TUBOS REUNIDOS INDUSTRIAL, S.L.

U
Barrio Sagarribai, 2 - 01470 AMURRIO (Spain)

QUALITY
MANAGEMENT
EN 10204:2004 / 3.1 SYSTEM
certified by
LRQA
CERTIFICADO DE CALIDAD
MILL TEST CERTIFICATE

THE BILLETS AND THE MATERIAL COVERED BY THIS CERTIFICATE ARE MANUFACTURED AT OUR STEEL PLANT IN AMURRIO, SPAIN.

PAG. 1 / 4
Nº 0000351454/1 Rev. 001
CLIENTE: BUHLMANN SINGAPORE PTE. LTD. PEDIDO / PARTIDA: PO-19-SG00403
CUSTOMER P.ORDER / ITEM 10.

PRODUCTO: TUBERÍA SIN SOLDADURA LAMINADA EN REF. FABRICA: 300020601

ARTICLE CALIENTE WORK ORDER 000010
HOT FINISHED SEAMLESS TUBES

EXTREMOS: LISOS A ESCUADRA PROTECCIÓN SUPERF: LACA EXTERIOR

ENDS SQUARE CUT PLAIN END EXT. COATING EXTERNALLY DRY LACQUERED

NORMA / GRADO: ASTM A333/A333M-18 / ASME II PROCESO FUSION: HORNO ELECTRICO

APL.STANDARD AND SA-333/SA-333M-19 / API 5L 2018 46TH ED. MELTING PROCESS ACERO TOTALMENTE CALMADO
GRADE PSL2 + ISO 3183:2012 ELECTRIC FURNACE // FULLY KILLED
L360N/X52N/6

DIMENSIONAL STD: ANSI/ASME B36.10M

ESPEC. BDSOS0025-CSLTP REV. 0_ TUBOS FAB. DE PALANQUILLA: COLADA CONTINUA

ADICIONALES: REUNIDOS BILLETS MANUFACTURE CONTINUOUS CASTING
ADITIONAL SPECS. NACE MR0175/ISO 15156 ED. 2015
NACE MR0103/ISO 17945 ED. 2015
ASME II.PART D.TABLE Y1
ASME BPVC

DIMENSIONES: 33,4 X 4,55 MM. X

DIMENSIONS 6 M.

MARCAS: ESTAMPADO: TRI A/SA 333 6 33,4 4,6 HN (HEAT)

MARKING DIE STAMPING

PINTADO: TRI API SPEC 5L 5L-0011 (SELLO API) (MM/AA) 33,4 4,6 L360N/X52N PSL2 S
STENCILLED MLS HN (HEAT) 20,5 MPA 6,000 M ASTM/ASME A/SA 333 6 ISO 3183 L360N/X52
N H.F. LT -50 PO-19-SG00403
CODIGO COLOR:
COLOUR CODE

TRAT. TERMICO: NORMALIZADO. HORNO CONTINUO. ENFRIADO AL AIRE / NORMALIZED (CONT. FURN
HEAT TREATMENT ACE) AIR COOLED
960 º C 10 MIN

DESCRIPCION SUMINISTRO / DESCRIPTION OF DELIVERY

ITEM FAB. ITEM CLI. LONG.INDIV (M) COLADA Nº TUBOS LONG. TOTAL PESO(KG)
T.R. ITEM CLIENTS ITEM INDIVIDUAL LENGTH CAST NR. QUANTITY (M) WEIGHT
LENGTH

000010 6,000 125122 356 2.136,000 6.861

TOTAL 356 2.136,000 6.861

Lista de Bultos / Packing 655492

List

TUBOS REUNIDOS INDUSTRIAL GARANTIZA QUE TODOS LOS TUBOS CUBIERTOS POR ESTE CERTIFICADO CUMPLEN LOS REQUISITOS
DEL PEDIDO Y CON LAS ESPECIFICACIONES ARRIBA MENCIONADAS.
TUBOS REUNIDOS INDUSTRIAL CERTIFY THAT ALL THE TUBES COVERED BY THIS CERTIFICATE COMPLY WITH ORDER REQUIREMENTS AND ABOVE MENTIONED
SPECIFICATIONS.

AMURRIO 07.05.2020 CONTROL DE CALIDAD DE TUBOS REUNIDOS

INDUSTRIAL
TUBOS REUNIDOS INDUSTRIAL (QUALITY CONTROL)

Alex Villanueva
P.O:. :
 TUBOS REUNIDOS INDUSTRIAL, S.L.U
Barrio Sagarribai, 2 - 01470 AMURRIO (Spain)

QUALITY
MANAGEMENT
EN 10204:2004 / 3.1 SYSTEM
certified by
LRQA
CERTIFICADO DE CALIDAD
MILL TEST CERTIFICATE

PAG. 2 / 4
Nº 0000351454/1 Rev. 001
ENSAYOS NO DESTRUCTIVOS / NON DESTRUCTIVE TESTS

ENSAYO / TEST %CONTROL / TEST RATE(%) REQUISITOS / REQUIREMENTS RESULTADO / RESULT

VISUAL Y DIMENSIONAL / 100% O.K.

VISUAL & DIMENSIONAL INSP.

P.HIDROSTATICA/ 100% 2.970,0 PSI 5 SEC. O.K.

HYDROTEST

CORRIENTES INDUCIDAS/ 100% ASTM E 309. N12.5/HS 3.2 O.K.

EDDY CURRENTS MM

DISPERSION FLUJO/ 100% ASTM E 570. N12.5 O.K.

FLUX LEAKAGE

MAGNETISMO RESIDUAL / MAX 30,0 GAUSS

RESIDUAL MAGNETISM

ENSAYOS TECNOLÓGICOS Y METALÚRGICOS / TECHNOLOGICAL AND METALLURGICAL TEST

APLASTADO AC/ A/SA333/5L2018. PSL2 -OK DOBLADO AC/ A/SA333/5L2018. PSL2 -OK
/FLATTENING /BENDING

ANALISIS DE COLADA / CAST ANALYSYS

C Mn Si P S Cr Ni Mo Cu V Sn Ti Nb B N C.E.
MIN. 0,29 0,10
MAX. 0,20 1,35 0,45 0,020 0,0100 0,300 0,3000 0,1200 0,4000 0,0800 0,0400 0,0200 0,0010 0,42
125122 0,1390 1,26 0,21 0,008 0,0027 0,080 0,0600 0,0200 0,1878 0,0680 0,0092 0,0025 0,0025 0,0004 0,0087 0,40

ANALISIS DE PRODUCTO / PRODUCT ANALYSIS

C Mn Si P S Cr Ni Mo Cu V Sn Ti Nb B N C.E.
MIN. 0,29 0,10
MAX. 0,20 1,35 0,45 0,020 0,0100 0,300 0,3000 0,1200 0,4000 0,0800 0,0400 0,0200 0,0010 0,42
125122 0,1400 1,26 0,22 0,010 0,0027 0,100 0,0800 0,0300 0,1900 0,0700 0,0090 0,0030 0,0030 0,0001 0,0100 0,41
125122 0,1300 1,25 0,22 0,009 0,0027 0,100 0,0800 0,0300 0,1900 0,0690 0,0090 0,0030 0,0030 0,0001 0,0100 0,40

FORMULAS

(01)
MIN.
MAX. 0,150
125122 0,076
125122 0,075

(01) Nb + Ti + V

AMURRIO 07.05.2020 CONTROL DE CALIDAD DE TUBOS REUNIDOS

INDUSTRIAL
TUBOS REUNIDOS INDUSTRIAL (QUALITY CONTROL)

Alex Villanueva
P.O:. :
 TUBOS REUNIDOS INDUSTRIAL, S.L.U
Barrio Sagarribai, 2 - 01470 AMURRIO (Spain)

QUALITY
MANAGEMENT
EN 10204:2004 / 3.1 SYSTEM
certified by
LRQA
CERTIFICADO DE CALIDAD
MILL TEST CERTIFICATE

PAG. 3 / 4
Nº 0000351454/1 Rev. 001
ENSAYOS DE TRACCIÓN / TENSILE TEST

COLADA Nº L/T TP DIMENSION L.ELAST. R.TRACC. ALARG. Estricción DUREZA E / R

CAST (1) (2) ( mm ) YIELD POINT T.STRENGTH ELONG. Reduction HARDNESS
( Mpa ) (3) ( Mpa ) ( % ) of Area ( HRB )
(4) (%)

MIN. 360 460

MAX. 530 760 99 0,00

125122 1 L T 33,40 x 5,000 412 560 44 86 0,74

125122 3 L T 33,40 x 5,100 405 526 44 83 0,77
125122 4 L T 33,40 x 5,000 419 539 43 84 0,78
125122 5 L T 33,40 x 5,000 386 565 44 86 0,68
125122 6 L T 33,60 x 5,000 411 565 44 86 0,73
125122 7 L T 33,40 x 5,100 421 551 44 86 0,76
125122 8 L T 33,50 x 5,000 395 550 43 86 0,72
125122 9 L T 33,60 x 5,200 410 568 44 86 0,72
125122 10 L T 33,50 x 5,200 416 549 44 84 0,76
125122 11 L T 33,40 x 5,100 418 552 44 86 0,76
125122 12 L T 33,50 x 5,000 417 561 43 86 0,74
125122 13 L T 33,50 x 5,100 410 529 44 83 0,78
125122 14 L T 33,40 x 5,000 419 543 43 83 0,77
125122 15 L T 33,50 x 5,200 396 562 44 86 0,70
125122 16 L T 33,60 x 5,000 411 566 44 86 0,73
125122 17 L T 33,40 x 5,100 385 535 44 86 0,72
125122 18 L T 33,50 x 5,200 402 565 44 86 0,71
125122 48-43 L T 33,50 x 5,000 417 565 44 86 0,74

(1) : L = LONGITUDINAL // T = TRANSVERSAL

(2) : T = Full size tube // P = Strip specimen // C = Cylindrical // F = Flat specimen
(3) : yield point (0,5%)
(4) : Lo = 2" (50 mm)
ENSAYOS DE IMPACTO - CHARPY V / IMPACT TEST

COLADA Nº L/T DIMENS Tª RESILIENCIA AVG

CAST (1) ( mm ) (º C) IMPACT TEST ( J )
( J )

10 10,00 -50 21 / 27
10 10,00 -45 14 / 18

125122 1 L 10 2,50 -56 28 28 27 28

125122 48-43 L 10 2,50 -50 30 30 31 30

(1) : L = LONGITUDINAL // T = TRANSVERSAL

ENSAYOS DE TRACCIÓN A ALTAS TEMPERATURAS (T) Y/O ENSAYOS POST SOLDADURA (P) /
TENSILE TEST AT ELEVATED TEMPERATURE (T) OR / AND PWHT ( POST WELDING HEAT TREATMENT ) (P)

COLADA Nº P/T L/T TP DIMENSION Tª TRACC L.ELAST. R.TRACC. ALARG. DUREZA

CAST (1) (2) (3) (mm) YIELD POINT T.STRENGTH ELONG. HARDNESS
( Mpa ) (4) ( Mpa ) (%) (5) ( HRC )

MIN.
MAX.

125122 1 T L P 12,40 x 5,000 300 º C 382 541 34

AMURRIO 07.05.2020 CONTROL DE CALIDAD DE TUBOS REUNIDOS

INDUSTRIAL
TUBOS REUNIDOS INDUSTRIAL (QUALITY CONTROL)

Alex Villanueva
P.O:. :
 TUBOS REUNIDOS INDUSTRIAL, S.L.U
Barrio Sagarribai, 2 - 01470 AMURRIO (Spain)

QUALITY
MANAGEMENT
EN 10204:2004 / 3.1 SYSTEM
certified by
LRQA
CERTIFICADO DE CALIDAD
MILL TEST CERTIFICATE

PAG. 4 / 4
Nº 0000351454/1 Rev. 001

(1) : P = Ensayo Post Soldadura (Post Welding heat treatment ) // T = Ensayo Tracción Alta Tª (Tensile test at elevated temperature)
(2) : L = LONGITUDINAL // T = TRANSVERSAL
(3) : T = Full size tube // P = Strip specimen // C = Cylindrical // F = Flat specimen
(4) : yield point (0,5%)
(5) : Lo = 2" (50 mm)
ANEXOS / ANNEX

FULLY KILLED
RADIATION FREE
MERCURY FREE
NO WELD REPAIR

"T.R.I, S.L.U. HAS A QUALITY MANAGEMENT SYSTEM APPROVED BY LRQA IN

AGREEMENT WITH POINT 4.3 ANNEX I OF THE PED 2014/68/EU"

AMURRIO 07.05.2020 CONTROL DE CALIDAD DE TUBOS REUNIDOS

INDUSTRIAL
TUBOS REUNIDOS INDUSTRIAL (QUALITY CONTROL)

Alex Villanueva
P.O:. :
 Vallourec Soluções Tubulares do Brasil S.A. MILL TEST CERTIFICATE
Barreiro Plant - Av. Olinto Meireles, 65 (According to DIN EN 10204.3.1)
ZIP 30640-010 - Belo Horizonte, MG N°.: 0030037887 / 01 Sheet:1 / 5

Customer: ARROW PIPES & FITTINGS FZCO

Country: Utd.Arab.Emir. Material Number: 277137
Work Order: 541375 / 180
Customer Order: 1281001986 / PO.1227/12/2018
Inspection: Vallourec Soluções Tubulares do Brasil S.A.
_

DESCRIPTION OF PRODUCTS: SEAMLESS STEEL PIPE, HOT FINISHED , BEVELED ENDS 37,5 DEG. , NORMALIZED
DIMENSIONS: 60,30 mm X 5,54 mm GRADE: X52N # 6
STANDARD: API SPEC 5L, 04.2018, 46TH EDITION - PSL 2
IN ACCORDANCE ALSO TO THE STANDARDS: ASTM A 333M - 18 ASTM A 999M - 18 # ASME SA-333M - 17 ASME SA 999M - 17
CUSTOMER SPECIFICATION: APF-TS-A333/API 5L /BS EN10210 , 07.08.2016
SURFACE PROTECTION: EXTERNAL: LACQUER PIPE ENDS PROTECTOR: PLASTIC CAP
TOLERANCES: OUTSIDE DIAMETER (PIPE BODY): -0,45 mm / +0,45 mm WALL THICKNESS: -0,69 mm / +0,83 mm
TOLERANCES(PIPE ENDS): OUTSIDE DIAMETER: -0,40 mm / +0,80 mm
LENGTH: RANDOM 10000,00 mm - 11800,00 mm
STANDARD MARKING: Paint stenciled in the pipe body: 541375/180 MANUFACTURER SPEC 5L-0150.4 API MONOGRAM MONTH/YEAR ASTM/ASME A/SA 333M 60,30 X 5,54 X52N /6 PSL2 SMLS HEAT NUMBER LENGTH HF S
SCH 080 LT -48C 20500 KPA NACE MR 0175 NDE VSB LOGO
SHIPPING MARKING: MADE IN BRAZIL * ARROW PIPES & FITTINGS FZCO * P.O 1227/12/2018 * JEBEL ALI
_

Heat Pieces Lengths(m)

175584 46 484,55
177955 191 1999,02
177957 97 1024,32
Total 334 3507,89
_

THE PRODUCT IS SATISFACTORY IN THE FOLLOWING TESTS / INSPECTIONS: DIMENSIONAL # VISUAL # FLATTENING TEST # ENDS INSPECTION : UNTESTED ENDS CROPPED # HYDROSTATIC TEST: 20500,0 KPA
5 S # RESIDUAL MAGNETISM: MAX 20 GAUSS # ULTRASONIC TEST : API 5L, N5,LONG,E/I # ULTRASONIC TEST FOR LAMINAR DEFECTS: ISO10893-8-BACK WALL ECO #
_
 MILL TEST CERTIFICATE
(According to DIN EN 10204.3.1)
N°.: 0030037887 / 01 Sheet:2 / 5

Chemical Composition (%) Process: Basic Oxygen Furnace, heats fully killed
Ceq: C+Mn/6+(Cr+Mo+V)/5 +(Ni+Cu)/15 PCM: CE Pcm CE1: Nb + V + Ti CE2: Al(sol)/N

C Mn P S Si Ni Cr Mo Al Cu V Nb B Ti N Ca Ceq Pcm CE1 CE2

Heat Analysis Min 0,290 0,100 2,000
Max 0,180 1,350 0,015 0,003 0,400 0,300 0,300 0,120 0,060 0,350 0,080 0,020 0,0010 0,040 0,420 0,24 0,100
Product Analysis Min 0,290 0,100 2,000
Max 0,180 1,350 0,015 0,003 0,400 0,300 0,300 0,120 0,060 0,350 0,080 0,020 0,0010 0,040 0,420 0,24 0,100
Heat Control Lot
175584 030003199835 0,11 1,31 0,010 0,001 0,30 0,02 0,14 0,09 0,023 0,038 0,053 0,016 0,0004 0,003 0,0042 0,0015 0,388 0,21 0,072 5,470
Check 1 0,11 1,28 0,009 0,000 0,29 0,02 0,14 0,09 0,022 0,038 0,049 0,014 0,0001 0,003 0,0041 0,0013 0,388 0,21 0,066 5,490
Check 2 0,12 1,28 0,010 0,001 0,29 0,02 0,14 0,09 0,022 0,038 0,050 0,014 0,0001 0,003 0,0041 0,0013 0,389 0,21 0,067 5,490
177955 030003198788 0,12 1,31 0,011 0,002 0,29 0,04 0,14 0,08 0,028 0,080 0,050 0,016 0,0004 0,001 0,0059 0,0019 0,400 0,22 0,067 4,740
Check 1 0,12 1,31 0,010 0,002 0,31 0,04 0,14 0,08 0,028 0,081 0,051 0,016 0,0002 0,001 0,0055 0,0020 0,401 0,21 0,065 4,750
Check 2 0,12 1,32 0,010 0,002 0,31 0,04 0,14 0,08 0,028 0,082 0,052 0,016 0,0002 0,001 0,0055 0,0019 0,402 0,21 0,065 4,750
177957 030003201135 0,12 1,31 0,011 0,001 0,28 0,04 0,15 0,08 0,034 0,110 0,060 0,017 0,0004 0,002 0,0059 0,0015 0,406 0,21 0,079 5,200
Check 1 0,12 1,32 0,010 0,001 0,28 0,04 0,15 0,08 0,031 0,113 0,055 0,017 0,0001 0,002 0,0055 0,0015 0,409 0,22 0,074 5,310
Check 2 0,12 1,29 0,010 0,001 0,28 0,04 0,15 0,08 0,033 0,116 0,055 0,016 0,0001 0,002 0,0060 0,0014 0,404 0,21 0,073 5,390
Ceq: Carbon Equivalent; PCM: Parameter for crack measu CE: Combined Elements;
Tensile Test
Specimen Direction: Longitudinal Temperature: Room Temperature Wall Thickness: 5,54 mm Gauge Length: L0=2"
Method:Elong.Total Under Load 0,50 %

Type of Specimen Area YS TS E

(MM2) (MPA) (MPA) (%)
Required: Min 360 460 22
Max 530 760
Heat Control Lot
175584 030003199835 STRIP WIDTH 19,05 MM 130,2 447 565 36
STRIP WIDTH 19,05 MM 131,0 450 560 36
177955 030003198788 STRIP WIDTH 19,05 MM 123,2 431 569 33
STRIP WIDTH 19,05 MM 125,0 436 573 34
177957 030003200993 STRIP WIDTH 19,05 MM 123,8 428 560 30
STRIP WIDTH 19,05 MM 121,8 425 555 30
030003201135 STRIP WIDTH 19,05 MM 144,0 395 530 29
 MILL TEST CERTIFICATE
(According to DIN EN 10204.3.1)
N°.: 0030037887 / 01 Sheet:3 / 5

Tensile Test
Specimen Direction: Longitudinal Temperature: Room Temperature Wall Thickness: 5,54 mm Gauge Length: L0=2"
Method:Elong.Total Under Load 0,50 %

Type of Specimen Area YS TS E

(MM2) (MPA) (MPA) (%)
Required: Min 360 460 22
Max 530 760
Heat Control Lot
STRIP WIDTH 19,05 MM 142,9 391 522 29
YS-Yield Strength; TS-Tensile Strength; E-Elongation;
Hardness Test Through Wall
Scale: HV

Individual
Required: Min
Max 246,0
MW1 MW2 MW3 Avg
Heat Control Lot
175584 030003199835 Q1 164,0 165,0 168,0 165,7
177955 030003198788 Q1 157,0 155,0 156,0 156,0
177957 030003200993 Q1 173,0 170,0 170,0 171,0
030003201135 Q1 162,0 160,0 161,0 161,0
MW - Middle Wall;
Impact Test
Test Specimen: CHARPY 10X55X3.33 V NOTCH Direction: Longitudinal Temperature: -58°C
Striker radius: 8 mm
AE1 AE2 AE3 AE4 AE5 AE Avg
(J) (J) (J) (J) (J) (J)
Required: Min 4 4 4 7
Max
Heat Control Lot
175584 030003199835 47 53 53 52
177955 030003198788 48 52 52 54
177957 030003200993 48 53 54 52
 MILL TEST CERTIFICATE
(According to DIN EN 10204.3.1)
N°.: 0030037887 / 01 Sheet:4 / 5

Impact Test
Test Specimen: CHARPY 10X55X3.33 V NOTCH Direction: Longitudinal Temperature: -58°C
Striker radius: 8 mm
AE1 AE2 AE3 AE4 AE5 AE Avg
(J) (J) (J) (J) (J) (J)
Required: Min 4 4 4 7
Max
Heat Control Lot
030003201135 46 51 48 48
AE - Absorbed Energy;
_

Remarks:
MATERIAL IN ACCORDANCE WITH NACE MR 0175
PAR. 3.2/ISO 15156 (LATEST EDITIONS),
ANNEX A.2.1.2/NACE MR0103 PAR.2.1. ALL LATEST EDITIONS

MATERIAL:
- FINE GRAIN PRACTICE
- FULLY KILLED STEEL.
- NO WELD REPAR
- FREE OF MERCURY
- MATERIAL FROM BRAZIL
- RADIATION FREE

- MATERIAL FLATTENING TEST.

- NORAMLIZED
TEMPERATURE 895°C
SOAKING TIME 42 MINUTES
METHOD OF COOLING : STILL AIR

Steel Making:
During the steel making process, Vacuum degassing of the steel was performed.
This certificate cancels and replaces the previous one0030037887/00. The revision reason is:
INCLUSION OF RADIATION FREE
 MILL TEST CERTIFICATE
(According to DIN EN 10204.3.1)
N°.: 0030037887 / 01 Sheet:5 / 5

We hereby certify that this product has been manufactured and examined in accordance with QUALITY CONTROL DEPARTMENT DATE
all requirements of the standards and specifications and all the results are found to be FAX: (55-31) 3328-2773 12.10.2020
satisfactory. This testimonial and certificate respectively is recorded by a computer system and
is valid without signature. Alteration or use for others products are regarded as falsification of e-mail:luiz.silva@vallourec.com ENG. LUIZ FERNANDO DA SILVA - CREA-MG 58834-D
documents and will be subject to criminal jurisdiction. TECHNICAL RESPONSIBLE
 ★

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