Risk Assessment Template – UG Labs

Background

Assessment Title: Reaction Kinetics/Fixed Bed Catalytic Reactor

Assessment Outline:
In the Adiabatic Reactor Experiment, we will add hydrogen peroxide or sodium thiosulphate to the system. The
impeller will then be activated, and we will wait for the temperature to reach and stabilize at the desired level.
Subsequently, using a funnel, the second reactant will be introduced, and we will wait until a steady-state is
attained. Concurrently, temperature readings will be taken. After appropriately disposing of and cleaning the
apparatus with deionized water, we will conduct an additional five experimental runs.

For the fixed bed catalytic reactor experiment, solutions will be ready according to the specifications in Table 1.
Employing the photometer and the solutions detailed in Tables 1 and 2, a calibration curve will be established. The
necessary steps for the indicator reaction in single-use cells will be executed for the indicator reactor solutions,
and the reaction will be repeated under various operating conditions. Upon activation, rinsing, and draining of the
unit, the saccharose solution (prepared in accordance with Table 1) will be added to duct tank B1. Adjusting the
feed pump speed to achieve the required flow rate, we will then activate the water pump, heater, and feed pump.
Upon initiating the feed pump, the start time will be recorded, and after a 30-minute wait, a sample will be
collected.

Location: LB21

People at Risk (Delete or Mark as appropriate):

 Employees  Undergraduates

Hazards, Consequences, and Control Measures

Hazard Leakage of sulphuric acid

Potential
Chemical exposure, skin irritation, inhalation risks.
Consequences

Wear appropriate personal protective equipment (PPE) when handling sulphuric acid.
Control Measures Avoid handling in close proximity to the mouth/nose. Wash immediately after handling.
Follow established safety protocols for chemical handling.

Hazard Leakage of solution

Potential
Slips, head injuries, bodily harm
Consequences

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 Alert relevant laboratory technicians, place spill signs, and, if safe, promptly clean up the
Control Measures
spill with a cloth. Regularly inspect containers to ensure they are free of cracks.

Hazard Pump and Heater Operation

Potential Leakage of solution due to equipment and ancillary equipment damange, equipment
Consequences malfunction, burns.

Conduct regular maintenance on pumps and heaters, follow proper start-up procedures,
Control Measures
and monitor equipment during operation.

Hazard Temperature Fluctuations

Potential
Burns, overheating of equipment.
Consequences

Monitor and control the temperature carefully. Use safety mechanisms to prevent
Control Measures
overheating. Ensure proper insulation.

Risk Level
Use the table below to work out the risk level for the assessment using the current control measures.

Risk Level

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Appendix 1 – Hierarchy of Control

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