellow. Vitreous to subadamantine polish
Subadamantine polish luster, conchoidal luster, conchoidal fracture with vitreous
fracture with subadamantine fracture to subadamantine fracture luster. Well-
luster. Heft reveals that loose stones are proportioned round brilliants might show
much heavier than diamonds of similar moderate see-through. Heft reveals that
size. Negative reaction to diamond tester. loose stones are much heavier than
diamonds of similar size and proportions.
Negative reaction to diamond tester.
RI OTL OTL
SR/DR/AGG SR SR
Magnification Generally inclusion free, but might have Might show gas bubbles
unmelted zirconium oxide particles and
gas bubbles.
Comments Key tests are negative reaction to dia- Key tests are negative reaction to diamond
mond tester, OTL RI reading, lack of tester, OTL RI reading, lack of doubling,
doubling, and SG. Conchoidal fracture and SG. GGG is a manmade material
distinguishes CZ from diamond. CZ is a with no natural counterpart.
manmade material with no gem-quality
natural counterpart.
250
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
ZIRCON
ZIRCON
Species Zircon
Prism
General observation Orangy yellow through reddish orange, often dark, brownish hues.
Facet edges might show chipping. Eye-visible doubling in larger
stones. Vitreous to subadamantine polish luster, conchoidal fracture 653.5
with vitreous to subadamantine fracture luster. Negative reaction to
diamond tester.
Diffraction
Typical cutting style Faceted
RI OTL
Zircon has a distinctive spectrum, with a key
Birefringence/doubling Up to 0.059 (strong). Not present or weak in low-type zircon. line at 653.5 nm.
SR/DR/AGG DR
Pleochroism Brown stones show weak to moderate purplish brown and brownish
yellow dichroism
Spectrum Key line at 653.5 nm, with several other lines possible
Comments Key tests are OTL RI reading, strong doubling, and spectrum.
251
GEM IDENTIFICATION LAB MANUAL
SPHENE
SPHENE ANDRADITE GARNET
RI OTL OTL
Comments Key tests are OTL RI reading, very Key tests are OTL RI reading,
strong doubling (almost twice that lack of doubling, and spectrum.
of zircon), and possibly spectrum. Sometimes sold as “topazolite”
440
in the trade.
252
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
SPESSARTITE GARNET
YAG SPESSARTITE GARNET
Prism
General observation Usually colorless, but might be Orange, brownish orange,
412 432
orange or yellow. Vitreous to yellowish orange, reddish 424
subadamantine polish luster, orange, red-orange (always
conchoidal to uneven fracture with has an orange component and
Diffraction
vitreous to subadamantine fracture never shows any purple).
luster. Well-proportioned round Vitreous to subadamantine
brilliants might show strong see- polish luster, conchoidal 412 432
through. Negative reaction to fracture with vitreous to sub- 424
diamond tester. adamantine fracture luster.
Typical cutting style Faceted Faceted Key features of spessartite’s spectrum are
bands in the violet at 412 nm, 424 nm, and
432 nm, along with bands at 505 nm, 527 nm,
Dispersion 0.028 (weak fire—might be 0.027 (weak fire—might be
and 575 nm in the green-yellow.
masked by bodycolor) masked by bodycolor)
SR/DR/AGG SR SR
Comments Key tests are negative reaction to Key tests are OTL RI reading,
diamond tester, OTL RI reading, lack of doubling, spectrum,
lack of doubling, and SG. YAG is a and possibly color.
manmade material with no natural
counterpart.
253
GEM IDENTIFICATION LAB MANUAL
YELLOW-GREEN GROSSULARITE-ANDRADITE
GARNET GROSSULARITE -ANDRADITE GARNET
Species Grossularite-andradite
Prism
Group Garnet
General observation Slightly greenish yellow to brown-orange and dark orangy brown.
440
Vitreous to subadamantine polish luster, conchoidal to uneven fracture
with greasy to vitreous fracture luster.
Diffraction
RI 1.773 to 1.779 (Orange to brown gems generally have higher RIs than
440
yellowish green or green stones)
Birefringence/doubling None
Yellow-green grossularite-andradite garnet
shows a strong band at 440 nm and weaker
SR/DR/AGG SR, often with moderate to strong ADR
bands at 465 nm and 495 nm. There’s also a
weak band at 415 nm in the violet.
Magnification Fingerprints (partially healed fractures), parallel growth planes, and
small mineral crystals. Many fine faceted gems are almost inclusion-
free.
Spectrum Strong band at 440 nm and weaker bands at 465 nm and 495 nm. Also
a weak band at 415 nm.
Fluorescence Inert
SG 3.67 to 3.68
Comments Key tests are RI, SR nature, and spectrum. Sometimes sold as “Mali”
or “grandite” garnet in the trade.
Tino Hammid/GIA
254
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Prism
Species Corundum
General observation Pale to dark yellow, brownish yellow, orangy yellow, and strong 450 471
orange to reddish or pinkish orange. Vitreous to subadamantine polish 460
Diffraction
Typical cutting style Faceted gems or cabochons
Prism
(high- or low-relief crystals) that might show angular faces; intact, fine,
needle-like rutile inclusions intersecting at 60° angles in the same
plane; other fine needles at near right angles; fingerprint inclusions, 450 471
intact two-phase inclusions, straight and hexagonal growth banding; 460
Diffraction
Heat-treated natural corundum—Altered, burned mineral inclusions
with rounded, often whitish, “snowball” or “cotton” appearance;
broken silk (partially reabsorbed rutile needles), ruptured two-phase
inclusions and negative crystals; sintered surface areas, especially 450 471
460
around the girdle; fine needles at near right angles. Discoid fractures
with tension halos (disk-like fractures with lace-like outer healing
rims, caused by expansion of inclusions) are also indicative of heat Some orange sapphires show fine lines due to
treatment, but these features might also occur in some untreated chromium in the red area of the spectrum and
corundum of magmatic origin. (see photos, page 259) bands due to iron at 450 nm, 460 nm, and
471 nm.
Spectrum Iron-rich yellow sapphires—Might show three strong lines in the
violet-blue of the spectrum at 450 nm, 460 nm, and 471 nm. The
450-nm band is usually the strongest.
Orange and dark pinkish orange sapphires—Might show a ruby-type
spectrum, with fine lines in the red, a broad absorption between 500 nm
and 600 nm, fine lines in the blue at 468 nm and 476 nm, and a cutoff at
450 nm. Others might show fine lines in the red together with bands in
the blue at 450 nm, 460 nm, and 471 nm.
Pale orange sapphires—Might show a vague chrome line around
690 nm, vague, broad absorption between 500 nm and 600 nm, and a
450-nm cutoff.
Stones treated with heat or lattice diffusion might show no character-
istic spectra at all.
SG 4.00 (+0.10/-0.05)
Comments Key tests for separating natural corundum from other similarly colored
natural gems are RI, birefringence, pleochroism, magnification, and
spectrum. Magnification is the key test for separating natural from syn-
thetic corundum. Fine pinkish orange gems are sold as padparadscha.
255
GEM IDENTIFICATION LAB MANUAL
Species Corundum
SR/DR/AGG DR
Use immersion with methylene iodide (see page 58 for heavy liquid
safety precautions) or mineral oil and look for a core that’s a different
color than at the stone’s surface. You might find a different surface-
related color that follows the gem’s outline. Very high temperatures
are used in the process, so an overgrowth of synthetic material can
form during treatment and might be present on the finished stone.
SG 4.00 (+0.10/-0.05)
256
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Prism
General observation Pale to dark yellow, orangy yellow, strong orange to reddish orange
and brown. Might show poor polish, with polishing marks on most 460 690
Diffraction
Typical cutting style Faceted gems or cabochons, often symmetrical and to precise
calibrated sizes. Often cut in brilliant style, including scissors cut.
460 690
RI 1.762 to 1.770 (+0.009/-0.005)
Pleochroism Same as natural, but might be visible directly through the table facet
Magnification Curved color banding might be visible when viewed with diffused
light, or preferably against a blue filter under magnification (see
photos, page 259). Strings of gas bubbles might resemble needles.
Twinning planes possible, but very rare or difficult to observe. When
present, they’re usually formed by rapid cooling of the boule. These
are known as Plato lines. They’re best seen with magnification,
polarized light, and immersion. The stone also has to be viewed
parallel to its optic axis. The twinning then appears as sets of lines
that intersect at 60° or 120° angles.
Spectrum Yellow—Lacks the set of iron bands at 450 nm, 460 nm, and 471 nm
that characterize some natural yellow corundum. Presence of a
690-nm line and no iron lines is a strong indication that stone is a
synthetic. A 460-nm cutoff by itself is another good indication of
synthetic origin.
Orange—If you see only thin lines in the red (including a fluorescent
line at 690 nm) and the stone is inclusion free, it’s probably synthetic.
SG 4.00 (+0.10/-0.05)
Comments The key test for separating flame-fusion synthetic corundum from
natural is magnification. Immersion might help with detection of faint
curved growth structures. Flame fusion and hydrothermal growth are
the most common methods for growing synthetic sapphire, but small
amounts of these colors might be produced by the crystal pulling and
floating zone methods.
257
GEM IDENTIFICATION LAB MANUAL
General observation Orange to reddish and pinkish orange (synthetic Medium to light-toned yellow to yellowish orange,
padparadscha) and brownish orange, with moderate to vivid orange, and orange-pink to reddish orange with moderate
saturation. Might be very strongly zoned in alternating saturation. Unlike flux-grown synthetic corundum, color in
straight or angular bands of lighter and darker color. Often hydrothermal synthetic corundum tends to be very evenly
heavily included with eye-visible clarity characteristics. distributed.
SR/DR/AGG DR DR
Magnification Flux inclusions are generally white and high-relief, but Strong growth zoning possible. To avoid confusing
might appear near-colorless, whitish, brownish, or yellow subparallel growth structures with those seen in natural
to orange. Flux might also appear as two-phase, wispy gems, examine stones in several orientations and look
veils that look like natural fingerprints, or as coarse for mosaic-type, chevron, or zigzag growth zoning.
globules that might appear drippy, tubular, rod-like, or Sometimes two- or three-phase inclusions in fingerprint
icicle-like, or as droplets or dashed lines or clouds of patterns; small whitish inclusions; possibly tiny, flake-like
minute particles. Flux corundum can have uniform, copper crystals that show a metallic luster in fiber-optic
parallel growth planes. Triangular or hexagonal platelets lighting.
or stubby needle-like inclusions (usually platinum)
strongly indicate synthetic. Platinum platelets appear
bright and metallic in reflected light, but black when
backlit. (see photos, page 259)
Fluorescence Under LW, orange synthetic stones show strong to very Orange stones show moderate orange under LW and weak
strong yellowish orange or reddish orange, with zones orange under SW.
of chalky yellow. SW response is a very weak to weak
version of the LW response, or weak pinkish red.
Comments The key test for separating synthetic from natural The key test for separating synthetic from natural
corundum is magnification. corundum is magnification.
258
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
INCLUSION PHOTOGRAPHS
Duncan Pay
Untreated natural corundum: Included Heat-treated natural yellow sapphire: Treated natural corundum: Heat-
apatite crystals. Melted inclusion with disk-shaped damaged sintered area near the girdle.
partially healed fracture.
Beryllium diffusion treated corundum: Beryllium diffusion treated corundum: Beryllium diffusion treated corundum:
Surface-related yellow color zoning Surface-related yellow color (left) and Melted inclusions with gas bubbles.
surrounding a colorless core. orange and yellow hexagonal color
zoning (right).
Lattice diffusion treated corundum: Beryllium diffusion treated corundum: Beryllium diffusion treated corundum:
Dark blue halos around rutile crystals. Areas of synthetic corundum over- Areas of synthetic corundum over-
growth in transmitted light. growth in cross-polarized light.
Flame-fusion synthetic yellowish Flux-grown synthetic sapphire: Flux-grown synthetic sapphire: Eye-
orange sapphire: Curved color band- Platinum platelets and opaque flux visible platinum platelet and opaque
ing, revealed by a blue filter. inclusions. flux inclusions.
259
GEM IDENTIFICATION LAB MANUAL
PYROPE-SPESSARTITE GARNET
PYROPE -SPESSARTITE GARNET
Species Pyrope-spessartite
Garnet
Prism
Group
General observation Usually light to dark slightly pinkish orange, reddish orange, or
410 430 505 575
527
orangy red to yellowish orange. Vitreous to subadamantine polish
420
luster, conchoidal fracture with vitreous fracture luster.
Diffraction
RI 1.750 to 1.780
410 430 505 575
420 527
Birefringence/doubling None
Malaya garnet’s spectrum shows strong bands SR/DR/AGG SR, often with ADR
at 410 nm, 420 nm, and 430 nm in the blue-
violet plus a combination of bands at 460 nm, Magnification Mineral inclusions (rutile, apatite, pyrite), often seen as intersecting
480 nm, 505 nm, 527 nm, and 575 nm in the
blue-green to yellow.
needles
Spectrum Strong bands at 410 nm, 420 nm, and 430 nm occasionally merge to
form a cutoff at 435 nm. Also often shows bands in the blue-to-green
and yellow areas of the spectrum at 460 nm, 480 nm, 505 nm, 527
nm, and 575 nm.
Fluorescence Inert
SG 3.78 to 3.85
Comments Key tests are color, RI, SR nature, and spectrum. Sometimes sold as
Robert Weldon/GIA “malaya” or “malaia” in the trade.
Malaya garnets range in color from pinkish to
reddish to yellowish orange.
260
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
General observation Yellow through strongly yellowish green to greenish Medium to dark orange to brownish orange (hessonite),
brown. Vitreous to subadamantine polish luster, con- yellow to yellow-green and colorless. Vitreous polish
choidal fracture with greasy to vitreous fracture luster. luster, conchoidal to uneven fracture with greasy to
vitreous fracture luster.
SR/DR/AGG DR SR
Magnification No characteristic inclusions, but might show finger- Hessonite usually shows stubby, rounded included crystals
prints, angular included crystals, liquid inclusions, and a “heat wave” or “scotch-in-water” effect.
needle-like inclusions, and twinning.
Spectrum Strong band at 444 nm due to iron Generally not diagnostic, but might show bands at 407 nm
and 430 nm
Fluorescence Yellowish and yellowish green stones are generally inert Yellow stones are inert to weak orange under LW and SW
to yellowish green under SW. Other colors are generally
inert.
Comments Key tests are RI, birefringence, optic character, and Key tests are RI, SR nature, and magnification (hessonite
spectrum. variety).
CHRYSOBERYL
Prism
444
Diffraction
261
GEM IDENTIFICATION LAB MANUAL
EPIDOTE
EPIDOTE IDOCRASE
Peter Johnston/GIA
Magnification Natural inclusions Not diagnostic
Epidote is one of the few gems that might give
you an optic figure that appears uniaxial but is Spectrum Very strong band at 455 nm and Line at 464 nm, weak line at
actually biaxial. This occurs when the angle sometimes a weak line at 475 nm 528.5 nm
between a biaxial gem’s optic axes is so small
that the brushes appear to intersect.
Fluorescence Generally inert Inert
Comments Key tests are RI, birefringence, Key tests are RI, birefrin-
optic character, spectrum, and gence, optic character (test
Prism
464
262
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
AXINITE
AXINITE SINHALITE
Prism
General observation Transparent to translucent brown, Transparent to translucent
purplish brown “clove” or “root greenish to brownish yellow.
beer” color, brownish yellow, rarely Vitreous polish luster, con-
violet or blue. Greasy to vitreous choidal fracture with vitreous
polish luster, conchoidal to uneven fracture luster.
Diffraction
fracture luster with vitreous fracture
luster. Distinct cleavage in one
direction.
RI 1.678 to 1.688 (+/-0.005) 1.668 to 1.707 (+0.005/-0.003) Axinite’s spectrum might show bands at
415 nm, 444 nm, 466 nm, 492 nm, 512 nm,
and 532 nm.
Birefringence/doubling 0.010 to 0.012 0.036 to 0.039
SINHALITE
SR/DR/AGG DR DR
Prism
Pleochroism Strong violet to purple, light yellow, Moderate light brown, dark
and red-brown brown, and greenish brown 452 475
463 493
Magnification Natural inclusions Natural inclusions
Diffraction
Spectrum Bands at 415 nm, 444 nm, 466 nm, Bands at 452 nm, 463 nm,
492 nm, 512 nm, and 532 nm 475 nm, 493 nm, and 526 nm
452 493
Fluorescence Generally inert. Yellow stones Inert 463 475
Terri Weimer/GIA
263
GEM IDENTIFICATION LAB MANUAL
KORNERUPINE
KORNERUPINE ENSTATITE
SR/DR/AGG DR DR
Spectrum Bands at 446 nm and 503 nm, faint Lines at 505 nm along with a
lines at 430 nm, 463 nm, and 540 nm band at 550 nm. Might show
gradual cutoff below 470 nm.
Comments Key tests are RI, birefringence, optic Key tests are RI, birefrin-
character, pleochroism, and possibly gence, optic character, and
spectrum and fluorescence. spectrum.
ENSTATITE
Prism
Diffraction
Terri Weimer/GIA
264
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
YELLOW SPODUMENE
SPODUMENE ANDALUSITE
Prism
General observation Normally light-toned yellow Yellowish green to brownish green
or greenish yellow. Vitreous and orangy brown. Due to strong
polish luster, uneven to splin- pleochroism, both green and orangy
tery fracture with vitreous pleochroic colors might be visible
fracture luster. Perfect cleavage through the crown. Vitreous polish
Diffraction
in two directions at nearly 90° luster, uneven to conchoidal fracture
angles to one another. with vitreous fracture luster.
Distinct cleavage in one direction.
RI 1.660 to 1.676 (+/-0.005) 1.634 to 1.643 (+/-0.005) Yellow spodumene’s spectrum shows lines at
433 nm and 438 nm.
Birefringence/doubling 0.014 to 0.016 0.007 to 0.013 (tends to be higher
when RI values are low)
SR/DR/AGG DR DR
Magnification Growth tubes and liquid Needles (probably rutile) and Eric Welch/GIA
inclusions crystals (probably apatite) Andalusite is one of the few gems with
eye-visible pleochroism.
Spectrum Look for lines near 433 nm Not diagnostic, but might show
and 438 nm in the blue area. clusters of fine lines around 485 nm
to 518 nm and around 550 nm.
Comments Key tests are RI and birefrin- Key tests are RI, birefringence,
gence. optic character, and pleochroism.
265
GEM IDENTIFICATION LAB MANUAL
YELLOW APATITE
APATITE DANBURITE
Spectrum Sets of fine lines at 520 nm Some stones might show a doublet
and 580 nm at 580 nm
Comments Key tests are RI, birefringence, Key tests are RI, birefringence,
optic character, and spectrum. optic character, and possibly SG.
Apatite’s low numerical RI is
generally higher than the low
numerical RI of tourmaline.
266
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
General observation Brown, yellowish brown, yellow Yellow to orange and brown. Might show eye- Transparent to translucent.
to pinkish yellow to pinkish visible pleochroism. Vitreous polish luster, Yellowish green to greenish
orange to orange. Vitreous polish conchoidal fracture with vitreous fracture luster. yellow and colorless (rare).
luster, conchoidal fracture with Vitreous polish luster, conchoidal
vitreous fracture luster. Perfect fracture with vitreous fracture
basal cleavage, possibly with luster. Perfect cleavage in one
iridescent cleavage planes. The direction.
color of some reddish orange
topaz results from treatment with
a surface coating.
Birefringence/doubling 0.008 to 0.010 Usually 0.018 to 0.020, but dark stones might 0.019 to 0.021
range up to 0.040
SR/DR/AGG DR DR DR
Optic character Biaxial positive (common point is Uniaxial negative Biaxial positive
0.001 from the low RI)
Pleochroism Generally weak Medium to strong, usually two tones of gem’s Weak, in tones of bodycolor
bodycolor
Magnification Two- and three-phase inclusions, Thread-like liquid and gas inclusions (trichites), Natural inclusions
liquid inclusions in planes. mirror-like gas-filled fractures, color zoning
Surface treatment results in spotty
color. Chips on facet junctions
might reveal colorless material
underneath.
Comments Key tests are RI, birefringence, Key tests are almost always RI and birefringence. Key tests are RI, birefringence,
and optic character. SG is helpful If birefringence isn’t obtainable, uniaxial optic and optic character. Brazilianite’s
if you can’t obtain birefringence. figure, pleochroism, and SG can be helpful. low numerical RI is always lower
Magnification is a key identifier Tourmaline’s low numerical RI is generally lower than tourmaline’s low numerical
of surface-treated topaz. than the low numerical RI of apatite and always RI.
higher than the low numerical RI of brazilianite.
267
GEM IDENTIFICATION LAB MANUAL
General observation Light toned, weakly to Greenish yellow to orangy Yellow, orange, brown, or red-brown, usually light in
moderately saturated, yellow. Vitreous polish luster, tone. Oregon material (rare) can range from pale yellow
slightly greenish yellow to conchoidal fracture with through orange, pinkish orange, and pink to deep red.
orangy yellow. Vitreous vitreous to resinous fracture Bicolor gems exist, but are extremely rare. Vitreous
polish luster, conchoidal luster. polish luster, uneven to splintery fracture with vitreous
fracture with vitreous to to pearly fracture luster. Two cleavage directions.
resinous fracture luster. Parting also common. The sunstone variety is typically
yellow to orange or brown and has a reddish or golden
sheen from highly reflective inclusions.
RI 1.577 to 1.583 (+/-0.017); 1.577 to 1.583 (+/-0.017) 1.559 to 1.568 (+/-0.005); Oregon material commonly
heliodor typically falls 1.563 to 1.572
toward the lower end of this
range
SR/DR/AGG DR DR DR
Optic character Uniaxial negative Uniaxial negative Biaxial positive (often shows twinning in the polariscope)
Pleochroism Weak. Greenish yellow Weak to moderate, different Yellow stones might show colorless and light yellow
and yellow, or two tones tones of bodycolor dichroism
of yellow.
Magnification Liquid, two-phase, or tubu- Undulating growth, chevron Repeated twinning, black needle-like inclusions, and
lar inclusions. growth zoning. Liquid and metallic appearing platelets (possibly hematite). Oregon
two-phase inclusions might material contains tiny orangy yellow copper platelets,
also be present. often visible even in facet-grade material at 10X.
Fluorescence Generally inert Inert Generally inert, but might be weak, patchy white under
both LW and SW
SG 2.72 (+0.18/-0.05) 2.72 (+0.18/-0.05) 2.70 (+/-0.05); Oregon material typically 2.67 to 2.72
Comments Key tests are RI, birefrin- The key test for separating Key tests are RI, birefringence, optic character, and
gence, and optic character. synthetic from natural beryl is magnification. Labradorite from Oregon is commonly
Magnification is the key test magnification. called sunstone whether or not it displays aventures-
for separating natural from cence.
synthetic beryl.
Maha Tannous/GIA
The light-toned hue of this Flat, reflective inclusions cause the
yellow beryl is typical. aventurescence in this sunstone.
268
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
General observation Yellow to colorless. Vitreous Pale yellow through strong yellow to Bicolored combination of amethyst and
polish luster, conchoidal yellowish orange, reddish orange and citrine colors. Vitreous polish luster,
fracture with vitreous fracture reddish brown. Dark-toned reddish conchoidal fracture with vitreous fracture
luster. Two cleavage directions. brown and brown colors of low luster.
saturation are smoky quartz. Vitreous
polish luster, conchoidal fracture
with vitreous fracture luster.
Typical cutting style Faceted Faceted gems or cabochons Faceted (often rectangular step cut)
RI 1.550 to 1.564 1.544 to 1.553 (very constant) 1.544 to 1.553 (very constant)
(+0.015/-0.014)
SR/DR/AGG DR DR DR
Optic character Uniaxial negative Uniaxial positive. Might show a Uniaxial positive. Might show a bull’s-eye
bull’s-eye or Airy’s spiral optic or Airy’s spiral optic figure and Brazil-law
figure and Brazil-law twinning twinning under crossed polarizing filters.
under crossed polarizing filters.
Pleochroism Weak to moderate in yellow Very weak, with different tones of Very weak, with different tones of yellow or
stones, with different tones of bodycolor orange in yellow areas, weak to moderate
yellow purple and reddish purple in purple areas
Magnification Not diagnostic Color zoning, twinning, liquid, two- Color zoning, twinning, liquid, two-phase
phase and three-phase inclusions, and three-phase inclusions, and negative
and negative crystals crystals
Comments Key tests are RI, birefringence, Key tests are RI, birefringence, optic Key tests are appearance, RI, birefringence,
optic character, and possibly character, and optic figure. Presence optic character, and optic figure.
fluorescence. of Brazil-law twinning separates
citrine from scapolite with similar
properties.
269
GEM IDENTIFICATION LAB MANUAL
General observation Most properties same as natural Most properties same as natural
Magnification Often inclusion-free, but might contain Often inclusion-free, but might contain
characteristics of hydrothermal growth characteristics of hydrothermal growth
like breadcrumb inclusions, two-phase like breadcrumb inclusions, two-phase
(liquid and gas) spicule inclusions (liquid and gas) spicule inclusions
Robert Weldon/GIA perpendicular to a seed plate, color perpendicular to a seed plate, color
Synthetic quartz can be banding parallel to a seed plate, and banding parallel to a seed plate, and
manufactured in a yellow flame-like twinning (rather than Brazil- flame-like twinning (rather than Brazil-
citrine color. law twinning). law twinning).
Comments Most synthetic quartz is virtually Most synthetic quartz is virtually inclusion-
inclusion-free. Some material might be free. Some material might be grown on
grown on twinned seed crystals, resulting twinned seed crystals, resulting in Brazil-
in Brazil-law twinning like natural law twinning like natural material. It
material. It might be impossible to might be impossible to distinguish between
distinguish between these synthetics and these synthetics and natural gems using
natural gems using conventional gem- conventional gem-testing equipment.
Taijin Lu/GIA testing equipment. Advanced laboratory Advanced laboratory testing can separate
You might see two-phase testing can separate hydrothermal hydrothermal synthetic quartz from natural
inclusions in a synthetic synthetic quartz from natural quartz. quartz.
ametrine.
270
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Typical cutting style Beads, cabochons, tumbled pieces Beads, cabochons, tumbled pieces
Alan Jobbins
RI 1.540 (+0.005/-0.001) 1.540 (-0.010) Treated amber often
contains disk-like “sun
Birefringence/doubling None None spangle” inclusions.
SR/DR/AGG SR, commonly with strong ADR (strain SR, commonly with strong ADR
colors common)
Magnification Gas bubbles, flow lines, insects and other Surface crazing common
organic and inorganic inclusions. Plastic
imitations with insect inclusions often
show a boundary layer or “zone of
encapsulation,” where an insect was
inserted, then had fresh plastic poured
over it. Treated material (heated with oil) Maha Tannous/GIA
shows disk-like fractures known in the This 306.72-ct. copal is an
trade as “sun spangles.” amorphous organic material
that’s actually immature amber.
Fluorescence Variable. Inert to strong yellowish green Inert to bluish white under LW, inert The two gem materials share
to orangy yellow, white, bluish white, or to strong bluish white under SW. many properties, but copal
blue under LW, weaker under SW. Whiter than amber’s reaction, espe- reacts strongly to acetone
cially under SW. while amber does not.
Comments Key test is SG. Amber generally floats in Use fluorescence and possibly SG to
saturated salt solution (SG 1.13), while separate copal resin from amber.
plastic (SG 1.30 +/-0.25) normally sinks. Another test—which is destructive—
uses acetone, which attacks copal
within two or three seconds. Amber
is either unaffected, or only slightly
affected, in the same period of time.
Copal is fossilized resin of more
recent origin than amber.
271
GEM IDENTIFICATION LAB MANUAL
ORTHOCLASE CALCITE
General observation Orange, yellow, and brown. Vitreous Occurs in almost all colors. Vitreous to
polish luster, uneven to splintery greasy polish luster. Three cleavage
fracture with vitreous to pearly fracture directions. Strong eye-visible doubling.
luster. Might show adularescence or
aventurescence.
Tino Hammid/GIA
RI 1.518 to 1.526 (+0.010) 1.486 to 1.658
Orthoclase feldspar can occur
in lovely yellow hues.
Birefringence/doubling 0.005 to 0.008 0.172 (use birefringence blink method)
SR/DR/AGG DR DR
Spectrum Yellow orthoclase shows broad bands at Not diagnostic. Any visible lines are
approximately 420 nm and 448 nm caused by impurities or dye.
Comments Key tests are RI, birefringence, optic Key tests are cleavage, RI, birefringence
character, and possibly spectrum and blink, doubling, SG, and possibly
fluorescence. appearance.
272
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Typical cutting style Faceted gems, cabochons, or freeforms Faceted gems, cabochons, carvings, or Eric Welch/GIA
beads
Natural fire opal comes in a
range of red and orangy red
RI 1.450 (+0.020/-0.080). Fire opal might 1.434 (+/-0.001) hues.
read as low as 1.37, but generally gives a
reading between 1.42 and 1.43.
Comments Key tests are RI, SR/ADR nature, and Key tests are RI, SG, and possibly
possibly magnification, which can cleavage.
separate natural from synthetic with
play-of-color. Red or orangy red stone
sold as fire opal in the trade and some-
times called Mexican opal. SG can help
separate opal from plastic (SG 1.05 to
1.55). Some natural opal is polymer-
impregnated to make it more stable or
improve its appearance.
273
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC OPAL
274
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
GLASS PLASTIC
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a
molded to a variety of shapes variety of shapes and finishes.
and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Comments Key tests are RI and magnifica- Key tests are RI and magnification.
tion. Low thermal conductivity Low heft (SG) and low thermal
(warm to the touch) might also conductivity (warm to the touch)
be helpful. might also be helpful.
275
GEM IDENTIFICATION LAB MANUAL
Diamond from zircon and sphene Diamond tester, doubling, pleochroism, spectrum, SG
Diamond from spessartite and andradite Diamond tester, spectrum, SG, possibly fluorescence
Sapphire from lattice diffusion treated Usually advanced laboratory testing. Also magnification
sapphire with immersion.
Kornerupine from enstatite Color, optic sign, pleochroism, spectrum, and possibly
optic figure
276
SEPARATING TRANSPARENT ORANGE, YELLOW, AND BROWN GEMS
Quartz from orthoclase and labradorite RI, optic character, optic figure
Orthoclase and labradorite from opal RI, birefringence, optic character, possibly play-of-
color and spectrum
277
GEM IDENTIFICATION LAB MANUAL
1.63 to 1.64 spot reading Chiastolite (andalusite) Idocrase, jadeite, nephrite, chalcedony
AGG (Page 282)
1.535 to 1.539 Chalcedony Jadeite, chiastolite, serpentine, golden coral, horn, tiger’s-eye
(1.53 or 1.54 spot reading) (Page 288) quartz, talc, amber, oligoclase, shell, orthoclase, calcite, opal
AGG
1.470 to 1.700 range Glass Any orange, yellow, or brown translucent-to-opaque gem material
SR (Page 295)
1.460 to 1.700 range Plastic Any orange, yellow, or brown translucent-to-opaque gem material
SR (Page 295)
279
GEM IDENTIFICATION LAB MANUAL
Translucent-to-opaque Orange, Yellow, and Brown Gems with RIs below 1.50
RI and SR/DR/AGG Gem Material Commonly confused with:
1.486 to 1.658 Calcite (including onyx marble) Jadeite, chalcedony, obsidian, opal
AGG (Page 293)
1.470 to 1.700 range Glass Any orange, yellow, or brown translucent-to-opaque gem
SR (Page 295) material
1.460 to 1.700 range Plastic Any orange, yellow, or brown translucent-to-opaque gem
SR (Page 295) material
280
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
PYRITE IDOCRASE
uneven fracture with metallic vitreous polish luster, conchoidal to This faceted pyrite displays its
fracture luster. uneven or granular fracture with metallic luster.
dull to vitreous fracture luster.
Typical cutting style Faceted into small rose cuts Carvings, beads, cabochons, tablets
Prism
SG 5.00 (+/-0.10) 3.40 (+0.10/-0.15)
464
Comments Key tests are appearance Key tests are RI, magnification, SG,
(color, metallic luster) and SG. and possibly spectrum.
Often sold as marcasite in the Diffraction
trade.
464
281
GEM IDENTIFICATION LAB MANUAL
JADEITE
JADEITE CHIASTOLITE
Comments Key tests are appearance, RI, Key tests are appearance, RI, and
spectrum, and SG. Might be SG.
heat-treated, polymer impreg-
nated, or dyed.
Maha Tannous/GIA
282
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
General observation Light to dark yellow to brown, Semitranslucent to opaque, with a distinctive Semitransparent to opaque. Usually
possibly with lighter or darker surface sheen. Color can be natural or result yellowish green, green, or greenish
mottling. Vitreous to greasy from bleaching of black or dark coral, yellow, brown or black. Waxy to greasy
polish luster, splintery to gran- resulting in dark brown to yellow material. polish luster, granular to uneven fracture
ular fracture with dull fracture Waxy to vitreous polish luster, conchoidal with dull to waxy fracture luster. Might
luster. to uneven fracture with dull fracture luster. show scratches and pits due to low
hardness (Mohs 2.5 to 6).
Typical cutting style Carvings, beads, cabochons Beads, cabochons Ornamental carvings, beads, cabochons
RI 1.606 to 1.632 (+0.009/-0.006) 1.560 to 1.570 (+/-0.010) 1.560 to 1.570 (+0.004/-0.070) (might
(1.61 spot reading common) be hard to obtain due to poor polish)
Magnification Not diagnostic Concentric, circular, tree-ring growth Translucent material might show tiny
structure. White crescents in cross-sections black inclusions (chromite or magnetite
of the branches. octahedra), white veining, or moss-like
inclusions.
Comments Key tests are appearance, RI, Key tests are appearance, RI, and Key tests are RI, magnification, and
and SG. magnification. possibly appearance and surface
condition.
Tree-ring growth structure is typical of naturally Black coral can be bleached to give it a Serpentine comes in a wide range of colors,
colored golden coral. It’s often eye-visible. “golden coral” appearance. including greenish yellow.
283
GEM IDENTIFICATION LAB MANUAL
General observation Semitransparent to opaque. Semitransparent to semitranslucent. Semitranslucent to opaque. Brownish yellow
Yellow to brown to almost Mottled yellow and brown, occasionally to brown to reddish brown, typically with
black. Resinous to vitreous black and white. Resinous to waxy wavy chatoyancy. Vitreous polish luster,
polish luster, uneven to polish luster, uneven to splintery splintery fracture with vitreous to silky
splintery fracture with resinous fracture with dull fracture luster. fracture luster. Eye might be visible even on
to dull fracture luster. flat surfaces.
Typical cutting style Carvings, inlays, decorative Carved objects, inlays Carvings, beads, cabochons, tablets, signets,
objects tumbled gems
Magnification Undulating, fibrous structure Characteristic mottling made up of Wavy, fibrous structure is usually distinctive.
numerous spherical particles (not seen
in plastic imitations)
Comments Key tests are appearance, RI, Key tests are appearance, RI, and Key tests are appearance (structure and
and magnification. magnification. chatoyancy) and RI. Might be heat-treated to
a reddish brown color or dyed to any color.
Horn is often used in carvings. It can have Tortoise shell is semitransparent to semitranslu- The rich color of tiger’s-eye quartz can be (left
yellow to brown or gray to black color and cent, with resinous to waxy polish luster. Its to right) natural, dyed, or heat treated.
resinous to vitreous polish luster. characteristic mottling is composed of numer-
ous spherical particles.
284
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
TALC AMBER
General observation White, gray, brown, light to Transparent to opaque. Light yellow to dark brown,
dark green, often veined or orange, red, or white. Occasionally greenish or
mottled. Waxy to greasy polish bluish due to strong fluorescence. Waxy to resinous
luster, uneven fracture with polish luster, conchoidal fracture with waxy to
dull to waxy fracture luster. resinous fracture luster.
Might show surface damage
due to very low hardness
(Mohs 1). Can often be
scratched with a fingernail.
Typical cutting style Ornamental carvings, decora- Beads, cabochons, tumbled pieces
tive objects
Magnification Not diagnostic Gas bubbles, flow lines, insects and other organic
and inorganic inclusions. Plastic imitations with
insect inclusions often show a boundary layer or
“zone of encapsulation,” where an insect was
inserted, then had fresh plastic poured over it.
Treated material (heated with oil) shows disk-like
fractures known in the trade as “sun spangles.”
Fluorescence Inert to weak pink under LW Variable. Inert to strong yellowish green to orangy
yellow, white, bluish white, or blue under LW,
weaker under SW.
Comments Key tests are poor quality of Key test is SG. Amber generally floats in
polished surface, RI, and SG. saturated salt solution (SG 1.13), while plastic
Also known in the trade as (SG 1.30 +/-0.25) normally sinks. A material called
steatite or, more commonly, ambroid or pressed amber results when small pieces
“soapstone.” of amber are consolidated under heat or pressure.
285
GEM IDENTIFICATION LAB MANUAL
General observation Transparent to translucent. Yellow, Opaque white to light yellow, but Opaque white to light yellow, but might
orange, or brown. Resinous to might be dyed almost any color. be dyed almost any color. Low hardness
vitreous polish luster, conchoidal to Low hardness (Mohs 2.5). (Mohs 2.5).
uneven fracture with resinous
fracture luster.
Typical cutting style Beads, cabochons, tumbled pieces Beads, cabochons, bangle bracelets, Beads, cabochons, bangle bracelets,
carvings carvings
Magnification Surface crazing common Remains of blood vessels appear Parallel, torpedo-shaped cells that appear
round or oval in cross-section and round in cross-section.
might also appear as dark spots on
the surface if they’ve been penetrated
by dirt.
Fluorescence Inert to bluish white under LW, Not diagnostic Not diagnostic
inert to strong bluish white under
SW. Whiter than amber’s reaction,
especially under SW.
Comments Use fluorescence and possibly SG Key test to separate bone from ivory Key test is magnification. Vegetable ivory
to separate copal resin from amber. is magnification. is derived from the seeds of certain palm
Another test—which is destructive— trees, and might also be called tagua nut
uses acetone, which attacks copal or corozo nut.
within two or three seconds. Amber
is either unaffected, or only slightly
affected, in the same period of time.
Copal is fossilized resin of more
recent origin than amber.
This 306.72-ct. copal is an amorphous organic Vegetable ivory is derived from the
material that’s actually immature amber. The seeds of certain palm trees. It’s often
two gem materials share many properties, but carved into animal shapes.
copal reacts strongly to acetone while amber
does not.
286
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
OLIGOCLASE IVORY
General observation Semitransparent to opaque yellow to orange or Translucent to opaque white to light yellow. Greasy to dull
brown, with a reddish or golden sheen from highly polish luster, splintery fracture with dull fracture luster.
reflective inclusions. Called sunstone if inclusions
are large enough to create distinct, glittery reflections.
Vitreous polish luster, uneven to splintery fracture
with vitreous to pearly fracture luster. Two cleavage
directions. Parting also common.
Magnification Reddish to golden metallic platelets, probably Wavy structure lines and “engine turning” are characteristic of
hematite elephant and mammoth ivory. These features distinguish this
material from the tusks of other mammals, bone imitations,
white coral, and “vegetable ivory” substitutes.
Fluorescence Generally inert Weak to strong bluish white or violet-blue under both LW and
SW (stronger under LW)
Comments Key tests are appearance, RI, birefringence, optic Key tests are RI, magnification, and SG. Fluorescence might
character, and magnification. also be helpful. Vegetable ivory also has a lower SG of around
1.40. “Ivory” traditionally refers to elephant tusk, although the
tusks or teeth of other mammals, including walrus, narwhal and
sperm whale, warthog, and hippopotamus, are also used for
carvings or jewelry objects.
Aventurescence is a key feature of This ivory napkin ring shows its distinctive
oligoclase sunstone feldspar. “engine turning” growth pattern.
287
GEM IDENTIFICATION LAB MANUAL
CHALCEDONY
SG 2.60 (+0.10/-0.05)
Comments Key tests are spot RI, SG, and possibly appearance and fracture.
288
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
PEARL
Species Pearl
General observation Might be almost any bodycolor, but usually white or light yellow,
and bodycolor might be modified by pink, green, or blue overtone.
Surface luster varies from dull to nearly metallic, depending on nacre
quality. Uneven fracture with dull to pearly fracture luster.
RI 1.530 to 1.685
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW.
SG Saltwater—2.61 to 2.85
Freshwater—2.66 to 2.78 (few are over 2.74)
Comments Key tests are RI, birefringence blink, and SG. Feels gritty when
rubbed against a tooth, while plastic and glass imitations feel smooth.
Heft can separate natural pearl from plastic imitations. X-radiography
separates natural from cultured pearl. Drill-hole might interfere with
accurate SG reading.
289
GEM IDENTIFICATION LAB MANUAL
CULTURED PEARL
General observation Colors same as natural (see descriptions below). Surface luster varies
from dull to nearly metallic, depending on nacre quality. Uneven
fracture with dull to pearly fracture luster.
Magnification Not usually diagnostic, unless you can examine a drill-hole and detect
the bead under the nacre.
South Sea cultured pearls come in a range of Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
creamy and yellowish colors. and SW. Naturally colored black pearls show weak to moderate red to
orangy red or brownish red under LW.
SG 2.72 to 2.78
Comments Key tests are RI, birefringence blink, magnification, and SG. Feels
gritty when rubbed against a tooth, while plastic and glass imitations
feel smooth. Heft can separate cultured pearl from plastic imitations.
X-radiography separates cultured from natural pearl. Cultured pearls
might be dyed, irradiated, or polymer-impregnated. Dye might be
detectable as concentrations in nacre, especially at the drill-hole.
Some irradiated colors are very intense and unnatural. Impregnation
might be visible with magnification. Drill-hole might interfere with
accurate SG reading.
290
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
General observation Pink, orange, yellow, and brown. Dull to Virtually any color, but usually white,
vitreous polish luster, uneven fracture with gray, brown, yellow, orange, or pink
dull fracture luster. Tridacna pearls have with layered or patterned coloring.
a yellowish to whitish, porcelain-like Might also show orient (mother-of-
appearance. pearl). Helmet shells, which are
commonly used for cameos, show Tino Hammid/GIA
layering in two colors, commonly These calcareous concretions
white and brown or white and orange. were produced by the melo
Shell cameos usually show concave melo sea snail.
backs due to the curved contours of the
shells they’re cut from. Greasy or
pearly polish luster, uneven to splintery
fracture with dull fracture luster.
Typical cutting style Baroque, oval, off-round Cameos, carvings, beads, cabochons,
inlays
Birefringence/doubling 0.155 (use birefringence blink method) 0.155 (use birefringence blink method) Flame structure is a distinctive
feature of conch “pearls.”
SR/DR/AGG AGG AGG
Comments Key tests are appearance, RI, birefringence Key tests are RI, birefringence blink, Shell’s layers make it
blink, and magnification (structure). These and magnification. Appearance might ideal for carving into
attractive cameos.
are basically non-nacreous concretions from also be helpful.
various mollusks, including conch and melo
melo snails and the giant clam (Tridacna).
291
GEM IDENTIFICATION LAB MANUAL
AMMONITE ORTHOCLASE
General observation Opaque gray to brown. Jewelry- Semitransparent to opaque, typically colorless
quality material displays iridescent to white, but can be orange, yellow, or brown.
Maha Tannous/GIA colors. Well-preserved specimens Adularescent, sometimes with chatoyancy,
Ammonite has an opaque show a spiral structure. Vitreous asterism, or aventurescence. Vitreous polish
gray to brown bodycolor and polish luster, uneven to granular luster, uneven to splintery fracture with
iridescent coloring. It might be fracture with greasy to dull fracture vitreous to pearly fracture luster. Two cleavage
sold whole to collectors or luster. directions. Parting also common.
as pieces to be inlayed into
other materials for jewelry or Typical cutting style Cabochons, freeforms, tablets. Also Cabochons, beads
ornamental objects. used in doublets and triplets.
This orthoclase moonstone Magnification Distinctive, often iridescent, mosaic Centipede-like inclusions. Material with aven-
has the added feature of a patterns turescence or asterism might contain reflective
four-rayed star.
inclusions such as fine needles or elongated
hematite flakes.
Fluorescence Variable, not diagnostic Generally inert to blue under LW, orange
under SW. Might fluoresce weak pink to red
under LW and SW.
Comments Key tests are appearance (including Key tests are appearance, phenomenon
iridescence) and possibly RI. (if present), and RI. Magnification and
Ammonite is the fossilized shell fluorescence might also be helpful.
of an extinct nautilus-like animal.
It’s often polymer-impregnated to
make it more stable or improve its
appearance. Might be sold as
“ammolite” in the trade.
292
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
OBSIDIAN CALCITE
Spectrum Not diagnostic Not diagnostic. Any visible lines are caused
by impurities or dye.
Comments Key tests are RI, SG, and Key tests are RI, birefringence blink, SG, and
possibly magnification. possibly appearance. Marble is a granular
aggregate, onyx marble is a banded marble.
Satinspar is a fibrous aggregate that’s often
chatoyant (the name is also used for a similar
variety of gypsum).
293
GEM IDENTIFICATION LAB MANUAL
General observation Yellow to brown. Vitreous to resinous polish luster, con- Semitransparent to semitranslucent orange to orangy red,
choidal to uneven fracture with subvitreous to waxy fracture yellow, and light to dark brown with play-of-color. Material
luster. Might show play-of-color. In some natural opals, with vivid bodycolor might be polymer impregnated. Con-
dehydration causes a network of fine cracks called crazing. choidal to uneven fracture with subvitreous fracture luster.
SR/DR/AGG SR, commonly with ADR due to strain SR with weak to moderate ADR
Magnification Possible play-of-color patterns include very small patches Play-of-color in a mosaic pattern across the surface, with a
or dots (pinfire); large areas that flash predominately one cellular, “chicken wire,” “snakeskin,” or scale-like structure
color as the gem is moved (flash); or even, distinct patches that’s visible with magnification and overhead or backlight-
with a “brush-stroke” appearance (harlequin). There might ing. Might show columnar structure when viewed from the
also be areas that lack play-of-color or that contain mineral side.
inclusions or patches of rock matrix. (Play-of-color in
synthetic opal tends to be much more regular.)
Fluorescence Inert to strong green or yellowish green under LW and Polymer-impregnated synthetics range from weak pink to
SW. Might phosphoresce. moderate pink-orange or weak yellow under LW and weak
to moderate pink-orange or moderate to strong orangy
yellow under SW. Newer untreated orange synthetics might
show very weak red under both LW and SW, with a slightly
stronger reaction to SW. Phosphorescence is rare and weak
if present.
SG 2.15 (+0.08/-0.90) 1.97 to 2.20 (typically lower than natural opal). Polymer-
impregnated synthetic opal is usually considerably lower
than natural opal, at 1.88 to 1.91. Newer untreated orange
synthetic opal is closer to natural opal, at 2.22 to 2.27.
Comments Key test is RI. Lack of surface structure and absence of bire- Magnification is the key to separating synthetic from
fringence blink distinguish non-phenomenal opal from shell natural opal. Fluorescence and phosphorescence might also
or coral. SG can help separate opal from plastic (SG 1.05 to be helpful. Synthetic opal is often polymer impregnated to
1.55). Some natural opal is polymer impregnated to make it make it more stable, and it has a considerably lower SG
more stable or improve its appearance. Magnification than most natural opal.
separates natural opal from synthetic opal with play-of-color.
294
SEPARATING TRANSLUCENT-TO-OPAQUE ORANGE, YELLOW, AND BROWN GEMS
GLASS PLASTIC
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Magnification Gas bubbles, cavities on sur- Gas bubbles, flow lines. Copper foil
face where gas bubbles were inclusions produce aventurescence
polished through, flow marks in goldstone plastic.
(swirls). Triangular or hexago-
nal copper inclusions produce
aventurescence in goldstone
glass.
SG Usually between 2.30 and 4.50 1.05 to 1.55 (goldstone plastic can
be higher)
Comments Key tests are RI and magni- Key tests are RI and magnification.
fication. Low thermal Low heft (SG) and low thermal
conductivity (warm to the conductivity (warm to the touch)
touch) might also be helpful. might also be helpful.
295
GEM IDENTIFICATION LAB MANUAL
Jadeite from soapstone (talc) Quality of surface polish, RI, jadeite spectrum
296
SEPARATING COLORLESS AND WHITE GEMS
There are few visual clues to the identities of transparent colorless gems, so you often have to rely on your testing skills to
identify them. This group includes quartz, topaz, corundum, zircon, CZ, and synthetic spinel.
COLORLESS GEMS
Transparent colorless gems are divided into two identification categories: those
that are over the limits (OTL) of the refractometer and those that yield readable
RIs. There are three main OTL gems: diamond, synthetic cubic zirconia (CZ), and
synthetic moissanite. Older diamond simulants like synthetic rutile, GGG, and
YAG aren’t readily available in today’s market, but you might see them in older
pieces. Zircon, like diamond, is a natural colorless OTL gem.
The most common colorless materials with RIs that fall within the refractometer’s
range are natural and synthetic sapphire, synthetic spinel, topaz, rock crystal
quartz, and manmade glass. Rarer colorless gems like euclase, enstatite, calcite,
and fluorite are occasionally cut for collectors.
297
GEM IDENTIFICATION LAB MANUAL
2.648 to 2.691 Synthetic moissanite Synthetic rutile, diamond, synthetic diamond, strontium titanate, CZ,
DR (Page 301) GGG, zircon, YAG
2.616 to 2.903 Synthetic rutile Synthetic moissanite, diamond, synthetic diamond, strontium titanate,
DR (Page 301) CZ, GGG, zircon, YAG
2.417 Synthetic diamond Synthetic moissanite, synthetic rutile, diamond, strontium titanate, CZ,
SR (Page 305) GGG, zircon, YAG
2.409 Strontium titanate Synthetic moissanite, synthetic rutile, diamond, synthetic diamond, CZ,
SR (Page 307) GGG, zircon, YAG
2.150 CZ (synthetic cubic zirconia) Synthetic moissanite, synthetic rutile, diamond, synthetic diamond,
SR (Page 307) strontium titanate, GGG, zircon, YAG
1.970 GGG (gadolinium gallium garnet) Synthetic moissanite, synthetic rutile, diamond, synthetic diamond,
SR (Page 307) strontium titanate, CZ, zircon, YAG
1.925 to 1.984 Zircon Synthetic moissanite, synthetic rutile, diamond, synthetic diamond,
1.810 to 1.815 (Page 308) strontium titanate, CZ, GGG, YAG
DR
1.833 YAG (yttrium aluminum garnet) Synthetic moissanite, synthetic rutile, diamond, synthetic diamond,
SR (Page 308) strontium titanate, CZ, GGG, zircon
298
SEPARATING COLORLESS GEMS
1.550 to 1.564 Scapolite Beryl, labradorite, quartz, synthetic quartz, oligoclase, orthoclase
DR (Page 313)
1.544 to 1.553 Quartz Beryl, labradorite, scapolite, synthetic quartz, oligoclase, orthoclase
DR (Page 314)
1.544 to 1.553 Synthetic quartz Beryl, labradorite, scapolite, quartz, oligoclase, orthoclase
DR (Page 315)
299
GEM IDENTIFICATION LAB MANUAL
300
SEPARATING COLORLESS GEMS
General observation Near-colorless to light yellow, green, or Almost always tinted slightly yellow or
gray, possibly with greenish tint. Shows slightly grayish blue. Extreme eye-visible
much more fire than a diamond of equiv- doubling, much more fire than a diamond
alent size and cut. Positive reaction to a of equivalent size and cut. Subadamantine
standard diamond tester. Always look for to submetallic polish luster, conchoidal
doubling, which is readily visible when to uneven fracture with subadamantine Shane Elen/GIA
you examine the stone through the crown fracture luster. Facet edges frequently dull
Synthetic moissanite shows
or pavilion facets (necessary because stone and abraded due to low hardness (Mohs 6
strong doubling through the
is often cut with optic axis perpendicular to 6.5). Well-proportioned round brilliants crown or pavilion facets.
to the table facet). show no see-through. Negative reaction to
diamond tester.
RI OTL OTL
Magnification Whitish or reflective needles, channels, Generally inclusion free, but might
negative crystals contain gas bubbles
Spectrum Not diagnostic, but a cutoff below 425 nm Not diagnostic. Cutoff possible around
allows separation from diamonds that 430 nm.
show the “cape” line at 415.5 nm
Comments Key tests are extreme fire, OTL RI Key tests are high luster, extreme fire, Eric Welch/GIA
reading, and strong doubling. Presence OTL RI reading, and eye-visible doubling. A faceted synthetic rutile
of greenish bodycolor tint might also be Yellow-tinted bodycolor and poor polish shows extreme fire.
helpful. Synthetic moissanite is a man- are also helpful.
made material with no gem-quality
natural counterpart.
301
GEM IDENTIFICATION LAB MANUAL
NEAR-COLORLESS DIAMOND
DIAMOND
Species Diamond
Prism
General observation Colorless to pale yellow, brown, green or gray. Under 10X, look for
naturals, waxy to granular (bruted) or faceted girdle surface, bearding,
415 sharp facet junctions. Adamantine polish luster, step-like fracture.
Perfect cleavage in four directions. Polish lines never oriented the
same way on adjacent facets. Positive reaction to diamond tester.
Diffraction
415
Dispersion 0.044 (moderate fire)
RI OTL
Some near-colorless diamonds show the
“cape” line in the violet at 415.5 nm, along with Birefringence/doubling None
weaker lines at 435 nm, 451 nm, 463 nm, and
478 nm. SR/DR/AGG SR
Spectrum Most near-colorless to light yellow stones show the “cape” line at
415.5 nm, along with weaker lines at 435 nm, 451 nm, 463 nm,
and 478 nm. (Cooling diamond with liquid nitrogen helps make its
spectrum more visible.)
Fluorescence Commonly inert or weak to strong blue, but might fluoresce any
Eric Welch/GIA
color under LW and SW. LW response is generally stronger than or
A well-polished diamond always has sharp equal to SW. Occasional phosphorescence of 30 seconds or less.
facet junctions.
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, OTL RI, SR nature, magnification, positive
reaction to diamond tester, and possibly spectrum. Magnification
separates untreated natural diamond from laser-drilled diamond and
fracture-filled diamond. Magnification, fluorescence, and possibly
spectrum separate natural diamond from synthetic diamond, although
advanced testing might be required.
302
SEPARATING COLORLESS GEMS
Species Diamond
General observation Same as natural. A small difference between the RI of the glass and
the RI of the diamond can produce color flashes when you view the
gem under magnification.
RI OTL
Birefringence/doubling None
SR/DR/AGG SR
To detect filled fractures, look for the flash effect. Start with reflected
light and look for a surface-reaching fracture. When you find one,
switch to darkfield and examine the fracture as it extends into the
stone’s interior. Then rock the stone under magnification. If a filling
is present, you’ll see the flash effect: one color when the background
is dark and another color when it’s light. Sometimes, you’ll see both
colors in the same position.
Also look for laser drill-holes that don’t end at a bleached inclusion
and examine them for evidence of fillers.
303
GEM IDENTIFICATION LAB MANUAL
General observation Same as natural. Treaters use lasers to reach Treatment using high pressure high
dark included crystals within a diamond. The temperature (HPHT) techniques can
laser drill-hole can reach the inclusion from sometimes produce colorless or
the surface or be completely internal (internal near-colorless diamonds.
laser drilling). Treaters often introduce acid
through a drill-hole or surface-reaching fracture
and bleach the inclusion or fill it with a glassy
material, making it less visible.
RI OTL OTL
SR/DR/AGG SR SR
Magnification Looks like a tiny round opening at the Etched or pitted naturals or feathers,
diamond’s surface. Under magnification, you tension fractures—often containing
might see a channel extending from a bleached graphite—around crystalline inclu-
white inclusion to the diamond’s surface. sions. Some surface areas might
show etching and pitting if not
Laser drill-holes are usually perpendicular to completely repolished. (see photos,
the facet where they enter the stone. Channels page 306)
might extend only a short way into the gem or
a longer distance, depending on the treated
inclusion’s relationship to the stone’s surface.
304
SEPARATING COLORLESS GEMS
General observation Colorless to near-colorless. Might appear very light Grown by chemical vapor deposition (CVD) rather than
blue, gray, or green due to faint internal growth zoning conventional HPHT techniques. Near-colorless, faint to
caused by impurities. Might be attracted to a magnet dark brown or gray, or might even be light to dark blue due
due to inclusions of metallic flux. Virtually all synthetic to impurities. Brownish material can be treated to colorless.
diamonds are grown by conventional high pressure Fashioned gems are typically shallow because they’re cut
high temperature (HPHT) techniques. from tabular crystals. Might be grown on a conventional
synthetic diamond or natural diamond seed, so fashioned
gems might include portions of either one.
RI OTL OTL
Magnification Elongated or rounded opaque inclusions of metallic Often inclusion free. Lower-quality material might contain
flux, often occurring as pinpoints and small groups of pinpoints and brown graining along with small, black,
larger grains. Impurities might cause occasional very irregularly shaped inclusions that might be graphite. If a
faint color zoning in a cross-shaped or hourglass- portion of the seed material is present, the fashioned gem
shaped pattern. (see photos, page 306) might contain flux inclusions typical of HPHT diamond.
Fluorescence Often unevenly distributed and related to internal Inert or weak orange to yellow-orange to LW,
growth structures, showing squares or octagons plus a weak to moderate orange to yellow-orange to SW.
cross-shaped pattern. Usually inert to LW. Weak to No phosphorescence.
moderate green, yellow, blue, or orange under SW.
SW reaction is typically stronger than LW. (Natural
diamonds generally react more strongly to LW or have
equal reactions to both LW and SW.) Commonly
phosphoresce weak to moderate blue, yellow, or green,
often for 60 seconds or longer.
Comments Key tests for high-pressure synthetics are magnification Very rare, produced only experimentally at time of writing.
and fluorescence patterns. If in doubt, submit diamond CVD synthetic diamonds require laboratory testing.
to a gemological laboratory for advanced testing.
Elizabeth Schrader/GIA
305
GEM IDENTIFICATION LAB MANUAL
INCLUSION PHOTOGRAPHS
Natural, untreated diamond: Natural, untreated diamond: Girdle with Natural, untreated diamond: Natural Natural, untreated diamond: Bearded
Dark inclusion with radiating naturals. with trigon. girdle.
circular cleavage.
Natural, untreated diamond: Natural, untreated diamond: Cloud of Natural, untreated diamond: Internal Fracture-filled diamond: Flattened gas
Well-formed mineral crystal pinpoints. graining. bubbles.
inclusion.
Fracture-filled diamond: Purple Fracture-filled diamond: Yellow flash Fracture-filled diamond: Bluish green Fracture-filled diamond: Pink-to-purple
flash effect against a light effect against a dark background. to greenish yellow flash effect against flash effect against a dark background.
background. a light background.
Fracture-filled diamond: Laser-drilled diamond: Drill-hole Laser-drilled diamond: Short laser drill- Internal laser-drilled diamond: Step-like
Crackled texture. reaching dark inclusion. hole. cleavages leading to an inclusion.
HPHT-treated diamond: HPHT-treated diamond: Inclusion High-pressure synthetic diamond: High-pressure synthetic diamond:
Cleavage that looks glassy surrounded by graphite, with radiating Metal flux inclusion. Elongated metal flux inclusion.
inside and frosted or grainy stress fractures.
near the surface.
306
SEPARATING COLORLESS GEMS
Species Strontium titanate CZ (synthetic cubic zirconia) GGG (gadolinium gallium garnet)
General observation Shows much more fire than Subadamantine polish luster, Usually colorless to light brown or yellow. Vitreous
a diamond of equivalent conchoidal fracture with sub- to subadamantine polish luster, conchoidal fracture
size and cut. Vitreous polish adamantine fracture luster. Heft with vitreous to subadamantine fracture luster.
luster with conchoidal reveals that loose stones are much Well-proportioned round brilliants might show
fracture. Well-proportioned heavier than diamonds of similar moderate see-through. Heft reveals that loose stones
round brilliants show no size. Well-proportioned round are much heavier than diamonds of similar size
see-through. Shows poor brilliants might show only slight and proportions (A 6-mm round brilliant GGG
polish due to low hardness see-through. Negative reaction to weighs about twice as much as an equivalent-size
(Mohs 5 to 6). Negative diamond tester. diamond). Negative reaction to diamond tester.
reaction to diamond tester.
Dispersion 0.190 (extreme fire) 0.060 (strong fire) 0.045 (moderate fire)
SR/DR/AGG SR SR SR
Magnification Small gas bubbles, polishing Generally inclusion free, but might Might show gas bubbles. Well-proportioned round
marks on surface contain unmelted zirconium oxide brilliants might show an orange and blue pavilion
and gas bubbles. Well-proportioned flash over most facets.
round brilliants might show an orange
pavilion flash over most facets.
Fluorescence Generally inert Greenish yellow to yellow-orange Inert to moderate orange under LW, moderate to
under LW, yellow or greenish strong pinkish orange under SW
yellow under SW
Comments Key tests are poor surface Key tests are negative reaction to Key tests are negative reaction to diamond tester,
polish, extreme fire, OTL diamond tester, OTL RI reading, OTL RI reading, moderate fire, lack of doubling,
RI reading, and lack of strong fire, lack of doubling, SG, fluorescence, SG, and orange and blue pavilion
doubling. Loose stones fracture, and orange pavilion flash flash in round brilliant cuts. GGG is a manmade
have noticeably greater heft in round brilliants. CZ is a manmade material with no natural counterpart.
than diamonds of similar material with no gem-quality natural
size and proportions. counterpart.
Strontium titanate is a
manmade material with no
natural counterpart.
Strontium titanate’s A round brilliant CZ often shows A round brilliant GGG shows an
extreme fire is visible even an orange flash when you view it orange and blue pavilion flash when
in an emerald-cut stone. from the pavilion and rock it back you view it from the pavilion and rock
and forth in darkfield lighting. it back and forth in darkfield lighting.
307
GEM IDENTIFICATION LAB MANUAL
ZIRCON
ZIRCON YAG
SR/DR/AGG DR SR
Comments Key tests are OTL RI reading, Key tests are negative reaction to
strong doubling, and spectrum. diamond tester, OTL RI reading,
lack of doubling, SG, and violet to
blue pavilion flash in round bril-
liants. Fluorescence might also be
helpful. YAG is a manmade material
with no natural counterpart.
308
SEPARATING COLORLESS GEMS
General observation Vitreous to subadamantine polish luster, conchoidal Might show poor polish, with polishing marks on most facets
fracture with vitreous fracture luster. due to rapid polishing.
Typical cutting style Faceted Faceted, often symmetrical and cut to precise calibrated sizes.
Often cut in brilliant style, including scissors cut.
SR/DR/AGG DR DR
Magnification Untreated natural corundum—Unaltered mineral Single gas bubbles or strings of gas bubbles that might resemble
inclusions (high- or low-relief crystals) that might needles. Twinning planes possible, but very rare or difficult to
show angular faces; intact, fine, needle-like rutile observe. When present, they’re usually formed by rapid cooling
inclusions intersecting at 60° angles in the same plane; of the boule. These are known as Plato lines. They’re best seen
other fine needles at near right angles; fingerprint with magnification, polarized light, and immersion. The stone
inclusions, intact two-phase inclusions, straight and also has to be viewed parallel to its optic axis. The twinning then
hexagonal growth banding; straight, angular, possibly appears as sets of lines that intersect at 60° or 120° angles.
hexagonal color banding; and twinning planes
Heat-treated natural corundum—Altered, burned
mineral inclusions with rounded, often whitish,
“snowball” or “cotton” appearance; broken silk
(partially reabsorbed rutile needles), ruptured two-
phase inclusions and negative crystals; sintered surface
areas, especially around the girdle; fine needles at
near right angles. Discoid fractures with tension halos
(disk-like fractures with lace-like outer healing rims,
caused by expansion of inclusions) are also indicative
of heat treatment, but these features might also occur
in some untreated corundum of magmatic origin.
Fluorescence Inert to moderate red to orange under LW and SW Inert to weak bluish white
Comments Key tests for separating natural corundum from The key test for separating synthetic from natural
other colorless natural gems are RI, birefringence, corundum is magnification. Fluorescence might also be helpful.
and magnification. Magnification is the key test for
separating natural from synthetic corundum.
Fluorescence might also be helpful.
Robert Weldon
309
GEM IDENTIFICATION LAB MANUAL
General observation Vitreous polish luster, con- Vitreous to subadamantine polish luster, Very rarely transparent and colorless.
choidal to uneven fracture conchoidal fracture with vitreous fracture Vitreous polish luster, uneven fracture
with greasy to vitreous luster. with vitreous to pearly fracture luster.
fracture luster. Distinct cleavage in two directions.
Magnification Might contain mineral inclu- Might contain gas bubbles (might be Natural inclusions
sions thread-like or, rarely, angular)
Comments Key tests are RI, SR nature, Key tests are RI, SR nature, polariscope Key tests are RI, birefringence, and
and SG. Magnification can reaction, magnification, and fluorescence. optic character.
often be helpful. There’s a translucent flame-fusion synthetic
spinel that imitates moonstone. It’s easily
separated by its much higher RI and SG.
310
SEPARATING COLORLESS GEMS
General observation Vitreous polish luster, Near-colorless stones some- Vitreous polish luster, Transparent to translucent.
uneven to splintery times display blue-green color conchoidal to uneven frac- Vitreous to greasy polish
fracture with vitreous zones. Vitreous polish luster, ture with vitreous fracture luster, uneven to subcon-
fracture luster. Perfect conchoidal fracture with luster. Surface might show choidal fracture with
cleavage in two directions vitreous fracture luster. Perfect abrasions due to low vitreous to greasy fracture
at nearly 90° angles to cleavage in one direction, hardness (Mohs 5). luster.
one another. with pearly luster on cleavage
surfaces.
RI 1.660 to 1.676 (+/-0.005) 1.652 to 1.671 (+0.006/-0.002) 1.634 to 1.638 1.630 to 1.636 (+/-0.003)
(+0.012/-0.006)
SR/DR/AGG DR DR DR DR
Optic character Biaxial positive Biaxial positive Uniaxial negative (distorted Biaxial positive or negative
(common point is 0.006 optic figure possible) (common point almost
from the high RI) halfway between low and
high RI)
Magnification Growth tubes and liquid Natural inclusions (red or Natural inclusions Natural inclusions
inclusions. blue plate-like inclusions are
common)
Spectrum Not diagnostic Two vague bands at 468 nm Not diagnostic in colorless Some stones might show a
and 455 nm stones doublet at 580 nm.
Fluorescence Inert Inert to weak Variable, not diagnostic Inert or strong light blue to
blue-green under LW,
weaker reaction to SW
Comments Key tests are RI, birefrin- Key tests are RI, birefringence, Key tests are RI, birefrin- Key tests are RI, birefrin-
gence, and optic character. and optic character. gence, and optic character. gence, optic character, and
Magnification can some- possibly SG.
times be helpful.
Detection of birefringence
blink separates colorless
spodumene from calcite.
311
GEM IDENTIFICATION LAB MANUAL
TOURMALINE TOPAZ
General observation Very rarely transparent and Vitreous polish luster, conchoidal
colorless. Vitreous polish fracture with vitreous fracture
luster, conchoidal fracture luster. Basal cleavage, possibly
with vitreous fracture luster. with iridescent cleavage planes.
Eric Welch/GIA
Typical cutting style Faceted Faceted
RI, birefringence, and optic
character identify topaz and RI 1.624 to 1.644 1.619 to 1.627 (+/-0.010);
separate it from diamond and (+0.011/-0.009) colorless material typically 1.609
other colorless gems. to 1.617
SR/DR/AGG DR DR
Natural topaz typically contains two-phase Spectrum Not diagnostic Not diagnostic
inclusions.
Fluorescence Generally inert Inert to weak yellow or green under
LW, generally weaker under SW
Comments Key tests are almost always Key tests are RI, birefringence, and
RI and birefringence. If bire- optic character. SG is helpful if you
fringence isn’t obtainable, can’t obtain birefringence.
uniaxial optic figure and SG
can be helpful.
312
SEPARATING COLORLESS GEMS
General observation Vitreous polish luster, con- Vitreous polish luster, uneven to splintery Vitreous polish luster, conchoidal
choidal fracture with vitreous fracture with vitreous to pearly fracture luster. fracture with vitreous fracture luster.
to resinous fracture luster. Might show adularescence. Two cleavage Two cleavage directions.
directions. Might show abrasions due to
relatively low hardness (Mohs 6 to 6.5).
SR/DR/AGG DR DR DR
Optic character Uniaxial negative Biaxial positive. Transparent material often Uniaxial negative
shows twinning in the polariscope.
Magnification Liquid, two-phase, or tubular Repeated twinning, black needle-like Not diagnostic
inclusions inclusions, metallic-looking platelets
Fluorescence Generally inert Inert to weak patchy white under LW and Inert to strong pink, orange, or yellow
SW
Comments Key tests are RI, birefringence, Key tests are RI, birefringence, optic Key tests are RI, birefringence, optic
and optic character. character, and magnification. Adularescent character, and sometimes fluorescence.
labradorite often sold as “rainbow moon- Scapolite’s RI is as high as beryl’s and
stone” in the trade. labradorite’s, but it has much higher
birefringence than either gem.
Goshenite’s RI, This nearly transparent Feldspar displays a series of Labradorite often shows black
birefringence, and labradorite shows a blue very thin, parallel plates needle-like inclusions under
DR nature identify it sheen, and is sometimes caused by twinning within its magnification.
as beryl. called “rainbow moonstone.” structure.
313
GEM IDENTIFICATION LAB MANUAL
QUARTZ
Species Quartz
Robert Weldon/GIA
General observation Vitreous polish luster, conchoidal fracture with vitreous fracture
If needles are numerous enough luster. The inclusions in sagenitic quartz are typically randomly
and well oriented, cat’s-eye oriented and might be rutile (often golden), tourmaline (usually
quartz results.
black), or actinolite. Quartz that contains a sufficient quantity of
oriented needle-like inclusions might display a cat’s-eye.
Birefringence/doubling 0.009
Clayton Welch/GIA
SR/DR/AGG DR
This sagenitic quartz contains
eye-visible needles of black
tourmaline. Optic character Uniaxial positive. Might show a bull’s-eye or Airy’s spiral optic
figure and Brazil-law twinning under crossed polarizing filters.
SG 2.66 (+0.03/-0.02)
Comments Key tests are RI, birefringence, optic character, and optic figure.
Iris or rainbow quartz is rock crystal that contains many iridescent
fractures. It might be produced by quench-crackling. There are many
Eric Welch/GIA
trade names for transparent quartz with distinctive inclusions.
Rainbow or iris quartz has
visible iridescence due to
numerous fractures.
314
SEPARATING COLORLESS GEMS
General observation Vitreous polish luster, conchoidal fracture with Usually translucent to opaque,
vitreous fracture luster. rarely transparent. Vitreous polish Maha Tannous/GIA
luster, uneven to splintery fracture Oligoclase sometimes
with vitreous to pearly fracture contains iridescent orange
luster. Two cleavage directions, inclusions.
parting also common.
Magnification Often inclusion free, but might contain character- Parallel, closely spaced twinning
istics indicating hydrothermal growth, such as planes. Transparent material might
breadcrumb inclusions and two-phase (liquid and contain eye-visible iridescent
gas) spicule inclusions perpendicular to a seed orange platelets.
plate.
Comments Synthetic quartz is virtually inclusion free and Key tests are appearance, RI,
might be difficult to distinguish from natural birefringence, and possibly optic
material. However, it’s unlikely for synthetic character.
colorless quartz to be grown on twinned seed
crystals, so the presence of Brazil-law twinning
indicates natural. Advanced laboratory testing
can often separate hydrothermal synthetic quartz
from natural quartz.
315
GEM IDENTIFICATION LAB MANUAL
ORTHOCLASE CALCITE
General observation Transparent to opaque, but rarely color- Vitreous to greasy polish luster. Three
less and transparent. Might be very pale cleavage directions. Strong, eye-visible
Terri Weimer/GIA yellow. Vitreous polish luster, uneven to doubling.
Moonstone displays a biaxial splintery fracture with vitreous to pearly
optic figure in the polariscope. fracture luster. Two possible cleavage
directions. Might show adularescence
(see page 424 for moonstone orthoclase
feldspar).
Typical cutting style Faceted Often sold as cleavage pieces, but trans-
parent material is occasionally faceted for
collectors.
316
SEPARATING COLORLESS GEMS
Typical cutting style Cabochons, carvings, freeforms; some- Cabochons, carvings, beads
times faceted
SR/DR/AGG SR, commonly with ADR due to strain SR with weak to moderate ADR
Fluorescence Inert to white to moderate light blue, Typically moderate bluish white to yellow
green or yellow under LW and SW. Might under LW, weak to strong blue to bluish
also phosphoresce. white to yellow under SW. Newer untreated
(not polymer-impregnated) synthetic opal
is very weak to weak chalky blue under
both LW and SW, with a slightly stronger
reaction under SW. Phosphorescence is
rare and weak if present.
Comments Key tests are RI, lack of doubling, and Magnification is the key to separating
possibly magnification. Some natural synthetic from natural opal. Fluorescence
opal is polymer impregnated to make it and phosphorescence might also be help-
more stable or improve its appearance. ful. Synthetic opal is often polymer
In the trade, slightly milky opal that impregnated to make it more stable, and it
shows play-of-color in transmitted and has a considerably lower SG than most
reflected light is called “contra luz.” natural opal.
Magnification is the key test for separating
natural from synthetic opal.
317
GEM IDENTIFICATION LAB MANUAL
General observation Transparent to translucent. Transparent to opaque, almost any appearance Transparent to opaque, almost any
Might be parti-colored. possible. Look for mold marks, orange-peel appearance possible. Look for mold
Vitreous to subvitreous luster, effect, concave facets, and rounded facet marks, orange peel effect, concave
conchoidal to step-like junctions. Warm to the touch compared to facets, and rounded facet junctions.
fracture with vitreous to sub- crystalline gemstones. Vitreous polish luster, Warmer to the touch than glass imita-
vitreous fracture luster. Perfect conchoidal fracture with vitreous fracture tions and crystalline gemstones. Low
octahedral cleavage in four luster. heft (SG), dull to waxy polish luster,
directions. Might have conchoidal fracture with waxy to
numerous pits and scratches vitreous fracture luster. Surface might
due to low hardness (Mohs 4). show numerous scratches due to low
hardness (Mohs 1.5 to 3).
Typical cutting style Faceted gems, cabochons, All styles. Can be faceted or molded to a All styles. Can be molded to a variety
carvings, or beads variety of shapes and finishes. of shapes and finishes.
Dispersion No visible fire Up to 0.041 (high-lead glass might have No visible fire
moderate fire)
RI 1.434 (+/-0.001) Usually between 1.470 and 1.700, but can 1.460 to 1.700
go to OTL
SR/DR/AGG SR SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Magnification Triangular (tetrahedral) nega- Gas bubbles, cavities on surface where gas Gas bubbles, flow lines
tive crystals and two-phase bubbles were polished through, flow marks
inclusions, liquid inclusions, (swirls)
strong color zoning
Fluorescence Variable, not diagnostic Variable, not diagnostic Variable, not diagnostic
Comments Key tests are RI, SG, and Key tests are RI and magnification. Low Key tests are RI and magnification.
possibly cleavage. thermal conductivity (warm to the touch) Low heft (SG) and low thermal con-
might also be helpful. ductivity (warm to the touch) might
also be helpful.
Eric Welch/GIA
318
SEPARATING COLORLESS GEMS
Diamond from synthetic diamond Magnification, fluorescence, possibly phosphorescence; advanced testing
often necessary
Diamond from CZ, strontium titanate, GGG, and YAG Appearance, luster, sharpness of facet junctions, girdle surface if unpolished,
magnification, SG, possibly spectrum
YAG from strontium titanate Fire, fluorescence, SG, possibly pavilion flash
GGG from strontium titanate Fire, fluorescence, SG, possibly pavilion flash
Zircon from synthetic rutile Fire, magnification, spectrum, possibly rutile’s bodycolor
Zircon and synthetic rutile from SR diamond simulants Doubling, magnification, zircon spectrum
Rock crystal quartz from orthoclase feldspar RI, birefringence, optic character, optic figure
Rock crystal quartz from calcite (Iceland spar) RI, birefringence blink, cleavage
Rock crystal quartz and orthoclase feldspar from glass Birefringence, optic character, optic figure, magnification, possibly RI
and plastic
Fluorite from glass Magnification and possibly SG (glass with an RI in fluorite’s range
typically has an SG of around 2.30)
319
GEM IDENTIFICATION LAB MANUAL
WHITE GEMS
By far, the most popular and commonly seen
white gems in the marketplace are cultured
pearls and opals. Natural pearls, which are
much rarer, are also prized.
Besides pearl, you’ll see other organic
materials like mother-of-pearl and coral.
You might even find elephant ivory in older
jewelry that predates bans on hunting. Pearl
and ivory are widely imitated by various
glasses and plastics, so always consider
these as possibilities.
Another thing to consider is that many gem
materials that occur in colors can also be
white. These include jadeite, nephrite, chal-
cedony, and feldspar.
Elizabeth Schrader/GIA
White Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
1.666 to 1.680 (1.66 spot reading) Jadeite Idocrase, nephrite, serpentine, talc
AGG (Page 322)
1.606 to 1.632 (1.61 spot reading) Nephrite Idocrase, jadeite, serpentine, talc
AGG (Page 323)
1.586 to 1.605 (1.59 spot reading) Howlite Serpentine, ivory, talc, alabaster, magnesite
AGG (Page 323)
1.559 to 1.568 (1.56 spot reading) Labradorite feldspar Oligoclase, orthoclase moonstone
DR or AGG (Page 324)
1.540 to 1.590 (1.54 spot reading) Talc (soapstone) Jadeite, nephrite, howlite, serpentine, alabaster
AGG (Page 324)
320
SEPARATING WHITE GEMS
1.535 to 1.540 (1.54 spot reading) Ivory Howlite, bone, vegetable ivory, alabaster, coral, calcite, plastic
AGG (Page 326)
1.535 to 1.539 (1.53 or 1.54 spot reading) Chalcedony Serpentine, horn, oligoclase, shell, moonstone, coral, calcite
AGG (Page 327)
1.530 to 1.685 Cultured pearl CZ, natural pearl, shell, glass, plastic
Usually too opaque to test (Page 329)
1.530 to 1.685 Shell (including mother-of-pearl) CZ, chalcedony, natural pearl, cultured pearl, coral, glass, plastic
AGG (Page 330)
1.520 to 1.529 (1.52 or 1.53 spot reading) Alabaster Howlite, serpentine, talc, ivory
AGG (Page 330)
1.518 to 1.526 (1.52 or 1.53 spot reading) Orthoclase feldspar (moonstone) Labradorite feldspar, oligoclase, chalcedony
DR or AGG (Page 331)
321
GEM IDENTIFICATION LAB MANUAL
CZ IDOCRASE JADEITE
General observation Translucent, uniform milky or bluish Transparent to opaque white to Semitransparent to opaque. White,
white in reflected light. Faintly banded gray. Vitreous to greasy polish often uneven, with mottling or root-
or striped appearance in strong transmit- luster, conchoidal to uneven or like markings. Vitreous to greasy
ted light. Subadamantine polish luster, granular fracture with vitreous to polish luster with a dimpled polished
conchoidal fracture with subadamantine dull fracture luster. surface, granular to splintery fracture
fracture luster. Negative reaction to with dull fracture luster.
diamond tester.
Typical cutting style Faceted gems, beads, cabochons, tablets Carvings, beads, cabochons, Carvings, beads, cabochons, tablets
tablets
Magnification Not diagnostic Not diagnostic Unevenly colored, often with root-like
mottling
Spectrum Not diagnostic Line at 464 nm, weak line at Generally a line at 437.5 nm
528.5 nm
Fluorescence Inert to LW, very weak light pink under Inert Inert to weak yellow under LW,
SW generally inert to SW
Comments Key tests are OTL RI reading, SG, Key tests are RI, spectrum, SG, Key tests are appearance, RI, spectrum,
appearance in transmitted light, and and possibly appearance. and SG. “Ice jade” can be nearly color-
possibly fluorescence. Might be sold as less. Jadeite might be heat-treated,
“pearl” CZ in the trade. polymer impregnated, or dyed.
JADEITE
Prism
437.5
Diffraction
437.5
Small quantities of white or “pearl” CZ Ice jade is an attractive jadeite that can be The spectrum of non-chrome jadeite generally shows a key
are manufactured for use as imitations. nearly colorless. line at 437.5 nm due to iron.
322
SEPARATING WHITE GEMS
General observation Translucent to opaque white, Semitranslucent to opaque white, Semitransparent to opaque, usually yellowish
possibly with lighter or darker often with dark gray or black matrix. green, green, or greenish yellow, white,
mottling. Vitreous to greasy Vitreous polish luster, granular brown, or black. Waxy to greasy polish
polish luster, splintery to granular fracture with dull fracture luster. luster, granular to uneven fracture with dull
fracture with dull fracture luster. to waxy fracture luster. Might show scratches
and pits due to low hardness (Mohs 2.5 to 6).
Typical cutting style Carvings, beads, cabochons Cabochons, beads Ornamental carvings, beads, cabochons
RI 1.606 to 1.632 (+0.009/-0.006) 1.586 to 1.605 (+/-0.003) (1.59 spot 1.560 to 1.570 (+0.004/-0.070) (might be
(1.61 spot reading common) reading) hard to obtain due to poor polish)
Birefringence/doubling Usually not detectable 0.019 (usually not detectable) Usually not detectable
Magnification Not diagnostic Might show spiderweb matrix Translucent material might show tiny black
octahedral inclusions, white veining, or
moss-like inclusions.
Comments Key tests are appearance, RI, and Key tests are appearance, RI, SW Key tests are RI, magnification, and possibly
SG. fluorescence, and SG. appearance and surface condition.
Eric Welch/GIA
323
GEM IDENTIFICATION LAB MANUAL
General observation Semitransparent to opaque, Adularescent, with strong blue or multicolor Semitranslucent to opaque white, gray,
white to gray to almost sheen against almost transparent, semitrans- brown, and light to dark green, often
black. Resinous to vitreous parent, or semitranslucent body. Vitreous polish veined or mottled. Waxy to greasy
polish luster, uneven to luster, uneven to splintery fracture with vitreous polish luster, uneven fracture with dull
splintery fracture with to pearly fracture luster. Two cleavage directions. to waxy fracture luster. Might show
resinous to dull fracture Parting also common. surface damage due to very low hard-
luster. ness (Mohs 1). Can often be scratched
with a fingernail.
RI 1.560 1.559 to 1.568 (1.56 spot reading common) 1.540 to 1.590 (+0.010/-0.002) (1.54
spot reading common)
Magnification Undulating, fibrous structure Polysynthetic twinning, tiny colorless inclusions Not diagnostic
Fluorescence Variable Moderate chalky blue under LW, weak pinkish Inert to weak pink under LW
orange under SW
Comments Key tests are appearance, Key tests are appearance, fracture, RI, Key tests are appearance, poor surface
RI, and magnification. fluorescence, and possibly birefringence. quality, RI, and SG. Also known in the
Adularescent examples often sold as “rainbow trade as steatite or, more commonly,
moonstone” in the trade. “soapstone.”
Rainbow moonstone labradorite has an The rainbow iridescence in some feldspar is Talc, or soapstone, is soft enough to be scratched with
attractive blue or multicolored adu- caused by light reflecting off tightly spaced a fingernail.
larescent sheen. twinning planes.
324
SEPARATING WHITE GEMS
General observation Opaque white to light yellow, but Opaque white to light yellow, but Usually translucent to opaque, rarely trans-
might be dyed almost any color. might be dyed almost any color. parent. Vitreous polish luster, uneven to
Low hardness (Mohs 2.5). Low hardness (Mohs 2.5). splintery fracture with vitreous to pearly
fracture luster. Two cleavage directions,
parting also common.
Typical cutting style Beads, cabochons, bangle Beads, cabochons, bangle bracelets, Cabochons, beads
bracelets, carvings carvings
Magnification Remains of blood vessels appear Parallel, torpedo-shaped cells that Parallel, closely spaced twinning planes.
round or oval in cross-section and appear round in cross-section. Transparent material might contain eye-
might also appear as dark spots visible iridescent orange platelets.
on the surface if they’ve been
penetrated by dirt.
Comments Key test to separate bone from Key test is magnification. Vegetable Key tests are appearance, RI, and possibly
ivory is magnification. ivory is derived from the seeds of birefringence and optic character.
certain palm trees, and might also be
called tagua nut or corozo nut.
Terri Weimer/GIA
Eric Welch/GIA
This decorative piece of bone This decorative scene is carved from vegetable ivory, also called
was carved to portray ocean tagua nut.
waves.
325
GEM IDENTIFICATION LAB MANUAL
IVORY
Species Ivory
General observation Translucent to opaque white to light yellow. Greasy to dull polish
luster, splintery fracture with dull fracture luster.
SR/DR/AGG AGG
Birefringence/doubling None
Eric Welch/GIA
Magnification Wavy structure lines and “engine-turning” are characteristic of
You can see the engine-turning surface
elephant and mammoth ivory. These features distinguish this
texture in this mammoth ivory carving.
material from the tusks of other mammals, bone imitations, white
coral, and vegetable ivory substitutes.
SG 1.70 to 2.00
Comments Key tests are RI, magnification, and SG. Fluorescence might also
Eric Welch/GIA
be helpful. “Ivory” traditionally refers to elephant tusk (from both
This cross-section through a mammoth prehistoric mammoths and modern-day elephants), although the
ivory tusk shows its engine-turning
tusks or teeth of other mammals, including walrus, narwhal and
pattern.
sperm whale, wart-hog, and hippopotamus, are also used for carvings
or jewelry objects.
326
SEPARATING WHITE GEMS
CHALCEDONY
Species Chalcedony
Typical cutting style Cabochons, carvings, beads. Some moss and dendritic agate might
be transparent enough to facet. Tino Hammid/GIA
SR/DR/AGG AGG
SG 2.60
Comments Key tests are RI and SG. Fracture and appearance might also be
helpful. Material sold in the trade as “milky” chalcedony is semi-
transparent to translucent, white or nearly colorless.
Some chalcedony resembles Moss agate has dark- Dendritic agate has contrasting Agate is often tumbled to show off its
moonstone, but lacks true colored inclusions branch-like patterns. curved or angular bands or layers.
adularescence. It also gives an that look like clusters
AGG polariscope reaction. of moss.
327
GEM IDENTIFICATION LAB MANUAL
PEARL
Species Pearl
General observation Translucent to opaque. Might be almost any bodycolor, but usually
white or light yellow. Bodycolor might be modified by pink, green,
or blue overtone. Polish luster varies from dull to nearly metallic,
depending on nacre quality. Uneven fracture with pearly to dull
fracture luster.
RI 1.530 to 1.685
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW
SG Saltwater—2.61 to 2.85
Freshwater—2.66 to 2.78 (few are over 2.74)
Comments Key tests are appearance, RI, birefringence blink, and SG. Feels
gritty when rubbed against a tooth, while plastic and glass imitations
feel smooth. Heft can separate natural pearl from plastic imitations.
X-radiography separates natural from cultured pearl. Drill-hole
might interfere with accurate SG reading.
328
SEPARATING WHITE GEMS
CULTURED PEARL
General observation Colors same as natural (see descriptions below). Surface luster varies
from dull to nearly metallic, depending on nacre quality. Uneven
fracture with pearly to dull fracture luster.
Akoya (bead nucleated)—Typical size range 2 mm to 11 mm.
Mostly spherical, but might be button, pear, oval, or baroque in
shape. Color can range from neutral to near-neutral whites and
creams with rosé or green overtones, but can sometimes be yellow,
pink (sometimes dyed), or blue.
Tahitian (bead nucleated)—Typical size range 8 mm to 14 mm.
Spherical, oval, button, drop, or baroque in shape (sometimes circled).
Color can range from near-neutral silver, cream, or brown to black or
gray, to blue, green, yellowish green, or purple, with green, blue, or
rosé overtone.
South Sea (bead nucleated)—Typical size range 10 mm to 15 mm. You can see the bead nucleus
Spherical, near-round, oval, button, drop, or semi-baroque (some- and dark conchiolin layer
through the drill-hole in this
times circled). Color can range from near neutral white, cream, or cultured pearl.
silver to yellow, yellowish orange, or blue, with green, blue, or rosé
overtone.
Freshwater (usually tissue nucleated)—Typical size range 2 mm to
13 mm. Spherical, near-round, oval, button, drop, or heavily baroque
(sometimes circled). Color can range from neutral to near-neutral
whites, grays, and creams to yellows, pinks, and purples, with blue
or green overtone and orient.
RI 1.530 to 1.685
Magnification Not usually diagnostic, unless you can examine a drill-hole and detect
the bead under the nacre or the dark conchiolin layer between the
bead and the nacre. Occasionally, if the nacre layer is very thin, you
can detect the “blinking” of the layers in the bead nucleus as you roll
a strand of pearls across a flat surface. Dyes might be detectable at
drill-holes, or on silk strands close to drill-holes.
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW
SG 2.72 to 2.78
Comments Key tests are RI, birefringence blink, SG, and magnification. Feels
gritty when rubbed against a tooth, while plastic and glass imitations
feel smooth. Heft can separate cultured pearl from plastic imitations.
X-radiography separates cultured from natural pearl. Cultured pearls
might be dyed, irradiated, or polymer impregnated. Dye might be
detectable as concentrations in nacre, especially at the drill-hole.
Some irradiated colors are very intense and unnatural. Impregnation
might be visible with magnification. Drill-hole might interfere with
accurate SG reading.
329
GEM IDENTIFICATION LAB MANUAL
SHELL ALABASTER
Comments Key tests are appearance, Key tests are appearance, RI, and
RI, birefringence blink, and SG. Quality of polished surface
magnification. indicates low hardness.
330
SEPARATING WHITE GEMS
General observation Semitransparent to opaque, typically Typically white, often dyed. Can Semitranslucent to opaque white, creamy
colorless to white with blue or white also be gray, yellow, or brown. white, or very light pink. Waxy to vitreous
adularescence. Some stones show cha- Often shows gray veining like polish luster, splintery to uneven fracture
toyancy or asterism along with howlite. Vitreous polish luster, with dull fracture luster.
adularescence. Vitreous polish luster, granular to uneven fracture with
uneven to splintery fracture with vitre- dull fracture luster. (Mohs 3.5
ous to pearly fracture luster. Two to 5)
cleavage directions, parting common.
Typical cutting style Cabochons, carvings, beads Cabochons, carvings, beads Cabochons, carvings
Birefringence/doubling 0.005 to 0.008 0.191 (use birefringence blink 0.172 (use birefringence blink method)
method)
Optic character Biaxial negative. Might show repeated Not usually detectable Not applicable
twinning under crossed polarizing filters.
Magnification Centipede-like inclusions Not diagnostic Cavities from polyps, waxy fibrous
structure. Branch or tree-like form if not
carved or cabochon-cut.
Fluorescence Generally inert to blue under LW, Generally inert Inert to weak to strong bluish white under
orange under SW. Might fluoresce LW and SW
weak pink to red under LW and SW.
Comments Key tests are appearance, RI, and mag- Possible key tests are appearance, Key tests are appearance, RI, birefrin-
nification. Optic character, fluorescence, RI, and birefringence blink. gence blink, and magnification.
and SG might also be helpful. Birefringence blink separates dyed Fluorescence might also be helpful.
magnesite from dyed howlite.
This moonstone cabochon This moonstone contains characteristic White magnesite often has gray veining. This is the characteristic sur-
displays attractive white centipede inclusions. . face structure of unfashioned
adularescence. white coral.
331
GEM IDENTIFICATION LAB MANUAL
CALCITE OPAL
332
SEPARATING WHITE GEMS
SYNTHETIC OPAL
General observation Typically semitranslucent to opaque white or light bluish gray, with
play-of-color. Conchoidal to uneven fracture with subvitreous
fracture luster.
RI 1.430 to 1.470
John Koivula/GIA
333
GEM IDENTIFICATION LAB MANUAL
GLASS PLASTIC
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a
molded to a variety of shapes variety of shapes and finishes.
and finishes.
Terri Weimer/GIA Comments Key tests are RI and Key tests are RI and magnification.
This is a plastic imitation pearl. magnification. Low thermal Light heft (SG) and low thermal
Surface damage reveals the conductivity (warm to the conductivity (warm to the touch)
plastic bead underneath. touch) might also be helpful. might also be helpful.
334
SEPARATING WHITE GEMS
Natural from cultured pearl Magnification (structure visible at drill-hole), advanced testing,
possibly candling
Natural or cultured pearl from glass or Birefringence blink, magnification (structure), possibly RI
plastic
Moonstone from translucent white chal- Phenomenon, cleavage, fracture, polariscope reaction, possibly
cedony fluorescence
335
SEPARATING GRAY AND BLACK GEMS
Advanced laboratory testing would be required to identify these as the rare natural saltwater pearls they are.
GRAY GEMS
Not many transparent gems are characteristically gray, but some transparent gems
appear gray if their hues are low in saturation—pale blue, pink, or purple sapphires
are a few examples. If low cost is a goal, manufacturers might use grayish diamonds
or near-colorless grayish topaz in inexpensive jewelry.
Translucent-to-opaque gray gems include materials that also occur in other colors.
The most popular gem in this category is probably cultured pearl. Another popular
gray gem is the phenomenal variety of labradorite, named for the broad flash of
shifting color, or labradorescence, it displays. Others include jadeite, nephrite,
idocrase, and serpentine.
337
GEM IDENTIFICATION LAB MANUAL
Gray Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
1.666 to 1.680 (1.65 or 1.66 Jadeite Hydrogrossular, idocrase, sillimanite, nephrite, serpentine,
spot reading common) (Page 344) chalcedony
AGG
338
SEPARATING GRAY GEMS
1.535 to 1.539 (1.53 to 1.54 Chalcedony Jadeite, serpentine, horn, talc, shell, orthoclase, obsidian,
spot reading common) (Page 348) calcite
AGG
1.520 to 1.680 Ammonite Opal with play-of-color, synthetic opal, opal doublets and
AGG (Page 350) triplets
339
GEM IDENTIFICATION LAB MANUAL
General observation Opaque dark gray to black, might show Opaque dark gray to black with Opaque, with metallic yellow
reddish color on fracture surfaces. Metallic metallic luster and conchoidal “brassy” appearance in larger
polish luster and splintery, granular, or fracture. Can generally be picked pieces. Small rose cuts used in
subconchoidal fracture with dull fracture up by a magnet. Intaglio pattern jewelry might appear gray or
luster. Might be slightly magnetic. High SG usually lacks graver lines. black in reflected light. Metallic
gives loose stones considerable heft. Intaglio polish luster, conchoidal to
pattern usually exhibits graver lines. uneven fracture with metallic
fracture luster.
Typical cutting style Beads, tablets, signets, intaglios Beads, tablets, signets, intaglios Faceted into small rose cuts
Comments Key tests are appearance, fracture, and SG Key tests are appearance, fracture, Key tests are appearance (color,
(heft). and magnetism. metallic luster) and SG. Often
sold as marcasite in the trade.
Hematite has metallic luster Natural hematite often shows a The designs on imitation The marcasite used in jewelry
and high heft. The carving splintery fracture. It might also have hematite intaglios are usually is actually the mineral pyrite.
marks, called graver lines, brownish red discoloration on its frac- stamped rather than carved,
identify this intaglio as natural ture surfaces. so they lack graver lines.
hematite.
340
SEPARATING GRAY GEMS
Prism
General observation Light-toned, low-saturation grays. Transparent gray to bluish
Under 10X, look for naturals, waxy gray and brownish gray. Facet
to granular or faceted girdle edges might show chipping. 415.5
Diffraction
step-like fracture. Perfect cleavage fracture with vitreous to
in four directions. Polish lines never subadamantine fracture luster.
oriented the same way on adjacent Negative reaction to diamond
facets. Positive reaction to diamond tester. 415.5
tester.
Very light gray to near-colorless diamonds
Typical cutting style Faceted. Girdle often faceted or Faceted might show a “cape” line at 415.5 nm in their
polished. spectra. Cooling the diamond in liquid nitrogen
helps make its spectrum more visible.
Dispersion 0.044 (moderate fire—might be 0.038 (moderate fire—might
masked by bodycolor) be masked by bodycolor)
Prism
SR/DR/AGG SR (might show strain colors) DR
Diffraction
Magnification Angular mineral inclusions, Might be inclusion-free
fractures and cleavages, bearding, or contain natural crystal
naturals with trigons, parallel inclusions. Moderate to strong
growth marks, surface and internal doubling might be eye-visible
graining in larger stones. Always 653.5
Comments Key tests are polish luster, OTL RI, Key tests are OTL RI reading,
SR nature, magnification, positive doubling, and spectrum.
reaction to diamond tester, and
possibly spectrum.
341
GEM IDENTIFICATION LAB MANUAL
CORUNDUM
Species Corundum
General observation Transparent bluish gray to brownish gray. Many corundum hues also
appear grayish in low saturations. Vitreous to subadamantine polish
luster, conchoidal fracture with vitreous fracture luster.
SR/DR/AGG DR
SG 4.00 (+0.10/-0.05)
Comments Key tests for separating natural corundum from other similarly colored
natural gems are RI, birefringence, and magnification. Magnification is
the key test for separating natural from synthetic corundum.
342
SEPARATING GRAY GEMS
HYDROGROSSULAR GARNET
HYDROGROSSULAR SPINEL
Prism
Group Garnet Not required
Diffraction
show black inclusions. Often grayish “lavender” color.
mixed with idocrase. Vitreous Vitreous to subadamantine
polish luster, uneven, granular, or polish luster, conchoidal
460
splintery fracture with greasy to fracture with vitreous fracture
vitreous fracture luster. luster.
Hydrogrossular’s spectrum usually shows a
Typical cutting style Carvings, beads, cabochons, tablets Faceted gems or cabochons cutoff at 460 nm.
Comments Key tests are spot RI and possibly Key tests are RI, SR nature, Maha Tannous/GIA
spectrum and SG. Appearance is and magnification. A low-saturation grayish violet is one of spinel’s
also distinctive. Because hydro- many hues.
grossular is often mixed with
idocrase, it might be impossible to
separate the two species.
343
GEM IDENTIFICATION LAB MANUAL
General observation Transparent to opaque gray to grayish brown Semitransparent and translucent to Transparent. Low-saturation hues
to grayish green. Jadeite-like variety often opaque gray to black. Vitreous to appear grayish. Vitreous polish
mixed with hydrogrossular garnet. Greasy to greasy polish luster with a dimpled luster, uneven to splintery fracture
vitreous polish luster, conchoidal to uneven polished surface, granular to with vitreous fracture luster.
or granular fracture with dull to vitreous splintery fracture with dull fracture Perfect cleavage in two directions
fracture luster. luster. at nearly 90° angles to one another.
Typical cutting style Carvings, beads, cabochons, tablets Carvings, beads, cabochons Faceted
RI 1.713 to 1.718 (+0.003/-0.013) (1.70 or 1.71 1.666 to 1.680 (+/-0.008) (1.65 or 1.660 to 1.676 (+/-0.005)
spot reading common, but might be lower) 1.66 spot reading common)
Optic character Uniaxial in single-crystal material Not detectable Biaxial positive (common point
is 0.006 from the high RI)
Magnification Not diagnostic Unevenly colored, often with root- Growth tubes and liquid inclusions
like mottling
Spectrum Line at 464 nm, weak line at 528.5 nm Generally a line at 437.5 nm Not diagnostic
Comments Key tests are RI, appearance, magnification, Key tests are spot RI, spectrum, Key tests are RI and birefringence.
SG, and possibly spectrum. Because and SG. Might be heat-treated,
idocrase is often mixed with hydrogrossular, polymer impregnated, or dyed.
it might be impossible to separate the two
species.
IDOCRASE JADEITE
Prism
Prism
464 437.5
Diffraction
Diffraction
464 437.5
The spectrum of gray or grayish idocrase shows a key line at The spectrum of non-chrome jadeite shows a key line at
464 nm. 437.5 nm due to iron.
344
SEPARATING GRAY GEMS
General observation Translucent gray, green, or brown (also blue Transparent. Low-saturation hues Translucent to opaque light to
and violet). Usually fibrous, with chatoyancy. appear grayish. Vitreous polish dark gray, possibly with lighter
Vitreous to silky polish luster, uneven fracture luster, conchoidal fracture with or darker mottling. Vitreous to
with vitreous to silky fracture luster. Perfect vitreous fracture luster. Perfect greasy polish luster, splintery to
cleavage in one direction. basal cleavage, possibly with granular fracture with dull
iridescent cleavage planes. fracture luster.
RI 1.659 to 1.680 (+0.004/-0.006) 1.619 to 1.627 (+/-0.010); gray 1.606 to 1.632 (+0.009/-0.006)
stones typically 1.609 to 1.617 (1.61 spot reading common)
Optic character Not detectable Biaxial positive (common point is Not detectable
0.001 from the low RI)
Magnification Usually appears fibrous Two- and three-phase inclusions, Not diagnostic
liquid inclusions in planes
Spectrum Weak bands at 410 nm, 441 nm, and 462 nm Not diagnostic Usually not detectable
Comments Key tests are appearance, RI, birefringence Key tests are RI, birefringence, and Key tests are appearance, RI, and
(if detectable), SG, and possibly spectrum. optic character. SG is helpful if you SG.
Sometimes confused with jade. can’t obtain birefringence.
Shane McClure/GIA
345
GEM IDENTIFICATION LAB MANUAL
General observation Transparent. Low-satura- Semitransparent to opaque gray. Waxy to Semitransparent to opaque yellow to
tion hues appear grayish. greasy polish luster, granular to uneven brown to gray to almost black. Resinous to
Vitreous polish luster, fracture with dull to waxy fracture luster. vitreous polish luster, uneven to splintery
conchoidal fracture with Might show scratches and pits due to low fracture with resinous to dull fracture luster.
vitreous to resinous hardness (Mohs 2.5 to 6). Bowenite variety
fracture luster. is harder, takes a better polish, and is an
effective jade substitute.
Typical cutting style Faceted gems or cabochons Ornamental carvings, beads, cabochons Carvings, inlays, decorative objects
Magnification Liquid, two-phase, or Translucent material might show tiny Undulating, fibrous structure
tubular inclusions black inclusions (chromite octahedra),
white veining, or moss-like inclusions
Comments Key tests are RI, birefrin- Key tests are appearance, magnification, Key tests are appearance, RI, and
gence, and optic character. and possibly surface condition. magnification.
Eric Welch/GIA
346
SEPARATING GRAY GEMS
General observation Typically gray to nearly black with Transparent to translucent. Low- Semitranslucent to opaque white,
labradorescent colors (typically green, saturation hues appear grayish, gray, brown, or light to dark
gold, or blue) visible at certain viewing especially in amethyst. Numerous green, often veined or mottled.
angles. Vitreous polish luster, uneven to inclusions might give it a milky Waxy to greasy polish luster,
splintery fracture with vitreous to appearance. Vitreous polish luster, uneven fracture with dull to waxy
pearly fracture luster. Two cleavage conchoidal fracture with vitreous fracture luster. Might show surface
directions, parting also common. fracture luster. damage due to very low hardness
(Mohs 1). Can often be scratched
with a fingernail.
Typical cutting style Faceted gems, beads, cabochons, Faceted gems, cabochons, or beads. Ornamental carvings, decorative
carvings Translucent material might be carved. objects
RI 1.559 to 1.568 (+/-0.005) 1.544 to 1.553 (very constant) 1.540 to 1.590 (+0.010/-0.002)
(1.54 spot reading common)
Optic character Biaxial positive Uniaxial positive. Might show a bull’s- Not detectable
eye or Airy’s spiral optic figure and
Brazil-law twinning under crossed
polarizing filters.
Magnification Repeated twinning, black needle-like Liquid, two-phase, and three-phase Not diagnostic
inclusions, and metallic-looking inclusions, negative crystals, and solid
platelets mineral crystals or needles. If the inclu-
sions are numerous enough, they might
produce a cat’s-eye or aventurescence.
Fluorescence Inert to weak patchy white under LW Generally inert Inert to weak pink under LW
and SW
Comments Key tests are appearance (including Key tests are RI, birefringence, optic Key tests are appearance, poor
phenomenon), RI, birefringence, character, and optic figure. quality of polished surface, RI,
optic character, and magnification and SG. Also known as steatite
(twinning). or, more commonly, “soapstone.”
Eric Welch/GIA
347
GEM IDENTIFICATION LAB MANUAL
CHALCEDONY PEARL
Comments Key tests are spot RI and SG. Key tests are appearance, RI,
Fracture and appearance might birefringence blink, and SG. Feels
also be helpful. gritty when rubbed against a tooth,
while plastic and glass imitations
feel smooth. Heft can separate
natural pearl from plastic imitations.
X-radiography separates natural
from cultured pearl. Drill-hole
might interfere with accurate SG
reading.
348
SEPARATING GRAY GEMS
CULTURED PEARL
General observation Colors same as natural (see descriptions below). Surface luster varies
from dull to nearly metallic depending on nacre quality. Uneven
fracture with dull to pearly fracture luster.
Akoya (bead nucleated)—Typical size range 2 mm to 11 mm.
Mostly spherical, but might be button, pear, oval, or baroque in
shape. Color can range from neutral to near-neutral grays, with rosé
or green overtones, but can sometimes be yellow, pink or blue. Tahitian cultured pearls
Tahitian (bead nucleated)—Typical size range 8 mm to 14 mm. often have silver to dark gray
Spherical, oval, button, drop, or baroque in shape (sometimes cir- bodycolor. Their luster can be
cled). Color can range from near-neutral silver, cream, or brown to nearly metallic.
black or gray, to blue, green, yellowish green, or purple, with green,
blue, or rosé overtone.
South Sea (bead nucleated)—Typical size range 10 mm to 15 mm.
Spherical, near-round, oval, button, drop, or semi-baroque (some-
times circled). Color can range from near-neutral white, cream, or
silver to yellow, yellowish orange, or blue, with green, blue, or rosé
overtone.
Freshwater (usually tissue nucleated)—Typical size range 2 mm to
13 mm. Spherical, near-round, oval, button, drop, or heavily baroque
(sometimes circled). Color can range from neutral to near-neutral
grays, whites, and creams to yellows, pinks and purples, with blue or
green overtone and orient.
RI 1.530 to 1.685
Magnification Not usually diagnostic, unless you can examine a drill-hole and
detect the bead under the nacre.
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW.
SG 2.72 to 2.78
Comments Key tests are appearance, RI, birefringence blink, SG, and magnifica-
tion. Feels gritty when rubbed against a tooth, while plastic and glass
imitations feel smooth. Heft can separate cultured pearl from plastic
imitations. X-radiography separates natural from cultured pearl.
Cultured pearls might be dyed, irradiated, or polymer-impregnated.
Dye might be detectable as concentrations in nacre, especially at the
drill-hole. Some irradiated colors are very intense and unnatural.
Impregnation might be visible with magnification. Drill-hole might
interfere with accurate SG reading.
349
GEM IDENTIFICATION LAB MANUAL
Variety Mother-of-pearl (when orient is present) Not required Moonstone (when adulares-
cence is present)
General observation Translucent to opaque. Virtually any Opaque gray to brown. Jewelry-quality Transparent to opaque gray.
color, but usually white, gray, brown, material displays iridescent colors. Large, Vitreous polish luster, uneven to
yellow, orange, or pink, with layered or well-preserved specimens show a spiral struc- splintery fracture with vitreous
patterned coloring. Might also show ture. Vitreous polish luster, uneven to granular to pearly fracture luster. Might
orient (mother-of-pearl). Shell cameos fracture with greasy to dull fracture luster. show adularescence.
usually show concave backs due to the
curved contours of the shells they’re cut
from. Greasy or pearly polish luster,
uneven to splintery fracture with dull
fracture luster.
Typical cutting style Cameos, carvings, beads, cabochons, Cabochons, freeforms, and tablets. Also used Faceted gems, cabochons
inlays in doublets and triplets.
RI 1.530 to 1.685 1.520 to 1.680 (varies with mineral content) 1.518 to 1.526 (+0.010)
Birefringence/doubling 0.155 (use birefringence blink method) Usually 0.155 (varies with mineral content) 0.005 to 0.008
Magnification Might show an irregular fibrous Distinctive, often iridescent, mosaic patterns Centipede-like inclusions,
structure or parallel banded structure twinning planes, possibly
(mother-of-pearl) oriented needles
SG 2.86 (+0.03/-0.16) Usually about 2.70 (varies with mineral 2.58 (+/-0.03)
content)
Comments Key tests are appearance, RI, birefrin- Key tests are appearance (including irides- Key tests are RI, birefringence,
gence blink, and magnification. cence) and possibly RI. Ammonite is the and possibly optic character.
fossilized shell of an extinct nautilus-like
animal. It’s often polymer-impregnated to
make it more stable or improve its appearance.
Might be sold as “ammolite” in the trade.
350
SEPARATING GRAY GEMS
OBSIDIAN CALCITE
General observation Transparent to opaque natural Transparent to opaque, occurs in almost all colors,
glass, sometimes with a sheen. often dyed. Vitreous to greasy polish luster. Three
Gray to black, often spotted with cleavage directions. Strong eye-visible doubling.
white (“snowflake” obsidian). Cleavage usually not visible in aggregate.
Vitreous polish luster, conchoidal Terri Weimer/GIA
Spectrum Not diagnostic Not diagnostic. Any visible lines are caused by
impurities or dye.
Comments Key tests are RI, SG, and possibly Key tests are doubling, cleavage, RI, birefringence
magnification. Obsidian is a type blink, SG, and possibly appearance. Marble is a
of natural glass. granular aggregate, onyx marble is a banded marble. Maha Tannous/GIA
Satinspar is a fibrous aggregate that’s often
“Rainbow” obsidian commonly
chatoyant (the name is also used for a similar displays sheen in different
variety of gypsum). colors against a gray to black
bodycolor.
351
GEM IDENTIFICATION LAB MANUAL
General observation Light to medium gray bodycolor, with or without play-of- Gray, bluish gray, or grayish blue, light to dark in tone,
color. Vitreous to resinous polish luster, conchoidal to with play-of-color. Conchoidal to uneven fracture with
uneven fracture with subvitreous to waxy fracture luster. subvitreous fracture luster.
In some natural opals, dehydration causes a network of
fine cracks called crazing.
SR/DR/AGG SR, commonly with ADR due to strain SR with weak to strong ADR
Magnification Possible play-of-color patterns include very small patches or Play-of-color in a mosaic pattern across the surface, with a
dots (pinfire); large areas that flash predominately one color cellular, “chicken wire,” “snakeskin,” or scale-like structure
as the gem is moved (flash); or even, distinct patches with a that’s visible with magnification and overhead or back-
“brush-stroke” appearance (harlequin). There might also be lighting. Might show columnar structure when viewed from
areas that lack play-of-color or that contain mineral inclu- the side.
sions or patches of rock matrix. (Play-of-color in synthetic
opal tends to be much more regular.)
Spectrum Not diagnostic Some gems show bands at 550 nm and 580 nm
Fluorescence Inert to white to moderate light blue, green, or yellow Typically moderate bluish white to yellow under LW, weak
under LW and SW. Might phosphoresce. to strong blue to bluish white to yellow under SW.
Phosphorescence is rare and weak if present.
Blue to bluish gray polymer-impregnated synthetic opal—
Inert to very weak blue under both LW and SW
Gray polymer-impregnated synthetic opal—Very weak
greenish yellow under LW, weak greenish yellow under
SW
SG 2.15 (+0.08/-0.90) 1.97 to 2.20 (typically lower than natural opal). Polymer-
impregnated synthetic opal is usually considerably lower
than natural opal, at 1.88 to 1.91. Newer untreated gray-
blue synthetic opal is closer to natural opal, at 2.22 to 2.27.
Comments Key tests are appearance, RI, SG, and possibly magnifica- Magnification is the key to separating synthetic from
tion. Fluorescence might also be helpful. SG can help natural opal. Fluorescence and phosphorescence might also
separate opal from plastic (SG 1.05 to 1.55). Some be helpful. Synthetic opal is often polymer impregnated to
natural opal is polymer impregnated to make it more make it more stable, and it has a considerably lower SG
stable or improve its appearance. than most natural opal.
Opal commonly has a dark gray Synthetic opal like this Gilson
bodycolor and play-of-color in a product results when manufac-
variety of patterns. tured silica spheres are allowed
to settle and compress.
352
SEPARATING GRAY GEMS
GLASS PLASTIC
General observation Transparent to opaque, almost any Transparent to opaque, almost any
appearance possible. Look for mold appearance possible. Look for mold
marks, orange-peel effect, concave marks, orange-peel effect, concave facets,
facets, rounded facet junctions. Warm rounded facet junctions. Warmer to the
to the touch compared to crystalline touch than glass imitations and crystalline
gemstones. Vitreous polish luster, con- gemstones. Low heft (SG), dull to waxy
choidal fracture with vitreous fracture polish luster, conchoidal fracture with
luster. waxy to vitreous fracture luster. Surface
might show numerous scratches due to
low hardness (Mohs 1.5 to 3).
Typical cutting style All styles. Can be faceted or molded to All styles. Can be molded to a variety of
a variety of shapes and finishes. shapes and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR (strain
colors common)
Magnification Gas bubbles, cavities on surface where Gas bubbles, flow lines
gas bubbles were polished through,
flow marks (swirls)
Comments Key tests are RI and magnification. Key tests are RI and magnification. Low
Low thermal conductivity (warm to the heft (SG) and low thermal conductivity
touch) might also be helpful. (warm to the touch) might also be helpful.
353
GEM IDENTIFICATION LAB MANUAL
Hematite from imitation hematite Appearance, fracture, intaglio quality (carved versus
stamped), magnetism
Serpentine from talc RI, possibly hardness (talc feels greasy or “soapy”
to the touch)
Talc from jadeite and nephrite Hardness, RI, SG, spectrum (jadeite)
Natural or cultured pearl from glass or plastic Birefringence blink, magnification/structure, possibly RI
354
SEPARATING BLACK GEMS
Tino Hammid/GIA
BLACK GEMS
Dyed black chalcedony is one of the most common black gems. It’s sold as black
onyx in the trade. Others include black (often dyed) cultured pearls and dark,
grayish black hematite. Large quantities of black onyx and hematite are used in
men’s jewelry.
Some normally transparent gems can be so dark that they appear black. You’ll also
often encounter very dark blue or greenish blue sapphires that appear almost
completely black in normal reflected light.
355
GEM IDENTIFICATION LAB MANUAL
Black Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
2.940 to 3.220 (OTL) Hematite Imitation hematite, diamond, irradiated synthetic diamond
Too opaque to test (Page 358)
1.535 to 1.539 (1.53 to 1.54 Chalcedony Jet, coral, horn, obsidian, glass, plastic
spot reading common) (Page 365)
AGG
356
SEPARATING BLACK GEMS
357
GEM IDENTIFICATION LAB MANUAL
General observation Opaque dark gray to black, might show Opaque dark gray to black with Opaque, with metallic yellow
reddish color on fracture surfaces. Metallic metallic luster and conchoidal “brassy” appearance in larger
polish luster and splintery, granular, or fracture. Can generally be picked pieces. Small rose cuts used in
subconchoidal fracture with dull fracture up by a magnet. Intaglio pattern jewelry might appear gray or
luster. Might be slightly magnetic. High SG usually lacks graver lines. black in reflected light. Metallic
gives loose stones considerable heft. Intaglio polish luster, conchoidal to
pattern usually exhibits graver lines. uneven fracture with metallic
fracture luster.
Typical cutting style Beads, tablets, signets, intaglios Beads, tablets, signets, intaglios Faceted into small rose cuts
Comments Key tests are appearance, fracture, and SG Key tests are appearance, fracture, Key tests are appearance (color,
(heft). and magnetism. metallic luster) and SG. Often
sold as marcasite in the trade.
358
SEPARATING BLACK GEMS
Species Diamond
General observation Black, with an almost metallic appearance. Color due to numerous
minute black inclusions lining internal cleavages and fractures.
Inclusions give a “salt-and-pepper” appearance in transmitted light.
Polished surface shows numerous fractures, pits, and polish lines in
reflected light. Extremely sharp facet junctions. Adamantine polish Elizabeth Schrader/GIA
luster, step-like fracture with adamantine fracture luster. Perfect Naturally colored black diamond has
cleavage in four directions. Polish lines never oriented the same way an almost metallic appearance in
on adjacent facets. Positive reaction to diamond tester. Irradiated reflected light.
black diamonds are dark blue or green throughout, with no colorless
areas. They appear very dark blue or green in transmitted light.
RI OTL
Fluorescence Some stones show a strong but patchy blue fluorescence to LW,
Robert Kane/GIA
intermixed with inert areas. Fluorescent areas correspond with the
more-transparent areas of the diamond. The more-transparent areas Natural black diamonds commonly
fluoresce a moderate chalky greenish yellow to SW. Other reactions have fractures and pits along with
polish and drag lines.
vary from inert to weak chalky greenish yellow under LW, but with
the same characteristic mottling.
SG 3.52 (+/-0.10)
Comments Key tests are polish luster, fracture, OTL RI, magnification, and
positive reaction to diamond tester. Appearance in transmitted light
separates irradiated black diamond from naturally colored black
diamond.
Shane McClure/GIA
Robert Kane/GIA
359
GEM IDENTIFICATION LAB MANUAL
IRRADIATED CZ
SYNTHETIC DIAMOND
General observation Black, almost metallic Opaque black in larger pieces, but
appearance. Color is actually smaller pieces are semitranslucent
very dark green or blue if when viewed with fiber-optic lighting.
observed in transmitted light. Bodycolor in smaller pieces is dark
Extremely sharp facet junc- brownish red, similar to dark-toned
Shane McClure/GIA tions. Adamantine luster, almandite garnet. Subadamantine
Fiber-optic lighting reveals that this synthetic step-like fracture with polish luster, conchoidal fracture with
black diamond is actually very dark blue. It also adamantine fracture luster. subadamantine fracture luster. Heft
contains a typical rod-shaped flux inclusion. Perfect cleavage in four reveals that loose stones are much
directions. Positive reaction heavier than diamonds of similar size.
to diamond tester. Negative reaction to diamond tester.
Dispersion 0.044 (fire masked by dark 0.060 (fire masked by dark bodycolor)
bodycolor)
RI OTL OTL
360
SEPARATING BLACK GEMS
CORUNDUM
Species Corundum
General observation Often very dark, strongly greenish blue, sometimes with angular
zoning and silk, in transmitted light. Vitreous to subadamantine
polish luster, conchoidal fracture with vitreous fracture luster.
SR/DR/AGG DR
Pleochroism Might show only in transmitted light. Very dark blue or violet blue
and very dark greenish blue.
Spectrum Powerful bands due to iron around 450 nm, visible only if you can
pass enough light through the stone
Fluorescence Inert
SG 4.00 (+0.10/-0.05)
Comments Key tests are RI, birefringence, and magnification. Spectrum might
also be helpful.
361
GEM IDENTIFICATION LAB MANUAL
SPINEL DIOPSIDE
General observation Vitreous to subadamantine polish luster, conchoidal Semitranslucent to opaque dark green to black. Might show a
fracture with vitreous fracture luster. cat’s-eye or four-rayed star under a penlight. Vitreous polish
luster, conchoidal to uneven fracture with vitreous to resinous
fracture luster. Perfect cleavage in two directions at nearly 90°
angles to one another.
RI 1.740 to 1.770 (black gems might be higher) 1.675 to 1.701 (+0.029/-0.010) (spot reading usually around 1.68)
Spectrum Might show a very dark version of a gahnite spectrum 505-nm line common
with reflected light, including a strong, broad band in
the blue centered on 459 nm and a strong but much
narrower band, also in the blue, at 480 nm. There’s also
a moderately strong band centered on 555 nm, at the
center of fainter broad absorption between 530 nm and
575 nm. Absorption increases in intensity from about
600 nm toward the red.
Comments Key tests are RI, SG, and spectrum. Key tests are RI, birefringence (if detectable), and possibly
spectrum and SG.
Robert Weldon/GIA
362
SEPARATING BLACK GEMS
General observation Semitransparent to opaque gray to Semitranslucent to opaque very dark Often very dark green or brown in
black. Vitreous to greasy polish brown to black. Resinous to vitreous transmitted light. Vitreous polish luster,
luster with a dimpled polished polish luster, conchoidal fracture with conchoidal fracture with vitreous
surface, granular to splintery dull to greasy fracture luster. Very low fracture luster.
fracture with dull fracture luster. heft. Warm to the touch. Becomes elec-
trically charged when rubbed on wool.
Typical cutting style Carvings, beads, cabochons Carvings, beads Faceted gems, carvings, cabochons
RI 1.666 to 1.680 (+/-0.008) (1.66 spot 1.660 (+/-0.020) (1.68 spot reading 1.620 to 1.644 (+0.011/-0.009) (black
reading common) (black gems common) gems might be higher)
might be higher)
Birefringence/doubling Usually not detectable None Usually 0.018 to 0.020, but can go as
high as 0.040
SR/DR/AGG AGG SR DR
Magnification Often unevenly colored, with root- Not diagnostic Mineral inclusions, possibly thread-
like mottling like liquid and gas inclusions and
mirror-like gas filled fractures
Comments Key tests are appearance, RI, Key tests are RI and SG (low heft). Key tests are almost always RI and
spectrum, and SG. Might be heat- Reacts to hot point with a coal-like or birefringence. If birefringence isn’t
treated, polymer impregnated, or oily odor. obtainable, uniaxial optic figure and
dyed. SG can be helpful. Some very dark
tourmaline is called “schorl” by
mineralogists.
JADEITE
Prism
437.5
Diffraction
Maha Tannous/GIA
363
GEM IDENTIFICATION LAB MANUAL
NEPHRITE CORAL
Black coral commonly shows a Typical cutting style Carvings, beads, cabochons Beads, cabochons
structure that resembles the
growth rings of a tree. RI 1.606 to 1.632 (+0.009/-0.006) 1.560 to 1.570 (+/-0.010)
(1.61 spot reading common)
(black gems might be higher)
Comments Key tests are appearance, RI, Key tests are appearance, RI,
and SG. birefringence, and magnification.
Eric Welch/GIA
364
SEPARATING BLACK GEMS
Variety Not required Onyx (when parallel black and Not required
white bands are present)
General observation Semitransparent to opaque Semitransparent to semitranslucent Translucent to opaque. Surface luster varies from
yellow to brown to almost black. Greasy to vitreous polish dull to nearly metallic, depending on nacre quality.
black. Resinous to vitreous luster, conchoidal to granular Uneven fracture with dull to pearly fracture luster.
polish luster, uneven to fracture with dull to waxy fracture
splintery fracture with luster. Might show bands or layers
resinous to dull fracture of lighter or darker coloration.
luster.
Typical cutting style Carvings, inlays, decorative Cabochons, carvings, inlays Not applicable
objects
Birefringence/doubling None Usually not detectable 0.155 (use birefringence blink method)
Fluorescence Variable Generally inert Variable. Inert to strong light blue, yellow, green,
or pink under LW and SW. Naturally colored black
pearls might show weak to moderate red to orangy
red or brownish red under LW.
Comments Key tests are appearance, Key tests are RI, SG, and Key tests are appearance, RI, birefringence blink,
RI, and magnification. possibly appearance and fracture. and SG. Feels gritty when rubbed against a tooth,
Routinely dyed and sold as while plastic and glass imitations feel smooth.
black onyx in the trade, almost Heft can separate natural pearl from plastic
always without disclosure of imitations. X-radiography separates natural from
color treatment. cultured pearl. Drill-hole might interfere with
accurate SG reading.
Eric Welch/GIA
365
GEM IDENTIFICATION LAB MANUAL
CULTURED PEARL
General observation Colors same as natural (see descriptions below). Surface luster varies
from dull to nearly metallic, depending on nacre quality. Uneven
fracture with dull to pearly fracture luster.
Akoya (bead nucleated)—Typical size range 2 mm to 11 mm.
Mostly spherical, but might be button, pear, oval, or baroque in
shape. Color can range from neutral to near-neutral grays with rosé
Tahitian cultured pearls can have or green overtones. Often irradiated or dyed black with silver nitrate.
true black color and a nearly Tahitian (bead nucleated)—Typical size range 8 mm to 14 mm.
metallic luster. Spherical, oval, button, drop, or baroque in shape (sometimes circled).
Color can range from near-neutral silver to black, gray, or purple,
with green, blue, or rosé overtones.
Freshwater (usually tissue nucleated)—Typical size range 2 mm to
13 mm. Spherical, near-round, oval, button, drop, or heavily baroque
(sometimes circled). Color can range from neutral to near-neutral
grays, whites, and creams to yellows, pinks and purples, with blue or
green overtone and orient. Can be irradiated or dyed black.
RI 1.530 to 1.685
Magnification Not usually diagnostic, unless you can examine a drill-hole and
detect the bead under the nacre
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW. Naturally colored black cultured pearls show weak to
moderate red to orangy red or brownish red under LW.
SG 2.72 to 2.78
Comments Key tests are appearance, RI, birefringence blink, magnification, and
SG. Feels gritty when rubbed against a tooth, while plastic and glass
imitations feel smooth. Heft can separate cultured pearl from plastic
imitations. X-radiography separates natural from cultured pearl.
Cultured pearls might be dyed, irradiated, or polymer-impregnated.
Dye might be detectable as concentrations in nacre, especially at the
drill-hole. Some irradiated colors are very intense and unnatural.
Impregnation might be visible with magnification. Drill-hole might
interfere with accurate SG reading.
366
SEPARATING BLACK GEMS
OBSIDIAN OPAL
General observation Transparent to opaque, sometimes Black, dark gray, blue, green, brown, or other
with a sheen. Gray to black, often dark bodycolor, with or without play-of-color.
spotted with white (“snowflake” Vitreous to resinous polish luster, conchoidal to
obsidian), brown to brownish uneven fracture with subvitreous to waxy frac- Robert Weldon/GIA
yellow, orange or red, rarely green, ture luster. In some natural opals, dehydration
“Snowflake” obsidian has
purple, or blue. Vitreous polish causes a network of fine cracks called crazing. white patches on gray to black
luster, conchoidal fracture with bodycolor. It’s commonly seen
vitreous fracture luster. in cabochons and beads.
SR/DR/AGG SR, commonly with ADR SR, commonly with ADR due to strain
Fluorescence Generally inert Inert to white to moderate light blue, green, or Robert Weldon/GIA
yellow under LW and SW. Might phosphoresce. Opals can have black
bodycolor or very dark
SG 2.40 (+0.10/-0.07) 2.15 (+0.08/-0.90) tones of gray and blue with
play-of-color.
Comments Key tests are RI, SG, and magnifi- Key tests are RI, magnification, and SG.
cation. Appearance can also be Fluorescence might also be helpful. SG can help
helpful. Obsidian is a type of separate opal from plastic (SG 1.05 to 1.55).
natural glass. Some natural opal is polymer impregnated to
make it more stable or improve its appearance.
367
GEM IDENTIFICATION LAB MANUAL
General observation Opaque, uniform black body- Resembles black opal, with a Colorless, white, gray, blue, or black, with play-
color. Polish often less lustrous dark brown mottled appearance of-color. Conchoidal to uneven fracture with
than naturally colored black and unnatural play-of-color. subvitreous fracture luster.
opal. Patchy or spotty play-of- Turns black when moisture is
color. applied to the surface, but
blackness goes away when
moisture dries. Surface
damages very easily.
Typical cutting style Cabochons, carvings Cabochons, carvings Cabochons, carvings, beads
Magnification Black carbon particles visible Surface indents when a pointer Play-of-color in a mosaic pattern across the surface,
in and around patches of gem probe is pressed gently against with a cellular, “chicken wire,” “snakeskin,” or
opal or filling voids in the it. Chipped surfaces reveal scale-like structure that’s visible with magnification
surrounding matrix. Play-of- whitish opal beneath the thin and overhead or backlighting. Might show columnar
color generally appears in a surface treatment. structure when viewed from the side.
mosaic pattern near the surface
of the stone. Chipped surfaces
reveal whitish opal beneath the
thin surface treatment.
Spectrum Not diagnostic Not diagnostic Some gems show bands at 550 nm and 580 nm
SG 1.98 to 2.05 (generally lower Generally lower than untreated 1.97 to 2.20 (typically lower than natural opal).
than untreated black opal) black opal Polymer-impregnated synthetic opal is usually
considerably lower than natural opal, at 1.88 to
1.91. Newer untreated synthetic opal is closer to
natural opal, at 2.22 to 2.27.
Comments Key tests are appearance, Key tests are appearance, Magnification is the key to separating synthetic from
magnification, RI, and possibly magnification, RI, and possibly natural opal. Fluorescence and phosphorescence
SG. SG. might also be helpful. Most synthetic opal is
polymer impregnated to make it more stable.
Sugar-treated opals display speckled Smoke-treated opals typically show a This synthetic opal displays Snakeskin structure is visible
colors against a black background. dark, broad texture under magnifica- both columnar and snakeskin against the play-of-color of this
tion. structures. Gilson synthetic opal.
368
SEPARATING BLACK GEMS
GLASS PLASTIC
Typical cutting style All styles. Can be faceted or All styles. Can be molded to a
molded to a variety of shapes variety of shapes and finishes.
and finishes.
SR/DR/AGG SR, commonly with ADR SR, commonly with strong ADR
(strain colors common)
Comments Key tests are RI and magnifica- Key tests are RI and magnifica-
tion. Low thermal conductivity tion. Low heft (SG) and low
(warm to the touch) might also thermal conductivity (warm to
be helpful. the touch) might also be helpful.
369
GEM IDENTIFICATION LAB MANUAL
Hematite from imitation hematite Appearance, fracture, intaglio quality (carved versus stamped),
magnetism
Natural black diamond from irradiated Magnification and appearance in transmitted light
black diamond
Black diamond from black CZ Appearance in transmitted light, diamond tester, SG, possibly
color filter
Natural from cultured pearl Magnification (structure visible at drill-hole), advanced testing
Dyed black chalcedony from obsidian Fracture luster, RI, SG, possibly polariscope reaction and
magnification
370
IDENTIFYING PHENOMENAL GEMS
The presence of a phenomenon greatly reduces the number of possible identities for a gem. This
natural black opal’s play-of-color limits your identification choices to opal, treated opal, assembled
natural or synthetic opal, synthetic opal, and plastic imitations.
STAR GEMS
Robert Weldon/GIA
Star gems display bands of light that reflect from intersecting needles or needle-like Star ruby is a corundum variety
inclusions. They create a shape that usually has four or six rays. The phenomenon whose identity can be determined
is called asterism. For best effect, star gems require careful cutting as cabochons. partly by observing its bodycolor and
Star sapphire is one of the best known of these, but there are many others in the phenomenon.
market. A variety of synthetics and imitations add to the separation challenges.
Assembled stones that display stars are also available in a variety of colors. You’ll
find complete information on them in the Assembled Stones section that starts on
page 437.
371
GEM IDENTIFICATION LAB MANUAL
Star Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
1.762 to 1.770 (1.76 or 1.77 Star corundum Synthetic star corundum, star garnet, star spinel, star diopside
spot reading) (Pages 373 and 374)
DR (AGG common)
1.762 to 1.770 (1.76 or 1.77 Synthetic star corundum Star corundum, star garnet, star spinel
spot reading) (Pages 375 and 376)
DR (AGG common)
1.750 to OTL range Star garnet (including almandite and Star corundum, synthetic star corundum, star spinel
SR pyrope-almandite)
(Page 376)
1.718 Star spinel Star corundum, synthetic star corundum, star garnet
(1.72 or 1.73 spot reading) (Page 377)
SR
1.544 to 1.553 (1.54 or 1.55 Star quartz Star beryl, star orthoclase
spot reading) (Page 379)
DR (AGG possible)
1.518 to 1.526 (1.52 spot Star orthoclase Star beryl, star quartz
reading) (Page 380)
DR (AGG common)
372
IDENTIFYING PHENOMENAL GEMS: ASTERISM
Prism
strongly greenish blue
Other colors—Designate by color (for example, black star sapphire)
468 476 693
Species Corundum
Diffraction
General observation Semitransparent to opaque, usually with a six-rayed star. Twelve-
rayed stars are rare, but when they occur, it’s usually in dark blue to
black gems. Light to dark purplish red to purple-red stones are star
ruby. Star sapphire occurs in purple, plum, violetish blue, blue, 468 476 693
greenish blue, gray, and dark tones of brown, green, and blue. The
trade sells dark grayish black or brownish black material as black The spectra of natural and synthetic rubies and pink
star sapphire. Orange and yellow star corundum is almost unknown, sapphires show lines at 659 nm, 668 nm, and 693 nm,
and green is rare. Combination of a six-rayed star that’s less than a broad absorption between about 500 nm and 610 nm,
perfect in terms of sharpness and orientation, less-intense bodycolor, and lines in the blue at 468 nm and 476 nm. There’s
rounded or bulged cabochon base, and non-calibrated size suggests also a strong cutoff in the violet. Purple sapphire might
natural origin. Vitreous to subadamantine polish luster, conchoidal show a mixture of ruby-type and sapphire-type spectra.
fracture with vitreous fracture luster. Twinned stones might show
BLUE AND GREEN SAPPHIRE
parting, which is especially obvious on black star sapphire.
Typical cutting style High, medium, or low cabochons, usually with weight-saving convex
Prism
bases
RI 1.762 to 1.770 (+0.009/-0.005) (1.76 or 1.77 spot reading common) 450 471
460
Diffraction
SR/DR/AGG DR (AGG reaction common)
Spectrum Red, pink, and purple stones—Lines at 659 nm, 668 nm, and 693
nm, a broad absorption between about 500 nm and 610 nm, and two
lines in the blue at 468 nm and 476 nm. There’s also a strong cutoff
in the violet. Purple sapphire might show a mixture of ruby-type and
sapphire-type spectra.
Blue and green stones—Bands at 450 nm, 460 nm, and 471 nm.
The 450-nm band is usually the strongest. Some heat-treated material Clayton Welch/GIA
shows only the 450-nm band, and some heated stones might show no Natural star corundum typically shows
bands at all. three sets of intact rutile needles that
intersect at 60° angles.
Fluorescence Red to pink stones—Almost inert to strong moderate red or orange-
red under both LW and SW
Blue stones—(especially light blue stones from Sri Lanka) Weak or
moderate to strong red under LW and SW. Dark stones are generally
inert to both.
SG 4.00 (+0.10/-0.05)
Robert Weldon/GIA
Comments Key tests are appearance, RI, and magnification. The trade allows a
wider color range for ruby when asterism is present. The angular growth in this star sapphire
proves that it’s natural. The perpendicular
orientation of at least one ray to the
growth pattern strongly suggests the
asterism is natural and not diffusion-
induced.
373
GEM IDENTIFICATION LAB MANUAL
Species Corundum
General observation Star might be unnaturally sharp. Color might be confined to the
stone’s surface and concentrated around the girdle edge.
In a natural star sapphire with a star that’s not a Birefringence/doubling 0.008 to 0.010 (usually not detectable on cabochon)
result of lattice diffusion treatment, at least one
of the star’s rays will be perpendicular to the SR/DR/AGG DR (AGG reaction common)
growth zoning.
Pleochroism Usually weak to none, depending on transparency
Magnification Rutile needles that strongly resemble those found in synthetic star
corundum and are confined to a thin surface layer. Localized or
blotchy color might be concentrated along girdle edge and bleed
into surface pits and fractures. Use diffused light to detect color
concentrations.
John Koivula/GIA
The strong, angular color zoning that appears under transmitted Corundum with asterism
light proves that these are natural gems with natural blue color induced by lattice diffusion
(left). The addition of overhead light reveals that none of the rays treatment often shows a
in their stars are perpendicular to the gems’ hexagonal color strong star.
banding (right). This indicates that the stars are a result of lattice
diffusion.
374
IDENTIFYING PHENOMENAL GEMS: ASTERISM
bodycolors, including brown, gray, and white, are possible. The typical features of these flame-fusion
synthetic star sapphires are their strong, sharp,
Typical cutting style Cabochons, precisely cut, sometimes in calibrated sizes and often well-centered stars and strong bodycolor.
with flat rather than curved bases
Magnification Gas bubbles, minute rutile needles confined to a shallow layer near Eric Welch/GIA
the surface, curved color banding. Curved striae in red stones. Most flame-fusion synthetic
Curved growth features might be especially visible on the flat backs star rubies and sapphires have
of cabochons. Some stones might have the manufacturer’s initial— flat bases with visible curved
the letter L—engraved on the back. growth.
Comments Magnification is the key test for separating this synthetic from
natural star corundum.
375
GEM IDENTIFICATION LAB MANUAL
General observation Semitransparent, with a slightly wavy, natural- Generally a dark-toned brownish orange to brownish red to purplish red
looking star hue with low saturation. Usually displays a four-rayed star, although
some stones might show six-rayed stars. Stones cut as spheres might
show both a six-rayed and a four-rayed star, depending on viewing
orientation. Vitreous to subadamantine polish luster, conchoidal fracture
with greasy to vitreous fracture luster.
Magnification Extremely fine needles, low-relief curved or Needle-like inclusions, usually intersecting at 70° and 110° angles in
wavy growth, bluish white smoke-like swirls, the same plane, high- and low- relief crystals, and zircon crystals with
and gas bubbles strain halos
Spectrum Same as natural Strong bands in the green and yellow of the spectrum at 505 nm, 527
nm, and 575 nm. Most red-garnet mixtures of pyrope and almandite,
including rhodolite, show this spectrum.
Fluorescence Very strong red under LW, strong to very strong Inert
red with moderate to strong chalky blue-white
overtone under SW
Comments Magnification is the key test for separating this Key tests are RI, magnification, spectrum, and SG.
synthetic from natural star ruby.
376
IDENTIFYING PHENOMENAL GEMS: ASTERISM
Variety Star
Prism
Species Spinel
Diffraction
both, depending on viewing orientation. Vitreous to subadamantine
polish luster, conchoidal fracture with vitreous fracture luster.
Pleochroism None
Prism
Magnification Not diagnostic (natural inclusions)
459
Spectrum Red stones—Might show a group of closely spaced lines in the red, 480
with the strongest one at 686 nm, plus a broad absorption of the
Diffraction
green area of the spectrum
Violet and purplish stones—Weaker version of the blue spinel
spectrum, with bands in the blue at 459 nm and 480 nm. There might
be weaker, diffused bands at 553 nm, 593 nm, and 632 nm. 459
480
Fluorescence Varies with bodycolor, but ranges from inert to weak red to orange-
red under SW and weak to strong red under LW
In its spectrum, natural blue spinel colored by
iron shows bands in the blue at 459 nm and
SG 3.60 (+0.10/-0.03) 480 nm. Bands at 553 nm, 593 nm, and
632 nm are not as sharp.
Comments Key tests are appearance of star, RI, and SG.
Robert Weldon/GIA
377
GEM IDENTIFICATION LAB MANUAL
Birefringence/doubling 0.024 to 0.030 (usually not 0.005 to 0.009 (usually not detectable on
detectable on cabochon) cabochon)
Comments Key tests are appearance of star, Key tests are RI, SG, and possibly
RI, and spectrum. magnification.
378
IDENTIFYING PHENOMENAL GEMS: ASTERISM
STAR QUARTZ
Species Quartz
Fluorescence Star rose quartz ranges from inert to weak purple under LW and
SW. Other colors inert.
SG 2.66 (+0.03/-0.02)
Comments Key tests are appearance, RI, and SG. Magnification and fluorescence
might also be helpful.
379
GEM IDENTIFICATION LAB MANUAL
STAR ORTHOCLASE
Species Orthoclase
Group Feldspar
Maha Tannous/GIA
This 14.77-ct. feldspar cabochon General observation Semitransparent to opaque, typically colorless to white with blue or
shows strong asterism as well as
white adularescence and asterism. Reddish brown aventurescent
aventurescence.
material might show eye-visible plate-like inclusions along with a
distinct four-rayed star. Silvery adularescence might also be seen along
the girdle edge. Vitreous polish luster, uneven to splintery fracture with
vitreous to pearly fracture luster. Two cleavage directions, parting also
common.
Shane McClure/GIA Optic character Biaxial negative, if detectable. Might show repeated twinning under
The aventurescence in star sunstone is caused crossed polarizing filters.
by a mass of needles and elongated hematite
inclusions. Magnification Centipede-like inclusions in star moonstone. Aventurescent material
contains two sets of reflective inclusions (fine needles and elongated
hematite flakes) that intersect at near 90° angles, causing the star.
Fluorescence Adularescent material is inert to blue under LW, orange under SW.
Might fluoresce weak pink to red under both LW and SW.
Aventurescent material is inert to both LW and SW.
SG 2.58 (+/-0.03)
Comments Key tests are appearance, RI, and magnification. Optic character,
fluorescence, and SG might also be helpful. As physical properties
of orthoclase and oligoclase feldspar overlap, it might require
advanced testing to separate them, especially if aventurescence is
present. Presence of adularescence indicates orthoclase.
380
IDENTIFYING PHENOMENAL GEMS: ASTERISM
Star corundum from corundum with lattice diffusion Magnification, orientation of asterism
induced star
Star ruby from star garnet Appearance, SR vs DR nature, optic character, pleochroism, magnification,
spectrum, possibly RI and fluorescence
Synthetic star ruby from star garnet Appearance, SR vs DR nature, optic character, magnification, spectrum,
pleochroism, possibly RI and fluorescence
Star spinel from star corundum RI, spectrum, SG, possibly appearance of star
Star spinel from star garnet RI, spectrum, SG, possibly fluorescence
Star diopside from black star sapphire Appearance of star, RI, spectrum, SG
Star quartz from star sapphire Appearance of star, RI, SG, magnification
Star quartz from star orthoclase Appearance of star, RI, possibly optic character and adularescence,
if present
381
GEM IDENTIFICATION LAB MANUAL
CAT’S-EYE GEMS
Cat’s-eye gems display a phenomenon called chatoyancy. When they’re properly
cut and light strikes them in just the right way, they show concentrated bands of
light across their cabochon-cut tops. The light is reflected from parallel, needle-
like inclusions or hollow tubes.
Many gems, such as garnet, corundum, and chrysoberyl, have chatoyant varieties.
Because cat’s-eye gems are in demand in the marketplace, you’ll also see many
synthetic and imitation versions of them.
Cat’s-eye Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
1.888 (OTL) Cat’s-eye andradite garnet Cat’s-eye spessartite, cat’s-eye chrysoberyl, cat’s-eye alexandrite,
SR (Page 384) synthetic cat’s-eye alexandrite
1.810 (OTL) Cat’s-eye spessartite garnet Cat’s-eye andradite, cat’s-eye chrysoberyl, cat’s-eye alexandrite, synthetic
SR (Page 384) cat’s-eye alexandrite
1.762 to 1.770 Cat’s-eye corundum Cat’s-eye chrysoberyl, cat’s-eye alexandrite, synthetic cat’s-eye
(1.76 or 1.77 spot reading) (Page 385) alexandrite
DR (AGG common)
1.746 to 1.755 (1.75 spot reading) Cat’s-eye alexandrite Cat’s-eye garnet, cat’s-eye corundum, synthetic cat’s-eye alexandrite
DR (AGG possible) chrysoberyl
(Page 386)
1.746 to 1.755 (1.75 spot reading) Synthetic cat’s-eye alexandrite Cat’s-eye garnet, cat’s-eye corundum, cat’s-eye alexandrite
DR (AGG possible) chrysoberyl
(Page 387)
1.691 to 1.700 (1.69 spot reading) Cat’s-eye zoisite Cat’s-eye apatite, cat’s-eye tourmaline
DR (AGG possible) (Page 387)
1.675 to 1.701 (1.68 spot reading) Cat’s-eye diopside Cat’s-eye kornerupine, cat’s-eye enstatite, cat’s-eye sillimanite, cat’s-eye
DR (AGG possible) (Page 388) peridot, cat’s-eye apatite, cat’s-eye tourmaline, cat’s-eye actinolite
1.667 to 1.680 Cat’s-eye kornerupine Cat’s-eye diopside, cat’s-eye enstatite, cat’s-eye sillimanite, cat’s-eye
DR (AGG possible) (Page 389) peridot, cat’s-eye tourmaline
1.663 to 1.673 Cat’s-eye enstatite Cat’s-eye diopside, cat’s-eye kornerupine, cat’s-eye sillimanite, cat’s-eye
(1.66 or 1.67 spot reading) (Page 389) tourmaline, cat’s-eye actinolite
DR (AGG possible)
1.659 to 1.680 Cat’s-eye sillimanite Cat’s-eye diopside, cat’s-eye kornerupine, cat’s-eye enstatite, cat’s-eye
AGG (Page 390) actinolite
1.654 to 1.690 Cat’s-eye peridot Cat’s-eye diopside, cat’s-eye kornerupine, cat’s-eye tourmaline
(1.65 to 1.69 spot reading) (Page 390)
DR
1.634 to 1.638 (1.63 spot reading) Cat’s-eye apatite Cat’s-eye zoisite, cat’s-eye diopside, cat’s-eye tourmaline, cat’s-eye
DR (AGG possible) (Page 391) actinolite
382
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
1.614 to 1.641 (1.63 spot reading) Cat’s-eye actinolite Cat’s-eye diopside, cat’s-eye enstatite, cat’s-eye sillimanite,
AGG (Page 392) cat’s eye apatite, cat’s-eye tourmaline
1.577 to 1.583 Cat’s-eye beryl (including cat’s-eye Cat’s-eye scapolite, cat’s-eye quartz, hawk’s-eye quartz,
DR (AGG possible) emerald) tiger’s-eye quartz, cat’s-eye moonstone
(Page 392)
1.550 to 1.564 (1.56 to 1.57 spot reading) Cat’s-eye scapolite Cat’s-eye beryl, cat’s-eye quartz, hawk’s-eye quartz, tiger’s-eye
DR (AGG possible) (Page 393) quartz
1.544 to 1.553 Cat’s-eye quartz Cat’s-eye beryl, cat’s-eye scapolite, hawk’s-eye quartz, tiger’s-eye
(1.54 or 1.55 spot reading) (Page 394) quartz, cat’s-eye moonstone
AGG if not too opaque to test
1.544 to 1.553 Hawk’s-eye quartz Cat’s-eye beryl, cat’s-eye scapolite, cat’s-eye quartz, tiger’s-eye
(1.54 or 1.55 spot reading) (Page 394) quartz
AGG if not too opaque to test
1.544 to 1.553 Tiger’s-eye quartz (including dyed) Cat’s-eye beryl, cat’s-eye scapolite, cat’s-eye quartz,
(1.54 or 1.55 spot reading) (Page 395) hawk’s-eye quartz
AGG if not too opaque to test
1.518 to 1.526 (1.52 spot reading) Cat’s-eye orthoclase (moonstone) Cat’s-eye beryl, cat’s-eye quartz
DR or AGG (Page 396)
1.470 to 1.700 range (chatoyant material Cat’s-eye glass Any cat’s-eye gem
often OTL) (Page 397)
SR or AGG
383
GEM IDENTIFICATION LAB MANUAL
It’s possible, but rare, for a RI 1.888 (OTL) 1.810 (+0.004/-0.020) (OTL)
spessartite garnet to show
chatoyancy. Birefringence/doubling None None
SPESSARTITE GARNET SR/DR/AGG SR, commonly with ADR SR, commonly with ADR
cause chatoyancy
384
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
CAT’S-EYE CHRYSOBERYL
CAT ’S-EYE CORUNDUM CAT ’S-EYE CHRYSOBERYL
Prism
Cat’s-eye sapphire—Light to
dark violet, bluish violet, pure
blue to strongly greenish blue
444
Other colors—Designate by
color
Diffraction
Species Corundum Chrysoberyl
Magnification Silk, sets of parallel needles, Fine needles or hollow tubes that
hexagonal growth lines, color resemble silk. Might also show
zoning, and mineral inclusions fingerprints, angular included crys-
tals, negative crystals, or twinning.
Comments Key tests are appearance, RI, Key tests are RI, SG, and spectrum.
and magnification. This gem Might be irradiated to a honey
is rare. brown bodycolor. This is rare,
but stones treated this way remain
significantly radioactive.
385
GEM IDENTIFICATION LAB MANUAL
Species Chrysoberyl
Magnification Fine needles or hollow tubes that resemble silk. Might also show
fingerprints, angular included crystals, negative crystals, or twinning.
and 680.5 nm; weaker ones at 645 nm and 655 nm; a broad absorp-
tion between about 540 nm and 605 nm; weak lines in the blue at
468 nm, 473 nm, and 476.5 nm; and a cutoff in the violet at about
470 nm
Green pleochroic direction—Strong lines in the red at 678 nm and
680.5 nm; weaker ones at 645 nm, 649 nm, 655 nm, and 665 nm; a
broad absorption between about 555 nm and 640 nm; and a cutoff in
In the green pleochroic direction, alexandrite the violet at about 470 nm
shows strong lines in the red at 678 nm and
Orange pleochroic direction—No strong absorptions
680.5 nm; weaker ones at 645 nm, 649 nm,
655 nm, and 665 nm; a broad absorption
between about 555 nm and 640 nm; and a Fluorescence Inert to moderate red under LW and SW
cutoff in the violet at about 470 nm.
SG 3.73 (+/-0.02)
Comments Key tests are appearance of color change (in combination with
chatoyancy), RI, SG, and spectrum. Magnification separates natural
from synthetic cat’s-eye alexandrite.
386
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
General observation Semitransparent. Bluish green Semitransparent to translucent. Usually green or Robert Weldon/GIA
in daylight or fluorescent light, violet-blue. Tanzanite variety is typically a medium- Cat’s-eye tanzanite is an
brownish red to purple-red in dark grayish violet-blue with a sharp chatoyant extremely rare zoisite variety.
incandescent light. Vitreous to band. Green material ranges from light to dark
subadamantine polish luster, bluish green to yellowish green. Vitreous polish
conchoidal fracture with luster, conchoidal to uneven fracture with vitreous
greasy to vitreous fracture fracture luster. Perfect cleavage in one direction.
luster. Displays chatoyancy.
Birefringence/doubling 0.008 to 0.010 (usually not 0.008 to 0.013 (usually not detectable on Shane McClure/GIA
detectable on cabochon) cabochon)
Parallel growth tubes produced
the chatoyancy in this green
SR/DR/AGG DR (AGG reaction possible) DR (AGG reaction possible) zoisite.
Pleochroism Strong green, orange, and Green zoisite is greenish yellow to greenish brown,
purple-red trichroism yellowish green, and bluish green to brownish
green. Tanzanite variety is usually strong blue,
purplish red, and greenish yellow, although
orientation to show a cat’s-eye might not show the
best pleochroic color.
Spectrum Same as natural Green material might show broad absorption of the
violet and most of the blue portion of the spectrum
and weak to distinct bands at 660 nm and 680 nm.
Tanzanite variety might show bands at 455 nm,
528 nm, and 595 nm.
Comments Magnification is the key test Key tests are RI, birefringence, optic character,
for separating synthetic and pleochroism. Chatoyant zoisite is extremely
from natural alexandrite. rare. Green cat’s-eye zoisite might strongly
Fluorescence might also be resemble cat’s-eye tourmaline of the same color.
helpful. RI and SG are usually enough to separate them.
387
GEM IDENTIFICATION LAB MANUAL
DIOPSIDE
CAT ’S-EYE DIOPSIDE
Variety Cat’s-eye
Prism
Species Diopside
General observation Bluish green to yellowish green to dark green and black. Vitreous
505
polish luster, conchoidal to uneven fracture with vitreous to resinous
fracture luster. Perfect cleavage in two directions at nearly 90°
Diffraction
Diopside’s spectrum shows bands at 456 nm, Birefringence/doubling 0.024 to 0.030 (usually not detectable on cabochon except by
493 nm, and 505 nm. The 505-nm band is birefringence blink)
diagnostic for the gem.
SR/DR/AGG DR (AGG reaction possible)
CHROME DIOPSIDE
Optic character Biaxial positive, if detectable
Spectrum Bands at 456 nm, 493 nm, and 505 nm. The 505-nm band is
diagnostic for the gem. Vivid green material might show a chrome-
Diffraction
type spectrum with lines at 505 nm, 508 nm, 635 nm, 655 nm, and
670 nm, and a cutoff in the blue around 450 nm.
SG 3.29 (+0.11/-0.07)
Chrome diopside’s spectrum shows lines
at 505 nm, 508 nm, 635 nm, 655 nm, and Comments Key tests are RI and spectrum. Might show birefringence blink.
670 nm, and a cutoff in the blue area of the
spectrum around 450 nm.
Robert Weldon/GIA
388
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
KORNERUPINE
CAT’S-EYE KORNERUPINE CAT ’S-EYE ENSTATITE
Prism
Species Kornerupine Enstatite
Diffraction
and colorless (rare), with fairly common in dark green stones
chatoyancy. Some might show (six-rayed asterism also possible,
asterism. Vitreous polish luster, but very rare). Vitreous polish luster,
conchoidal fracture with uneven fracture with vitreous to
vitreous fracture luster. Perfect pearly fracture luster. Distinct
cleavage in two directions. cleavage in two directions.
Kornerupine’s spectrum shows bands at 446 nm
Typical cutting style Cabochons Cabochons
and 503 nm along with faint lines at 430 nm,
463 nm, and 540 nm. It’s best observed in the
RI 1.667 to 1.680 (+/-0.003) 1.663 to 1.673 (+/-0.010) (1.66 or gem’s green pleochroic direction
1.67 spot reading common)
Pleochroism Strong green, yellow, and red- Weak to strong green and yellowish Kornerupine can show fine-
quality chatoyancy.
brown trichroism typical for green or brown and yellow
brownish green stones ENSTATITE
Spectrum Bands at 446 nm and 503 nm Key lines in the green at 505 nm
plus faint lines at 430 nm, 463 and 550 nm. Some strongly colored
505 550
nm, and 540 nm. green stones might show vague
chrome lines in the red.
Diffraction
Comments Key tests are RI and spectrum. Key tests are RI, spectrum, and
Pleochroism, fluorescence, and fracture. Pleochroism and SG Of the many bands and lines in enstatite’s
SG might also be helpful. might also be helpful. spectrum, the most diagnostic ones are at
505 nm and 550 nm.
Eric Welch/GIA
389
GEM IDENTIFICATION LAB MANUAL
Magnification Usually appears fibrous. Might Numerous tiny, very thin, dark
show long, straight needles brown inclusions (probably
throughout stone. ilmenite), oriented in specific
crystal directions
Spectrum Weak bands at 410 nm, 441 Narrow bands at 453 nm, 477 nm,
nm, and 462 nm and 497 nm
390
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
YELLOW APATITE
CAT’S-EYE APATITE CAT ’S-EYE TOURMALINE
Prism
Species Apatite Tourmaline
General observation Usually bluish green to Can be almost any color, but
520 580
yellowish green, with a fairly commonly dark bluish green to dark
well-defined chatoyant band greenish blue. Chatoyancy caused
Diffraction
that generally rolls easily. by numerous parallel hollow tubes,
Vitreous polish luster, con- so it has a coarser, less-focused eye
choidal to uneven fracture with than cat’s-eye chrysoberyl. Vitreous
vitreous fracture luster. polish luster, conchoidal fracture
520 580
with vitreous fracture luster.
Birefringence/doubling 0.002 to 0.008 (usually not Usually 0.018 to 0.020 (usually not
detectable on cabochon) detectable on cabochon)
Comments Key tests are RI, spectrum, Key tests are RI, pleochroism, and
fluorescence, and SG. SG. Magnification and fluorescence
Robert Weldon/GIA
might also be helpful.
Because the inclusions in cat’s-
eye tourmaline are larger than
those in cat’s-eye chrysoberyl, its
chatoyant band is coarser and
less focused.
391
GEM IDENTIFICATION LAB MANUAL
General observation Usually translucent, but can be Various bodycolors, with chatoyancy.
semitransparent to opaque. Light to Vitreous polish luster, conchoidal
dark green, yellowish green, and fracture with vitreous to resinous
black. Cat’s-eyes usually green to fracture luster.
yellowish green. Vitreous polish
luster, uneven fracture with dull to
vitreous fracture luster.
Shane McClure/GIA RI 1.614 to 1.641 (+0.014) (1.63 spot 1.577 to 1.583 (+/-0.017)
Chatoyancy can be present in beryl of reading common)
any color, but cat’s-eye emerald is the
most valuable. Birefringence/doubling 0.022 to 0.027 in transparent 0.005 to 0.009 (usually not detectable
material. Use the birefringence on cabochon)
blink method on cabochons
(usually not detectable).
Comments Key tests are appearance, RI, bire- Key tests are RI, SG, and possibly
fringence blink, magnification, magnification.
and spectrum. AGG polariscope
reaction might help separate cat’s-
eye actinolite from cat’s-eye
apatite, which usually shows a DR
reaction.
392
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
Variety Cat’s-eye
Species Scapolite
Spectrum Not diagnostic, except in pink stones, which might show lines at 652
nm and 663 nm.
Fluorescence Inert to strong pink, orange, or yellow. Some reddish brown material
might be inert to LW and strong red under SW.
SG 2.68 (+0.06/-0.08)
393
GEM IDENTIFICATION LAB MANUAL
RI 1.544 to 1.553 (1.54 or 1.55 1.544 to 1.553 (1.54 or 1.55 spot reading)
spot reading)
SR/DR/AGG AGG if not too opaque to test AGG if not too opaque to test
Comments Key tests are RI, SG, and Key tests are color, appearance (especially
possibly birefringence. Cat’s- structure and wavy chatoyancy), and RI.
eye quartz is generally more
transparent than either tiger’s-
eye or hawk’s-eye quartz and
Terri Weimer/GIA usually gives a DR polariscope
The chatoyancy in hawk’s-eye reaction.
quartz is caused by its fibrous
structure. Its color is typically
gray to grayish blue.
394
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
Typical cutting style Cabochons, beads, tablets, carvings Cabochons, beads, tablets, carvings
RI 1.544 to 1.553 (1.54 or 1.55 spot 1.544 to 1.553 (1.54 or 1.55 spot
reading) reading)
SR/DR/AGG AGG if not too opaque to test AGG if not too opaque to test
Comments Key tests are color, appearance Key tests are appearance and Eric Welch/GIA
395
GEM IDENTIFICATION LAB MANUAL
Comments Key tests are appearance, RI, and Key tests are RI, magnification,
magnification. Optic character, and SG. This gem is rare.
fluorescence, and SG might also
be helpful.
396
IDENTIFYING PHENOMENAL GEMS: CHATOYANCY
SR/DR/AGG SR, commonly with ADR due to SR with ADR, or AGG due to fiber-optic
strain (AGG reaction possible) structure
Comments Key tests are RI, SG, and Key tests are magnification and appear-
magnification. ance. Sold as “Cathaystone,” “Catseyte,”
or “Fiber-eye” in the trade.
Magnification often reveals a honey-
comb structure in cat’s-eye glass.
397
GEM IDENTIFICATION LAB MANUAL
Cat’s-eye tourmaline from cat’s-eye apatite Appearance, RI, birefringence, pleochroism, magnification, spectrum
Cat’s-eye tourmaline from cat’s-eye actinolite Appearance, transparency, magnification, polariscope reaction, possibly
pleochroism
Cat’s-eye tourmaline from cat’s-eye sillimanite Appearance, transparency, magnification, RI, birefringence blink,
possibly spectrum
Cat’s-eye diopside from cat’s-eye kornerupine RI, birefringence blink, possibly magnification and pleochroism
Cat’s-eye kornerupine from cat’s-eye enstatite Birefringence blink, spectrum, possibly pleochroism
Cat’s-eye apatite from cat’s-eye actinolite Appearance, transparency, birefringence blink, polariscope reaction,
magnification, spectrum
Cat’s-eye apatite from cat’s-eye sillimanite Appearance, transparency, birefringence blink, polariscope reaction,
magnification, spectrum
Cat’s-eye scapolite from cat’s-eye beryl Possibly RI, SG, and birefringence blink
Cat’s-eye quartz from hawk’s-eye and tiger’s-eye Appearance of eye (fine needles rather than wavy chatoyancy),
quartz magnification
Cat’s-eye opal from cat’s-eye quartz RI, magnification, possibly birefringence and SG
398
IDENTIFYING PHENOMENAL GEMS: COLOR CHANGE
Alexandrite chrysoberyl displays striking color change from incandescent (top) to fluorescent
lighting (bottom).
COLOR-CHANGE GEMS
There’s a very special category of gems that change color when they’re exposed
to different types of light. Alexandrite chrysoberyl is the most familiar color-
change gem on the market, but other gem species also include color-change
varieties.
399
GEM IDENTIFICATION LAB MANUAL
Color-change Gems
RI and SR/DR/AGG Gem Material Commonly confused with:
1.762 to 1.770 (1.76 or 1.77 Corundum, color-change sapphire Synthetic color-change sapphire, color-change garnet, alexandrite,
spot reading) (Page 402) synthetic alexandrite, color-change spinel
DR
1.762 to 1.770 (1.76 or 1.77 Synthetic corundum, synthetic color- Color-change sapphire, color-change garnet, alexandrite, synthetic
spot reading) change sapphire alexandrite, color-change spinel
DR (Page 403)
1.750 to 1.780 Color-change garnet Color-change sapphire, synthetic color-change sapphire, alexandrite,
SR (Page 404) synthetic alexandrite, color-change spinel
1.746 to 1.755 Alexandrite chrysoberyl Color-change sapphire, synthetic color-change sapphire, color-
DR (Page 405) change garnet, synthetic alexandrite, color-change spinel
1.746 to 1.755 Synthetic alexandrite chrysoberyl Color-change sapphire, synthetic color-change sapphire, color-
DR (Page 406) change garnet, alexandrite, color-change spinel
400
IDENTIFYING PHENOMENAL GEMS: COLOR CHANGE
COLOR-CHANGE CZ
RI OTL
Birefringence/doubling None
SR/DR/AGG SR
Comments Key tests are detection of color change, OTL RI reading, lack of
doubling, SG, and possibly fracture. Color-change CZ has greater
heft than OTL color-change glass. CZ is a manmade material with
no gem-quality natural counterpart.
401
GEM IDENTIFICATION LAB MANUAL
Species Corundum
SG 4.00 (+0.10/-0.05)
Comments Key tests are detection of color change, RI, birefringence, and
magnification.
402
IDENTIFYING PHENOMENAL GEMS: COLOR CHANGE
Prism
Species Synthetic corundum
General observation Transparent. Typically purple in incandescent light and grayish blue
in daylight and fluorescent lighting. Vitreous to subadamantine 474
Diffraction
Typical cutting style Faceted gems, cabochons
Spectrum Cutoff at about 460 nm, strong line due to vanadium at 474 nm,
faint broad absorption between 550 nm and 610 nm, and possibly a
fluorescent line in the red at 690 nm
Fluorescence Moderate orange to red under LW and SW. Might fluoresce red
under LW and mottled blue under SW.
Both by Terri Weimer/GIA
SG 4.00 (+0.10/-0.05)
Flame-fusion synthetic color-change sapphire
typically appears purple under incandescent
Comments Key tests are detection of color change, RI, birefringence, magnifica- light (left) and grayish blue under fluorescent
tion, and spectrum. light (right).
403
GEM IDENTIFICATION LAB MANUAL
COLOR-CHANGE GARNET
COLOR-CHANGE GARNET
Variety Color-change
Prism
Species Pyrope-spessartite
Group Garnet
General observation Transparent. Wide variety of colors. Generally intense pink to red
Diffraction
Color-change garnet’s spectrum might show Typical cutting style Faceted gems, cabochons
only a broad absorption centered on 571 nm.
Its spectrum might also be more complex, with RI 1.750 to 1.780
bands at 410 nm, 421 nm, and 430 nm that
can merge to form a cutoff at 435 nm, along Birefringence/doubling None
with some combinations of bands at 460 nm,
480 nm, 505 nm, 525 nm, and 575 nm. The
SR/DR/AGG SR with weak to strong ADR
575-nm band is broader and stronger in gems
with strong color change.
Pleochroism None
Fluorescence Inert
Both by Tino Hammid/GIA
SG 3.88 to 3.91
Most color-change garnets are varieties of
pyrope-spessartite garnet. This color-change
Comments Key tests are RI, SR nature, magnification, and possibly spectrum.
“malaya” garnet is shown in incandescent light
(left) and fluorescent light (right). Lack of pleochroism helps separate garnet from alexandrite if RIs
are close.
404
IDENTIFYING PHENOMENAL GEMS: COLOR CHANGE
Variety Alexandrite
Prism
Species Chrysoberyl
General observation Transparent. Color change from orangy or brownish red to purplish red
in incandescent light to yellowish, brownish, grayish, or bluish green in
daylight or fluorescent light. Vitreous to subadamantine polish luster,
Diffraction
conchoidal fracture with greasy to vitreous fracture luster.
Magnification Might show fingerprints, angular included crystals, liquid inclusions, ALEXANDRITE (GREEN DIRECTION)
needle-like inclusions, or twinning
Prism
Purple-red pleochroic direction—Strong lines in the red at 678 nm
and 680.5 nm; weaker ones at 645 nm and 655 nm; a broad absorption
between about 540 nm and 605 nm; weak lines in the blue at 468 nm,
473 nm, and 476.5 nm; and a cutoff in the violet
Green pleochroic direction—Strong lines in the red at 678 nm and
Diffraction
680.5 nm; weaker ones at 645 nm, 649 nm, 655 nm, and 665 nm; a
broad absorption between about 555 nm and 640 nm; and a cutoff in
the violet at about 470 nm
Orange pleochroic direction—No strong absorptions
This alexandrite shows a fine-quality color change, Natural alexandrite often contains Negative crystals are among The angular apatite
from reddish purple in incandescent light (left) to angular fluorite crystals that the clarity characteristics crystals in this
green in fluorescent light (right). can help you separate it from found in natural alexandrite. alexandrite identify it
synthetic material. as natural.
405
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC ALEXANDRITE
SR/DR/AGG DR
Parallel growth features give a Fluorescence Moderate to strong red under LW and SW
venetian-blind effect in flux-
grown synthetic alexandrite. SG 3.73 (+/-0.02)
Comments Magnification is the key test for separating synthetic from natural
alexandrite. Strong red fluorescence indicates synthetic.
Semitransparent to translucent synthetic alexandrite can also display
a cat’s-eye.
Shane McClure/GIA
406
IDENTIFYING PHENOMENAL GEMS: COLOR CHANGE
Typical cutting style Faceted gems, cabochons All styles. Can be faceted or molded to
a variety of shapes and finishes.
Magnification Natural mineral inclusions, negative Gas bubbles, cavities on surface, flow
crystals, fingerprints, needles marks (swirls)
Comments Key tests are detection of color Key tests are detection of color
change, RI, and SG. Lack of change, RI, and magnification. Low
doubling, polariscope reaction, lack thermal conductivity (warm to the
of pleochroism, and spectrum help touch) might also be helpful.
separate spinel from other color-
change gems. Rare.
407
GEM IDENTIFICATION LAB MANUAL
Alexandrite chrysoberyl from color-change sapphire Appearance of color change, RI, birefringence, spectrum, SG
Alexandrite chrysoberyl from synthetic color-change Appearance of color change, RI, birefringence, magnification, spectrum
sapphire
Color-change glass from color-change garnet, alexan- RI (usually below 1.70), magnification
drite, and color-change sapphire
408
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
1.520 to 1.680 Ammonite Opal, synthetic opal, glass and plastic opal imitations
AGG (Page 413)
1.450 Opal Andradite, iris agate, fire agate, mother-of-pearl, ammonite, sugar- and
SR (Page 414) smoke-treated opal, synthetic opal, glass and plastic opal imitations
1.450 Fire opal Synthetic opal, glass and plastic opal imitations
SR (Page 415)
1.430 to 1.470 range Synthetic opal Ammonite, opal, fire opal, glass and plastic opal imitations
SR (Page 417)
1.500 to 1.520 range Glass imitation opal Ammonite, opal, fire opal, synthetic opal, plastic imitation opal
SR (Page 418)
1.480 to 1.530 range Plastic imitation opal Ammonite, opal, fire opal, synthetic opal, glass opal imitations
SR (Page 418)
409
GEM IDENTIFICATION LAB MANUAL
General observation Semitranslucent to opaque, with Semitransparent to translucent, Semitranslucent to opaque, with
iridescent color in angled bands, with iridescent colors best seen iridescent colors against a dark reddish
parallel zones, or sometimes in a in thin slices with transmitted brown bodycolor. Botryoidal structure,
mosaic pattern against a dark brown or light. Greasy to vitreous polish which resembles a bunch of grapes.
black body. Vitreous to subadamantine luster, conchoidal fracture. Greasy to vitreous polish luster,
polish luster, conchoidal to uneven conchoidal fracture.
fracture with vitreous fracture luster.
Might show abrasions due to relatively
low hardness (Mohs 6.5 to 7).
RI 1.888 (OTL) 1.535 to 1.539 (1.53 or 1.54 spot 1.535 to 1.539 (1.53 or 1.54 spot
reading) reading)
Birefringence/doubling None Usually not detectable (rarely Usually not detectable (rarely 0.004)
0.004)
SR/DR/AGG SR, often with ADR (usually too AGG AGG if not too opaque to test
opaque to test)
Comments Key tests are OTL RI reading, SG, and Key tests are RI, SG, and appear- Key tests are appearance, structure,
magnification. Appearance and spectrum ance in transmitted light. RI, and SG.
might also be helpful. This gem is rare.
Andradite might show The iridescence of iris agate shows up best Fire agate is often fashioned in a
iridescence. It’s some- in transmitted light. freeform style to best display its
times confused with iridescence.
black opal, although
gemological properties
easily separate the two.
410
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
PEARL
Species Pearl
General observation Translucent to opaque. Might be almost any bodycolor, but usually
white or light yellow. Bodycolor might be modified by pink, green,
or blue overtone. Orient is most commonly seen on irregularly
shaped (baroque) pearls. Polish luster varies from dull to nearly
metallic, depending on nacre quality. Uneven fracture with pearly to
dull fracture luster.
RI 1.530 to 1.685
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW. Naturally colored black pearls show weak to moderate red
to orangy red or brownish red under LW.
SG Saltwater—2.61 to 2.85
Freshwater—2.66 to 2.78 (few are over 2.74)
Comments Key tests are appearance, RI, birefringence blink, and SG. Feels
gritty when rubbed against a tooth, while plastic and glass imitations
feel smooth. Heft can separate natural pearl from plastic imitations.
X-radiography separates natural from cultured pearl.
411
GEM IDENTIFICATION LAB MANUAL
CULTURED PEARL
General observation Colors same as natural (see descriptions below). Surface luster varies
from dull to nearly metallic, depending on nacre quality. Orient is
most commonly seen on irregularly shaped (baroque) pearls. Uneven
fracture with pearly to dull fracture luster.
Akoya (bead nucleated)—Typical size range 2 mm to 11 mm.
Mostly spherical, but might be button, pear, oval, or baroque in
shape. Color can range from neutral to near-neutral whites and
creams with rosé or green overtones, but can sometimes be yellow,
Robert Weldon/GIA pink (sometimes dyed), or blue.
Cultured pearls might show Tahitian (bead nucleated)—Typical size range 8 mm to 14 mm.
orient, especially in baroque Spherical, oval, button, drop, or baroque in shape (sometimes circled).
and circled shapes. Color can range from near-neutral silver, cream, or brown to black or
gray, to blue, green, yellowish green, or purple, with green, blue, or
rosé overtone.
South Sea (bead nucleated)—Typical size range 10 mm to 15 mm.
Spherical, near-round, oval, button, drop, or semi-baroque (sometimes
circled). Color can range from near-neutral white, cream, or silver to
yellow, yellowish orange, or blue, with green, blue, or rosé overtone.
Freshwater (usually tissue nucleated)—Typical size range 2 mm to
13 mm. Spherical, near-round, oval, button, drop, or heavily baroque
(sometimes circled). Color can range from neutral to near-neutral
grays, whites, and creams to yellows, pinks, and purples, with blue
or green overtone and orient.
RI 1.530 to 1.685
Magnification Not usually diagnostic, unless you can examine a drill-hole and detect
the bead under the nacre. Occasionally, if the nacre layer is very thin,
you can detect the “blinking” of the layers in the bead nucleus as you
roll a strand of pearls across a flat surface. Dyes might be detectable
at drill-holes or on silk strands close to drill-holes.
Fluorescence Variable. Inert to strong light blue, yellow, green, or pink under LW
and SW. Naturally colored black pearls show weak to moderate red
to orangy red or brownish red under LW.
SG 2.72 to 2.78
Comments Key tests are RI, birefringence blink, SG, and magnification. Feels
gritty when rubbed against a tooth, while both plastic and glass
imitations feel smooth. Heft can separate cultured pearl from plastic
imitations. X-radiography separates natural from cultured pearl.
Cultured pearls might be dyed, irradiated, or polymer impregnated.
Dye might be detectable as concentrations in nacre, especially at the
drill-hole. Some irradiated colors are very intense and unnatural.
Impregnation might be visible with magnification.
412
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
SHELL AMMONITE
Birefringence/doubling 0.155 (use birefringence blink Usually 0.155 (varies with mineral
method) content—use birefringence blink method)
Comments Key tests are appearance, RI, Key tests are appearance (including
birefringence blink, and magnifi- iridescence) and possibly RI. Ammonite is
cation. Items fashioned from the fossilized shell of an extinct nautilus-
abalone (paua) shell show intense like animal. It’s often polymer-impregnated
orient against a gray background. to make it more stable or improve its
appearance. Might be sold as “ammolite”
in the trade.
Maha Tannous/GIA
413
GEM IDENTIFICATION LAB MANUAL
OPAL
Species Opal
General observation Colorless, white, gray, bluish gray, brown, or black, with or without
play-of-color. Sometimes fashioned to include rock matrix as backing
when opal layer is thin (boulder opal).Vitreous to resinous polish
luster, conchoidal to uneven fracture with subvitreous to waxy
fracture luster.
RI 1.450 (+0.020/-0.080)
Birefringence/doubling None
Eric Welch/GIA
SR/DR/AGG SR, commonly with ADR due to strain
Boulder opal incorporates rock matrix into
finished pieces to improve the durability of thin Magnification Possible play-of-color patterns include very small patches or dots
opal layers. (pinfire); large areas that flash predominately one color as the gem
is moved (flash); or even, distinct patches with a “brush-stroke”
appearance (harlequin). There might also be areas that lack play-of-
color or that contain mineral inclusions or patches of rock matrix.
(Play-of-color in synthetic opal tends to be much more regular.)
Fluorescence Inert to white to moderate light blue, green, or yellow under LW and
SW. Might also phosphoresce.
SG 2.15 (+0.08/-0.90)
414
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
FIRE OPAL
Species Opal
RI 1.450 (+0.020/-0.080) (Generally between 1.420 and 1.430, but Eric Welch/GIA
might read as low as 1.370) Fire opal sometimes shows play-of-
color along with its unique bodycolor.
Birefringence/doubling None
SG 2.15 (+0.08/-0.09)
415
GEM IDENTIFICATION LAB MANUAL
General observation Opaque, uniform black bodycolor. Resembles black opal, with a dark brown
Polish often less lustrous than mottled appearance and unnatural play-of-
naturally colored black opal. color. Turns black when moisture is
Patchy or spotty play-of-color. applied to the surface, but blackness goes
away when moisture dries. Surface
Both by Shane McClure/GIA damages very easily.
Sugar-treated opals display speckled
colors against a black background. Typical cutting style Cabochons, carvings Cabochons, carvings
SR/DR/AGG SR SR
Magnification Black carbon particles visible Surface indents when a pointer probe
in and around patches of gem is pressed gently against it. Chipped
opal or filling voids in the surfaces reveal whitish opal beneath the
Smoke-treated opals typically show surrounding matrix. Play-of-color thin surface treatment.
a dark, broad texture under generally appears in a mosaic
magnification. pattern near the surface of the
stone. Chipped surfaces reveal
whitish opal beneath the thin
surface treatment.
SG 1.98 to 2.05 (generally lower Generally lower than untreated black opal
than untreated black opal)
Comments Key tests are appearance, Key tests are appearance, magnification,
magnification, RI, and possibly RI, and possibly SG.
SG.
416
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
SYNTHETIC OPAL
Fluorescence Typically moderate bluish white to yellow under LW, weak to strong
Eric Welch/GIA
blue to bluish white to yellow under SW. Phosphorescence is rare
and weak if present. Polymer-impregnated synthetic opal comes in a
variety of colors.
Newer production of untreated synthetic opal:
Colorless and white—Very weak to weak chalky blue under both
LW and SW, slightly stronger reaction to SW
Orange—Very weak red under both LW and SW (stronger under
SW)
Black—Inert to both LW and SW
Polymer-impregnated synthetic opal:
Purplish pink to orangy pink—Weak to strong orangy pink under
LW, weak to moderate orangy pink under SW
Reddish orange—Moderate pink-orange under LW, weak to moderate
pink-orange under SW
Orangy yellow—Weak yellow under LW, moderate to strong orangy
Terri Weimer/GIA
yellow under SW
Dark brown—Moderate orange under both LW and SW This polymer-impregnated synthetic
opal shows a columnar structure.
Blue to grayish blue—Inert to very weak blue under both LW and
This is a typical characteristic of all
SW synthetic opals.
White—Weak purplish blue under LW, moderate blue under SW
Gray—Very weak greenish yellow under LW, weak greenish yellow
under SW
Black—Inert to LW, very weak orange under SW
417
GEM IDENTIFICATION LAB MANUAL
Comments Key tests are appearance, RI, and Key tests are RI and SG. Fluorescence
magnification. Might be called might also be helpful.
Slocum Stone in the trade. Some
glass imitation opals appear to be
manufactured with layers of differ-
The metallic flakes that imitate
ently colored glass. They might
opal’s play-of-color in a glass
imitation are visible in resemble opal doublets. However,
transmitted light. both layers should contain gas
bubbles.
Maha Tannous/GIA
418
IDENTIFYING PHENOMENAL GEMS: PLAY-OF-COLOR, PLAY-OF-COLOR-LIKE EFFECTS, IRIDESCENCE, OR ORIENT
Key Separations for Gems with Play-of-color, Play-of-color-like Effects, Iridescence, or Orient
Key Separations Key Tests
Fire agate from opal Appearance, RI, magnification, SG, possibly fluorescence
Natural from cultured pearl Magnification (if structure is visible at drill-hole), possibly blinking and
advanced testing
Natural or cultured pearl from glass or plastic Birefringence blink, magnification, structure, possibly RI
419
GEM IDENTIFICATION LAB MANUAL
1.563 to 1.572 Sunstone labradorite feldspar Aventurine quartz, iolite, sunstone oligoclase, goldstone glass and
DR (Page 421) plastic
1.544 to 1.553 Aventurine quartz Sunstone labradorite, dyed quartzite, iolite, sunstone oligoclase,
AGG (Page 422) goldstone glass and plastic
1.542 to 1.551 Bloodshot iolite Sunstone labradorite, aventurine quartz, sunstone oligoclase,
DR (Page 423) goldstone glass and plastic
1.539 to 1.547 Sunstone oligoclase feldspar Sunstone labradorite, aventurine quartz, iolite, sunstone orthoclase,
DR or AGG (Page 424) goldstone glass and plastic
1.470 to 1.700 range Goldstone glass Sunstone labradorite, aventurine quartz, iolite, sunstone oligoclase,
SR (Page 426) sheen obsidian
1.460 to 1.700 range Goldstone plastic Sunstone labradorite, aventurine quartz, iolite, sunstone oligoclase,
SR (Page 426) sheen obsidian
420
IDENTIFYING PHENOMENAL GEMS: ADULARESCENCE, LABRADORESCENCE, OR AVENTURESCENCE
LABRADORITE LABRADORITE
Typical cutting style Faceted gems, cabochons, carvings Faceted gems, cabochons
Magnification Oregon material contains tiny orangy Repeated twinning, black needle-like Terri Weimer/GIA
yellow copper platelets, often visible inclusions, metallic-looking platelets This labradorite feldspar shows
even in facet-grade material at 10X. a multicolored flash that’s
If these are numerous enough, mostly blue, green, and yellow.
aventurescence occurs.
Comments Key tests are RI, birefringence, Key tests are appearance of phenome-
optic character, and magnification. non, RI, birefringence, optic character,
Material from Oregon is sold in the and magnification.
trade as “sunstone” even though not Terri Weimer/GIA
421
GEM IDENTIFICATION LAB MANUAL
General observation Strong blue or multicolor sheen Translucent to opaque green (due to
against almost transparent, semi- inclusions); rarely gray, yellow, or
transparent, or semitranslucent brown; with aventurescence. Vitreous
Robert Weldon/GIA body. Vitreous polish luster, uneven polish luster, granular to conchoidal
This nearly transparent labradorite to splintery fracture with vitreous to fracture with vitreous fracture luster.
shows a blue sheen. This gem is pearly fracture luster. Two cleavage
sometimes called “rainbow directions. Parting also common.
moonstone.”
Typical cutting style Cabochons Cabochons
Fluorescence Moderate chalky blue under LW, Inert to weak grayish green or reddish
weak pinkish orange under SW under LW and SW
William Videto/GIA Comments Key tests are appearance, RI, Key tests are RI, magnification,
Chrome mica inclusions cause the fracture, fluorescence, and possibly spectrum, fluorescence, and SG.
aventurescence in aventurine quartz. birefringence. Might be called
They’re visible under magnification and “rainbow moonstone” in the trade.
sometimes with the unaided eye.
422
IDENTIFYING PHENOMENAL GEMS: ADULARESCENCE, LABRADORESCENCE, OR AVENTURESCENCE
SR/DR/AGG AGG DR
Dyed quartzite shows dye con-
centrations in surface-reaching
Optic character Not applicable Biaxial negative
fractures. This feature can help
you separate it from aventurine
Pleochroism None Might show trichroism. quartz, but the mica inclusions in
Violet stones—Light violet, dark violet, and aventurine can break the surface,
yellow-brown so careful examination is required.
Blue stones—Colorless to yellow, blue-gray,
and dark violet
Spectrum Cutoff at around 450 nm, band Weak bands at 426 nm and 645 nm
between approximately 630 nm (generally not diagnostic)
and 660 nm in dyed green
material
423
GEM IDENTIFICATION LAB MANUAL
Terri Weimer/GIA
General observation Semitransparent to opaque yellow to Semitransparent to opaque, typically
Sunstone oligoclase feldspar is orange or brown, with a reddish or colorless to white, but can be orange,
less transparent than sunstone golden sheen from highly reflective yellow, or brown. Displays adulares-
labradorite feldspar.
inclusions. Called sunstone feldspar cence, sometimes also with chatoyancy
if inclusions are large enough to or asterism. Vitreous polish luster,
create distinct, glittery reflections. uneven to splintery fracture with
Vitreous polish luster, uneven to vitreous to pearly fracture luster.
splintery fracture with vitreous to Two cleavage directions, parting also
pearly fracture luster. Two cleavage common.
directions. Parting also common.
Magnification commonly reveals Fluorescence Generally inert Inert to blue under LW, orange under
centipede inclusions in moonstone SW. Might fluoresce weak pink to red
orthoclase feldspar. under LW and SW.
Comments Key tests are appearance, RI, Key tests are RI, optic character
birefringence, optic character, and (biaxial interference figure in
magnification. As physical proper- polariscope), and magnification.
ties of aventurescent oligoclase and Fluorescence and SG might also be
orthoclase feldspar overlap, advanced helpful.
testing might be needed to separate
them. Presence of adularescence
indicates orthoclase.
424
IDENTIFYING PHENOMENAL GEMS: ADULARESCENCE, LABRADORESCENCE, OR AVENTURESCENCE
Magnification Aventurescent material contains two sets Gas bubbles, stubby needle-
of reflective inclusions (fine needles and like inclusions. Might be
elongated hematite flakes). If they intersect banded. Sheen caused by
at near 90° angles, they give rise to a star. numerous oriented inclusions.
Comments Key tests are appearance, RI, and magnifi- Key tests are RI, magnifica-
cation. Optic character, fluorescence, and tion, and SG
SG might also be helpful. As physical
properties of aventurescent orthoclase and
oligoclase feldspar overlap, advanced
testing might be needed to separate them.
Presence of adularescence indicates
orthoclase.
425
GEM IDENTIFICATION LAB MANUAL
General observation Transparent to opaque, with aven- Translucent to opaque, with aventures-
turescence. Usually brown or blue, cence. Look for mold marks,
but might be any color. Filled with orange-peel effect, concave facets,
Terri Weimer/GIA
tiny copper platelets. Warm to the rounded facet junctions. Warmer to
The goldstone glass at left and touch compared to crystalline the touch than glass imitations and
the goldstone plastic at right are gemstones. Vitreous polish luster, crystalline gemstones. Low heft (SG),
popular sunstone imitations.
conchoidal fracture with vitreous dull to waxy polish luster, conchoidal
fracture luster. fracture with waxy to vitreous fracture
luster. Surface might show numerous
scratches due to low hardness (Mohs
1.5 to 3).
Typical cutting style Cabochons, beads, tablets, tumbled All styles. Can be molded to a variety
stones of shapes and finishes.
Metallic inclusions create the Fluorescence Variable, not diagnostic Variable, not diagnostic
glittery effect in this plastic sunstone
imitation. SG Usually between 2.30 and 4.50 Usually around 2.10 due to presence
of metallic inclusions
Comments Key tests are appearance, RI, Key tests are appearance, RI, and
and magnification. Low thermal magnification. Low heft (SG) and low
conductivity (warm to the touch) thermal conductivity (warm to the
might also be helpful. touch) might also be helpful.
426
SEPARATING PHENOMENAL GEMS: ADULARESCENCE, LABRADORESCENCE, OR AVENTURESCENCE
Sunstone feldspar from goldstone glass Appearance, magnification, optic character, possibly RI
Orthoclase sunstone from oligoclase sunstone Presence of adularescence indicates orthoclase. Advanced testing might
be necessary to separate orthoclase from oligoclase.
427
IDENTIFYING GLASS, PLASTIC, ASSEMBLED
STONES, ROUGH GEMS, AND SYNTHETIC
CRYSTALS
Glass and plastic can effectively imitate a wide variety of gems. These glass beads make up a convincing imitation of a pearl necklace.
429
GEM IDENTIFICATION LAB MANUAL
MOLDAVITE
Species Moldavite
RI 1.490 (+0.020/-0.010)
Birefringence/doubling None
Magnification Round and elongated gas bubbles, flow lines, roiled effect
Eric Welch/GIA
Spectrum Not diagnostic
The surface of moldavite rough is typically
bumpy and pockmarked.
Fluorescence Generally inert
SG 2.36 (+/-0.04)
Comments Key tests are RI, SR nature, magnification, and SG. Color might also
be helpful. Moldavite is a type of natural glass
430
IDENTIFYING GLASS AND PLASTIC
OBSIDIAN
Species Obsidian
RI 1.490 (+0.020/-0.010)
Birefringence/doubling None
SG 2.40 (+0.10/-0.07)
Comments Key tests are RI, SR nature, SG, and possibly magnification.
Obsidian is a type of natural glass.
431
GEM IDENTIFICATION LAB MANUAL
BLUE GLASS
GLASS
Species Glass
Prism
General observation Transparent to opaque, almost any appearance and color possible.
Look for mold marks and concave facets with slightly pitted and
535 635 uneven surfaces (the orange-peel effect). You might also see rounded
590 facet junctions, but this feature is also possible on most natural gems.
Warm to the touch compared to crystalline gemstones. Vitreous polish
Diffraction
535 635 Typical cutting style All styles. Can be faceted or molded to a variety of shapes and finishes.
590
Birefringence/doubling None
SR/DR/AGG Can be SR, SR with ADR, or AGG. Transparent material often shows
strong ADR in the form of snake-like bands and might even give a false
DR reaction during the polariscope confirmation test. Translucent-to-
semitranslucent material often shows an AGG reaction.
Magnification Often contains gas bubbles, which might be spherical, oval, elongated,
tubular, or even drawn out and appear to have tails. Cutting through
gas bubbles during fashioning leaves semicircular cavities on the
finished surface. Flow marks (swirls) and patchy color distribution are
also typical.
Tino Hammid/GIA
Spectrum Mostly not diagnostic, except for blue glass colored by cobalt, which
Glass is a versatile material that can effectively produces bands at 535 nm, 590 nm, and 635 nm. The central band is
imitate almost any thinner than the two outer ones. Red glass colored by selenium might
transparent-to-opaque gem
show a broad absorption in the green and orange-yellow areas of the
material.
spectrum.
Fluorescence Variable and not diagnostic, but often appears chalky under both LW
and SW
Comments Key tests are RI, SR nature, and magnification. Low thermal conduc-
tivity (warm to the touch) might also be helpful. The optical and
physical properties of glass rarely match the optical and physical
properties of the gems it imitates.
John Koivula/GIA
Molded glass imitations Swirl marks and elongated This manmade glass jewel
generally have concave facets, gas bubbles are typical displays typical swirl marks.
rounded facet junctions, and features of manmade glass.
pitted surfaces.
432
IDENTIFYING GLASS AND PLASTIC
Transparent gemstones Gems of all colors and colorless gems, especially diamond, ruby,
sapphire, emerald, and tanzanite
Imitations that simulate Various types of glass beads, produced with or without iridescent
orient coatings, to imitate natural and cultured pearls
This color-change glass appears purplish under incandescent “Opalized” glass is used as an
lighting (left) and green under fluorescent lighting (right). opal imitation, but it lacks the
play-of-color displayed by the
natural opal at left.
433
GEM IDENTIFICATION LAB MANUAL
Glass from pearl and cultured pearl Texture (glass is smooth when rubbed against a tooth), birefringence
blink
Glass from natural glass (moldavite and obsidian) Magnification, possibly color and RI. Caution: gas bubbles and flow
lines occur in both materials. Advanced testing might be necessary.
Glass from transparent SR and DR gem materials Magnification, possibly spectrum for some colors. Combination of RI,
polariscope reaction, and SG, as glass rarely duplicates all the proper-
ties of the gem materials it imitates.
Glass from fluorite Cleavage, RI (glass rarely below 1.48), magnification, possibly SG
434
IDENTIFYING GLASS AND PLASTIC
PLASTIC
Species Plastic
General observation Transparent to opaque, almost any appearance and color possible.
Look for mold marks and concave facets with slightly pitted and
uneven surfaces (the orange-peel effect). You might also see rounded
facet junctions, but this feature is also possible on most natural
gems. Feels warm to the touch compared to crystalline gemstones
and even compared to glass. Waxy to vitreous polish luster, con-
choidal to uneven fracture with dull to vitreous fracture luster. Facet
edges often abraded due to low hardness (Mohs 1.5 to 3).
Typical cutting style All styles. Can be molded to a variety of shapes and finishes.
Robert Weldon/GIA
RI 1.460 to 1.700 (generally low) Plastic’s lower luster and polish quality make it
a better imitator of translucent-to-opaque gems
Birefringence/doubling None than of transparent ones.
Magnification Flow lines, patchy color distribution, and gas bubbles are typical.
Gas bubbles might be spherical, oval, elongated, tubular, or even
drawn out and appear to have tails. Cutting through gas bubbles
during fashioning leaves semicircular cavities on the finished surface.
Comments Key tests are RI, magnification, and possibly SG. Burns with a hot
point, generally producing an acrid odor, although other possible
odors are camphor, carbolic acid, vinegar, sweet fruit, formaldehyde,
fish, and sour milk. This test is destructive. Do not use it on GIA
stones. The optical and physical properties of plastic rarely match
the optical and physical properties of the gems it imitates.
Copper foil inclusions create the glittery effect This plastic imitation shows typical orange-peel
in this plastic sunstone imitation. surface texture and rounded facet edges.
435
GEM IDENTIFICATION LAB MANUAL
Transparent gemstones Gems of all colors and colorless gems, including diamond, ruby,
sapphire, and emerald
Translucent-to-opaque Gems of all colors, especially jadeite, nephrite, turquoise, and all
gemstones varieties of chalcedony
Organic gems Especially pearl and amber, but also red-to-pink and black coral,
Maha Tannous/GIA shell, ivory, jet, and tortoise shell
Plastic opal imitations can display true
play-of-color. RI and SG usually separate Aventurescent imitations Plastic with copper foil-strip inclusions can resemble goldstone
them from natural and synthetic opal. glass (copper inclusions can raise the material’s SG)
Imitations with orient Materials that imitate both pearl and mother-of-pearl shell
436
IDENTIFYING ASSEMBLED STONES
GARNET-AND-GLASS DOUBLET
garnet
glass
colorless
synthetic spinel
SYNTHETIC SPINEL TRIPLET
colored cement
layer
Eric Welch/GIA
colorless synthetic
spinel Assembled stones come in a wide range of
colors. Careful observation with the unaided
eye and under magnification separates them
SAPPHIRE AND SYNTHETIC from the gems they imitate.
RUBY DOUBLET
natural sapphire
synthetic ruby
OPAL DOUBLET
opal layer
backing
OPAL TRIPLET
colorless dome
opal layer
backing
Peter Johnston/GIA
Assembled stones consist of two or more parts cemented or fused together. You’ll usually see a
separation plane where the parts meet. You might also see differences in luster or wear if the parts
are made of different materials.
437
GEM IDENTIFICATION LAB MANUAL
Assembled Stones
RI and SR/DR/AGG Gem Material Commonly confused with:
1.750 to OTL top Garnet-and-glass doublet Manufactured in all colors; also some face-up colorless
Base usually in 1.600s (Page 439)
Both SR
1.762 to 1.770 top Synthetic sapphire and strontium titanate doublet Diamond
DR (Page 441)
OTL base
SR
1.666 to 1.680 (1.66 spot Jadeite triplet Fine-color natural green jadeite
reading common) (Page 442)
AGG
1.54 to 1.55 spot reading Star foilback quartz Star ruby or star sapphire, other colors possible
DR (Page 443)
1.450 Synthetic opal doublet Natural opal, opal doublet, opal triplet
Usually too opaque to test (Page 446)
1.450 Synthetic opal triplet Natural opal, opal doublet, opal triplet
Usually too opaque to test (Page 446)
Variable properties, Glass (foilback, triplet) All colors possible (backing adds brilliance, color, or
depending on material (Page 447) phenomenon)
438
IDENTIFYING ASSEMBLED STONES
General observation All colors possible, even colorless. Although the garnet cap is red,
the glass base determines the doublet’s face-up color. You should be
able to detect a difference in luster and polish quality between the
Face down, a garnet-and-glass doublet of
vitreous to subadamantine garnet cap and the vitreous glass base.
almost any color displays a distinctive red ring.
With the stone table-down against a white background, you should be This is due to the presence of the garnet cap.
able to see a red ring in all colors except red and violet, or unless the
garnet cap is very thin.
Spectrum If the garnet cap is thick enough, you might see a faint almandite
spectrum consisting of three bands in the green and yellow of the
spectrum at 505 nm, 527 nm, and 575 nm.
Fluorescence The garnet cap is inert to both LW and SW. The glass base might
fluoresce any color, but often appears chalky under both LW and SW.
View parallel to the girdle plane.
Mike Havstad/GIA
Comments Key tests are luster differences between the components, RI, and In a garnet-and-glass doublet, the luster
magnification. Fluorescence might also be helpful. difference between the glass base and the
garnet cap should be apparent.
439
GEM IDENTIFICATION LAB MANUAL
SAPPHIRE AND SYNTHETIC SAPPHIRE DOUBLET SAPPHIRE AND SYNTHETIC RUBY DOUBLET
Species Sapphire and synthetic sapphire doublet Sapphire and synthetic ruby doublet
Construction Natural sapphire crown, normally green or dark greenish Crown is normally green or dark greenish blue natural
blue. Flame-fusion synthetic blue sapphire pavilion. sapphire, pavilion is flame-fusion synthetic ruby.
Separation plane usually located at the girdle. Separation plane usually located at the girdle.
General observation Blue, violetish blue, or greenish blue, often dark in tone. Red, purplish red, orangy red. Might look deceptively
Might look deceptively natural. Expect shallow to very natural. Expect shallow to very shallow crown, deep
shallow crown, deep pavilion, and non-calibrated or pavilion, and non-calibrated or near-calibrated size.
near-calibrated size.
RI Natural sapphire crown—Usually 1.762 to 1.770 Natural sapphire crown—Usually 1.762 to 1.770
(+0.009/-0.005) (+0.009/-0.005)
Flame-fusion synthetic sapphire pavilion—1.762 to Flame-fusion synthetic ruby pavilion—1.762 to 1.770
1.770
Birefringence/doubling 0.008 to 0.010 (crown and pavilion) 0.008 to 0.010 (crown and pavilion)
Magnification Crown—Contains natural inclusions such as high- and Crown—Natural inclusions such as high- and low-relief
low-relief crystals, silk, and hexagonal growth banding. crystals, silk, and hexagonal growth banding. Separation
Gas bubbles in the cement layer at the separation plane. plane shows gas bubbles in the cement layer.
Pavilion—Gas bubbles and curved color banding Pavilion—Gas bubbles, curved striae
Spectrum Observe through crown and pavilion separately: Observe through crown and pavilion separately:
Crown—Generally a natural green sapphire spectrum, Crown—Generally a natural green sapphire spectrum,
with three strong lines in the violet-blue at 450 nm, with three strong lines in the violet-blue at 450 nm,
460 nm, and 471 nm due to iron 460 nm, and 471 nm due to iron
Pavilion—Not diagnostic Pavilion—Typical ruby spectrum, with fine lines in the
orange-red at 659 nm, 668 nm, and 693 nm, and a broad
absorption over the yellow and most of the green at about
500 nm to 610 nm. Also two fine, dark lines in the blue at
468 nm and 476 nm and a strong cutoff in the violet.
Fluorescence Crown generally inert to LW and SW. Pavilion inert to Crown generally inert to LW and SW. Pavilion moderate
LW, but usually weak-to-moderate chalky blue to SW. to strong red under both LW and SW. View parallel to the
View parallel to the girdle plane. girdle plane.
Comments Key tests are general observation and magnification. Key tests are general observation and magnification.
Spectrum and fluorescence might also be helpful. Spectrum and fluorescence might also be helpful.
Immersion makes green crown and blue pavilion clearly Immersion makes green crown and red pavilion clearly
visible. visible.
The separation plane is obvious in this A separation plane divides this doublet’s natural
doublet. You can also see green bodycolor green sapphire crown from its synthetic ruby
in the natural sapphire crown and curved pavilion.
color banding in the flame-fusion synthetic
sapphire pavilion.
440
IDENTIFYING ASSEMBLED STONES
Species Synthetic sapphire and strontium Synthetic spinel and strontium titanate doublet
titanate doublet
Construction Top is colorless flame-fusion synthetic Top is colorless flame-fusion synthetic spinel,
sapphire, base is strontium titanate. base is strontium titanate. Often joined below the
Often joined below the girdle plane. girdle plane.
General observation Colorless. Synthetic sapphire top has Colorless. Synthetic spinel top has Mohs hardness
Mohs hardness of 9. Strontium titanate of 8. Strontium titanate base has Mohs hardness of
base has Mohs hardness of only 5 to 6, only 5 to 6, so it often has poor polish, scratches,
so it often has poor polish, scratches, and abraded facet junctions. Top has no noticeable
and abraded facet junctions. Top has no fire, base has extreme fire due to strontium
noticeable fire, base has extreme fire titanate’s 0.190 dispersion value.
due to strontium titanate’s 0.190
dispersion value.
Magnification Top might contain gas bubbles that can Top might contain gas bubbles that can be thread-
resemble needles and occur singly or like or rarely angular. Base might contain small
in string-like arrangements. Base might gas bubbles and have surface polishing marks due
contain small gas bubbles and have to low hardness. Synthetic spinel top has very low
surface polishing marks due to low relief in methylene iodide or mineral oil, while the
hardness. Synthetic sapphire top has strontium titanate base has significantly greater
very low relief in methylene iodide or relief.
mineral oil, while the strontium titanate
base has significantly greater relief.
Fluorescence Not usually diagnostic. Top is inert to Top is moderate to strong chalky blue or strong
weak bluish white, base is generally greenish blue under SW, sometimes weak green
inert. under LW. Base is generally inert.
Comments Key tests are general observation, RI, Key tests are general observation, RI, and
and magnification with immersion. magnification with immersion.
John Koivula/GIA
441
GEM IDENTIFICATION LAB MANUAL
Construction Crown and pavilion of colorless Three pieces of carefully cut translu- Crown and pavilion of colorless or
flame-fusion synthetic spinel joined cent white jadeite in a hollow very lightly colored beryl, joined by
by a colored cement layer, usually at construction filled with a green colored cement layer, usually at the
the girdle plane jelly-like substance that gives the girdle plane
assembly its color.
General observation Usually green, yellow-green, or Green color imitates fine green Usually green to imitate emerald, but
violet to purple, but might be any jadeite. Surface has typical jadeite might be any other color. If you shine
color. When you shine a penlight characteristics of vitreous to greasy a penlight through the girdle area from
through the girdle area from behind, polish luster and dimpled surface. behind, crown and pavilion might
crown and pavilion might appear appear colored while girdle appears
colored, while girdle appears color- colorless.
less.
RI 1.728 (+0.012/-0.008) (crown and 1.666 to 1.680 (1.66 spot reading 1.577 to 1.583 (crown and pavilion)
pavilion) common)
Magnification Immersion reveals colorless crown Gas bubbles in the jelly-like layer or in Look for gas bubbles in the
and pavilion joined by a flat, colored the contacts between the components cement layer at the separation
cement layer at the girdle. Gas plane. Immersion reveals assembly
bubbles often visible in the cement components.
layer.
Spectrum Not diagnostic Same as dyed green jadeite, with a Not diagnostic
single broad band in the red-orange
area. Naturally colored green jadeite
has three lines in the same area.
Fluorescence Variable. Cement layer might Inert Variable. Cement layer might fluoresce
fluoresce differently from synthetic differently from beryl portion, which is
spinel portion, which is sometimes generally inert.
weak green under LW and moderate
to strong chalky blue or strong
greenish blue under SW.
Comments Key tests are general observation, Key tests are general observation, Key tests are general observation, RI,
RI, and magnification. magnification to reveal the assembly, and magnification.
and spectrum to demonstrate the
artificial nature of the assembled
material’s color.
John Koivula/GIA
Synthetic spinel triplets duplicate the appearance of a variety of Magnification with immersion reveals Although the separation plane appears
transparent colored gems. the separation plane in a synthetic colorless in this beryl triplet, it actually
spinel triplet. contains colored cement.
442
IDENTIFYING ASSEMBLED STONES
Construction Crown and pavilion of rock Quartz crown and beryl pavilion, or some- Star quartz backed by foil or some
crystal quartz, joined by colored times beryl crown and quartz pavilion. Joined other nontransparent substance to
cement layer by colored cement, usually at the girdle enhance or create a star and cause
plane. color similar to star sapphire or
star ruby.
General observation Usually green to imitate emerald, Usually green to imitate emerald, but might Usually red or blue, but other
but might be any other color. be any other color. If you shine a penlight colors are possible. If you examine
If you shine a penlight through through the girdle area from behind, crown the stone parallel to the girdle,
the girdle area from behind, and pavilion might appear colored while you’ll see the usually pink color
crown and pavilion might appear girdle appears colorless. of the quartz unchanged by the
colored while girdle appears color of the backing.
colorless.
RI 1.544 to 1.553 (crown and Rock crystal quartz crown (or pavilion)— 1.54 or 1.55 spot reading
pavilion) 1.544 to 1.553
Beryl pavilion (or crown)—1.577 to 1.583
Birefringence/doubling 0.009 (crown and pavilion) Rock crystal quartz crown (or pavilion)— Usually not detectable
0.009
Beryl pavilion (or crown)—0.005 to 0.009
Magnification Look for gas bubbles in the Look for gas bubbles in the cement layer at Typical quartz characteristics
cement layer at the separation the separation plane. Immersion reveals such as liquid, two-phase, and
plane. Immersion reveals assembly components. three-phase inclusions; negative
assembly components. crystals; and solid mineral crystals
or needles
Comments Key tests are general observation, Key tests are general observation, RI, and Key tests are general observation
RI, and magnification. magnification. and RI.
443
GEM IDENTIFICATION LAB MANUAL
MABÉ PEARL
General observation Dome-shaped, with a flat or low-domed back. Unmounted, its nature
is evident due to a clear junction plane between pearl nacre and
mother-of-pearl backing. Mounting conceals the separation plane.
Maha Tannous/GIA
Mabé pearls typically range in size from 8 to 18 mm, rarely over 20
A cross-section of a dyed black mabé mm. They might appear as symmetrical domes, pears, or heart
assembled cultured blister pearl
reveals its construction.
shapes. Colors are typically neutral to near-neutral whites and
creams with rosé or green overtones, but can sometimes be yellow-
ish. Mabés are also cultured from abalone, producing gems with
striking pink, blue, or green orient against a gray bodycolor. Surface
luster varies from dull to nearly metallic, depending on nacre quality.
Uneven fracture with pearly to dull fracture luster.
RI 1.530 to 1.685
Magnification Not usually diagnostic, unless the separation plane and mother-of-
pearl backing are visible.
Comments Key tests are RI, birefringence blink, and magnification. Typical
dome shape, flat back, and size are distinctive. Feels gritty when
rubbed against a tooth, while plastic and glass imitations feel
smooth.
444
IDENTIFYING ASSEMBLED STONES
Construction Thin piece of opal, commonly backed Colorless cabochon cap, usually rock crystal
by dyed black chalcedony or possibly quartz or colorless glass, glued to a thin piece
by glass, potch opal, or matrix. Glued of opal with colorless cement, then glued to a
with black cement. backing of dyed black chalcedony, glass, or
potch opal using black cement. Some manu-
facturers use tiny chips of opal rather than a
complete opal layer and sell the finished
stones as “opal mosaic triplets.”
General observation Assembled nature should be obvious Resembles good-quality black or gray opal.
when you examine the stone from the The mosaic pattern of the opal layer in an
side. opal mosaic triplet is readily apparent and
easily identified. Eric Welch/GIA
Magnification Not diagnostic unless the separation Not diagnostic unless the separation plane
plane and backing material are visible. and backing material are visible. Opal layer
Opal cap might show a variety of play- might show a variety of play-of-color pat-
of-color patterns, which include very terns, which include very small patches or
small patches or dots; large areas that dots; large areas that flash predominately one
flash predominately one color as the color as the gem is moved; or even, distinct
gem is moved; or even, distinct patches patches with a “brush-stroke” appearance.
with a “brush-stroke” appearance. There might be areas that lack play-of-color
There might also be areas that lack or that contain mineral inclusions or patches
play-of-color or that contain mineral of rock matrix. Synthetic opal has a much
inclusions or patches of rock matrix. more regular play-of-color pattern.
Synthetic opal has a much more regular
play-of-color pattern.
Comments Key tests are appearance and magnifi- Key tests are appearance and magnification.
cation. A cutter might leave a naturally If the gem isn’t mounted and you can
occurring layer of matrix or potch as a examine it from the side, its assembled
backing on natural opal. Don’t mistake nature should be obvious.
this type of natural opal for an assem-
bled stone.
445
GEM IDENTIFICATION LAB MANUAL
Construction Thin piece of synthetic opal, Same as the opal triplet, but with a thin
commonly backed by dyed piece or pieces of synthetic opal instead
black chalcedony or possibly by of natural opal
glass, potch opal, or matrix.
Glued with black cement.
RI Synthetic opal portion should You can’t take the synthetic opal layer’s
give a typical RI of 1.450 or RI, but you might get a quartz or glass
slightly lower RI reading from the cap. This will alert
you that the gem isn’t solid synthetic
opal.
Magnification Synthetic opal portion shows Synthetic opal portion shows mosaic
mosaic patches of color with a patches of color with a snakeskin or
snakeskin or scale-like structure scale-like structure or wavy patterns. If
or wavy patterns. If unmounted, unmounted, the separation plane and
the separation plane and back- backing material might be visible.
ing material might be visible.
Comments Key tests are appearance and Key tests are appearance and
magnification. magnification.
446
IDENTIFYING ASSEMBLED STONES
Species Glass triplet Foilback (list species of material involved—for example, foilback
quartz, foilback glass, etc.)
Construction Colorless cabochon cap, usually rock crystal or Any material with foil or a nontransparent coating covering the back
colorless glass, glued to a thin piece of glass facets to add brilliance, color, or a phenomenon
imitation opal with colorless cement, then
glued to a backing of dyed black chalcedony
or glass using black cement.
General observation Resembles good-quality black or gray opal. All colors possible. Foilbacking is obvious unless the stone is
The glass layer that imitates opal often contains mounted. A transparent gem that’s foilbacked transmits little if any
multicolored, iridescent, metallic foil inclusions light through the backing. Virtually any gem material or imitation
that resemble cellophane in transmitted light. might be foilbacked, so many different properties are possible. When
present, note foilbacking in your identification.
RI You can’t take the imitation opal layer’s RI, Varies, depending on material
but you might get a quartz or glass RI reading
from the cap. This will alert you that the gem
isn’t opal.
Magnification Magnification might reveal gas bubbles. Opaque metallic foil shows on pavilion or cabochon base
Comments Key tests are appearance and RI. If the gem Very distinctive appearance. Rhinestones are foilbacked diamond
isn’t mounted and you can examine it from the imitations usually made of glass.
side, its assembled nature should be obvious.
Robert Weldon/GIA
447
GEM IDENTIFICATION LAB MANUAL
IDENTIFYING NATURAL
The Seven Crystal Systems
Minerals are divided into seven crystal systems based on ROUGH GEMS
the shape and arrangement of their crystal faces and the Although most of the gems you’ll encounter are
angular relationships between them. fashioned, you might occasionally have to identify a
rough gem. Fortunately, many gem crystals have
distinctive shapes that can help you recognize them.
A rough gem’s characteristic external crystal shape
or form is called its habit. It’s a valuable clue to a
rough gem’s identity. Basic knowledge of crystal
habits and rough-gem characteristics can help you
spinel garnet avoid costly mistakes. For example, it can help you
Cubic
separate rough ruby from rough spinel, and either
one from rough red garnet or tourmaline. These are
essential separations for any busy gem business.
Gemologists classify gems into seven categories,
zircon
called crystal systems, by studying the shape and
Tetragonal arrangement of their crystal faces and the angular
relationships between them. Crystals that belong to
the cubic crystal system are the most symmetrical,
while those belonging to the triclinic crystal system
are the least.
apatite beryl Cubic (or isometric)—Diamond, fluorite, garnet,
Hexagonal pyrite, spinel
Tetragonal—Scapolite, zircon
Hexagonal—Apatite, beryl
Trigonal (or rhombohedral)—Calcite, corundum,
quartz, tourmaline
quartz corundum Orthorhombic—Andalusite, chrysoberyl, danburite,
Trigonal
iolite, peridot, topaz, zoisite (tanzanite)
Monoclinic—Diopside, epidote, feldspar (orthoclase),
spodumene
Triclinic—Feldspar (amazonite), kyanite
Monoclinic
spodumene
Triclinic feldspar
Peter Johnston/GIA
448
IDENTIFYING NATURAL ROUGH GEMS
Beryl
DESCRIBING NATURAL CRYSTALS AND ROUGH GEMS pinacoid
termination
These are some of the terms that gemologists use to describe rough gems:
Anhedral—Lacking obvious crystal faces, like many gems that were tumbled in rivers
hexagonal cross section
Bipyramid—Shape with a pyramid at each end All by Peter Johnston/GIA
Dome—Termination made up of a variety of differently shaped crystal faces on the end of a Peridot pyramid-like
prism termination
Euhedral—Well formed, with sharp crystal faces, like most gems from pegmatite pockets prism
Pinacoid—Shape with a flat face at one or both ends Peridot forms in the orthorhombic
crystal system. Its crystals are often
Prismatic crystal or prism—Columnar crystal with 3, 4, 6, 8, or 12 parallel faces rounded or irregular rather than well
formed.
Pyramid—Shape with equal near-triangular faces that often meet in a point
Diamond
one of 8 triangular
Striations—Parallel growth markings, which can be horizontal, as on quartz and corundum octahedral faces
crystals, or vertical, as on tourmaline and topaz crystals
trigons
Tabular—Short and flattened crystal habit
prism
flat 6-sided
prism re-entrant angle
vertical striations
Tourmaline forms in the trigonal Corundum forms in the trigonal Chrysoberyl is an orthorhombic
crystal system. Its typical habit crystal system. Typical habits crystal that usually forms as a
is an elongated triangular are tabular prisms like this ruby cyclic twin. This formation looks
prism with vertical striations. crystal as well as elongated like three crystals growing
bipyramids. together around a central point.
449
GEM IDENTIFICATION LAB MANUAL
CLEAVAGE
Besides shape, cleavage is another factor that can help you identify rough gemstones. Cleavage is
a smooth, flat break in a gemstone parallel to planes of atomic weakness, caused by weak or
fewer bonds between atoms, or both. The appearance of a gem’s cleavage surfaces depends on its
crystal structure. Gemologists describe cleavage with these terms:
Perfect—A gem’s cleavage surfaces are perfectly smooth, often appearing polished (fluorite, for
example)
Easy—The gem or mineral cleaves easily with only a sharp blow (topaz, for example)
Difficult or imperfect—Cleavage is present, but hard to develop. The gem won’t break easily
along a cleavage plane (beryl, for example)
PARTING
Calcite has perfect cleavage in three Topaz has basal cleavage, which The cleavage planes in this This ruby’s large, flat crystal
directions, resulting in smooth cleavage means any cleavage break would be single-crystal rhodochrosite “face” is actually a break
surfaces. parallel to the crystal’s base. resulted in step-like surfaces. called parting. It’s parallel to
one of the gem’s twinning
planes.
450
IDENTIFYING NATURAL ROUGH GEMS
Beryl Hexagonal 1, very difficult 458 Six- or twelve-sided prism, sometimes with pyramids
Tourmaline Trigonal None 461 Elongated, striated prism with rounded triangular cross section
Spodumene Monoclinic 2, perfect 467 Elongated, striated prism with irregular terminations
Amazonite feldspar Triclinic 2, perfect 467 Blocky prism with wedge-shaped faces
Oligoclase feldspar Triclinic 2, perfect 468 Blocky prism with wedge-shaped faces
451
GEM IDENTIFICATION LAB MANUAL
Species Diamond
Prism
Spectrum Most near-colorless to light yellow stones show the “cape” line
at 415.5 nm. (Cooling diamond in liquid nitrogen helps make its
spectrum more visible.)
SG 3.52
Comments Key tests are crystal habit, distinctive growth marks (trigons), and
Maha Tannous/GIA spectrum.
The well-formed octahedron is a common
rough diamond habit.
Diamond crystals are This macle—a flattened and Distinctive trigons occupy
sometimes rounded dodeca- twinned diamond crystal— the surface of this octahedral
hedrons. has raised triangular growth diamond crystal.
markings.
452
IDENTIFYING NATURAL ROUGH GEMS
FLUORITE (FLUORSPAR)
Species Fluorite
Mohs hardness 4
Toughness Poor
SG 3.18
Comments Key tests are distinctive habit, low hardness, four cleavage directions,
and possibly fluorescence. The Iceland spar variety of calcite can
look similar, but has only three cleavage directions. Calcite’s strong
doubling also distinguishes it from SR colorless fluorite. Fine,
untwinned, cube-shaped crystals and interpenetrant twinned cubes
are valued by collectors as mineral specimens. Octahedral cleavage
pieces are commonly sold at rock and mineral shows.
453
GEM IDENTIFICATION LAB MANUAL
ALMANDITE GARNET
GARNET
orange, red-orange
Grossularite—Near-colorless to orange, yellow, or brown, to very pale
green to dark green
505 575 Hessonite—Medium to dark orange to brownish orange
527 Tsavorite—Medium to dark green to yellowish green
Andradite—Yellow to slightly greenish yellow or brown, to green
The main features of almandite’s spectrum are Demantoid—Green through yellow-green
three very strong bands at 505 nm, 527 nm,
and 575 nm in the green and yellow areas. Group Garnet
SPESSARTITE GARNET Appearance Transparent to opaque, usually dark red to purple, but might be
orange, yellow, brown, or dark to very pale green
Common habits Dodecahedron and trapezohedron (a crystal form with 24 equal faces).
412 432
Mixtures of these two forms are also common. Often found as water-
424 worn crystals.
Diffraction
Cleavage None
Key features of spessartite’s spectrum are Spectrum Almandite, pyrope-almandite (including rhodolite)—Strong bands in
bands in the violet at 412 nm, 424 nm, and the green and yellow of the spectrum at 505 nm, 527 nm, and 575 nm
432 nm, along with bands at 505 nm, 527 nm, Spessartite—Manganese-related bands at 412 nm, 424 nm, and
and 575 nm in the green-yellow. 432 nm—which sometimes merge to form a cutoff at around 430 nm—
along with iron-related bands at 505 nm, 527 nm, and 575 nm.
Andradite—Dark band at 440 nm
Demantoid—Dark band at 443 nm in yellowish green stones. Cutoff
below 443 nm with fine lines at 620 nm, 632 nm, 693 nm, and 700 nm
in rich green stones.
SG 3.61 to 4.15
Robert Weldon/GIA
454
IDENTIFYING NATURAL ROUGH GEMS
Prism
Appearance Opaque, metallic, “brassy” Transparent to opaque orange to red
yellow and pink; purple, blue, and violet to
black
Diffraction
Common habits Cube with parallel striations, Octahedron. Well-formed crystals are
dodecahedron with five- fairly common. Might also form flat-
sided crystal faces (so tened twin crystals that resemble
distinctive that gemologists diamond macles (spinel twins).
call it a pyritohedron),
and interpenetrating twin Red spinel’s spectrum often shows closely
crystals. Might also be spaced lines in the red, with the strongest one
massive. at 686 nm. There’s also broad absorption in the
green area.
Cleavage None Not visible in gem-quality
NATURAL BLUE SPINEL COLORED BY IRON
material
Prism
Toughness Good Good
459
Spectrum Not diagnostic Red spinel—Strong chromium 480
spectrum with a closely spaced group
Diffraction
of up to ten fluorescent lines in the red,
with the strongest ones at 684 nm and
686 nm. There are more lines at
632 nm, 642 nm, 650 nm, 656 nm,
459
665 nm, and 675 nm, plus a broad 480
absorption of the green area of the
spectrum.
In its spectrum, natural blue spinel colored by
Blue spinel—Strong, broad band
iron shows bands in the blue at 459 nm and
centered on 459 nm, and a strong but 480 nm. Bands at 553 nm, 593 nm, and
much narrower band at 480 nm. Also 632 nm are not as sharp.
diffuse bands centered on 553 nm,
593 nm, and 632 nm.
it from gold. separate spinel from similarly colored Although spinel usually crystallizes as
corundum or garnet. Dichroscope an octahedron, a flattened twin crystal
separates spinel from similarly colored resembling a diamond macle is also
common.
corundum or tourmaline.
Terri Weimer/GIA
455
GEM IDENTIFICATION LAB MANUAL
SCAPOLITE ZIRCON
Zircon crystals are typically four-sided prisms Comments Cleavage and SG separate Key tests are spectrum and SG.
with pyramid-shaped terminations. scapolite from similarly Shows uranium spectrum and
colored corundum, tourma- moderate to high heft. Found
line, topaz, and spodumene. mainly in alluvial deposits, so
Spectroscope might be helpful crystals might be little more than
for pink stones. Fluorescence rounded pebbles. Doubling might
might be helpful for separating be visible if rough is transparent
colorless to yellow scapolite enough.
from similarly colored quartz.
ZIRCON
Prism
653.5
Diffraction
653.5
456
IDENTIFYING NATURAL ROUGH GEMS
APATITE
Species Apatite
Common habits Six-sided prism terminated by a pyramid. Might also form flattened,
tabular, six-sided prisms with numerous faces, terminated by flat
faces (pinacoids).
Mike Havstad/GIA
Cleavage Imperfect, in two directions (rarely seen) Apatite crystals often form as multi-sided
prismatic crystals with pyramid terminations.
Mohs hardness 5
Toughness Fair
SG 3.18
Comments Spectrum might help identify yellow or colorless stones. Has higher
SG than similarly colored beryl, danburite, feldspar, tourmaline, and
quartz, but lower SG than topaz and corundum.
YELLOW APATITE
Prism
Diffraction
457
GEM IDENTIFICATION LAB MANUAL
EMERALD
BERYL
Species Beryl
Diffraction
Appearance Rich green to light green to light-toned bluish green and greenish
blue, as well as yellow, red, pink, and colorless
646 683
662
Crystal system Hexagonal
Emerald’s spectrum features distinct lines at
Common habits Elongated or columnar, six-sided or twelve-sided prism terminated
680.5 nm and 683 nm, less distinct lines at
646 nm and 662 nm, and a broad absorption by flat faces, sometimes with striations along its length. Aquamarine
between 580 nm and 630 nm. crystals tend to be more columnar than emerald crystals, and they’re
often terminated by pyramid faces. Morganite (pink beryl) crystals
tend to be much shorter, flatter combinations of six-sided prisms and
pyramid faces
Toughness Poor (many emerald crystals are heavily fractured) to good (other
beryl varieties)
Spectrum Emerald—Distinct lines at 680.5 nm and 683 nm, less distinct lines
at 646 nm and 662 nm, a broad band between 580 nm and 630 nm,
and almost complete absorption of the violet
SG 2.72
Emerald crystals typically form Aquamarine usually grows as Morganite crystals are gener-
as six-sided prisms with a prismatic crystal with pina- ally more flattened and tabular
pinacoid terminations. coid terminations. It’s often than the crystals of other beryl
more columnar than emerald. varieties.
458
IDENTIFYING NATURAL ROUGH GEMS
Species Calcite
Common habits Various types of prisms, often six-sided, but usually seen as
rhombohedral cleavage pieces
SG 2.70
459
GEM IDENTIFICATION LAB MANUAL
greenish blue
Other colors—Describe by color (for example, orange sapphire, etc.)
468 693
476 Species Corundum
Diffraction
The spectra of natural and synthetic rubies and Common habits Most common ruby habit is a flattened, tabular, six-sided prism
pink sapphires show lines at 659 nm, 668 nm, terminated by flat faces, often with raised triangular growth markings
and 693 nm, a broad absorption between or fine lines intersecting at 120º or 60º angles. Sapphire crystals are
500 nm and 610 nm, and lines in the blue at usually tapering hexagonal bipyramids, barrel shapes, or tabular
468 nm and 476 nm. There’s also a strong cut- prisms. Bipyramidal crystals often have horizontal striations.
off in the violet. Purple sapphire might show a
mixture of ruby-type and sapphire-type spectra. Cleavage None, but twinned gems might show parting
Spectrum Ruby, pink and purple sapphire, orange and dark pinkish orange
sapphire—Chromium spectrum with fine lines at 659 nm, 668 nm,
450 471 and 693 nm (often appears as a bright fluorescent line), and a broad
460 absorption at approximately 500 nm to 610 nm. Two fine, dark lines
at 468 nm and 476 nm distinguish ruby from red garnet and spinel.
Diffraction
There’s also a strong cutoff in the violet. Purple sapphire might show
a mixture of ruby-type and sapphire-type spectra, with chrome lines
in the red and iron bands in the blue.
450 471 Sapphire and green and iron-rich yellow sapphire—Iron spectrum
460
with three strong lines in the violet-blue at 450 nm, 460 nm, and
471 nm. The 450-nm band is usually the strongest.
The spectra of natural blue and green Pale orange sapphire—Might show a vague chrome line around
sapphires show bands at 450 nm, 460 nm, and 690 nm, vague, broad absorption between 500 nm and 600 nm, and a
471 nm. The 450-nm band is usually the cutoff around 450 nm.
strongest.
SG 4.00
460
IDENTIFYING NATURAL ROUGH GEMS
Appearance Transparent to opaque, almost all colors. Transparent to opaque. All colors possible, Transparent to opaque brown-
Colored varieties often display color as well as distinctive color zoning parallel ish to yellowish green to
zoning. to length or in cross-section (watermelon orangy brown, or opaque
tourmaline) with cross-shaped pattern
(chiastolite). Transparent
crystals show strong eye-
visible pleochroism.
Common habits Six-sided prism, usually with distinctive Very distinctive elongated triangular or Long, slender, four-sided
horizontal striations and pyramid-like six-sided prism with rounded triangular prisms with pyramid or dome-
termination cross-section, almost always with very shaped terminations
strong vertical striations parallel to its
length
Comments Distinctive crystal habit and lower Distinctive crystal habit and SG separate Crystal shape and SG
SG distinguish quartz from similarly tourmaline from similarly colored corun- distinguish andalusite from
colored topaz, corundum, spodumene, dum, spodumene, chrysoberyl, andalusite, tourmaline, zoisite, and
tourmaline, and corundum. Lack of scapolite, beryl, and quartz. Strong epidote. Both epidote and
cleavage separates quartz from feldspar. dichroism separates it from SR spinel and zoisite also show cleavage,
garnet. while andalusite doesn’t.
Robert Weldon/GIA
461
GEM IDENTIFICATION LAB MANUAL
Species Chrysoberyl
Common habits Long prismatic crystals terminated by pyramid faces or domes. Triple
interpenetrant twins forming a hexagonal shape, with notch-shaped
In the purple-red pleochroic direction, alexandrite’s depressions (re-entrant angles) marking the boundary of each twin
spectrum has strong lines in the red at 678 nm crystal.
and 680.5; weaker ones at 645 nm and 655 nm;
a broad absorption between 540 nm and Cleavage Imperfect in three directions (rarely seen)
605 nm; weak lines in the blue at 468 nm,
473 nm, and 476.5 nm; and a cutoff in the violet.
Mohs hardness 8.5
at 678 nm and 680.5 nm; weaker ones at 645 nm and 655 nm; a broad
absorption between about 540 nm and 605 nm; weak lines in the blue
at 468 nm, 473 nm, and 476.5 nm; and a cutoff in the violet
Alexandrite, green pleochroic direction—Strong lines in the red at
Diffraction
678 nm and 680.5 nm; weaker ones at 645 nm, 649 nm, 655 nm, and
665 nm; a broad absorption between about 555 nm and 640 nm; and a
cutoff in the violet at about 470 nm.
Alexandrite, orange pleochroic direction—No strong absorptions
CHRYSOBERYL (NON-PHENOMENAL)
Prism
444
Diffraction
444
Chrysoberyl often forms in a variety of Alexandrite can show
twinned arrangements, including the cyclic a distinct color
twins at left and center. It might rarely be change from reddish
Chrysoberyl’s spectrum reveals a strong found as a prismatic untwinned crystal like or grayish purple in
diagnostic band at 444 nm. the example at lower left. incandescent light
(top) to bluish green
in fluorescent light
(bottom).
462
IDENTIFYING NATURAL ROUGH GEMS
DANBURITE IOLITE
Common habits Slender four-sided prism with Short prism that might appear hexagonal.
pyramid or dome-shaped termi- Often found as crystal fragments or irregu-
nations lar masses rather than well-formed
crystals.
Mike Havstad/GIA
SG 3.00 2.61
463
GEM IDENTIFICATION LAB MANUAL
PERIDOT
PERIDOT TOPAZ
Well-formed peridot Most peridot rough Spectrum Strong, narrow bands at 453 Not diagnostic
crystals often feature occurs as irregular nm, 477 nm, and 497 nm
domes and vertical nodules rather than
striations. well-formed crystals. SG 3.34 3.53
These topaz crystals show typical chisel- Topaz crystals are often multi-faced prisms with
shaped terminations and basal cleavage. vertical striations.
464
IDENTIFYING NATURAL ROUGH GEMS
DIOPSIDE
ZOISITE DIOPSIDE
Prism
violetish blue to violet
Diffraction
bluish purple, violet, brown, yellowish green, brown, and
yellow to green black. Might show chatoyancy or
asterism.
505
Crystal system Orthorhombic Monoclinic
Common habits Multi-faced prism, often with Columnar prism with pyramid or
Diopside’s spectrum shows bands at 456 nm,
vertical striations and pyramid dome terminations 493 nm, and 505 nm. The 505-nm band is
or dome-shaped terminations diagnostic for the gem.
Prism
Spectrum Not diagnostic Ordinary green—Diagnostic band
at 505 nm, with bands also at 456
nm and 493 nm 505
508
Chrome-type—Lines at 505 nm,
508 nm, 635 nm, 655 nm, and 670
Diffraction
nm, and a cutoff around 450 nm
Black—505-nm line common
505
SG 3.35 3.29 508
Shane McClure/GIA
Shane McClure/GIA
465
GEM IDENTIFICATION LAB MANUAL
EPIDOTE
EPIDOTE ORTHOCLASE
SG 3.40 2.58
Robert Weldon/GIA
A well-formed orthoclase
feldspar crystal typically has a
blocky habit.
466
IDENTIFYING NATURAL ROUGH GEMS
SPODUMENE AMAZONITE
Common habits Elongated, vertically striated prism Prismatic, blocky, with wedge-shaped
with irregular terminations, often faces
with lozenge or rhomb-shaped
cross-section. Tops of crystals
might bear distinctive rounded,
triangular raised etch markings.
Cleavage Perfect in two directions, parallel Perfect and easy in two directions Eric Welch/GIA
to length of crystal
Triangular etch marks often occur on a
spodumene crystal’s surface.
Mohs hardness 6.5 to 7 6 to 6.5
SG 3.18 2.56
Comments Crystal habit and cleavage separate Distinctive appearance, cleavage, and
spodumene from similarly colored SG help identify amazonite.
tourmaline and quartz. SG separates
it from topaz, beryl, and
chrysoberyl.
467
GEM IDENTIFICATION LAB MANUAL
Appearance Transparent to opaque. Typically Transparent to opaque. Typically Transparent to opaque. Light blue to
gray to nearly black (might show yellow, orange to brown, or brownish dark blue to green, often zoned in
labradorescence), colorless, green, red. Might also show aventurescence, bands of blue, green, and colorless.
yellow, orange to brown and asterism, or chatoyancy. Colorless, dark blue, and violet-blue
brownish red (might also show pleochroism. Might also be yellow,
aventurescence, asterism, or gray, brown, or rarely colorless.
chatoyancy)
Common habits Usually seen in compact aggregates. Usually seen in compact aggregates. Forms long, flat prisms or distinctive
Prismatic, blocky crystals with Prismatic, blocky crystals with elongated blade-like crystals.
wedge-shaped faces appear very wedge-shaped faces appear very Commonly color zoned in bands of
rarely. Twinning common. rarely. green, blue, and colorless. Might
appear fibrous.
Cleavage Perfect and easy in two directions. Perfect and easy in two directions. Perfect in one direction, distinct in
Parting is also common. Parting is also common. another direction. Parting is also
common.
Comments Distinctive phenomena separate Key tests are cleavage and SG. When Key tests are pleochroism and possibly
labradorite from most other black present, aventurescence distinguishes hardness.
to gray materials. SG separates oligoclase from most other gem
transparent labradorite from most materials.
other gem materials. Cleavage and
multiple twinning planes seen under
the polariscope separate transparent
yellow labradorite from similarly
colored quartz or beryl.
468
IDENTIFYING SYNTHETIC CRYSTALS
Maha Tannous/GIA
Eric Welch/GIA
469
GEM IDENTIFICATION LAB MANUAL
Maha Tannous/GIA
A 10X loupe can be enough to help you detect flux or plate-like inclusions of
platinum or gold in many synthetic crystals grown by these methods.
Synthetic quartz, corundum, and beryl grown by the hydrothermal process might
all have a similar flattened shape with an irregular, or “cobbled,” surface texture
that makes them different from their natural counterparts. They might also show
clearly visible seed plates along with remnants of the wires used to suspend them
in the growth chamber.
Don’t forget that synthetic materials can be fashioned to resemble natural rough.
People who handle natural gem materials in mining areas are often the most
skilled at crafting imitations. For example, buyers in Vietnam have been fooled by
flame-fusion corundum fashioned to resemble natural pyramid-shaped sapphire
crystals, complete with correctly oriented growth marks. Magnification would
reveal the curved growth and gas bubbles typical of this type of synthetic.
470
IDENTIFYING SYNTHETIC CRYSTALS
These are some of the terms that gemologists use to describe synthetic crystals:
Chevron growth pattern—A feature of some hydrothermal synthetic gems that looks like
rows of pointed arches.
Curved striae—Curved growth patterns seen in flame-fusion synthetics such as ruby and
color-change sapphire. They represent stages in the growth of the boule.
Flame fusion—A melt process in which powdered chemicals are dropped through a high-
temperature flame, where they melt onto a rotating pedestal to produce a synthetic crystal.
Used to grow corundum and spinel.
Floating zone—A melt process where a heating unit passes over a rotating solid rod of
chemicals that melt to form a synthetic crystal.
Melt process—A synthetic-crystal growth method in which the chemical mixture is melted,
then recrystallized. Includes the flame-fusion, pulling, and floating zone methods.
Pulling—A melt process in which the synthetic crystal grows from a seed that is dipped
into a chemical melt, then pulled away as it gathers material. Also called the Czochralski
method. Used to grow corundum, chrysoberyl, and YAG.
Seed crystal—A tiny crystal used to initiate crystal growth and as a template to control the
size, speed, or direction of growth and the shape of a growing crystal.
Skull melt—A synthetic-crystal growth method that uses cooling pipes around an interior
of melted chemical ingredients. Used specifically to grow CZ.
Solution process—A growth method in which the synthetic crystal grows from a dissolved
chemical mixture, sometimes at high temperature and pressure. Includes flux and
hydrothermal growth methods.
471
GEM IDENTIFICATION LAB MANUAL
Synthetic beryl Hexagonal 1, very difficult 476 Six-sided prisms, tabular crystals
with cobbled surfaces
472
IDENTIFYING SYNTHETIC CRYSTALS
SYNTHETIC DIAMOND
SG 3.52
Comments Key tests for high-pressure material are crystal shape (typically a
mixture of cube and octahedron), magnification (color zoning
parallel to cube and octahedral faces, and metallic flux inclusions),
and cross-shaped fluorescence patterns. Some crystals might be
attracted to a magnet due to numerous flux-metal inclusions. CVD
synthetic diamond is extremely rare at time of writing.
Maha Tannous/GIA
473
GEM IDENTIFICATION LAB MANUAL
CZ GGG YAG
Species CZ (synthetic cubic zirconia) GGG (gadolinium gallium garnet) YAG (yttrium aluminum garnet)
Appearance Transparent to opaque. Produced Transparent. Usually colorless, but Transparent. Colorless, green, blue,
in all colors as well as colorless. might be light brown or yellow. Small pink, red, purple, orange, or yellow
Color-change material also avail- amounts of orange and blue have also material possible.
able. been produced.
Crystal shape Produced by skull-melt process. As Bell-shaped or cylindrical boules with Pulled—Bell-shaped or cylindrical
material cools, it splits into irregular round cross-sections, generally grown boules, up to hundreds of carats in
columnar crystals, which might be by the crystal pulling method size, with circular cross-sections.
several centimeters in length and Might contain gas bubbles.
weigh several hundred carats. Flux grown—Tabular crystals, often
with numerous flux inclusions
Comments Key tests are shape of rough and Key tests are cylindrical shape and SG. Key tests are shape and SG. YAG is a
SG. Higher SG and heft separate GGG’s high SG separates it from manmade material with no natural
CZ from YAG of similar color. CZ similarly colored CZ and YAG. GGG counterpart.
is a manmade material with no is a manmade material with no natural
gem-quality natural counterpart. counterpart.
Growers produce CZ in a wide range of colors in both CZ can be produced GGG is produced by the YAG might be produced by
transparent (top) and opaque (bottom) forms. They with an opaque metallic pulling process, resulting in the crystal pulling process,
share the same irregular columnar shape appearance that simulates cylindrical boules. This resulting in a cylindrical boule
marcasite or pyrite. GGG crystal—the top (top), or by flux growth,
portion of a larger boule— resulting in a tabular crystal
weighs 15 oz. (447 g.). (bottom).
474
IDENTIFYING SYNTHETIC CRYSTALS
Prism
Appearance Transparent to opaque. Flame-fusion material manufactured in a
range of colors, including a light-toned blue resembling aquamarine,
a greenish blue resembling zircon, a dark grayish green resembling
tourmaline, a vivid, dark, slightly greenish blue resembling sapphire,
a light-toned yellowish green resembling peridot, and a pale pink.
Diffraction
There’s also a translucent material that imitates moonstone and an
opaque blue “sintered” material that imitates lapis lazuli. Flux-grown
material is typically red or blue, but scientists have grown a related
mineral—synthetic gahnite—experimentally by the flux method in a
variety of other colors.
Flux-grown synthetic blue spinel’s spectrum has
bands between 535 nm and 550 nm, 560 nm
Crystal shape Flame fusion—Cylindrical boule that tapers toward the base, often
and 590 nm, and 615 nm and 635 nm, together
with a slightly square cross-section. Might be several centimeters in with a weak absorption at 430 nm that increases
length. through the violet.
Flux grown—Octahedral shape similar to natural crystal, with
relatively flat, smooth faces and sharp edges. Base of crystal has
an irregular surface, which might be a point of attachment (natural
crystals often have intact octahedral points). Magnification might
reveal flux inclusions. Synthetic crystals have been grown over 10
carats in size.
Mohs hardness 8
Terri Weimer/GIA
Toughness Good Most synthetic spinel is produced by flame
fusion. The cylindrical shape of this blue spinel
SG Flame fusion—3.64 (+0.02/-0.12) boule is typical.
Flux grown—3.61 (+/-0.03)
Comments Flame fusion—Key tests are crystal shape, SG, and spectrum.
Magnification might reveal gas bubbles. Boules might show strong
ADR (crosshatch effect common) with polariscope. Color filter and
spectrum separate blue flame-fusion synthetic spinel from similarly
colored flame-fusion synthetic sapphire boules. Crystal shape and
SG separate blue flame-fusion spinel from similarly colored
hydrothermal synthetic quartz.
Both by Terri Weimer/GIA
Flux grown—Key test is magnification, which reveals flux inclusions.
Spectrum is a key test for blue material, which lacks iron-related Some flame-fusion synthetic spinel boules have
sides that are nearly straight (left) and cross-
bands at 459 nm and 480 nm in the blue. Vivid color and sharpness
sections that are rounded squares (right).
of junctions between crystal faces might indicate synthetic.
Flux-grown synthetic spinel This Russian flux-grown synthetic spinel has the same
crystals can be up to 10 arrangement of triangular faces (left) as a natural crystal. Its
carats in size. They have the broken base (right) indicates its synthetic nature, as the points
same crystal shape as natural on most natural gem-quality spinel crystals are intact.
rough.
475
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC BERYL
Terri Weimer/GIA Appearance Green, blue-green to greenish blue, pink, and red. Bicolor synthetic
Although the synthetic emerald crystals in beryl crystals, including “watermelon” type, have been grown
this 237.94-ct. Chatham flux-grown cluster experimentally.
look very similar to natural crystals, their
vivid color and inclusions mark them as Crystal system Hexagonal
synthetics.
Crystal shape Flux grown—Synthetic emerald is usually flux grown, although
hydrothermal growth is becoming the preferred method. Resembles
natural material. Six-or twelve-sided columns terminated by flat
faces. Often seen as small groups of radiating columnar crystals.
Vivid nature of color and sharpness of junctions between crystal
faces might indicate synthetic.
Hydrothermal—Tabular crystals with irregular (cobbled) top and
bottom surfaces typical of this growth method. Seed plates and wires
(used to suspend the seed plate in growth medium) often visible.
Emerald, aquamarine, and red to pink beryl are grown by the
hydrothermal process.
Toughness Synthetic emerald is poor to good, and slightly tougher than natural
Both by Eric Welch/GIA emerald. Good in other varieties.
These Russian-grown synthetic
emeralds’ tabular shapes, SG Flux grown—Synthetic emerald 2.66 to 2.69
cobbled surface textures (top), Hydrothermal—Synthetic aquamarine 2.72 (+0.18/-0.05), synthetic
and colorless seed plates emerald 2.61 to 2.76, synthetic red and pink beryl 2.67 to 2.70
(bottom) identify them as prod-
ucts of hydrothermal growth.
Comments Flux grown—Key tests are six-sided columnar shape and magnifica-
tion, which might reveal wispy veils and flux inclusions as well as
platinum or gold platelets that appear metallic with reflected lighting.
Vivid color and sharpness of junctions between crystal faces often
indicate synthetic.
Hydrothermal—Key tests are tabular crystal shape with cobbled or
cobblestone texture on some faces and presence of seed plate.
Magnification might reveal seed plate, nailhead spicules, platinum or
gold platelets, and chevron or mosaic growth patterns.
Eric Welch/GIA
476
IDENTIFYING SYNTHETIC CRYSTALS
SYNTHETIC CORUNDUM
Cleavage None
Mohs hardness 9
477
GEM IDENTIFICATION LAB MANUAL
SYNTHETIC QUARTZ
Appearance Transparent, all colors seen in nature, plus bright cobalt blue, green-
ish yellow, and grayish green not seen in nature. Pink material (more
transparent than rose quartz) and limited quantities of aventurescent
material also manufactured.
Both by Terri Weimer/GIA Crystal shape Tabular crystals with irregular (cobbled) top and bottom surfaces
typical of hydrothermal growth method. Seed plates and wires (used
Vivid blue color, tabular shape,
colorless seed plate (top), and to suspend the seed plate in growth medium) often visible. Large
cobbled surface texture (bottom), crystals up to several centimeters in length are produced. Crystals
identify this 39-oz. (1.107-kg) grown on natural seeds (rare) might display habit identical to natural.
crystal as hydrothermal
synthetic quartz. Cleavage None
Mohs hardness 7
Toughness Good
SG 2.66 (+0.03/-0.02)
Comments Key tests are tabular shape, with cobbled or cobblestone texture on
some faces, presence of seed plate, and possibly unnatural color. Blue
material might show cobalt bands through the spectroscope. Pink
material is typically much more transparent than natural rose quartz.
478
IDENTIFYING SYNTHETIC CRYSTALS
SYNTHETIC CHRYSOBERYL
Toughness Excellent
SG 3.73 (+/-0.02)
479
GEM IDENTIFICATION RI CHART
This chart lists all the gem materials in the manual. The listings are in descending RI
order to make it easy for you to find a gem with a known RI. The chart also lists basic
information on each gem’s birefringence, transparency, and possible color range.
Page references in the last column will direct you to the detailed entry or entries for
each gem, broken down by color, phenomenon, and sometimes treatment.
GEM IDENTIFICATION RI CHART
Gem RI Birefringence Transparency Possible colors Lab manual page
Hematite OTL 0.280 (usually not O Metallic, dark gray to Gray—Page 340
2.940 to 3.220 detectable) black Black—Page 358
Pyrite OTL Too opaque to test O Metallic, brassy yellow Orange, yellow—Page 281
Gray—Page 340
Black—Page 358
Rough—Page 455
HPHT synthetic OTL None (SR) TP Yellow, brown, blue Red (treated color)—Page
diamond 2.417 green, colorless; any 85
color possible through Blue—Page 140
treatment Green—Page 188
Yellow to brown—Page 246
Colorless—Page 305
Irradiated black—Page 360
Crystal—Page 473
CVD synthetic OTL None (SR) TP Brown, brownish Brown, yellow—Page 248
diamond 2.417 yellow, colorless Colorless—Page 305
481
GEM IDENTIFICATION LAB MANUAL
CZ (synthetic cubic OTL None (SR) TP to O Typically colorless, but Red, pink (TP)—Page 86
zirconia) 2.150 might be any color Pink (TL)—Page 119
Translucent pink: Blue, violet—Page 141
2.140 Green—Page 189
Yellow, orange—Page 250
Colorless—Page 307
White—Page 322
Black—Page 360
Color-change—Page 401
Crystal—Page 474
GGG (gadolinium gallium OTL None (SR) TP Typically colorless, but Blue—Page 141
garnet) 1.970 (+0.060) might be blue, yellow, Yellow, brown—Page 250
brown Colorless—Page 307
Crystal—Page 474
Zircon OTL High-type: 0.059 TP Almost all colors Red, pink, purple—Page 86
High-type: 1.925 to Low-type: might Blue—Page 142
1.984 approach zero Green—Page 189
(+/-0.040) Yellow to brown—Page 251
Low-type: 1.810 Colorless—Page 308
to 1.815 Gray—Page 341
(+/-0.030) Rough—Page 456
YAG (yttrium aluminum OTL None (SR) TP Typically colorless, but Red, pink, purple—Page 86
garnet) 1.833 might be any color Blue—Page 143
(+/-0.100) Green—Page 191
Yellow, orange—Page 253
Colorless—Page 308
Crystal—Page 474
Gahnite 1.800 (might be None (SR) TP to TL Very dark blue or green Blue—Page 143
nearly OTL) to black
(+0.005/-0.010)
482
RI CHART
Almandite garnet 1.780 to OTL None (SR) TP Purple to brownish red Red, pink, purple—Page 87
Star—Page 376
Rough—Page 454
Corundum 1.762 to 1.770 0.008 to 0.010 TP to O All colors, colorless; Red, pink, purple—Page 88
(+0.009/-0.005) might show asterism, Red, lattice diffusion
1.76 or 1.77 spot chatoyancy, or color treated—Page 89
RI change Color-change—Page 95,
194, and 402
Blue, violet—Page 144
Blue, lattice diffusion
treated—Page 145
Green—Page 192
Yellow to brown—Page 255
Yellow, lattice diffusion
treated—Page 256
Colorless—Page 309
Gray—Page 342
Black—Page 361
Star—Page 373
Star, lattice diffusion
treated—Page 374
Cat’s-eye—Page 385
Rough—Page 460
Synthetic corundum 1.762 to 1.770 0.008 to 0.010 TP All colors, colorless; Red, pink, purple (flame
(+0.009/-0.005) might show asterism or fusion)—Page 90
1.76 or 1.77 spot color change Red, pink, purple (pulled)—
RI Page 91
Red, pink, purple (floating
zone)—Page 91
Red, pink, purple (flux)—
Page 92
Red, pink, purple
(hydrothermal)—Page 92
Red, pink, purple (over-
growth)—Page 94
Color-change—Pages 95
and 403
Blue, violet (flame fusion)—
Page 145
Blue, violet (flux)—Page 146
Blue, violet (hydrothermal)—
Page 146
Green (flame fusion)—
Page 193
Green (hydrothermal)—
Page 193
Yellow to brown (flame
fusion)—Page 257
Yellow to brown (flux)—
Page 258
Yellow to brown (hydrother-
mal)—Page 258
Colorless—Page 309
Star (flame fusion)—Page
375
Star (pulled)—Page 376
Crystal—Page 477
483
GEM IDENTIFICATION LAB MANUAL
Ruby-in-zoisite Ruby crystals: 1.76 Not detectable O Purplish red ruby crys- Red—Page 120
to 1.77 spot tals in green zoisite Green—Page 226
Zoisite matrix: 1.70 and black hornblende
spot matrix
Gahnospinel 1.760 (+/-0.020) None (SR) TP to TL Very dark blue or green Blue—Page 148
to black
Benitoite 1.757 to 1.804 0.047 (blinks to OTL) TP Blue to violet Blue—Page 148
Grossularite-andradite Green: 1.762 to None (SR) TP Green to yellow and Green—Page 195
garnet 1.764 brown, chatoyant in Yellow, brown—Page 254
Yellowish green: rare cases
1.752 to 1.769
Orange to brown:
1.773 to 1.779
Pyrope-spessartite garnet 1.750 to 1.780 None (SR) TP Pinkish orange, reddish Red, pink—Page 96
orange, orange; might Orange—Page 260
show color change Color-change—Page 404
Pyrope-almandite garnet 1.750 to 1.780 None (SR) TP Purple, purplish red to Red, purple—Page 96
brownish red Star—Page 376
Rough—Page 454
Synthetic non-phenome- 1.742 to 1.755 0.008 to 0.010 TP Intense green Green—Page 198
nal chrysoberyl (+0.004/-0.006) Crystal—Page 479
484
RI CHART
Single-crystal rhodonite 1.733 to 1.747 0.010 to 0.014 TP Red, orangy red, pink Red, pink—Page 99
(+0.010/-0.013)
Opaque rhodonite 1.733 to 1.747 None (AGG) O Red, brownish to pur- Red, pink—Page 121
(1.73 to 1.75 spot plish red, pink
RI)
Azurmalachite Azurite: 1.730 to Azurite: 0.106 O Bands of blue and Blue—Page 167
1.836 (+/-0.010) Malachite: 0.254 green Green—Page 224
Malachite: 1.655 to
1.909
Azurite 1.730 to 1.836 0.106 STP to O Dark blue to violetish Blue—Page 167
(+/-0.010) blue
Pyrope garnet 1.730 to 1.750 None (SR) TP Purplish red to brown- Red, pink, purple—Page 99
(1.740 normal, but ish red, light pink (rare) Rough—Page 454
can go as low as
1.717)
Unakite 1.729 to 1.768 None (AGG) O Mottled green, pink, Red, pink—Page 121
(1.74 to 1.76 or and gray appearance Green—Page 224
1.52 to 1.54 spot
RI, depending on
where you test)
Epidote 1.729 to 1.768 0.019 to 0.045 TP to TL Green, brown, yellow, Green—Page 199
(+0.012/-0.035) black Yellow, brown—Page 262
Rough—Page 466
Flame-fusion synthetic 1.728 None (SR) TP Red (rare), pink, blue, Red, pink—Page 100
spinel (+0.012/-0.008) light green, colorless Blue—Page 149
Red (very rare): Green—Page 200
1.722 (+/-0.003) Colorless—Page 310
Crystal—Page 475
Flux-grown synthetic Red, pink: 1.719 None (SR) TP Red, pink, blue Red, pink—Page 100
spinel (+/-0.003) Blue—Page 150
Blue: 1.714 Crystal—Page 475
(+/-0.003)
Taaffeite 1.719 to 1.723 0.004 to 0.005 TP Pink, red, purple, violet, Red, pink, purple—
(+/-0.002) brown, colorless Page 101
Spinel 1.718 None (SR) TP to O Red, pink, purple, blue, Red, pink—Page 101
(+0.017/-0.008) violet, black Blue—Page 150
1.72 or 1.73 spot Gray—Page 343
RI Black—Page 362
Black: 1.740 to Star—Page 377
1.770 or higher Color-change—Page 407
Rough—Page 455
485
GEM IDENTIFICATION LAB MANUAL
Kyanite 1.716 to 1.731 0.012 to 0.017 TP to TL Blue, often with green Blue—Page 152
(+/-0.004) and colorless zones Rough—Page 468
Transparent idocrase 1.713 to 1.718 0.001 to 0.012 TP Green, yellow, brown Green—Page 200
(+0.003/-0.013) Yellow, brown—Page 262
Gray—Page 344
Translucent-to-opaque 1.713 to 1.718 Usually not detectable TL to O Green, yellowish Green—Page 226
idocrase (+0.003/-0.013) green, brownish yellow, Yellow, brown—Page 281
1.70 or 1.71 spot gray, and white White—Page 322
RI Gray—Page 344
Zoisite 1.691 to 1.700 0.008 to 0.013 TP to TL Blue, violet, purple Purple—Page 102
(+/-0.005) (tanzanite), green Blue, violet—Page 152
1.69 spot RI (transparent green Green—Page 201
zoisite) Cat’s-eye—Page 387
Rough—Page 465
Thulite zoisite 1.691 to 1.700 Usually not detectable TL to O Pink to orangy pink to Pink, red—Page 122
(+/-0.005) red, often mottled with
1.70 spot RI com- gray or white
mon, but might be
low to mid-1.50s
due to impurities
Diopside 1.675 to 1.701 0.024 to 0.030 TP to O Green or black. Might Green—Page 201
(+0.029/-0.010) show chatoyancy or Black—Page 362
1.68 spot RI asterism Star—Page 378
Cat’s-eye—Page 388
Rough—Page 465
Sinhalite 1.668 to 1.707 0.036 to 0.039 TP to TL Yellow, brown Yellow, brown—Page 263
(+0.005/-0.003)
Jadeite 1.666 to 1.680 Usually not detectable STP to O Green, yellow, laven- Lavender—Page 123
(+/-0.008) der, white, gray, black; Dyed lavender—Page 123
1.66 spot RI often shows mottling Blue—Page 168
Gray: 1.65 or 1.66 Green—Page 227
spot RI Dyed green—Page 228
Treated green—Page 228
Yellow, brown—Page 282
White—Page 322
Gray—Page 344
Black—Page 363
486
RI CHART
Spodumene 1.660 to 1.676 0.014 to 0.016 TP Pink to violet-pink, Pink (kunzite)—Page 102
(+/-0.005) green, yellow, color- Violet (kunzite)—Page 153
less, possibly gray Green—Page 203
Yellow—Page 265
Colorless—Page 311
Gray—Page 344
Rough—Page 467
Jet 1.660 None (SR) STL to O Very dark brown to Black—Page 363
(+/-0.020) black
1.68 spot RI
Malachite 1.655 to OTL 0.254 (use blink O Curved or angular Green—Page 224
(1.909) technique) banding in different
intensities of green
Euclase 1.652 to 1.671 0.019 to 0.020 TP Blue, green, colorless Blue—Page 153
(+0.006/-0.002) Green—Page 204
Colorless—Page 311
Synthetic forsterite 1.635 to 1.670 0.034 to 0.035 TP Blue to violet Blue—Page 154
Andalusite 1.634 to 1.643 0.007 to 0.013 TP Green, red, orange to Red—Page 102
(+/-0.005) brown Green—Page 204
Yellow, brown—Page 265
Rough—Page 461
Chiastolite andalusite 1.63 or 1.64 spot Usually not detectable TL to O Brown, gray Brown—Page 282
RI
Apatite 1.634 to 1.638 0.002 to 0.008 TP Almost all colors, color- Pink—Page 103
(+0.012/-0.006) Colorless: 0.002 to less; might show Blue—Page 154
1.63 spot RI 0.006 chatoyancy Green—Page 205
Yellow—Page 266
Colorless—Page 311
Cat’s-eye—Page 391
Rough—Page 457
487
GEM IDENTIFICATION LAB MANUAL
Topaz: red, pink, purple, 1.629 to 1.637 0.008 to 0.010 TP Pink, red to purple, Red, pink, purple—Page 103
yellow, and brown Topaz range: 1.619 reddish orange to Yellow to brown—Page 267
to 1.627 (+/-0.010) yellow and brown Rough—Page 464
Tourmaline 1.624 to 1.644 0.018 to 0.020 TP All colors, colorless; Red, pink, purple—Page 104
(+0.011/-0.009) (up to 0.040 possible might show chatoyancy Parti-colored—Pages 104,
Black: 1.620 to in dark stones) 155, and 206
1.644 Blue—Page 155
(+0.011/-0.009) Green—Page 205
1.62 or 1.64 Yellow to brown—Page 267
spot RI Colorless—Page 312
Black—Page 363
Cat’s-eye—Page 391
Rough—Page 461
Prehnite 1.616 to 1.649 0.020 to 0.033 STP to TL Light green to yellow- Green—Page 229
1.63 spot RI ish “celery” green
Actinolite 1.614 to 1.641 0.022 to 0.027 TP to O Light to dark green, Cat’s-eye—Page 392
(+0.014) yellowish green, black;
1.63 spot RI with chatoyancy
Lazulite 1.612 to 1.643 0.031 TP to O Medium to dark green- Blue (TP)—Page 156
(+/-0.005) ish blue to violetish Blue (TL to O)—Page 168
blue
Turquoise 1.610 to 1.650 Usually not detectable STL to O Greenish blue, bluish Blue—Page 169
1.61 spot RI green Impregnated blue—Page
Impregnated: as 170
low as 1.56 spot RI Green—Page 229
Synthetic turquoise 1.610 to 1.650 Usually not detectable STL to O Light to medium blue Blue—Page 170
1.61 spot RI and green Green—Page 230
Topaz: colorless to blue 1.609 to 1.617 0.008 to 0.010 TP Blue, colorless, gray Blue—Page 156
Topaz range: 1.619 Treated green—Page 207
to 1.627 (+/-0.010) Colorless—Page 312
Gray—Page 345
Rough—Page 464
Sugilite 1.607 to 1.610 Usually not detectable STP to O Red-purple to violetish Red, pink, purple—Page
(+0.001/-0.002) purple, rarely pink 124
Might be 1.54 spot
due to quartz
impurities
Nephrite 1.606 to 1.632 Usually not detectable TL to O Light to dark green, Dyed lavender—Page 124
(+0.009/-0.006) yellow to brown, white, Green—Page 230
1.61 spot RI gray, black; often mot- Yellow, brown—Page 283
common tled White—Page 323
Gray—Page 345
Black—Page 364
488
RI CHART
Pectolite 1.599 to 1.628 0.029 to 0.038 STP to O Slightly grayish to Blue—Page 171
(+0.017/-0.004) yellowish white, green
1.60 spot RI or blue, sometimes
common light pink
Single-crystal 1.597 to 1.817 0.220 TP Pink to dark red Pink, red—Page 105
rhodochrosite (+/-0.003)
Translucent-to-opaque 1.597 to 1.817 0.220 TL to O Pink, brownish red, Pink, red—Page 125
rhodochrosite (+/-0.003) orangy pink, often with
agate-like banding
Howlite 1.586 to 1.605 0.019 (usually not STL to O White, might be dyed Dyed red, pink—Page 125
(+/-0.003) detectable) any color Dyed blue—Page 171
1.59 spot RI White—Page 323
Beryl (other than red 1.577 to 1.583 0.005 to 0.009 TP to O Usually light-toned, Pink (morganite)—Page 106
beryl and emerald) (+/-0.017) Morganite: 0.007 to slightly yellowish green, Blue (aquamarine)—Page
Morganite: 1.583 0.008 greenish blue to blue- 156
to 1.590 green, yellow to Maxixe (blue)—Page 157
(+0.012/-0.011) colorless, gray; pink Green—Page 207
Aquamarine: 1.569 to purplish pink Yellow (heliodor)—Page 268
to 1.575 (morganite) Colorless (goshenite)—
Page 313
Gray—Page 346
Star—Page 378
Cat’s-eye—Page 392
Rough—Page 458
Hydrothermal synthetic 1.577 to 1.583 0.005 to 0.009 TP Same as natural Blue (aquamarine)—Page
beryl (other than synthetic (+/-0.017) 157
emerald and synthetic red Yellow—Page 268
beryl) Crystal—Page 476
Hydrothermal synthetic 1.571 to 1.578 0.006 to 0.008 TP Red to orange-red Red—Page 106
red beryl (+0.002/-0.003)
Hydrothermal synthetic 1.571 to 1.577 0.004 to 0.008 TP Medium-light to dark Green—Page 210
emerald (+0.007/-0.002) (depends on manufac- green, slightly yellowish Crystal—Page 476
(depends on turer) to bluish green
manufacturer)
Red beryl 1.566 to 1.572 0.006 to 0.008 TP Purplish red to Red—Page 107
(+0.002/-0.003) orange-red
489
GEM IDENTIFICATION LAB MANUAL
“Overgrowth” and “sand- 1.566 to 1.570 0.006 (overgrowth) TP Medium to medium- Green—Page 210
wich” hydrothermal (overgrowth) 0.004 (sandwich) dark green to very
synthetic emerald 1.575 to 1.581 slightly bluish green
(sandwich)
Flux synthetic emerald 1.562 to 1.566 0.003 to 0.005 TP Medium-light to dark Green—Page 211
(+/-0.003) (depends on green, slightly yellowish Crystal—Page 476
(depends on manufacturer) to bluish green
manufacturer)
Variscite 1.560 to 1.590 Usually not detectable TL to O Yellowish green, bluish Green—Page 230
(+0.003/-0.006) green, often mottled
1.57 spot RI with yellow matrix
Coral 1.560 to 1.570 None STL to O Dark brown, black, Golden—Page 283
(+/-0.010) golden Black—Page 364
Serpentine 1.560 to 1.570 Usually not detectable STP to O Green to greenish Green—Page 231
(+0.004/-0.070) yellow, white, brown, Yellow, brown—Page 283
gray, black (often White—Page 323
mottled) Gray—Page 346
Horn 1.560 None STP to O Yellow to brown, white, Yellow, brown—Page 284
gray to almost black White—Page 324
Gray—Page 346
Black—Page 365
Labradorite feldspar 1.559 to 1.568 0.009 TP to O Colorless, green, Red, pink—Page 107
(+/-0.005) yellow, orange to Green—Page 213
1.56 spot RI brownish red; might Yellow, orange (including
Oregon material show labradorescence, sunstone)—Page 268
commonly 1.563 aventurescence, or Colorless—Page 313
to 1.572 adularescence White—Page 324
Gray—Page 347
Sunstone (general infor-
mation)—Page 421
General information—Page
421
Moonstone (including rain-
bow)—Page 422
Rough—Page 468
Tortoise shell 1.550 (-0.010) None STP to STL Mottled yellow and Yellow, brown—Page 284
brown
Scapolite 1.550 to 1.564 0.005 to 0.038 TP to O Violet, red, purple, Red, purple—Page 108
(+0.015/-0.014) Yellow: 0.004 to orange, yellow, green, Blue, violet—Page 157
Purple to violet: 0.037 blue, colorless; might Green—Page 213
1.536 to 1.541 show chatoyancy Yellow to brown—Page 269
Brown cat’s-eye: Colorless—Page 313
1.560 to 1.585 Cat’s-eye—Page 393
Rough—Page 456
490
RI CHART
Charoite 1.550 to 1.559 Usually not detectable STL to O Purple with swirls of Purple—Page 125
(+/-0.002) black, gray, white, and
1.55 or 1.56 spot brownish orange,
RI fibrous appearance
Gilson imitation coral 1.55 spot RI Weak, but sometimes STL to O Red, pink Red, pink—Page 126
detectable
Hawk’s-eye quartz 1.544 to 1.553 Usually not detectable STL to O Dark grayish blue with General information—Page
1.54 or 1.55 spot wavy chatoyancy 394
RI
Tiger’s-eye quartz 1.544 to 1.553 Usually not detectable STL to O Brownish yellow to Yellow, brown—Page 284
1.54 or 1.55 spot reddish brown with General information—Page
RI wavy chatoyancy 395
Dyed—Page 395
Synthetic quartz 1.544 to 1.553 0.009 TP Pink, purple, yellow, Amethyst (purple)—Page
orange, colorless 109
Ametrine—Pages 110 and
270
Pink—Page 110
Blue—Page 158
Amethyst (blue)—Page
159
Citrine—Page 270
Colorless—Page 315
Crystal—Page 478
491
GEM IDENTIFICATION LAB MANUAL
Dyed quartzite 1.544 to 1.553 Usually not detectable TL to O Can be dyed any color, Red, pink, purple—Page
sometimes shows 126
aventurescence Green—Page 232
Aventurescent—Page 423
Iolite 1.542 to 1.551 0.008 to 0.012 TP to O Violet through slightly Blue, violet—Page 160
(+0.045/-0.011) violetish blue Bloodshot—Page 423
Rough—Page 463
Talc (soapstone) 1.540 to 1.590 0.050 STL to O White, gray, brown, Green—Page 232
(+0.010/-0.002) Usually not detectable green; often veined or Brown—Page 285
1.54 spot RI mottled White—Page 324
Gray—Page 347
Amber 1.540 None (SR) TP to O Yellow, brown, orange, Orange, yellow, brown
(+0.005/-0.001) white (TP)—Page 271
Orange, yellow, brown (TL
to O)—Page 285
Copal resin 1.540 (-0.010) None (SR) TP to TL Yellow, orange, brown Orange, yellow, brown
(TP)—Page 271
Orange, yellow, brown
(TL)—Page 286
Oligoclase feldspar 1.539 to 1.547 0.007 to 0.010 STP to O Yellow, orange, brown, Yellow to brown—Page
(+0.004/-0.006) to brownish red vari- 287
eties might show Colorless—Page 315
aventurescence (sun- White—Page 325
stone); also colorless, Sunstone—Page 424
gray, white Rough—Page 468
Ivory (elephant) 1.535 to 1.540 None TL to O White to light yellow Yellow—Page 287
(usually 1.540) White—Page 326
Chalcedony 1.535 to 1.539 Usually not detectable STP to O Virtually all colors, Red—Page 127
1.53 to 1.54 sometimes banded or Dyed blue—Page 172
spot RI patterned; might show Dyed blue jasper—Page
Green, orange, iridescence 173
white, black, iris: Dyed green—Page 233
1.53 to 1.54 Green—Page 234
Orange, brown—Page 288
White—Page 327
Gray—Page 348
Black—Page 365
Iris agate—Page 410
Fire agate—Page 410
492
RI CHART
Chrysocolla-in-chalcedony 1.535 to 1.539 Usually not detectable TL to STL Blue to green-blue; Blue—Page 173
1.53 to 1.54 spot often unevenly colored; Green—Page 233
RI might resemble fine
turquoise
Chrysoprase chalcedony 1.535 to 1.539 Usually not detectable STP to TL Light to medium-dark Green—Page 233
1.53 or 1.54 spot yellowish green
RI
Chrome chalcedony 1.535 to 1.539 Usually not detectable TL to STL Green to slightly bluish Green—Page 234
1.53 or 1.54 spot green
RI
Natural pearl 1.530 to 1.685 0.155 TL to O Usually white or light Pink—Page 128
yellow, might be gray Yellow—Page 289
or black; might have White—Page 328
pink, green, or blue Gray—Page 348
overtones Black—Page 365
General information—Page
411
Cultured pearl 1.530 to 1.685 0.155 TL to O Usually white or light Pink—Page 128
yellow or even black; Yellow—Page 290
might have pink, green, White—Page 329
or blue overtones; Gray—Page 349
might be dyed any Black—Page 366
color General information—Page
412
Calcareous concretions 1.530 to 1.685 0.155 TL to O Pink, orange, yellow, Pink—Page 129
brown Yellow—Page 291
Maw-sit-sit 1.53 to 1.74 spot None O Green with dark green Green—Page 225
RI to black veining or
mottling
Gilson imitation lapis 1.530 to 1.550 None O Intense medium blue to Blue—Page 174
(often vague) violetish blue; might
contain gold-colored
inclusions
Amazonite microcline 1.522 to 1.530 0.008 (usually not TL to O Light green to greenish Blue—Page 174
feldspar (+/-0.004) detectable) blue with grid-like Green—Page 235
1.53 spot RI appearance Rough—Page 467
493
GEM IDENTIFICATION LAB MANUAL
Alabaster 1.520 to 1.529 0.009 to 0.010 TL to O White, gray, impurities White—Page 330
(+/-0.001) Usually not detectable might make it yellow-
1.52 or 1.53 spot ish, reddish, brownish
RI or greenish; might be
banded like marble
Orthoclase feldspar 1.518 to 1.526 0.005 to 0.008 TP to O Colorless, orange, Orange, yellow, brown—
(+0.010) yellow to brown Page 272
1.52 spot RI Colorless—Page 316
Gray—Page 350
Sunstone—Page 425
Rough—Page 466
Moonstone orthoclase 1.518 to 1.526 0.005 to 0.008 STP to O Yellow, brown, orange, Yellow to brown—Page 292
feldspar (+0.010) white, colorless, green White—Page 331
1.52 spot RI Star—Page 380
Cat’s-eye—Page 396
General information—Page
424
Rough—Page 466
Magnesite 1.509 to 1.700 0.191 TL to O White, often dyed any Dyed red, pink, purple—
color Page 129
Dyed blue—Page 175
White—Page 331
Lapis lazuli 1.50 or 1.67 spot None STL to O Medium to dark, slightly Blue—Page 175
RI greenish blue to
(depends on violetish blue; mottled
where you test) with white calcite and
specks of pyrite
Eilat stone 1.50 or 1.61 to Might be 0.250 STL to O Mottled blue to green Blue—Page 176
OTL (depends on where
you test)
Calcareous coral 1.486 to 1.658 0.172 STL to O Pink to dark red, white Red, pink—Page 130
White—Page 331
494
RI CHART
Calcite 1.486 to 1.658 0.172 TP to O Occurs in almost all Red (TP)—Page 111
colors (might be dyed) Red (TL to O)—Page 130
Blue, violet (TP)—Page 160
Blue, violet (TL to O)—Page
176
Green (TP)—Page 215
Green (STL to O)—Page
235
Yellow (TP)—Page 272
Yellow (STL to O)—Page
293
White—Page 332
Gray—Page 351
Sodalite 1.483 None (SR) STP to O Dark blue to violetish Blue—Page 177
(+/-0.004) blue, often with white
veining
Glass 1.470 to 1.700 None (SR/ADR) TP to O All colors Pages 430 to 434, plus
(might go to OTL) entry in each color/trans-
parency section
Cat’s-eye—Page 397
Color change—Page 407
Imitation opal—Page 418
Goldstone—Page 426
Plastic 1.460 to 1.700 None (SR/ADR) TP to O All colors Pages 435 to 436, plus
entry in each color/
transparency section
Imitation opal—Page 418
Goldstone—Page 426
Opal 1.450 None (SR) TP to O Yellow, orange, red, Red (fire opal)—Page 111
(+0.020/-0.080) colorless, black, gray, Red, pink (TL to O)—Page
1.44 or 1.45 spot white, green, blue, vio- 131
RI (some fire opal let; with or without Blue, violet—Page 177
as low as 1.37) play-of-color Green—Page 236
Smoke-treated: Orange, yellow, brown
1.380 to 1.390 (TP)—Page 273
Orange, yellow, brown (TL
to O)—Page 294
Colorless—Page 317
White—Page 332
Gray—Page 352
Black—Page 367
Sugar-treated—Pages 368
and 416
Smoke-treated—Pages 368
and 416
Cat’s-eye—Page 397
General information—Page
414
Fire opal—Page 415
495
GEM IDENTIFICATION LAB MANUAL
Fluorite 1.434 None (SR) TP to O Pink, purple, blue, Pink (TP)—Page 112
(+/-0.001) violet, green, orange, Pink (TL to O)—Page 132
yellow, brown, color- Blue, violet (TP)—Page 161
less Blue, violet (TL to O)—Page
178
Green—Page 215
Yellow, orange—Page 273
Colorless—Page 318
Rough—Page 453
Synthetic opal 1.430 to 1.470 None (SR) STP to O Play-of-color against Red, pink (STP)—Page 112
gray, black, white, Red, pink (STL)—Page 131
colorless, red, orange, Blue (STP)—Page 161
blue, or yellow back- Blue (STL)—Page 178
ground Green (STP)—Page 216
Green (STL)—Page 236
Orange, yellow (STP)—
Page 274
Orange, yellow (STL)—
Page 294
Colorless—Page 317
White—Page 333
Gray—Page 352
Black—Page 368
General information—Page
417
Assembled stones Varies with Varies with TP Can be any color Pages 438 to 447
components components
496
GEM IDENTIFICATION