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Chinese Journal of Aeronautics, (2021), 34(4): 540–567

Chinese Society of Aeronautics and Astronautics


& Beihang University
Chinese Journal of Aeronautics
cja@buaa.edu.cn
www.sciencedirect.com

Machining of SiC ceramic matrix composites:


A review
Qinglong AN, Jie CHEN, Weiwei MING, Ming CHEN *

State Key Laboratory of Mechanical System and Vibration, School of Mechanical Engineering, Shanghai Jiao Tong
University, Shanghai 200240, China

Received 29 May 2020; revised 16 June 2020; accepted 11 July 2020


Available online 13 August 2020

KEYWORDS Abstract Continuous fiber reinforced SiC ceramic matrix composites (FRCMCs-SiC) are cur-
Ceramic matrix composites; rently the preferred material for hot section components, safety–critical components and braking
Machining; components (in the aerospace, energy, transportation) with high value, and have triggered the
Material removal mecha- demand for machining. However, the high brittleness, anisotropy, and heterogeneity of materials
nisms; bring great challenges to machining, due to high mechanical and thermal loads, severe tool wear,
Quality; and poor machining quality. With the increasing demand of FRCMCs-SiC parts, high-quality
Surface integrity and high-efficient machining has become a hot issue. This review paper provides a detailed literature
survey on the machining of FRCMCs-SiC. The material removal mechanism, defect form, and
interfacial mechanical properties of FRCMCs-SiC were summarized. The machining processes of
FRCMCs-SiC were introduced, and their respective advantages and disadvantages were compared.
Given the low machinability (high hardness, high brittleness, anisotropy, and heterogeneity) of
FRCMCs-SiC, preliminary experiments have proved that ultrasonic-assisted machining and
laser-assisted machining have shown unique advantages in reducing force and tool wear, improving

Abbreviations: 2D, two-dimensional; 3D, three-dimensional; AMG, Advanced Materials Gas-Generator; AWJ, abrasive waterjet; CBN, cubic
boron nitride; CD, conventional drilling; CF, conventional filing; Cf/SiC, carbon fiber reinforced SiC ceramic matrix composites; CFRP, carbon
fiber-reinforced polymer; CG, conventional grinding; CM, conventional machining; CMCs-SiC, silicon carbide ceramic matrix composites; CVD,
chemical vapor deposition; CVI, chemical vapor infiltration; DCLL, dual-coolant lithium lead; EDM, electrical discharge machining; FRCMCs,
continuous fiber reinforced ceramic matrix composites; FS, femtosecond; HCCB, helium-cooled ceramic breeder; IHPTET, Integrated High
Performance Turbine Engine Technology; LAM, laser-assisted machining; MQL, minimal quantity lubrication; MS, millisecond; NMQL,
nanofluid minimal quantity lubrication; NTM, non-traditional machining; OC, orthogonal cutting; PCD, polycrystalline diamond; PIP, polymer
infiltration pyrolysis; PLA, pulsed laser ablation; PS, picosecond; RMI, reactive melt infiltration; RUFM, rotary ultrasonic face milling; RUM,
rotary ultrasonic machining; RUSM, rotary ultrasonic slot machining; SCLL, self-cooled lithium lead; SiCf/SiC, SiC fiber reinforced SiC ceramic
matrix composites; UAF, ultrasonic-assisted filing; UAG, ultrasonic-assisted grinding; UAM, ultrasonic-assisted machining; UEET, Ultra-
Efficient Engine Technology
* Corresponding author.
E-mail address: mchen@sjtu.edu.cn (M. CHEN).
Peer review under responsibility of Editorial Committee of CJA.

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https://doi.org/10.1016/j.cja.2020.08.001
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This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Machining of SiC ceramic matrix composites 541

machining quality and machining efficiency. The machined surface integrity was discussed, the
influence of process parameters on the machined surface quality was analyzed, and the machining
defects of FRCMCs-SiC were summarized. But for FRCMCs-SiC, the existing quantitative evalu-
ation of the machined surface integrity was weak and unsystematic.
Ó 2020 Chinese Society of Aeronautics and Astronautics. Production and hosting by Elsevier Ltd. This is
an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

1. Introduction oxidation resistance of carbon materials, and have excellent


properties of lightweight, high-temperature resistance, good
With the development of aerospace and national defense, hot oxidation resistance, good corrosion resistance, good wear
section components of high thrust -weight ratio aeroengine, resistance, high damage tolerance. The United States, France,
thermal protection systems of hypersonic vehicles, hot section Japan, and other industrial powers have carried out a lot of
components of heavy launch vehicle propulsion systems, and researches on the preparation and application of ceramic
reusable rocket propulsion systems are in urgent need of new matrix composite materials, such as the USA IHPTET (Inte-
generation high-temperature materials. Taking aeroengine as grated High Performance Turbine Engine Technology), UEET
an example, the materials of hot section components need to (Ultra-Efficient Engine Technology) plan, and Japan AMG
withstand the high temperature of about 1100 °C.1 At present, (Advanced Materials Gas-Generator) plan, and have made
the most commonly used high-temperature materials of aero- many achievements in material development, preparation,
engine are nickel-base alloys, which can meet the service and application.7
requirements utilizing ultra-high temperature thermal barrier At present, there are two kinds of FRCMCs-SiC which are
coating.2 However, the combustion temperature of the new- widely used, carbon fiber reinforced SiC ceramic matrix com-
generation aeroengine will be further increased, and the tem- posites (Cf/SiC) and SiC fiber reinforced SiC ceramic matrix
perature reaching the surface of the material will reach at least composites (SiCf/SiC). The difference in performance leads
1400–1700 °C. The continuous increase of cooling has brought to their different application fields.
about an increase in the inefficiency loss of the aeroengine, so Cf/SiC composites are mainly used in friction materials and
the scheme of nickel-base alloys combined with ultra-high tem- high-temperature materials with short service life. Due to the
perature thermal barrier coating is difficult to meet the increasing demands on the speed, load, and safety of vehicles,
demand.3 Under the dual requirements of specific strength ordinary friction materials will fail under extreme braking con-
and high-temperature resistance, as shown in Fig. 1, compared ditions. Cf/SiC composites have many excellent properties:
with metal materials, silicon carbide ceramic matrix compos- high and stable friction coefficient, which is insensitive to
ites (CMCs-SiC) have advantages.4 Continuous fiber rein- changes in speed, load, and temperature; good wear resistance,
forced ceramic matrix composites (FRCMCs) is a kind of not easy to scratch and stick to the surface of the friction cou-
tough ceramic material, which is toughened by continuous ple, good run-in performance; strong environmental adaptabil-
fiber reinforced phase, and optimized by suitable weak inter- ity, good corrosion resistance, oil resistance, and humidity
phase between the SiC matrix and fibers.5 The toughening resistance; good mechanical properties; low density; long ser-
mechanism of FRCMCs is crack deflection and crack bridging, vice life, so it is regarded as the first choice for the new gener-
so high strength and high fracture toughness are both pos- ation of high-performance friction materials.8,9 In the field of
sessed.6 FRCMCs overcome the shortcomings of low- aircraft braking systems, the brake discs developed by DACC
temperature resistance and high density of metal materials, (South Korean) for the F16 fighter have been widely used. In
high brittleness and poor reliability of ceramic materials, poor the field of limousine braking systems, Cf/SiC brake discs have
been widely used in Porsche GT2 (as shown in Fig. 2(a)), Fer-
rari Enzo, Mercedes-Benz AMG, Corvette ZR1. In the field of
high-speed train braking systems, Cf/SiC brake discs have been
widely used in the French TGV NG, the British Heathrow
Express train, and the South Korean TCV train. The Cf/SiC
braking pads and brake discs of high-speed trains developed
by Central South University have been applied to high-speed
trains. Besides, Cf/SiC composites have been used in the brake
discs of construction machinery, wind turbines and heavy-duty
trucks.10 On the other hand, with the rapid development of
aerospace technology, the near-space, and space astronautics
technology involved in the new reusable hypersonic space sub-
orbital or orbital maneuvering vehicle has attracted increasing
attention, which puts forward strict requirements for the
design and manufacture of the thermal protection systems.
To meet the main technical characteristics (high reliability
and reusability) of the aircraft during hypersonic flight, orbit
or sub-orbit reentry, long-term in orbit reconnaissance, the
Fig. 1 Relationship between specific strength and temperature of thermal protection structural parts of the hypersonic aircraft
alternative aerospace materials.4 are required to have excellent comprehensive performance,
542 Q. AN et al.

Fig. 2 Application cases of Cf/SiC composites.

including heat protection, heat insulation, and load- (ARCOCE plug), which have been applied to CFM56 engines.
bearing.11,12 Cf/SiC composites not only have good chemical Since the late 1980s, GE began to study the preparation tech-
and thermal stability, high specific strength, low specific grav- nology of SiCf/SiC composites and has completed the applica-
ity and low thermal expansion coefficient, but also have high- tion verification of SiCf/SiC hot section components such as
temperature resistance, wear-resistance, and insensitivity to the insert for the leading edge of turbine rear frame, the inter-
cracks. So Cf/SiC composites are listed as key development stage platform, and the high-pressure turbine stator vane (as
materials of the thermal protection structural parts, such as shown in Fig. 3(a)) of the aeroengine.27 The LEAP-X1C
nose cone (as shown in Fig. 2(b)), guide vane, wing and cover engine used in the COMAC C919 aircraft was developed by
plate, for the new generation aerospace vehicles and hyper- CFM (a 50/50 joint company of Safran Aircraft Engines and
sonic vehicles.13–15 For missile and rocket engines, the engine GE), and some of the hot section parts, such as the low-
is developing in the direction of greater thrust, higher specific pressure turbine guide vane and high-pressure turbine shroud,
impulse, and higher thrust- weight ratio to increase the lift use SiCf/SiC composites. After investigation, the aeroengine
capacity. Therefore, it is inevitable to increase the area ratio hot section stator parts that have maturely applied SiCf/SiC
of the nozzle extension, use the nozzle material with better composites include first-stage and second-stage high-pressure
temperature resistance and lighter weight.16,17 Cf/SiC compos- turbine nozzles, first-stage high-pressure turbine shroud and
ites has been used in the HM7 cryogenic engine of the Euro- low-pressure turbine guide vane of CFM LAP-X engine; com-
pean Ariane upper stage, the RL10B-2 engine of the Delta Ⅴ bustion chamber inner/outer lining, first-stage high-pressure
upper stage, the RL10C-1 engine of the Atlas Ⅴ, the Vinci turbine shroud, first-stage and second-stage high-pressure tur-
engine of the Ariane Ⅴ upper stage, and the engine of China bine nozzles of GE9X engine28; third-stage low-pressure tur-
Yuanzheng 3 (as shown in Fig. 2(c)).18,19 Besides, Cf/SiC com- bine guide vane of F136 engine; combustion chamber lining
posites are used in aeroengines (such as outer flaps for M53-2 (CERASEP A415,29 as shown in Fig. 3(b)) and flameholder
and M88-2 jet engine20), satellite reflectors (such as the reflec- (CERASEP A410).30 The aeroengine hot section rotor parts
tor of the German Donier satellite space telescope, the reflector that have maturely applied SiCf/SiC composites include low-
of USA space telescope NGST, the reflector of Dutch radar pressure turbine rotor blades of F414 turbofan engine (as
telescope ATLID),21,22 sealing devices, magnetic vertical skid, shown in Fig. 3(c))24,30; low-pressure turbine rotor blades of
coal water slurry pressurized gasifier burner23. GE9x engine. Rocket engines that have successfully applied
SiCf/SiC composites are mainly used in high-temperature SiCf/SiC composites include: the integral thrust chamber of
structural parts and functional parts with long service life.24 the liquid rocket engine jointly developed by Hyper-Therm
SiCf/SiC composites have better oxidation resistance at high and Air Force Research Laboratory; the SCD-SEP rocket test
temperatures. Compared with nickel-base alloys, its working engine prepared by SEP (French).31 In the field of nuclear
temperature can be raised by more than 200 °C, which is suit- fusion, SiCf/SiC composites are considered promising candi-
able for manufacturing hot section components of aeroengine. dates for nuclear fusion reactors due to good radiation stabil-
It can reduce the weight of parts by more than 30%, improve ity and low tritium permeation. The application of SiCf/SiC
the fuel efficiency by more than 10%, and greatly reduce the composites in nuclear fusion reactors is mainly parts on the
emission of nitrogen oxides and other pollutants. SiCf/SiC first wall, flow channel inserts and divertors of the blanket.32
composites have been the first choice for the hot section com- As the material of first wall/blanket structure, SiCf/SiC com-
ponents of the new generation of high thrust-weight ratio aero- posites have good radiation damage resistance, good room
engines. Currently, hot section components such as exhaust temperature, and high-temperature mechanical properties,
nozzles of aeroengines, guide vanes, turbine blades, and tur- and can withstand high surface heat load. The blankets of
bine shroud are main applications.25,26 As the representatives the first wall made of SiCf/SiC composites are mainly SCLL
of the industry, SNECMA (France) and GE (USA), two major (Self-Cooled Lithium Lead) breeder blanket and HCCB
global aeroengine manufacturing giants, have invested a lot in (Helium-Cooled Ceramic breeder) blanket. The former
the design and preparation of SiCf/SiC composites compo- includes PPCS-D and TAURO of EU, ARIES-I and
nents, and developed a series of SiCf/SiC hot section compo- ARIES-AT of USA, and the latter includes DREAM and A-
nents with high reliability and long service life. Since the SSTR2 of Japan.33 The blankets of the flow channel inserts
early 1980s, SNECMA has successfully developed SiCf/SiC made of SiCf/SiC composites are mainly DCLL (Dual-
hot section parts such as engine nozzle flaps and exhaust cone Coolant Lithium Lead) blanket, including FDS-II of China,
Machining of SiC ceramic matrix composites 543

Fig. 3 Application cases of SiCf/SiC composites.

PPCS-C of EU.34,35 The blankets of the divertors made of as high as 2840–3320 kg/mm2, second only to diamond and
SiCf/SiC composites are mainly PPCS-D and TAURO of cubic boron nitride (CBN), so the tool wear is severe during
EU, ARIES-AT of USA and DREAM of Japan.36 Besides, cutting. And its high brittleness is easy to cause cracks, pits,
SiCf/SiC composites can absorb the energy of electromagnetic fiber damage, interface debonding, and other defects on the
waves and dissipate into thermal energy, which reduces elec- machined surface.43 Different from metal materials, there is
tromagnetic wave reflection, and has excellent absorption per- no surface strengthening to improve the machined surface of
formance at room temperature and high temperature. FRCMCs-SiC after finishing. Therefore, the defects and dam-
Therefore, SiCf/SiC composites are particularly suitable for ages caused by machining will permanently exist in the parts,
high-temperature stealth materials, used for heads of cruise which directly affect the thermal–mechanical properties, relia-
missiles, nozzles of the engine, and the surface of hypersonic bility, and service life of the parts. The existing machining pro-
vehicles, to achieve the radar stealth function of weapon cesses have the limitations of poor machining quality, low
equipment.37,38 precision, extremely low machining efficiency, and extremely
For FRCMCs-SiC parts, the process of part preparation or high machining cost, and are unable to meet the high-quality
repair of damaged parts is shown in Fig. 4. The SiC matrix and efficient requirements for the machining of FRCMCs-
preparation processes of FRCMCs mainly include polymer SiC parts, and are also difficult to meet the damage tolerance
infiltration pyrolysis (PIP),39 chemical vapor infiltration design and long-life service performance requirements. So far,
(CVI),40,41 and reactive melt infiltration (RMI),42 etc. Different the material removal mechanism and machining process of
preparation processes have their advantages. During the FRCMCs-SiC are still being explored.
preparation of the FRCMCs-SiC, the dimensional accuracy This paper comprehensively reviews the research progress
and geometric tolerance cannot be accurately guaranteed, of the material removal mechanism, machining process, and
and the surface quality is poor. Therefore, for the assembly surface integrity in the machining of FRCMCs-SiC (as shown
surface and functional surface, machining is indispensable in in Fig. 5). By summarizing the achievements of different
the preparation process of FRCMCs-SiC parts.43 research teams, the challenges needed to be urgently solved
With the development of the preparation technology, the of machining FRCMCs-SiC in a wide range of engineering
application of FRCMCs-SiC in aerospace, transportation, applications are pointed out, and the further research direc-
energy, and other fields is becoming more and more extensive. tions of FRCMCs-SiC machining is prospected.
Machining technology has become one of the main technical
bottlenecks restricting its extensive engineering application, 2. Material removal mechanism
while the research on the machining of FRCMCs-SiC is still
in infancy. FRCMCs-SiC has the characteristics of high hard- Machining is a kind of subtractive manufacturing, which uses
ness, high brittleness, heterogeneity, and anisotropy, so the cutting tools or abrasive particles to remove materials. The
machinability is extremely poor. The microhardness of SiC is material removal mechanism directly affects the physical phe-
nomena during machining (force, heat, deformation, etc.) and
the quality after machining. Therefore, it is of great signifi-
cance to understand the material removal mechanism of
FRCMCs-SiC for realizing high quality and high-efficiency
machining.

2.1. Material removal mechanism based on orthogonal cutting

For machining (such as milling, drilling, turning) using cutting


edge tools, orthogonal cutting (OC) is the most commonly
used basic experiment to study the material removal mecha-
nism. In order to explore the material removal mechanism
Fig. 4 Conventional process of preparation and repair of and ductile–brittle transition in the cutting, Diaz and Axinte44
FRCMCs-SiC parts. conducted orthogonal cutting experiments on three typical
544 Q. AN et al.

Fig. 5 Content overview on material removal mechanism, machining processes and surface integrity evaluation of FRCMCs-SiC.

fiber orientations of Cf/SiC composites. As shown in Fig. 6, the 2.2. Material removal mechanism based on scratching
material removal mechanism is significantly different along
different fiber orientations and in different cutting depths. For machining (such as grinding) using abrasive, scratch
When the cutting thickness is small, the cutting is dominated experiments are often used to study the material removal
by the shear behavior of composites when cutting along longi- mechanism. In order to study the grinding characteristics of
tudinal fibers and the shear behavior of matrix when cutting 2D Cf/SiC composites in different fiber orientations, Liu et al.45
along across fibers and transverse fibers, which is similar to carried out a single abrasive scratch experiment with a dia-
the ductile removal. When the cutting thickness increases to mond indenter on a grinding machine and analyzed the grind-
a certain value, the cutting is dominated by the initiation ing mechanism. Within the scratch depth range (from 10 lm to
and propagation of the fiber–matrix interface crack when cut- 50 lm), the brittle removal combining the layered brittle frac-
ting along longitudinal fibers and across fibers and the ture of carbon fibers and the cracking of SiC matrix was the
bending-induced fracture of fibers when cutting along trans- material removal mechanism. Fig. 7 shows the scratch mor-
verse fibers, which is a typical brittle removal. On this basis, phology of 0°-fiber and 90°-fiber along the scratch angle of
an analytical cutting model based on the inelastic behavior 0° and 45° respectively. The tearing damage caused by bending
and fracture mechanics of orthotropic anisotropic brittle com- and peeling off of carbon fibers is observed. Li et al.46 designed
posites has been proposed, which is helpful to understand the a new single abrasive scratch test by using CNC machining
surface integrity in the machining.
Machining of SiC ceramic matrix composites 545

Fig. 6 Pictures of material removal captured by high-speed camera.44

center, and carried out experiments along longitudinal fibers nism. Therefore, it is worth exploring the interfacial mechani-
and along across fibers. Within the set scratch depth range cal properties of FRCMCs-SiC, which provides a basis for the
(from 10 lm to 100 lm), the conclusion that brittle fracture research of material removal mechanism and simulation
(including matrix cracking, fiber breakage, fiber pull-out and modeling.
fiber–matrix interfacial debonding) is the main material To evaluate the properties of fiber–matrix interphase,
removal mechanism in grinding of Cf/SiC composites was also micromechanical tests are effective means, such as single fiber
obtained, and brittle fracture led to severe subsurface damage. pull-out tests, microbond tests, fiber push-out tests, and single
Therefore, under large scratch depth, the brittle fracture, fiber fragmentation tests.47 For Cf/SiC composites, Zhang
which is composed of matrix crushing, debonding of the et al.48 used Berkovich indenter to push out and push back car-
fiber–matrix interface, and fiber fracture (bending fracture, bon fiber of 50–100 lm thick sample on Nanoindenter to test
compression fracture, and shear fracture), is the recognized the interfacial shear strength and interfacial friction coefficient
material removal mechanism. of pyrolytic carbon. Fig. 8 shows the load–displacement curve
and interfacial crack propagation diagram of the typical fiber
2.3. Nano/micro-scale material properties and removal extrusion process, which can be divided into four stages: elastic
mechanism deformation of carbon fiber, push in stage (crack initiation),
push out stage (crack propagation), and contact between
Fiber-SiC matrix interphase is an important component of indenter and matrix. Based on this, the interfacial shear
FRCMCs-SiC. The debonding of weak interphase leads to strength can be calculated. Furthermore, the interfacial fric-
stress relaxation at the crack tip, which achieves the purpose tion coefficient of pyrolytic carbon can be obtained by pushing
of material toughening and damage tolerance improvement.5 the debonded carbon fiber back. This study provides a theoret-
Weak interfaces are prone to damage such as debonding dur- ical basis for the numerical simulation of interfacial mechanics
ing machining, and free fibers caused by interphase debonding and the analysis of the material removal mechanism in the
have an important influence on the material removal mecha- machining.
546 Q. AN et al.

Fig. 7 Scratch morphology.45

Fig. 8 Load-displacement curve and interfacial crack propagation diagram of single fiber push-out test with Berkovich indenter.48

Besides understanding the material removal mechanism on regime of Cf/SiC composites can be subdivided into micro brit-
the macro scale, studying the material fracture and removal of tle fracture regime and macro brittle fracture regime. In the
FRCMCs-SiC at the micro/nano scale is of great significance micro brittle fracture regime, under the extrusion of the inden-
for analyzing the mechanism of defect formation during mate- ter, cracks initiate inside the carbon fiber and propagate
rial removal and improving machining quality. Nano scratch between the graphite crystallites, resulting in the material
experiments is an effective method to study the fracture behav- removal of the fiber. In the macro brittle fracture regime, fibers
ior and damage mechanism of materials.49 Generally, as the are debonded from the SiC matrix under the extrusion of the
scratch depth increases, the elastic deformation, plastic defor- indenter, and then bending fracture (or compression fracture
mation, ductile–brittle transition and brittle fracture appear in and shear fracture) occurs. Fig. 9 shows graphic illustrations
the scratches of single-phase hard and brittle materials in of the micro–macro brittle fracture transition of carbon fibers
sequence.49–51 However, FRCMCs-SiC contain fiber- when scratching along different fiber orientations. Different
reinforced phase, SiC matrix, and weak interphase, and the material removal mechanisms form different machined sur-
material removal mechanism in the brittle fracture is more faces and cause different machining defects.
complicated. The SiC matrix is always removed by crushing For SiCf/SiC composites, Diaz et al.54 obtained the
in the brittle regime. But the material removal mechanism of machined surface by drilling. The material fracture behavior
fibers in the brittle regime is more complicated. The high- and removal mechanism in the cutting was understood based
hardness SiC ceramic matrix has good support for fibers. on the microstructure, residual stress, and element distribu-
When the scratch depth is sufficiently large, bending-induced tion. The material fracture behavior and removal mechanism
fracture, compression-induced fracture, and shear-induced of each phase were summarized, as shown in Fig. 10. Hi-
fracture are the fracture forms of fibers,45,46 which are consis- Nicalon fiber is composed of 3C SiC nanocrystals and graphite
tent with the fracture forms of fibers in carbon fiber-reinforced microcrystals, which are removed by a brittle transgranular
polymer (CFRP).52 But when the scratch depth is small, the cleavage fracture during cutting. The SiC matrix prepared by
brittle fracture mode of the fiber changes. Chen et al.53 con- the MI process is composed of 6H-SiC microcrystalline, which
ducted nano-scratch experiments on unidirectional Cf/SiC simultaneously occurs ductile removal and brittle fracture (in-
composites along different fiber orientations. According to tergranular fracture) during cutting. The interphase layer of
whether the brittle fracture of the carbon fiber occurs inside CVI-SiC is formed by ultrafine columnar crystals, which frac-
the fiber or the whole fiber as the smallest unit, the brittle ture along the columnar direction during cutting. The fracture
Machining of SiC ceramic matrix composites 547

ior. These basic works are beneficial to analyze the mechanism


of machined surface generation and machining defects in the
machining of FRCMCs-SiC, and also have guiding signifi-
cance for process optimization.

3. Machining process of FRCMCs-SiC

The processing technology of FRCMCs-SiC is the key factor


to promote industrial application. NASA mentioned in the
‘‘Aeronautical technologies for the twenty-first century” that
the preparation process and processing technology of ceramic
matrix composites will be given priority in the future research
plan of engine materials.55 The processing technologies of
FRCMCs-SiC mainly includes conventional machining (CM)
(such as grinding, milling, drilling), ultrasonic-assisted machin-
ing (UAM) and laser-assisted machining (LAM), non-
traditional machining (NTM) (such as abrasive waterjet
(AWJ) machining, electrical discharge machining (EDM),
pulsed laser ablation (PLA)), etc. Besides, some basic
researches (such as orthogonal cutting and scratching) have
also been carried out. Papers on the processing of FRCMCs-
SiC were collected (since the core contents of most theses
had been published in various journals, so the theses are not
counted in the figure), and were classified, as shown in
Fig. 11. Since 2015, the number of publications on
FRCMCs-SiC processing has grown significantly, especially
for machining, and most of the research teams are from China.
Different processing technologies have different functions.
Machining is mainly used for the material removal of large
machining allowance and obtaining high-precision/high-
quality structures and surfaces. AWJ is mostly used for
through cut. EDM is suitable for obtaining complex structural
parts. PLA is mainly used for the processing of fine structures
(micro-holes, micro-grooves).
Because of the wide application and various challenges of
FRCMCs-SiC machining, the following is an overview of
machining, including CM, UAM, LAM.

3.1. Conventional machining (CM)

Conventional machining is indispensable in the study of


machining. It is of great significance to understand the mate-
rial removal mechanism of FRCMCs-SiC during machining,
optimize the machining parameters, and provide directions
for the improvement of machining processes. In this section,
the conventional machining of FRCMCs-SiC will be dis-
cussed. Grinding and cutting will be introduced separately.
As hard materials, SiC matrix and fibers cause severe tool
wear during machining. Therefore, at the current research
stage, most researchers use diamond abrasive tools to study
Fig. 9 Graphic illustrations of micro–macro brittle fracture
the grinding process. For the study of surface grinding, on
transition of carbon fibers caused by the increase of scratch
the one hand, it is to study the processing technology of planar
depth.53
structure, on the other hand, it is to explore the influence of
grinding parameters and the material removal mechanism in
behavior and material removal mechanism of each phase are the grinding process. Tashiro et al.56 conducted a dry grinding
different due to the difference in the microstructure. test of Cf/SiC composites, and found that carbide tools cannot
According to the researches of the mechanism, the physical be used due to catastrophic tool wear, and diamond wheels are
phenomena of SiC ceramic matrix composites in the mechan- better than WA wheels. Tawakoli and Azarhoushang57,58
ical material removal process are well understood, such as developed a metal-bonded segmented diamond wheel and pro-
material fracture mechanism, material removal mechanism, posed that intermittent grinding can reduce the grinding force
interfacial mechanical properties, and material damage behav- and grinding temperature, but the acting force on each
548 Q. AN et al.

Fig. 10 Material removal mechanism of each phase of SiCf/SiC composites during cutting.54

Fig. 11 Summary of publications on processing of FRCMCs-SiC.109-126

abrasive is large, and the main wear mechanisms of the seg- on the grinding force, force ratio, specific grinding energy, sur-
mented wheel are the inter-crystalline grain fracture and grain face topography, surface roughness, and grinding chips. Du
pull-out. Zhang et al.59,60 conducted grinding experiments on et al.62 explored the effects of different grinding directions
three typical fiber orientations of unidirectional Cf/SiC com- (essentially different fiber orientations) on the grinding process
posites, and proposed that besides grinding parameters (feed and surface roughness of 2D Cf/SiC composites. Qu et al.63
rate, grinding depth, grinding speed), fiber orientations also studied the effects of grinding parameters on the surface
greatly affected grinding force and surface morphology, and roughness of 2.5D needle Cf/SiC composites, and proposed
preliminary proposed the material removal mechanism of that the changes of grinding parameters mainly play a role
Cf/SiC composites in grinding. As shown in Fig. 12, brittle by changing the undeformed chip thickness. Qu et al.64 also
fracture is the main material removal mechanism in grinding. mentioned that the fiber orientation angle was an important
When grinding along across fibers, the interface is subject to parameter that affected the grinding process of Cf/SiC com-
the first failure form (opening mode), and the fiber is mainly posites. In general, grinding force and surface roughness
subjected to shear stress. When grinding along longitudinal increase with the increase of grinding depth and feed rate,
fibers, the interface is subjected to the second failure mode and decrease with the increase of grinding depth, and fiber ori-
(shearing mode), and the fiber is subjected to in-plane shear entation is also an important factor. As for the material
stress. When grinding along transverse fibers, the interface is removal mechanism in the grinding, there is consensus that
subjected to the third failure mode (tearing mode), and the brittle fracture is the main removal mechanism.59–64 Under
fiber is subjected to shear stress and tensile stress. Liu et al.61 the respective experimental conditions, the material failure
conducted grinding experiments on 2D Cf/SiC composites, modes are basically described as matrix breakage, fiber frac-
and systematically studied the effects of grinding parameters ture, and interfacial debonding.
Machining of SiC ceramic matrix composites 549

the MQL grinding performance of unidirectional Cf/SiC com-


posites, and optimized based on grinding force and surface
roughness. Furthermore, Qu et al.70 proposed carbon nano-
fluid MQL (NMQL) to grind Cf/SiC composites, and verified
the effectiveness of NMQL in reducing grinding force and
improving surface roughness through experiments. But it is
worth noting that FRCMCs-SiC contains pores limited by
the preparation process. Therefore, the liquid in the MQL
grinding process may penetrate into the pores of the workpiece
through capillary action, and it is difficult to remove. Whether
these liquids will directly affect the performance of the parts is
worth discussing, and in some extreme service environments
(ultra-high temperature, vacuum), these liquids may directly
damage the FRCMCs-SiC parts through vaporization. There-
fore, just like CFRP, the use of MQL (or other coolants) in the
machining of FRCMCs-SiC requires further cautious research.
For hole machining, Xing et al.71 conducted drilling exper-
iments of unidirectional Cf/SiC composites by using brazed
diamond drills, analyzed the influence of drilling parameters
on thrust force, delamination factor, hole surface quality,
and tool wear, and adopted supported graphite plate to reduce
the exit damage. The experimental results showed that high
speed and low feed rate were effective in improving the drilling
quality.
Because of the high hardness of FRCMCs-SiC, diamond
abrasives are used in most machining processes, but the limita-
tions of low machining efficiency and low machining accuracy
are obvious. The use of cutting edge tools for machining can
improve machining accuracy and increase machining effi-
ciency. Diaz et al.54,72 tried to use the cutting process to
machining SiCf/SiC composites. As shown in Fig. 13, the ran-
dom positions and sizes of warp, weft, and porosity in the
matrix were simulated by a probabilistic method based on
the random relative content of fiber and matrix faced by the
main cutting edge of the bit. Considering the randomness of
the inhomogeneous structure of the material, the hard charac-
teristics of the material are coupled to calculate the tensile
stress of the tool according to its diameter. And the influence
of material heterogeneity and high hardness on the premature
tool breakage of small diameter bit in the drilling of SiCf/SiC
composites was analyzed. Zhang et al.73,74 used carbide tools
to mill Cf/SiC composites, studied the influence of milling
parameters on milling force and surface roughness and estab-
lished a milling force analysis model of Cf/SiC composites con-
sidering the randomness of fiber distribution and tool wear.
Due to the ultra-high hardness of FRCMCs-SiC, the wear
Fig. 12 Schematic diagrams of grinding along three typical
of carbide tools in the machining is sharp and difficult to meet
directions.59
the demand. In order to solve the catastrophic tool wear of
carbide tools, Hu et al.75, Chen et al.76 and Zou et al.77 respec-
Because of the problems of high force, serious wheel wear, tively discussed the feasibility of polycrystalline diamond
and low surface quality in grinding, minimal quantity lubrica- (PCD) tools used in milling and drilling of Cf/SiC composites,
tion (MQL) was tried. MQL is a green, clean and efficient and obtained good effects. Hu et al.75 successfully explored the
cooling and lubrication method, which has been widely used use of PCD tools for slot milling 2D Cf/SiC composites. Chen
in the machining of ceramics and various metals.65,66 Based et al.76 explored the use of PCD tools for drilling experiments,
on this successful application, MQL is tried to be used in the analyzed the impact of thrust force on the hole exit defects, dis-
machining of FRCMCs-SiC. Adibi et al.67 and Esmaeili et al.68 covered the transition of the material removal mechanism of
proposed the application of MQL when grinding Cf/SiC com- carbon fibers in the brittle regime caused by changes in drilling
posites. By comparing with dry grinding, it was found that parameters, and creatively defined the micro brittle fracture
MQL grinding effectively reduced grinding force and surface and macro brittle fracture. As shown in Fig. 14, with the
roughness, alleviated grinding wheel wear, and improved increase of cutting depth, the material removal mechanism of
grinding efficiency. Qu et al.69 studied the influence of nozzle carbon fibers changes from micro brittle fracture to macro
direction, air pressure, oil flow rate and nozzle distance on brittle fracture. The micro brittle fracture of carbon fibers in
550 Q. AN et al.

Fig. 13 Probability modeling of tool imbalance in cutting of hard heterogeneous materials (SiCf/SiC composites).72

different fiber orientations is caused by the initiation and prop- and efficiency.78–81 For the surface, slot, hole, and cavity struc-
agation of microcracks generated by the extrusion of cutting tures of FRCMCs-SiC parts, corresponding UAM are pro-
edge. However, the macro brittle fracture in different fiber ori- posed respectively. In this section, UAM processes will be
entations is different, including bending-induced fracture, introduced for different structural features to be machined.
compression-induced fracture, shear-induced fracture, and Grinding is the main process of high-quality surface finish-
interfacial debonding. Zou et al.77 studied the effect of PCD ing. Azarhoushang and Tawakoli82 invented a block sonotrode
tool angles (clearance angle and point angle) on the thrust to achieve ultrasonic assisted grinding of Cf/SiC composites on
force, hole exit damage and surface quality in 2D Cf/SiC com- a traditional grinder by ultrasonically vibrating the workpiece,
posites drilling and tried to improve the efficiency of hole exit and proved that the grinding force was reduced by 20% and
quality evaluation by using the damage identification method the surface roughness was reduced by 30% under ultrasonic
based on image processing technology. vibration. Ding et al.83 clamped the diamond brazed grinding
Obviously, conventional machining of FRCMCs-SiC can wheel on the ultrasonic tool holder, realized the ultrasonic-
be realized by using superhard tools (diamond abrasive tools, assisted grinding of Cf/SiC composites through the ultrasonic
PCD tools). However, the disadvantages of CM are inevitable, vibration of the wheel, and proved that the normal grinding
such as high force during the machining, poor machined sur- force was reduced by 9–21%, the tangential grinding force
face quality, serious machining defects, and serious tool wear. was reduced by 9.7–19.4%, and the maximum reduction per-
In order to meet the indexes of the machining quality, the centage of surface roughness was 12%. Workpiece vibration
machining efficiency is often sacrificed in the production, and tool vibration are two ways to realize UAM (as shown
which is detrimental to reduce the machining costs. in Fig. 15). Based on the principle of relative motion, the effect
of the two methods is the same, and which one should be
3.2. Ultrasonic-assisted machining (UAM) selected in the production should take into account the existing
equipment and cost.
In the process of CM, the problems of large cutting (grinding) For the inner surface machining of deep cavity parts, the
force, many machining defects, large surface roughness and tool holder and parts are easy to interfere, and the machining
low machining efficiency need to be solved. UAM technologies accuracy and quality are difficult to guarantee, which are great
are applied to FRCMCs-SiC. For hard and brittle materials, challenges. Wang et al.84 elaborated the concept of ultrasonic-
UAM has an excellent effect in improving machining quality assisted filing (UAF) and first applied it to the machining of
Machining of SiC ceramic matrix composites 551

Fig. 14 Material removal mechanism of carbon fibers in cutting of Cf/SiC composites.76

Cf/SiC composites. Compared with conventional grinding ultrasonic-assisted drilling experiments on an ultrasonic dril-
(CG) and conventional filing (CF), UAF reduced surface ling machine and first proposed that ultrasonic-assisted drilling
roughness and improves shape accuracy. of Cf/SiC composites had advantages in machinability and cost
For larger-size holes, drilling is essential. For compared to other feasible machining processes. Li et al.86 pio-
FRCMCs-SiC, the machining technology which combines dia- neered the use of rotary ultrasonic machining (RUM) in the
mond abrasive tool and UAM is concerned. Hocheng et al.85 drilling of SiCf/SiC panels, studied the influence of machining
used abrasive slurry and stainless steel tools to carry out parameters (spindle speed, feed rate, ultrasonic power) on the
552 Q. AN et al.

Fig. 15 Two modes to realize RUM.

force, material removal rate, and hole quality, and proposed ment. Based on the grinding principle and parameter fitting,
that RUM significantly reduced the cutting force by about Zhang et al.93 and Yuan et al.94 established a dynamic cutting
50% and improved the machining efficiency by about 10%, force model for side-milling of Cf/SiC composites in RUM,
and high-quality holes could be obtained under the appropri- and analyzed the change of cutting force with spindle speed,
ate machining parameters. Ding et al.87 used diamond core feed rate and milling width based on the model and experi-
drill to drill Cf/SiC composites, and studied the influence of ment. Li et al.95,96 used the conical diamond abrasive tool
machining parameters on drilling force and drilling quality. for rotary ultrasonic face milling (RUFM) (as shown in
Compared with conventional drilling (CD), in rotary ultra- Fig. 17(b)), and proposes that compared with conventional
sonic drilling, the thrust force was reduced by 7.4%–23%, milling, the machining efficiency of RUFM was improved by
the torque was reduced by 8.5%-47.6%, the surface roughness 5.8 times and the surface quality of RUFM was improved by
of hole wall was reduced and the maximum reduction percent- 54.4%. Different from cylindrical diamond tools, the conical
age was 23%. Feng et al.88 and Wang et al.89 discussed the surface of the tool made abrasive grains cut intermittently
RUM of Cf/SiC composites (as shown in Fig. 16(a)). The under ultrasonic vibration (in other words, the abrasive grains
effects of machining parameters (spindle speed, feed rate, and the workpiece have periodic separation characteristics).
ultrasonic amplitude) on the exit defects and the microstruc- The milling force model of Cf/SiC composites was established
ture of the machined surface were studied. It is proposed that based on the abrasive kinematics and indentation principle,
the ultrasonic vibration of diamond abrasive tools improved and the influence of milling parameters on milling force was
the surface quality by changing the mechanism of fiber frac- analyzed. Based on the research of Li, Yuan et al.97 proposed
ture, and the tearing defect at the hole exit was averagely to quantify the material removal mode by the maximum pen-
reduced by more than 50%, but the mechanism has not been etration depth of diamond abrasive in the workpiece material
studied in depth. Wang et al.90 analyzed the correlation and proposed the transition of material removal mechanism
between cutting force and ultrasonic power and proposed that from ductile to brittle fracture. Babbar et al.98 used diamond
the adverse effect of tool wear on the increase of cutting force abrasive tools for rotary ultrasonic milling of Cf/SiC compos-
was restrained by adjusting the tuning frequency. In addition, ites. The effects of material density, feed speed, and axial
Wang et al.91 proposed to use a compound step-taper drill (as milling depth on the machining were investigated. It was found
shown in Fig. 16(b)) to reduce the exit damage in the RUM of that as the material density increased, machinability decreased
Cf/SiC composites, and the experimental results showed that but surface quality improved.
the tearing size was reduced by 30%. Overall, the effect of Besides ultrasonic-assisted machining with diamond abra-
RUM in reducing drilling force, hole wall roughness and sive tools, ultrasonic-assisted milling with cutting edge tools
machining defects on hole exit is considerable. is also an option. Liu et al.99 performed ultrasonic-assisted
RUM is also used in slot milling and face milling. Bertsche milling experiments of Cf/SiC composites by using CVD dia-
et al.92 first proposed the application of rotary ultrasonic slot mond coated carbide milling tool. Compared with conven-
machining (RUSM) in the milling of FRCMCs-SiC (as shown tional milling, UAM respectively reduces the wear band
in Fig. 17(a)), and optimized the milling parameters and width of the side edge and the bottom edge flank by 28.06%
designed diamond tools. Compared with the conventional dia- and 33.12%. But obviously, for Cf/SiC composites, the wear
mond grinding, RUSM reduced the radial force by 20%, of diamond coated carbide tools is still very serious. Chen
reduced the axial force by 9%, reduced tool wear by 36%, et al.100 studied the feasibility of using PCD tools for Cf/SiC
but increased the surface roughness slightly, which may be composites UAM (as shown in Fig. 18). The experimental
related to the influence of fiber orientation during measure- results showed that the appropriate ultrasonic amplitude
Machining of SiC ceramic matrix composites 553

Fig. 16 Rotary ultrasonic machining-drilling.

Fig. 17 Rotary ultrasonic machining-milling.


554 Q. AN et al.

effectively reduced the surface roughness, but increased the LAM process is still in the exploratory stage. Rozzi and Bar-
specific milling energy. The nano-scratch experiment proved ton106 first used the laser to preheat the Cf/SiC composites,
that there is a micro–macro brittle fracture transition of Cf/ and then used a PCD tool to remove the material (Fig. 19
SiC composites during material removal.53 This transition still (a)). Compared with conventional milling, the cutting force
exists in milling. The high-frequency hammering of the cutting during LAM was greatly reduced by 40%, which was con-
edge on the workpiece promotes the initiation and propagation ducive to improving machining efficiency and reducing pro-
of micro-cracks within the carbon fiber due to the appropriate duction costs. Therefore, LAM is a feasible process for
tool amplitude, thereby promoting the removal of the carbon FRCMCs-SiC. For laser-assisted micro-slot milling of SiCf/
fiber material with micro-brittle fracture, which effectively SiC composites (as shown in Fig. 19(b)), Dong et al.107 opti-
reduces the machined surface roughness. And the cutting- mized the machining parameters based on the finite element
edge hammering effect reduces the tensile residual stress, and simulation of the three-dimensional transient temperature field
even generates compressive residual stress. and studied the influence of laser heating on tool wear and tool
Extensive experiments have proved that, for both abrasive life. Compared with conventional milling, LAM reduced tool
tools and cutting-edge tools, UAM is beneficial to reduce wear by up to 76%, improved tool life by up to 3.8 times,
machining force, machined surface roughness, and machining and reduced the tool costs by up to 32.3%. Erdenechimeg
defects, which is of guiding significance for the machining of et al.108 optimized the machining parameters of laser-assisted
FRCMCs-SiC. From the perspective of machining quality, milling of Cf/SiC composite laminates. The preheating temper-
UAM can effectively reduce machining defects and machined ature was simulated based on the finite element method to
surface roughness. From the perspective of machining cost determine the effective cutting depth. Based on the Taguchi
(without considering the equipment cost), compared with method, the experimental design was performed, and the vari-
CM, UAM is beneficial to improve machining efficiency under ance analysis was used to analyze the experimental results.
the same machining quality indexes, thereby reducing the When other machining conditions were the same, LAM
machining cost. But the effects of high-frequency vibration reduced the cutting force by up to 40.7% and reduced the sur-
of cutting edge and abrasive grains on the material removal face roughness by up to 33.8%.
mechanism and damage behavior of FRCMCs-SiC need to Limited by the equipment, there is relatively little research
be further explored. on LAM of FRCMCs-SiC, and the focus is on feasibility anal-
ysis. For FRCMCs-SiC, LAM is a feasible process to reduce
3.3. Laser-assisted machining (LAM) machining force and improve machining quality. However,
more exploration is needed, such as the effect of laser on mate-
Due to the high hardness and high brittleness of FRCMCs- rial thermal damage, process parameter optimization, LAM
SiC, the material is removed by brittle fracture during cutting equipment development.
and grinding, so the machined surface quality is poor, and the The advantages and disadvantages of FRCMCs-SiC
tool wear is serious. Inducing strength loss of materials machining processes are summarized in Table 1.
through high temperature during machining is an effective
method to solve the poor machinability caused by high hard- 4. Machining quality of FRCMCs-SiC
ness and high brittleness high hardness and high brittleness,
thereby extending the tool life, improving machining quality The service environment of FRCMCs-SiC is generally extre-
and machining efficiency.101,102 LAM provides an effective mely harsh. Besides the original defects generated during the
way for the machining of ceramics, glass, hard and brittle met- preparation of the material, surface integrity also affects ser-
als, and other materials.103–105 However, for FRCMCs-SiC, vice performance and fatigue life. Unlike metal materials, there

Fig. 18 Ultrasonic assisted milling.100


Machining of SiC ceramic matrix composites 555

Fig. 19 Laser-assisted milling.

Table 1 Advantages and disadvantages of FRCMCs-SiC machining processes.


Machining Advantages Disadvantages
process
CM Relatively mature technology, less equipment investment, high Relying on diamond tools, catastrophic tool wear, low
machining accuracy machining efficiency, poor machined surface quality
UAM Relatively mature technology, affordable equipment investment, high Relying on diamond tools, severe tool wear
machining accuracy, high machined surface quality, high machining
efficiency, suitable for machining brittle materials
LAM Low cutting force, prolonged tool life, high machined surface quality Immature technology, expensive, complicated
equipment upgrades

is no surface strengthening process to improve the machined Zhang et al.59 conducted grinding experiments on three typical
surface of FRCMCs-SiC. Therefore, the defects and damages fiber orientations, as shown in Fig. 21. The results showed that
caused by machining will permanently exist in the parts, which both Ra and Rz followed the following rule: Longitudi-
directly affect the thermal–mechanical properties, reliability, nal > Normal > Transverse. For surface grinding using dia-
and service life of the parts. Therefore, it is valuable to study mond wheels, Qu et al.64 defined the deflection angle as a, b,
the mechanism of machining defects of FRCMCs-SiC and to c according to the reference plane, and proposed that when
explore the few-defects or non-defects machining process of a = 90°, b = 90°, c = 0°, Sa and Sz were the minimum. Wang
FRCMCs-SiC. et al.89 discussed the effect of fiber orientation angle on surface
roughness when using a diamond core drill for Cf/SiC compos-
4.1. Surface morphology and machined surface roughness ites rotary ultrasonic drilling, and proposed that Sq was the
smallest when the angle was 90°. In addition, the fiber of
The roughness of machined surface is the most common index FRCMCs-SiC actually used usually has a woven or needled
to evaluate the machined surface quality. In the studies, both structure. Du et al.62 conducted grinding experiments of 2D
two-dimensional feature parameters (such as Ra, woven Cf/SiC composites along with different directions, and
Rz)57,59,61,67,68,82,92,98 and three-dimensional feature parame- Zhang et al.73 conducted milling experiments of 2.5D woven
ters (such as Sa, Sq, Sz, Sku, Sdr, Sbi)62–64,69,70,73,75–77,83,84,87 Cf/SiC composites along with different directions, experimen-
,89,95,97,100,108
are used. However, in view of the anisotropy tal results all proved that different machining directions also
and heterogeneity of FRCMCs-SiC, two-dimensional feature affected roughness. Besides, Babbar et al.98 studied the effect
parameters may be difficult to accurately evaluate the rough- of material density on the surface quality in RUM of Cf/SiC
ness of the machined surface. Therefore, three-dimensional composites by using a diamond abrasive tool. If the material
feature parameters have been used more. Generally, the 3D density was high, the initial surface roughness of the sample
surface morphology is obtained by non-contact optical mea- was small, but the reduction in machined surface roughness
surement methods (as shown in Fig. 20), and then three- was also small.
dimensional feature parameters are obtained. The geometric parameters of the tool used for machining
Material properties play a decisive role in the machined sur- also affect the surface roughness. Tawakoli et al.57 found that
face quality. As a typical anisotropic and heterogeneous mate- the use of segmented grinding wheel increased Ra and Sa in the
rial, the effect of carbon fiber orientations and machining grinding of Cf/SiC composites. The reason is that the use of a
direction on machined surface roughness obviously exists. segmented grinding wheel increased the maximum undeformed
556 Q. AN et al.

Fig. 20 3D surface morphology of machined surface.63,76,89

Fig. 21 Effect of fiber orientations on machined surface roughness.59

chip thickness, and each segment of the grinding wheel had a grinding depth increased in MQL grinding of Cf/SiC compos-
mechanical impact on the workpiece. Zou et al.77 analyzed ites, due to the reduction in grinding wheel wear. When drilling
the influence of point angle and clearance angle of PCD drill Cf/SiC composites by using PCD tools, Chen et al.76 found
bit on Sa and Sz. that if the cutting speed was too high, the tool would be unsta-
For various machining processes, the variation of machined ble due to excessive load, resulting in a sharp increase in the
surface roughness with machining parameters is widely dis- machined surface roughness. When drilling Cf/SiC composites
cussed. The most consensus is that the machined surface by using a diamond core drill, Ding et al.87 found that if the
roughness decreases with the increase of spindle speed (or cut- density of materials was low (the porosity was too high), the
ting speed), increases with the increase of feed rate and grind- influence of machining parameters on surface roughness was
ing depth (or cutting depth).57,59,61,63,73,75,76,82,83,97,98,100,108 unstable.
For grinding processes (including filing, drilling and milling Besides the effects of material properties and machining
by using diamond abrasive tools), the grinding parameters parameters on the surface roughness, the effects of assisted
affect the material removal mechanism by changing the maxi- machining parameters have also been discussed. For MQL,
mum undeformed chip thickness, which affects the machined Adibi et al.67, Esmaeili et al.68 and Qu et al.69 all proposed that
surface roughness. For cutting processes, the cutting parame- in the grinding of Cf/SiC composites, compared with dry
ters affect the material removal mechanism by changing the grinding, fluid grinding (wet grinding) and MQL grinding
cutting thickness, which affects the machined surface rough- effectively reduced the machined surface roughness, due to
ness. Since the specific cutting energy is the embodiment of good cooling and washing effect. It is worth noting that
material removal mechanism in energy, Chen et al.100 pro- MQL grinding only uses a small amount of lubricating oil to
posed that there was a negative correlation between the obtain good comprehensive performance, with both effect
machined surface roughness and specific milling energy, as and environmental protection. On this basis, Qu et al.69 dis-
shown in Fig. 22. But there are also some unusual conclusions. cussed the effect of MQL parameters (nozzle direction, air
Du et al.62 conducted a grinding experiment on Cf/SiC com- pressure, oil flow rate, and nozzle distance) on the machined
posites, and the results showed that as the feed rate increased, surface roughness. In addition, Qu et al.70 further proposed
both Sa and Sq decreased. And the influence of the maximum the application of NMQL in the grinding of Cf/SiC compos-
undeformed chip thickness on the surface roughness was not ites. The experimental results are shown in Fig. 23 indicated
significant due to the fiber orientation. Adibi et al.67 and that the effectiveness of NMQL for reducing the machined sur-
Esmaeiliet al.68 proposed that Ra decreased slightly as the face roughness.
Machining of SiC ceramic matrix composites 557

cutting, the high-frequency hammering effect of the cutting


edge promotes the initiation and propagation of microcracks
inside the carbon fiber, causing nano-scale brittle fracture of
carbon fibers, which reduced the machined surface rough-
ness.100 Furthermore, the effect of ultrasonic amplitude on
the surface roughness has also been studied. In UAF experi-
ments of Cf/SiC composites, Wang et al.84 found that Sz and
Sq decreased with the increase of ultrasonic amplitude. In
RUM experiments of Cf/SiC composites, Wang et al.89 pro-
posed that when the spindle speed was low, the hole surface
quality was better as the ultrasonic amplitude increased, But
when the spindle speed was further increased, the increase in
ultrasonic amplitude had no obvious benefit to the further
improvement of the hole surface quality. The results of
UAM of Cf/SiC composites by Chen et al.100 showed that Sa
decreased with the increase of ultrasonic amplitude, but when
Fig. 22 Correlation between surface roughness and specific the amplitude exceeded the threshold value of micro-scale brit-
milling energy.100 tle fracture of carbon fibers, the increase in amplitude instead
increased Sa.
For FRCMCs-SiC, UAM is recommended. Compared with There are few studies on LAM of FRCMCs-SiC. However,
CM, UAM effectively reduced the machined surface rough- based on the LAM experiments of Cf/SiC composites, Erdene-
ness, whether grinding82,83 (including filing,84 drilling87,89 and chimeg et al.108 proposed that LAM improved the machined
milling95 by using diamond abrasive tools) or cutting. How- surface quality, and as the preheating temperature increased,
ever, Bertsche et al.92 found that the surface roughness of the surface roughness decreased.
UAM was higher than that of CM in slot milling of SiCf/
SiC composites. But Bertsche also admitted that this conclu- 4.2. Machining defects
sion may be inaccurate, due to the surface was evaluated by
Ra and the influence of fiber orientation and measurement The components of FRCMCs-SiC are complex, anisotropic,
position. For grinding, the ultrasonic vibration of the abrasive and heterogeneous. After removing the materials, various
makes the cutting path of the abrasive longer (as shown in machining defects will be formed on the fiber, the SiC matrix,
Fig. 24), and the reduction of the maximum undeformed chip and the interface. Many scholars have also explored the
thickness results in the reduction of chips.84,87 Another point machined surface defects, subsurface defects, and edge defects.
of view is that the ultrasonic vibration makes the contact Researches on machined surface defects are the most.
between the abrasive and the workpiece from continuous to Zhang et al.59,60 first summarized that the machining defects
intermittent, which results in smaller chips.82,97 And Wang of unidirectional Cf/SiC composites in grinding were the com-
et al.89 proposed that ultrasonic vibration changed the fracture bination of matrix cracking, fiber fracture, and interfacial
mode of carbon fibers, and the fracture of carbon fibers in the debonding. Liu et al.61 analyzed the grinding of 2D Cf/SiC
cutting plane was conducive to the reduction of roughness. For composites, Zhang et al.73 analyzed the milling of 2.5D Cf/
SiC composites and Hu et al.75 analyzed the milling of 2D
Cf/SiC composites, the same conclusion was proposed. This
conclusion is relatively preliminary, and this expression has
been further expanded with the in-depth observation and anal-
ysis of the machined surface. Du et al.62 described machining
defects in detail for three typical fiber orientations. Along

Fig. 23 Effect of lubrication conditions on machined surface


roughness.70 Fig. 24 Grain trajectories of RUM and CD.87
558 Q. AN et al.

longitudinal fibers, laminated fractures, shear fracture, and a


compression fracture of carbon fibers, spallation of SiC
matrix, and cracks in the SiC matrix were observed. Along
transverse fibers, various fiber fractures and interfacial failures
were observed. Along across fibers, grooves, fiber pull-out, and
fiber broken were observed. Qu et al.63,64 thought that fiber
fracture, matrix cracks, interfacial debonding and fiber wear
were the basic forms of Cf/SiC composite damage, and pro-
posed that changes in machining parameters would not cause
changes in the material removal mechanism, but the propor-
tion of different damage forms would be changed. As the
grinding speed increased, the grinding length and vertical force
of the single abrasive became smaller resulting in small cracks,
which improved the quality of the machined surface. As the
feed rate increased, the maximum undeformed chip thickness
increased and more cracks were generated. As the grinding
depth increased, the area of fiber wear decreased, but the inter-
facial debonding and fiber fractures increased. For the cutting
of SiCf/SiC composites, Diaz et al.54 proposed that the
machining defects in the fiber-rich region were fiber fractures,
fiber pulling out, fiber unpulling out and radial cracks of CVI-
SiC, the machining defect in the matrix-rich region was SiC
grains pulling out. Furthermore, Qu et al.69,70 proposed that
the fiber fracture mode was affected by machining parameters,
the sharpness of the abrasive, and the lubrication conditions.
The extrusion and shearing of the abrasive particles led to long
cracks and deep interfacial debonding. However, in MQL and
NMQL grinding, the length and depth of matrix cracks and
interfacial debonding were limited, and machining defects were
reduced. Adibi et al.67 proposed that MQL grinding brought
narrower scratches on the machined surface, more uniform
surface, and better-machined surface quality. Wang et al.84
found that during conventional filing, carbon fibers were cut
or pulled out by the abrasive, the matrix and fibers were sepa-
rated, the carbon fiber circumferentially fractured without
axial damage. But when UAF, carbon fibers had obvious
scratches along the axial direction. Liu et al.99 believed that
compared with conventional milling, UAM was beneficial to
improve the matrix breakage, but the effect of improving fiber
breakage was not obvious. Babbar et al.98 proposed that fiber
pulling out was the main machining defect. When using PCD
tools to drill 2D Cf/SiC composites, Zou et al.74 found that
braided layer separation and bifurcation of yarn were also typ-
ical machining defects for this woven fiber bundle structure.
Based on the above conclusions, in summary, the surface
machining defects of FRCMCs-SiC included fiber fractures
(cut off, crushing, pulling out, outcrop), fiber broken (fiber
Fig. 25 Machining defects on machined surface of FRCMCs-
damage), grooves, and matrix breakage, spallation of SiC
SiC.
matrix, matrix cracks, interfacial debonding, braided layer

Fig. 26 Machined surface defects in the grinding of 3D needled Cf/SiC composites.83


Machining of SiC ceramic matrix composites 559

separation and bifurcation of yarn. Fig. 25 shows the images of observed the machined surface of 3D needled Cf/SiC compos-
these defects. ites by grinding and proposed that 0° fibers and needled fibers
Because FRCMCs-SiC is fiber-rich materials, carbon fibers have a lamellar brittle fracture, 90° fibers have brittle fracture
have a large number of machining defects and has a great and fiber pull out, which all caused pits on the machined sur-
impact on surface quality, which should be focused on. There- face, as shown in Fig. 26. The size of the surface pits decreased
fore, some studies have focused on the machining defects with increasing grinding speed and increases with increasing
caused by material removal on carbon fibers. Ding et al.83 feed rate and grinding depth. UAM effectively reduced the size

Fig. 27 Micro-morphology of machined surface in milling of 2D Cf/SiC composites.100


560 Q. AN et al.

Fig. 28 Machining defects on machined subsurface of 2D Cf/SiC composites.

Fig. 30 Relationship between thrust force and tearing factor.88

were the main machining defects on the machined surface.


The change of machining parameters resulted in the transition
of the material removal mechanism of carbon fibers. As shown
in Fig. 27, if carbon fibers occur nano-scale brittle fracture, the
Fig. 29 Machining defects at hole exit of Cf/SiC composites.91
machined surface of composites is flat, but the machined sur-
face of the carbon fiber is rough. If carbon fibers occur
and depth of lamellar brittle fracture, which has been verified micro-scale brittle fracture (bending-induced fracture,
in ultrasonic-assisted grinding83 and ultrasonic-assisted compression-induced fracture, shear-induced fracture), the
drilling.87 Chen76,100 proposed that Cf/SiC composite was a machined surface has pits, because the fractures of carbon
kind of fiber-rich material, and the material removal mecha- fibers are not in the cutting plane and the fractures of carbon
nism of carbon fibers directly determined the machined surface fiber are inclined. The high-frequency hammering of cutting
quality. The pits formed after brittle fracture of carbon fibers edge caused by ultrasonic-assisted milling promoted the
Machining of SiC ceramic matrix composites 561

initiation and propagation of micro-cracks inside carbon fiber,


and induced carbon fiber to be removed with nano-scale brittle
fracture, thus effectively reducing the machined surface
defects.100
Besides surface machining defects, subsurface machining
defects are also an important component of machined surface
quality. Surface machining defects are easy to observe, using
an optical microscope or scanning electron microscope
(SEM). But subsurface defects are not easy to observe. Sam-
ple preparation is a challenge. One of the methods is to cut
the workpiece before machining, grind and polish the section,
and then glue them together. After machining, separate them
to observe the subsurface morphology. Ding et al.83 used this
method to observe the subsurface defects of CG and UAG of
Cf/SiC composites. The pits formed by the fracture of fibers
and fiber bundles were the main defects, and UAG effectively
reduced such defects, as shown in Fig. 28(a) and (b). If the
combination of mechanical cutting and mechanical polishing
is used, the mechanical damage during the sample prepara-
tion have a great impact on the subsurface machining defects
and some of which may not be observed. Diaz et al.54
observed subsurface defects during micro-drilling of SiCf/
SiC composites and found that there were fiber fracture, fiber
pull-out, and fiber unpull-out. Qu et al.70 focused on fiber
pull-out and proposed that NMQL grinding had a good
effect on reducing fiber pull-out, as shown in Fig. 27(c) and
(d).
Some of the structures (such as through-hole and groove)
produced by machining has edges. For these machining pro-
cesses, machining defects of the edge has an important impact
on the quality of parts. Hole machining is the most widely
implemented process. The defects at the hole exit of
FRCMCs-SiC has not been uniformly named. In some
researches, delamination by directly referring to the defects
of CFRP is used, and the delamination factor is used in the
quantitative evaluation.71 And in some researches, hole exit
defects are defined as tearing, and the tearing factor is used
in the quantitative evaluation.87,88,91 In view of the variety of
defects at the hole exit, including tearing, edge chipping, and
burr (as shown in Fig. 29), the damage factor is used in the
quantitative evaluation.76,77 The reason for the damage at
the hole exit is that fibers deform under the action of the axial
force due to the lack of support of the materials when the tool
is fed close to the exit. Therefore, many studies have shown
that the axial force is a direct factor affecting the hole exit
Fig. 31 Calculation of 2D damage factors based on image
defects.76,77,85,87,88 Feng et al.88 obtained the positive correla-
processing technology.77
tion diagram between the tearing factor and the thrust force
as shown in Fig. 30 through experiments. Therefore, various
variables affect the quality of the hole exit by changing the
thrust force in machining. Increasing the spindle speed and The machining defects to the edge during slot milling are
reducing the feed rate can reduce the defects of the hole also worthy of attention. Hu et al.75 proposed that the edge
exit.71,76,86,87,88,91 In addition, compared with the CM, the defects in slot milling of Cf/SiC composites include fiber pro-
effectiveness of RUM to reduce the hole exit defects has been trusion, surface damage, and both of them (as shown in
widely recognized85–88,91, and with the increase of amplitude, Fig. 32). The damage width and count were used to evaluate
the exit quality is improved88,91. Furthermore, Wang et al.91 the damage quantitatively. The results showed that the surface
designed a new compound step-taper drill, which effectively damage was far more than the fiber protrusion. And the dam-
reduced the tearing due to the reprocessing effect. According age increased with the feed rate increases.
to the difference in color and shape between the hole exit
defects and the composites, Zou et al.77 calculated the 2D dam- 4.3. Residual stress
age factor based on the image processing technology (as shown
in Fig. 31), which improved the efficiency of hole exit quality Residual stress is an important index to evaluate the machined
evaluation. surface quality. However, compared with metal materials, the
562 Q. AN et al.

Fig. 32 Three main forms of machined defects of side edges.75

Fig. 33 Residual stress analysis based on Raman spectroscopy.54


Machining of SiC ceramic matrix composites 563

100
Fig. 34 Effect of feed rate and ultrasonic amplitude on residual stress.

impact of the residual stress on the machined surface on service trometer, and the residual stress of the machined surface can
performance and service life of FRCMCs-SiC parts has not be measured by extracting the peak displacement and convert-
been clearly concluded. Therefore, there are only a few prelim- ing according to the formula. Chen et al.100 further adopted
inary explorations of the residual stress on the machined sur- the Raman Mapping method (as shown in Fig. 34(a)) to obtain
face of FRCMCs-SiC. Azarhoushang et al.58 measured the the Raman spectrum of the measured surface and converted it
residual stress of the machined surface based on X-ray diffrac- into a residual stress distribution map based on the peak shift.
tion during the evaluation of the performance of the seg- Based on this method, the residual stress of the machined sur-
mented grinding wheel in the grinding of Cf/SiC composites. face in milling of Cf/SiC composites was measured and ana-
The results indicated that Cf/SiC composites have tensile resid- lyzed. And for Cf/SiC composites, the effectiveness of UAM
ual stress on machined surface. The application of segmented to reduce the tensile residual stress was confirmed (Fig. 34(b)).
grinding wheels was beneficial to reduce residual stress because
the initiation and propagation of a large number of micro- 5. Conclusions
cracks during material removal had a stress relief effect. Diaz
et al.54 characterized the surface stress and chemical composi- FRCMCs-SiC is an excellent high-temperature material and
tion of SiCf/SiC composites by micro-Raman spectroscopy friction material, which has promising applications in the aero-
and discussed the sources of the residual stress of different space, energy, transportation, and other industries. Machining
phases and the relationship between the fracture behavior of is indispensable in the preparation of parts, and the machining
the material and the residual stress. Fig. 33 shows the residual quality has a significant impact on the service performance and
stress measured based on Raman spectroscopy. The peak posi- service life of parts. Many scholars have actively explored the
tion of the Raman spectrum of the material will shift under the material removal mechanism, machining processes, and sur-
action of stress, and the peak shift value has a certain mapping face integrity, and achieved some results. Based on the litera-
with the stress. Therefore, the Raman spectrum of the ture survey, the following conclusions are drawn:
machined surface is obtained by using a micro-Raman spec-
564 Q. AN et al.

 The material removal mechanism of FRCMCs-SiC in  The quantitative evaluation indexes of machined surface
machining can be broadly summarized as brittle fracture quality are also urgently needed to be determined. At pre-
(including matrix crushing, interfacial debonding, fiber sent, the evaluation of FRCMCs-SiC machined surface is
fracture). Furthermore, the brittle fracture mechanism of still using the single evaluation indexes of metal materials
the fiber is worth subdividing into nano-scale brittle frac- or CFRP, which is obviously insufficient. In establishing a
ture and micro-scale brittle fracture. The weak fiber–matrix machining quality evaluation system for FRCMCs-SiC,
interface is beneficial to improve the toughness of the mate- the mapping between the surface integrity indexes (such
rial, but it is a challenge to avoid interface defects during as roughness, damage layer thickness, defects, etc.) and
machining. An in-depth exploration of the material removal the service performance indexes (such as mechanical prop-
mechanism can facilitate understanding machined surface erties, fatigue properties, bonding properties with the envi-
generation mechanisms and provide ideas for avoiding ronmental thermal barrier coating, etc.) is also worth
machining defects. considering.
 For machining FRCMCs-SiC, the processes of CM, UAM
and LAM have their own advantages. Based on preliminary
experimental exploration, compared to CM, UAM can Declaration of Competing Interest
reduce the force by 7.4–%, reduce the surface roughness by
12–30%, improve machining efficiency by 10–480%, and The authors declare that they have no known competing
reduce tool wear by 28.06–36%, LAM can reduce the force financial interests or personal relationships that could have
by 40–40.7%, reduce the surface roughness by about 33.8%, appeared to influence the work reported in this paper.
and increase the tool life by 3.8 times. Overall, UAM has obvi-
ous advantages in improving machining efficiency, and LAM Acknowledgement
has obvious advantages in improving tool life.
 Considering the extreme service environment, the machining This study was supported by the National Natural Science
quality of FRCMCs-SiC parts is the most concerned in Foundation of China (No. 51975368).
machining. The effects of machining parameters, material
properties (fiber orientation, machining direction, material
References
density), and tool parameters on the roughness are widely dis-
cussed. Besides, a great variety of machining defects is an 1. Winstone MR, Partridge A, Brooks JW. The contribution of
important feature of FRCMCs-SiC machining. Fiber frac- advanced high-temperature materials to future aero-engines.
tures (cut off, crushing, pulling out, outcrop), fiber broken Proc I Mech Eng L–J 2001;215(2):63–73.
(fiber damage), grooves, and matrix breakage, spallation of 2. Gloria A, Montanari R, Richetta M, et al. Alloys for aeronautic
SiC matrix, matrix cracks, interfacial debonding, braided applications: state of the art and perspectives. Metals 2019;9:662.
layer separation and bifurcation of yarn are all observed, 3. Zhu D. Aerospace ceramic materials: Thermal, environmental
and there are also edge chipping, burr and tearing at the struc- barrier coatings and SiC/SiC ceramic matrix composites for
tural edge. Because the influence of the residual stress of the turbine engine applications. NASA Glenn Research Center; 2018.
4. Marshall DB, Cox BN. Integral textile ceramic structures. Annu
machined surface on the service performance of FRCMCs-
Rev Mater Res 2008;38(1):425–43.
SiC parts is not clear, there are few related researches.
5. Yin XW, Cheng LF, Zhang LT, et al. Fibre-reinforced multi-
functional SiC matrix composite materials. Int Mater Rev
2017;62(3):117–72.
6. Prospective outlook 6. Binner J, Porter M, Baker B, et al. Selection, processing,
properties and applications of ultra-high temperature ceramic
matrix composites, UHTCMCs–a review. Int Mater Rev
Researches on the machining of FRCMCs-SiC is preliminary
2019;1–56.
but has been concerned. With the further expansion of the 7. Ohnabe H, Masaki S, Onozuka M, et al. Potential application of
application of FRCMCs-SiC, the requirements for manufac- ceramic matrix composites to aero-engine components. Compos
turing will be further increased. For machining, more in- A Appl Sci Manuf 1999;30(4):489–96.
depth and systematic researches are urgently needed. 8. Krenkel W, Heidenreich B, Renz R. C/C-SiC composites for
advanced friction systems. Adv Eng Mater 2002;4(7):427–36.
 Up to now, the removal mechanism and damage behavior 9. Kumar P, Srivastava VK. Tribological behaviour of C/C–SiC
of FRCMCs-SiC under the assistance of various energy composites—A review. J Adv Ceram 2016;5(1):1–12.
fields are still unknown, so it is necessary to carry out mech- 10. Xiao P, Xiong X, Li Z. Preparation, performance and application
anism experiments for different assisted machining pro- of carbon ceramic friction materials. 1st ed. Beijing: Science Press;
2016 [Chinese].
cesses, which is of great significance to deeply understand
11. Behrens B, Müller M. Technologies for thermal protection
the mechanism and optimization direction of assisted systems applied on re-usable launcher. Acta Astronaut
machining processes. More scientifically, it is also expected 2004;55:529–36.
to establish theoretical or numerical models to describe 12. Arai Y, Inoue R, Goto K, et al. Carbon fiber reinforced ultra-
material removal mechanisms. high temperature ceramic matrix composites: A review. Ceram
 For machining processes, improving conventional processes Int 2019;45(12):14481–9.
and designing production equipment suitable for new pro- 13. Glass DE. Ceramic matrix composite (CMC) thermal protection
cesses are significant issues, and there is an urgent need to systems (TPS) and hot structures for hypersonic vehicles. 15th
develop machining tools (such as cutting-edge tools and AIAA international space planes and hypersonic systems and
abrasive tools) suitable for FRCMCs-SiC. technologies conference; April 28–May 1; Dayton, USA, 2008.
Machining of SiC ceramic matrix composites 565

14. Ferraiuolo M, Scigliano R, Riccio A, et al. Thermo-structural 37. Chen L, Yin X, Fan X, et al. Mechanical and electromagnetic
design of a Ceramic Matrix Composite wing leading edge for a shielding properties of carbon fiber reinforced silicon carbide
re-entry vehicle. Compos Struct 2019;207:264–72. matrix composites. Carbon 2015;95:10–9.
15. Chen Y, Zhang Lu, Zhao Y, et al. Mechanical behaviors of C/ 38. Tian H, Liu H-T, Cheng H-F. A high-temperature radar
SiC pyramidal lattice core sandwich panel under in-plane absorbing structure: Design, fabrication, and characterization.
compression. Compos Struct 2019;214:103–13. Compos Sci Technol 2014;90:202–8.
16. Bansal NP, Lamon J. Ceramic matrix composites: materials, 39. Yang X, Hu H-F, Zhang Y-d, et al. Thermal shock properties of
modeling and technology. Hoboken: John Wiley & Sons; 2014. 3D-C/SiC composites prepared via polymer infiltration pyrolysis
17. Padture NP. Advanced structural ceramics in aerospace propul- (PIP). Ceram Int 2014;40(7):9087–94.
sion. Nature Mater 2016;15(8):804–9. 40. Xu Y, Zhang L, Cheng L, et al. Microstructure and mechanical
18. Schmidt S, Beyer S, Knabe H, et al. Advanced ceramic matrix properties of three-dimensional carbon/silicon carbide compos-
composite materials for current and future propulsion technology ites fabricated by chemical vapor infiltration. Carbon 1998;36(7-
applications. Acta Astronaut 2004;55(3):409–20. 8):1051–6.
19. Liu G, Qiu J, Chen M. Research progress of composites nozzle 41. Luo Z, Zhou X, Yu J, et al. Mechanical properties of SiC/SiC
extension for liquid rocket engine. J Rocket Propul 2019;04:1–8 composites fabricated by PIP process with a new precursor
[Chinese]. polymer. Ceram Int 2014;40(1):1939–44.
20. Naslain R, Christin F. SiC-matrix composite materials for 42. Guo W, Ye Y, Bai S, et al. Preparation and formation
advanced jet engines. MRS Bull 2003;28(9):654–8. mechanism of C/C–SiC composites using polymer-Si slurry
21. Christin F. Design, fabrication, and application of thermostruc- reactive melt infiltration. Ceram Int 2020;46(5):5586–93.
tural composites (TSC) like C/C, C/SiC, and SiC/SiC composites. 43. Diaz OG, Luna GL, Liao Z, et al. The new challenges of
Adv Eng Mater 2002;4(12):903–12. machining Ceramic Matrix Composites (CMCs): Review of
22. Enya K, Nakagawa T, Kaneda H, Onaka T, Ozaki T, surface integrity. Int J Mach Tools Manuf 2019;139:24–36.
Kume M. Microscopic surface structure of C/SiC composite 44. Diaz OG, Axinte DA. Towards understanding the cutting and
mirrors for space cryogenic telescopes. Appl Opt 2007;46 fracture mechanism in ceramic matrix composites. Int J Mach
(11):2049–56. Tool Manuf 2017;118:12–25.
23. Krenkel W, Berndt F. C/C–SiC composites for space applications 45. Liu Q, Huang G, Xu X, et al. Influence of grinding fiber angles
and advanced friction systems. Mater Sci Eng, A 2005;412(1- on grinding of the 2D–Cf /C–SiC composites. Ceram Int 2018;44
2):177–81. (11):12774–82.
24. Wang P, Liu F, Wang H, Li H, Gou Y. A review of third 46. Li Y, Ge X, Wang H, et al. Study of material removal
generation SiC fibers and SiCf/SiC composites. J Mater Sci mechanisms in grinding of C/SiC composites via single-abrasive
Technol 2019;35(12):2743–50. scratch tests. Ceram Int 2019;45(4):4729–38.
25. Gao T, Hong Z, Yang J. Application and prospect of ceramic 47. Wang Q. Experimental study on fiber interfacial micromechanics
matrix composite components for commercial aircraft engine. by Raman spectroscopy [dissertation]. Dalian: Dalian University
Aeron Manuf Technol 2014;450(6):14–21 [Chinese]. of Technology; 2013 [Chinese].
26. LIU X, SHEN X, GONG L, LI P. Multi-scale thermodynamic 48. Zhang L, Ren C, Zhou C, et al. Single fiber push-out charac-
analysis method for 2D SiC/SiC composite turbine guide vanes. terization of interfacial mechanical properties in unidirectional
Chin J Aeronaut 2018;31(1):117–25. CVI-C/SiC composites by the nano-indentation technique. Appl
27. Zou H, Wang Y, Liu G, et al. Development situation and Surf Sci 2015;357:1427–33.
application of SiC/SiC ceramic matrix composites in aeroengine. 49. Li C, Zhang F, Meng B, et al. Material removal mechanism and
Aeron Manuf Technol 2017;60(15):76–84 [Chinese]. grinding force modelling of ultrasonic vibration assisted grinding
28. Katoh Y, Snead LL, Henager Jr CH, et al. Current status and for SiC ceramics. Ceram Int 2017;43(3):2981–93.
recent research achievements in SiC/SiC composites. J Nucl 50. Bandyopadhyay P, Dey A, Roy S, et al. Effect of load in scratch
Mater 2014;455(1):387–97. experiments on soda lime silica glass. J Non-Cryst Solids
29. Liu Q, Huang S, He A. Application requirements and challenges 2012;358(8):1091–103.
of CMC-SiC composites on aero-engine. J Mater Eng 2019;47 51. Wasmer K, Parlinska-Wojtan M, et al. Sequence of deformation
(2):1–10 [Chinese]. and cracking behaviours of Gallium–Arsenide during nano-
30. Liu H, Yang J, Jiao J. Fabrication technique and application scratching. Mater Chem Phys 2013;138(1):38–48.
prospect of continuous Si C fiber reinforced ceramic matrix 52. Wang C, Liu G, An Q, et al. Occurrence and formation
composites for aeroengine. Aeron Manuf Technol 2017;60 mechanism of surface cavity defects during orthogonal milling
(16):90–5 [Chinese]. of CFRP laminates. Compos Part B Eng 2017;109:10–22.
31. Wang N, Li H, Xu F, et al. Recent development of advanced 53. Chen J, An Q, Chen M. Transformation of fracture mechanism
materials for liquid rocket thruster chambers. Aerosp Mater and damage behavior of ceramic-matrix composites during nano-
Technol 2019;49(3):1–8 [Chinese]. scratching. Compos A Appl Sci Manuf 2020;130:105756.
32. Naslain R. Design, preparation and properties of non-oxide 54. Gavalda Diaz O, Axinte DA, Butler-Smith P, et al. On
CMCs for application in engines and nuclear reactors: an understanding the microstructure of SiC/SiC Ceramic Matrix
overview. Compos Sci Technol 2004;64(2):155–70. Composites (CMCs) after a material removal process. Mater Sci
33. Ihli T, Basu TK, Giancarli LM, et al. Review of blanket designs Eng, A 2019;743:1–11.
for advanced fusion reactors. Fusion Eng Des 2008;83(7- 55. National Research Council. Aeronautical technologies for the
9):912–9. twenty-first century. New York: National Academies Press; 1992.
34. Wu Y. Conceptual design of the China fusion power plant FDS- 56. Tashiro T, Fujiwara J, Takenaka Y. Grinding of C/C-SiC
II. Fusion Eng Des 2008;83(10-12):1683–9. composite in dry method. The 11th International Conference on
35. Norajitra P, Bühler L, Fischer U, et al. The EU advanced lead Precision Engineering (ICPE); 2006 Aug 16-18; Tokyo,
lithium blanket concept using SiCf/SiC flow channel inserts as Japan. New York: Springer; 2007.
electrical and thermal insulators. Fusion Eng Des 2001;58- 57. Tawakoli T, Azarhoushang B. Intermittent grinding of ceramic
59:629–34. matrix composites (CMCs) utilizing a developed segmented
36. Norajitra P, Abdel-Khalik SI, Giancarli LM, et al. Divertor wheel. Int J Mach Tools Manuf 2011;51(2):112–9.
conceptual designs for a fusion power plant. Fusion Eng Des 58. Azarhoushang B. Wear of non-segmented and segmented
2008;83(7-9):893–902. diamond wheels in high-speed deep grinding of carbon
566 Q. AN et al.

fibre-reinforced ceramics. Int J Adv Manuf Technol 2014;74(9- 79. Xu W-X, Zhang L-C. Ultrasonic vibration-assisted machining:
12):1293–302. principle, design and application. Adv. Manuf. 2015;3(3):173–92.
59. Zhang L, Ren C, Ji C, et al. Effect of fiber orientations on surface 80. Jia D, Li C, Zhang Y, et al. Experimental evaluation of surface
grinding process of unidirectional C/SiC composites. Appl Surf topographies of NMQL grinding ZrO2 ceramics combining
Sci 2016;366:424–31. multiangle ultrasonic vibration. Int J Adv Manuf Technol
60. Zhang L, Wang S, Li Z, et al. Influence factors on grinding force 2019;100:457–73.
in surface grinding of unidirectional C/SiC composites. Appl 81. Gao T, Zhang X, Li C, et al. Surface morphology evaluation of
Compos Mater 2019;26(3):1073–85. multi-angle 2D ultrasonic vibration integrated with nanofluid
61. Liu Q, Huang G, Xu X, et al. A study on the surface grinding of minimum quantity lubrication grinding. J Manuf Process
2D C/SiC composites. Int J Adv Manuf Technol 2017;93(5- 2020;51:44–61.
8):1595–603. 82. Azarhoushang B, Tawakoli T. Development of a novel ultrasonic
62. Du J, Ming W, Ma J, et al. New observations of the fiber unit for grinding of ceramic matrix composites. Int J Adv Manuf
orientations effect on machinability in grinding of C/SiC ceramic Technol 2011;57(9-12):945–55.
matrix composite. Ceram Int 2018;44(12):13916–28. 83. Ding K, Fu Y, Su H, et al. Study on surface/subsurface breakage
63. Qu S, Gong Y, Yang Y, et al. Surface topography and roughness in ultrasonic assisted grinding of C/SiC composites. Int J Adv
of silicon carbide ceramic matrix composites. Ceram Int 2018;44 Manuf Technol 2017;91(9-12):3095–105.
(12):14742–53. 84. Wang Y, Sarin VK, Lin B, et al. Feasibility study of the
64. Qu S, Gong Y, Yang Y, et al. Grinding characteristics and ultrasonic vibration filing of carbon fiber reinforced silicon
removal mechanisms of unidirectional carbon fibre reinforced carbide composites. Int J Mach Tools Manuf 2016;101:10–7.
silicon carbide ceramic matrix composites. Ceram Int 2019;45 85. Hocheng H, Tai NH, Liu CS. Assessment of ultrasonic drilling of
(3):3059–71. C/SiC composite material. Compos A Appl Sci Manuf 2000;31
65. Yang M, Li C, Zhang Y, et al. Predictive model for minimum (2):133–42.
chip thickness and size effect in single diamond grain grinding of 86. Li ZC, Jiao Y, Deines TW, et al. Rotary ultrasonic machining of
zirconia ceramics under different lubricating conditions. Ceram ceramic matrix composites: feasibility study and designed exper-
Int 2019;45(12):14908–20. iments. Int J Mach Tools Manuf 2005;45(12-13):1402–11.
66. Li B, Li C, Zhang Y, et al. Grinding temperature and energy ratio 87. Ding K, Fu Y, Su H, et al. Experimental studies on drilling tool
coefficient in MQL grinding of high-temperature nickel-base load and machining quality of C/SiC composites in rotary
alloy by using different vegetable oils as base oil. Chin J Aeronaut ultrasonic machining. J Mater Process Technol 2014;214
2016;29(4):1084–95. (12):2900–7.
67. Adibi H, Esmaeili H, Rezaei SM. Study on minimum quantity 88. Feng P, Wang J, Zhang J, et al. Drilling induced tearing defects
lubrication (MQL) in grinding of carbon fiber-reinforced SiC in rotary ultrasonic machining of C/SiC composites. Ceram Int
matrix composites (CMCs). Int J Adv Manuf Technol 2018;95(9- 2017;43(1):791–9.
12):3753–67. 89. Wang J, Zhang J, Feng P. Effects of tool vibration on fiber
68. Esmaeili H, Adibi H, Rezaei SM. An efficient strategy for fracture in rotary ultrasonic machining of C/SiC ceramic matrix
grinding carbon fiber-reinforced silicon carbide composite using composites. Compos B Eng 2017;129:233–42.
minimum quantity lubricant. Ceram Int 2019;45(8):10852–64. 90. Wang J, Feng P, Zhang J, et al. Experimental study on vibration
69. Qu S, Gong Y, Yang Y, et al. Investigating Minimum Quantity stability in rotary ultrasonic machining of ceramic matrix
Lubrication in Unidirectional Cf/SiC composite grinding. Ceram composites: Cutting force variation at hole entrance. Ceram Int
Int 2020;46(3):3582–91. 2018;44(12):14386–92.
70. Qu S, Gong Y, Yang Y, et al. An investigation of carbon 91. Wang J, Feng P, Zheng J, et al. Improving hole exit quality in
nanofluid minimum quantity lubrication for grinding unidirec- rotary ultrasonic machining of ceramic matrix composites using a
tional carbon fibre-reinforced ceramic matrix composites. J compound step-taper drill. Ceram Int 2016;42(12):13387–94.
Cleaner Prod 2020;249:119353. 92. Bertsche E, Ehmann K, Malukhin K. Ultrasonic slot machining
71. Xing Y, Deng J, Zhang G, et al. Assessment in drilling of C/C- of a silicon carbide matrix composite. Int J Adv Manuf Technol
SiC composites using brazed diamond drills. J Manuf Process 2013;66(5-8):1119–34.
2017;26:31–43. 93. Zhang C, Yuan S, Amin M, et al. Development of a cutting force
72. Diaz OG, Axinte DA, Novovic D. Probabilistic modelling of tool prediction model based on brittle fracture for C/SiC in rotary
unbalance during cutting of hard-heterogeneous materials: A ultrasonic facing milling. Int J Adv Manuf Technol 2016;85(1-
case study in Ceramic Matrix Composites (CMCs). Compos B 4):573–83.
Eng 2018;148:217–26. 94. Yuan S, Fan H, Amin M, et al. A cutting force prediction
73. Zhang X, Yu T, Li M, et al. Effect of machining parameters on dynamic model for side milling of ceramic matrix composites C/
the milling process of 2.5D C/SiC ceramic matrix composites. SiC based on rotary ultrasonic machining. Int J Adv Manuf
Mach Sci Technol 2020;24(2):227–44. Technol 2016;86(1-4):37–48.
74. Zhang X, Yu T, Zhao J. An analytical approach on stochastic 95. Li Z, Yuan S, Zhang C. Research on the rotary ultrasonic facing
model for cutting force prediction in milling ceramic matrix milling of ceramic matrix composites. Procedia CIRP
composites. Int J Mech Sci 2020;168:105314. 2016;56:428–33.
75. Hu M, Ming W, An Q, et al. Experimental study on milling 96. Li Z, Yuan S, Song H, et al. A cutting force model based on
performance of 2D C/SiC composites using polycrystalline kinematics analysis for C/SiC in rotary ultrasonic face machin-
diamond tools. Ceram Int 2019;45(8):10581–8. ing. Int J Adv Manuf Technol 2018;97(1-4):1223–39.
76. Chen J, An Q, Ming W, et al. Hole exit quality and machined 97. Yuan S, Li Z, Zhang C, et al. Research into the transition of
surface integrity of 2D Cf/SiC composites drilled by PCD tools. J material removal mechanism for C/SiC in rotary ultrasonic face
Eur Ceram Soc 2019;39(14):4000–10. machining. Int J Adv Manuf Technol 2018;95(5-8):1751–61.
77. Zou F, Chen J, An Q, et al. Influences of clearance angle and 98. Babbar A, Sharma A, Jain V, et al. Rotary ultrasonic milling of
point angle on drilling performance of 2D Cf/SiC composites C/SiC composites fabricated using chemical vapor infiltration
using polycrystalline diamond tools. Ceram Int 2020;46 and needling technique. Mater Res Express 2019;6(8):085607.
(4):4371–80. 99. Liu Y, Liu Z, Wang X, et al. Experimental study on tool wear in
78. Brehl DE, Dow TA. Review of vibration-assisted machining. ultrasonic vibration–assisted milling of C/SiC composites. Int J
Precis Eng 2008;32(3):153–72. Adv Manuf Technol 2020;107(1-2):425–36.
Machining of SiC ceramic matrix composites 567

100. Chen J, Ming W, An Q, et al. Mechanism and feasibility of 113. Yue X, Li Q, Yang X. Influence of thermal stress on material
ultrasonic-assisted milling to improve the machined surface quality removal of Cf_SiC composite in EDM. Ceram Int 2020;46
of 2D Cf/SiC composites. Ceram Int 2020;46(10):15122–36. (6):7998–8009.
101. Kim K-S, Kim J-H, Choi J-Y, et al. A review on research and 114. Chen X, Lotshaw WT, Ortiz AL, et al. Laser drilling of advanced
development of laser assisted turning. Int J Precis Eng Manuf materials: Effects of peak power, pulse format, and wavelength. J
2011;12(4):753–9. Laser Appl 1996;8(5):233–9.
102. Lee C-M, Kim D-H, Baek J-T, et al. Laser assisted milling device: 115. Tuersley IP, Hoult TP, Pashby IR. The processing of SiC/SiC
A review. Int J Precis Eng Manuf Green Technol 2016;3 ceramic matrix composites using a pulsed Nd–YAG laser: Part I:
(2):199–208. Optimisation of pulse parameters. J Mater Sci 1998;33(4):955–61.
103. Yang B, Shen X, Lei S. Mechanisms of edge chipping in laser- 116. Tuersley IP, Hoult TP, Pashby IR. The processing of SiC/SiC
assisted milling of silicon nitride ceramics. Int J Mach Tools ceramic matrix composites using a pulsed Nd-YAG laser: Part II
Manuf 2009;49(3-4):344–50. The effect of process variables. J Mater Sci 1998;33(4):963–7.
104. Ito Y, Kizaki T, Shinomoto R, et al. High-efficiency and 117. Wang C, Zhang L, Liu Y, et al. Ultra-short pulse laser deep
precision cutting of glass by selective laser-assisted milling. Precis drilling of C/SiC composites in air. Appl Phys A 2013;111
Eng 2017;47:498–507. (4):1213–9.
105. Masood SH, Armitage K, Brandt M. An experimental study of 118. Liu Y, Wang C, Li W, et al. Effect of energy density and feeding
laser-assisted machining of hard-to-wear white cast iron. Int J speed on micro-hole drilling in C/SiC composites by picosecond
Mach Tools Manuf 2011;51(6):450–6. laser. J Mater Process Technol 2014;214(12):3131–40.
106. Rozzi JC, Barton MD. The laser-assisted edge milling of ceramic 119. Zhang R, Li W, Liu Y, et al. Machining parameter optimization
matrix compositesASME 2009 International Manufacturing of C/SiC composites using high power picosecond laser. Appl
Science and Engineering Conference; 2009 Oct 4-7; West Surf Sci 2015;330:321–31.
Lafayette, USA. American Society of Mechanical Engineers 120. Li W, Zhang R, Liu Y, et al. Effect of different parameters on
Digital Collection; 2009. p. 845–52. machining of SiC/SiC composites via pico-second laser. Appl Surf
107. Dong X, Shin YC. Improved machinability of SiC/SiC ceramic Sci 2016;364:378–87.
matrix composite via laser-assisted micromachining. Int J Adv 121. Liu Y, Wang J, Li W, et al. Effect of energy density and feeding
Manuf Technol 2017;90(1-4):731–9. speed on micro-holes drilling in SiC/SiC composites by picosec-
108. Erdenechimeg K, Jeong HI, Lee CM. A study on the laser- ond laser. Int J Adv Manuf Technol 2016;84(9-12):1917–25.
assisted machining of carbon fiber reinforced silicon carbide. 122. Zhai Z, Wang W, Zhao J, et al. Influence of surface morphology
Materials 2019;12(13):2061. on processing of C/SiC composites via femtosecond laser.
109. Ramulu M, Jenkins MG, Guo Z. Abrasive water jet machining Compos A Appl Sci Manuf 2017;102:117–25.
mechanisms in continuous-fiber ceramic composites. J Compos 123. Liu Y, Zhang R, Li W, et al. Effect of machining parameter on
Technol Res 2001;23(2):82. femtosecond laser drilling processing on SiC/SiC composites. Int
110. Hashish M, Kotchon A, Ramulu M. Status of AWJ machining of J Adv Manuf Technol 2018;96(5-8):1795–811.
CMCS and hard materials. INTERTECH 2015; 2015 May 19-20; 124. Zhai Z, Wang W, Mei X, et al. Effect of the surface microstruc-
Indianapolis, USA. ture ablated by femtosecond laser on the bonding strength of
111. Wei C, Zhao L, Hu D, et al. Electrical discharge machining of EBCs for SiC/SiC composites. Opt Commun 2018;424:137–44.
ceramic matrix composites with ceramic fiber reinforcements. Int 125. Pan S, Li Q, Xian Z, et al. The effects of laser parameters and the
J Adv Manuf Technol 2013;64(1-4):187–94. ablation mechanism in laser ablation of C/SiC composite.
112. He W, He S, Du J, et al. Fiber orientations effect on process Materials 2019;12(19):3076.
performance for wire cut electrical discharge machining 126. Zhai Z, Wei C, Zhang Y, et al. Investigations on the oxidation
(WEDM) of 2D C/SiC composite. Int J Adv Manuf Technol phenomenon of SiC/SiC fabricated by high repetition frequency
2019;102(1-4):507–18. femtosecond laser. Appl Surf Sci 2020;502:144131.

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