OREAS 605 DataPack

Table 1.
Abbreviations used for OREAS 605
Abbreviation
Std.Dev.
Rel.Std.Dev.
PDM3
NR
<
Method Codes:
4A*AAS
4A*MS
4A*OES
4A*OES/AAS
4A*OES/MS
AR*AAS
AR*MS
AR*OES
AR*OES/AAS
AR*OES/MS
FA*AAS
FA*GRAV
FA*OES
INAA
IRC
PF*MS
PF*OES
Legend:-
Individual
Batch & Limits

Table 1. Abbreviations used for OREAS 605
Explanation
one sigma standard deviation

one sigma relative standard deviation
percent deviation of lab mean from corrected mean of means
not reported
‘less than’
4-acid (HF-HNO3-HClO4-HCl) digest with AAS finish

4-acid (HF-HNO3-HClO4-HCl) digest with ICP-MS finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES finish
4-acid (HF-HNO3-HClO4-HCl) digest with either AAS or ICP-OES finish as appropriate
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES or ICP-MS finish as appropriate
aqua regia digest with AAS finish
aqua regia digest with ICP-MS finish
aqua regia digest with ICP-OES finish
ore grade aqua regia digest with either AAS or ICP-OES finish as appropriate
aqua regia digest with ICP-OES or ICP-MS finish as appropriate
fire assay with AAS finish
fire assay with gravimetric finish
fire assay with ICP-OES finish
INAA using a charge weight as deemed appropriate
infrared combustion furnace
sodium peroxide fusion with ICP-MS finish
sodium peroxide fusion with ICP-OES finish
(for Method Group Tabulated Results omitted in the determination of Certified Values)
- Outlying individual values
- Outlying laboratory batch data sets and superfluous limit values

NB. Formatted area for below table ends at row 46 inclusive, allowing for 40 maximum potential laboratories.
Table 5. Participating Laboratory List used for OREAS 605
Lab Slot
1.21
1.23
2.01
1.20
1.06
1.05
1.03
1.08
1.04
1.07
1.24
1.27
1.25
1.26
1.11
1.12
1.02
1.14
1.09
1.15
1.22
1.01
1.16
1.18
1.19
1.17
1.13
1.10
Formatted area for below table ends at row 46 inclusive, allowing for 40 maximum potential laboratories.
Table 5. Participating Laboratory List used for OREAS 605
Laboratory Name and Location
Accurassay, Thunder Bay, Ontario, Canada

Acme (BV), Santiago, Chile
Actlabs, Ancaster, Ontario, Canada
AH Knight, Spartanburg, SC, USA
ALS, Johannesburg, South Africa
ALS, Lima, Peru
ALS, Reno, Nevada, USA
ALS, Townsville, QLD, Australia
ALS, Val-d'or, Quebec, Canada
ALS, Vancouver, BC, Canada
Bureau Veritas Geoanalytical, Adelaide, SA, Australia
Bureau Veritas Geoanalytical, Kalgoorlie, WA, Australia
Bureau Veritas Geoanalytical, Perth, WA, Australia
Bureau Veritas Kalassay, Kalgoorlie, WA, Australia
Inspectorate (BV), Lima, Peru
Inspectorate (BV), Sparks, Nevada, USA
Intertek Genalysis, Adelaide, SA, Australia
Intertek Genalysis, Perth, WA, Australia
Intertek Testing Services, Cupang, Muntinlupa, Philippines
Intertek Testing Services, Shunyi, Beijing, China
MINTEK Analytical Services, Randburg, South Africa
PT Geoservices Ltd, Cikarang, Jakarta Raya, Indonesia
SGS de Mexico, Durango, Mexico
SGS Geosol Laboratorios Ltda, Vespasiano, Minas Gerais, Brazil
SGS Lakefield Research Ltd, Lakefield, Ontario, Canada
SGS South Africa Pty Ltd, Booysens, Gauteng, South Africa
Shiva Analyticals Ltd, Bangalore North, Karnataka, India
SRL, Perth, WA, Australia
Table 2. Certified Values, SD's, 95% Confidence and Tolerance Limits for OREAS 605
95% Confidence 95% Tolerance
Certified
Constituent SD Limits Limits
Value Low High Low High
Pb Fire Assay
Ag, Silver (ppm) 965 25 948 982 943 987
Au, Gold (ppm) 1.67 0.086 1.63 1.70 1.64 1.69
4-Acid Digestion
Ag, Silver (ppm) 972 28 958 986 960 985
Al, Aluminium (wt.%) 5.43 0.149 5.35 5.51 5.33 5.53
As, Arsenic (ppm) 1602 102 1553 1651 1564 1640
Be, Beryllium (ppm) 0.67 0.08 0.64 0.71 0.65 0.70
Bi, Bismuth (ppm) 16.3 2.7 15.3 17.3 15.6 17.0
Ca, Calcium (wt.%) 0.276 0.009 0.272 0.281 0.267 0.286
Cd, Cadmium (ppm) 12.5 0.97 12.0 13.0 12.2 12.9
Ce, Cerium (ppm) 21.4 4.0 17.5 25.3 20.4 22.4
Co, Cobalt (ppm) 90 6.0 87 93 88 93
Cr, Chromium (ppm) 30.4 4.2 28.4 32.5 27.3 33.6
Cs, Cesium (ppm) 1.57 0.107 1.50 1.65 1.47 1.67
Cu, Copper (wt.%) 5.02 0.152 4.95 5.09 4.94 5.09
Dy, Dysprosium (ppm) 1.02 0.083 0.93 1.11 0.96 1.08
Er, Erbium (ppm) 0.39 0.037 0.35 0.43 0.35 0.43
Fe, Iron (wt.%) 3.76 0.260 3.64 3.88 3.67 3.85
Ga, Gallium (ppm) 30.3 2.29 29.1 31.6 29.4 31.2
Gd, Gadolinium (ppm) 1.60 0.094 1.50 1.70 1.50 1.70
Ge, Germanium (ppm) <5 IND IND IND IND IND
Hf, Hafnium (ppm) 2.58 0.174 2.47 2.70 2.45 2.71
Ho, Holmium (ppm) 0.15 0.03 0.12 0.18 IND IND
In, Indium (ppm) 3.78 0.346 3.52 4.04 3.65 3.92
K, Potassium (wt.%) 1.04 0.055 1.01 1.06 1.01 1.07
La, Lanthanum (ppm) < 20 IND IND IND IND IND
Li, Lithium (ppm) 21.7 2.13 20.5 23.0 20.9 22.5
Lu, Lutetium (ppb) 54 5 49 60 IND IND
Mg, Magnesium (ppm) 476 42 456 495 466 485
Mn, Manganese (ppm) 91 5.3 89 94 89 94
Mo, Molybdenum (ppm) 4.82 0.70 4.52 5.13 4.53 5.12
Na, Sodium (wt.%) 0.580 0.022 0.570 0.591 0.567 0.594
Nb, Niobium (ppm) 6.92 0.557 6.53 7.30 6.66 7.17
Nd, Neodymium (ppm) 10.7 1.7 8.8 12.5 10.1 11.2
Ni, Nickel (ppm) 1522 65 1491 1552 1489 1555
P, Phosphorus (ppm) 507 36 488 527 479 536
Pb, Lead (ppm) 1297 136 1235 1358 1250 1343
Pr, Praseodymium (ppm) 2.97 0.38 2.56 3.38 2.77 3.18
Rb, Rubidium (ppm) 29.2 3.3 26.8 31.6 28.4 30.0
S, Sulphur (wt.%) 8.34 0.571 8.05 8.62 8.15 8.52
Sb, Antimony (ppm) 294 16 286 302 283 305
Sc, Scandium (ppm) 5.03 0.66 4.70 5.36 4.79 5.27
Se, Selenium (ppm) 76 7.2 71 82 74 79
Sm, Samarium (ppm) 2.09 0.138 1.93 2.24 1.96 2.22
Sn, Tin (ppm) 2.73 0.29 2.49 2.97 2.52 2.94
Sr, Strontium (ppm) 373 73 338 409 356 390
Ta, Tantalum (ppm) <1 IND IND IND IND IND
Tb, Terbium (ppm) 0.20 0.02 0.18 0.23 0.19 0.22
Te, Tellurium (ppm) 31.8 4.8 27.2 36.4 30.1 33.5
Th, Thorium (ppm) 5.12 0.82 4.50 5.74 4.78 5.45
Ti, Titanium (wt.%) 0.177 0.012 0.170 0.183 0.171 0.182
Tl, Thallium (ppm) 15.0 1.22 14.2 15.7 14.6 15.4
U, Uranium (ppm) 2.79 0.167 2.69 2.90 2.68 2.91
V, Vanadium (ppm) 39.9 1.81 39.0 40.7 38.4 41.3
W, Tungsten (ppm) 27.0 3.2 24.8 29.2 26.0 27.9
Y, Yttrium (ppm) 4.26 0.320 4.07 4.46 4.13 4.40
Yb, Ytterbium (ppm) 0.37 0.05 0.32 0.43 0.32 0.43
Zn, Zinc (wt.%) 0.216 0.009 0.212 0.220 0.212 0.220
Zr, Zirconium (ppm) 84 6.0 81 87 82 86
Aqua Regia Digestion
Ag, Silver (ppm) 984 29 967 1000 966 1002
Al, Aluminium (wt.%) 0.730 0.123 0.674 0.786 0.707 0.753
As, Arsenic (ppm) 1613 131 1552 1674 1583 1644
Au, Gold (ppm) 1.66 0.081 1.61 1.70 1.63 1.68
B, Boron (ppm) < 10 IND IND IND IND IND
Be, Beryllium (ppm) 0.16 0.03 0.13 0.18 IND IND
Bi, Bismuth (ppm) 16.7 3.0 15.4 17.9 15.8 17.5
Ca, Calcium (wt.%) 0.182 0.013 0.177 0.188 0.174 0.190
Cd, Cadmium (ppm) 12.9 1.5 12.2 13.6 12.5 13.3
Co, Cobalt (ppm) 93 6.9 90 96 91 95
Cr, Chromium (ppm) 27.5 3.1 26.2 28.8 25.8 29.2
Cs, Cesium (ppm) 0.48 0.07 0.42 0.54 0.45 0.51
Cu, Copper (wt.%) 4.98 0.157 4.90 5.06 4.92 5.04
Dy, Dysprosium (ppm) 0.52 0.051 0.46 0.58 0.49 0.55
Er, Erbium (ppm) 0.15 0.03 0.11 0.19 IND IND
Eu, Europium (ppm) 0.21 0.04 0.16 0.26 0.19 0.24
Fe, Iron (wt.%) 3.75 0.181 3.67 3.83 3.67 3.83
Ga, Gallium (ppm) 6.66 0.86 6.07 7.26 6.31 7.01
Gd, Gadolinium (ppm) 0.87 0.17 0.69 1.06 0.83 0.92
Hf, Hafnium (ppm) 0.55 0.11 0.45 0.64 0.52 0.57
Hg, Mercury (ppm) <4 IND IND IND IND IND
Ho, Holmium (ppb) 73 12 62 84 IND IND
In, Indium (ppm) 3.75 0.51 3.35 4.15 3.59 3.90
K, Potassium (wt.%) 0.134 0.024 0.123 0.145 0.118 0.150
La, Lanthanum (ppm) 3.95 0.86 3.29 4.62 3.72 4.19
Li, Lithium (ppm) 5.17 0.99 4.59 5.75 4.98 5.36
Lu, Lutetium (ppb) 11 1 10 13 IND IND
Mg, Magnesium (ppm) 289 52 268 310 IND IND
Mn, Manganese (ppm) 86 4.8 83 88 83 88
Mo, Molybdenum (ppm) 4.75 0.424 4.57 4.93 4.37 5.13
Na, Sodium (ppm) 328 60 298 358 IND IND
Nb, Niobium (ppm) 0.45 0.06 0.39 0.51 0.40 0.50
Nd, Neodymium (ppm) 6.10 1.15 4.82 7.38 5.83 6.37
Ni, Nickel (ppm) 1538 64 1509 1568 1504 1572
P, Phosphorus (ppm) 116 24 105 126 108 123
Pb, Lead (ppm) 856 40 837 874 836 876
Pr, Praseodymium (ppm) 1.74 0.24 1.42 2.06 1.62 1.86
Rb, Rubidium (ppm) 5.75 0.96 5.00 6.49 5.41 6.09
S, Sulphur (wt.%) 7.86 0.491 7.57 8.15 7.68 8.04
Sb, Antimony (ppm) 228 46 206 250 223 233
Sc, Scandium (ppm) 1.05 0.12 0.99 1.11 1.00 1.09
Se, Selenium (ppm) 75 11 68 82 72 78
Sm, Samarium (ppm) 1.16 0.20 0.95 1.37 1.10 1.22
Sn, Tin (ppm) 1.92 0.22 1.73 2.11 1.82 2.01
Sr, Strontium (ppm) 28.1 5.5 25.2 30.9 26.7 29.5
Tb, Terbium (ppm) 0.11 0.02 0.09 0.13 0.10 0.12
Te, Tellurium (ppm) 33.1 2.60 30.7 35.4 31.8 34.4
Th, Thorium (ppm) <3 IND IND IND IND IND
Ti, Titanium (ppm) 100 12 93 107 IND IND
Tl, Thallium (ppm) 15.3 1.6 14.3 16.2 14.7 15.8
U, Uranium (ppm) 0.95 0.13 0.85 1.05 0.89 1.01
V, Vanadium (ppm) 8.33 1.08 7.80 8.86 7.69 8.97
W, Tungsten (ppm) 5.90 1.16 4.94 6.85 5.61 6.18
Y, Yttrium (ppm) 1.91 0.34 1.67 2.15 1.82 2.00
Yb, Ytterbium (ppm) 0.099 0.017 0.077 0.121 IND IND
Zn, Zinc (wt.%) 0.217 0.010 0.212 0.221 0.211 0.222
Zr, Zirconium (ppm) 19.0 2.7 17.3 20.6 18.5 19.5
Infrared Combustion
S, Sulphur (wt.%) 8.79 0.330 8.60 8.99 8.68 8.91
Table 3. Indicative Values for OREAS 605
Constituent Unit Value Constituent Unit Value Constituent Unit Value
Pb Fire Assay
Pd ppm 13.43 Pt ppm 2.21
4-Acid Digestion
B ppm < 20 Eu ppm 0.43 Re ppb 2
Ba ppm 5557 Hg ppm <1 Tm ppm 0.052
Ba ppm 25.3 Pd ppm 11.83 Ru ppb <2
Ce ppm 12.3 Pt ppm 2.22 Ta ppm < 0.01
Ge ppm 0.41 Re ppb 1 Tm ppm 0.018
Infrared Combustion
C wt.% 0.043
Table 3. Indicative Values for OREAS 605
Constituent Unit Value Constituent Unit Value Constituent Unit Value
Laser Ablation ICP-MS

Ag ppm 989 Ho ppm 0.20 Sn ppm 3.10
As ppm 1615 In ppm 3.75 Sr ppm 548
Ba ppm 13150 La ppm 19.4 Ta ppm 0.61
Be ppm 0.90 Lu ppm 0.050 Tb ppm 0.19
Bi ppm 16.6 Mn wt.% 0.009 Te ppm 36.7
Cd ppm 13.9 Mo ppm 4.90 Th ppm 6.78
Ce ppm 31.4 Nb ppm 7.22 Ti wt.% 0.182
Co ppm 94 Nd ppm 12.1 Tl ppm 16.0
Cr ppm 35.0 Ni ppm 1415 Tm ppm 0.040
Cs ppm 1.61 Pb ppm 1390 U ppm 2.69
Cu ppm 47800 Pr ppm 3.70 V ppm 39.4
Dy ppm 1.11 Rb ppm 31.6 W ppm 25.8
Er ppm 0.44 Re ppm 0.013 Y ppm 4.99
Eu ppm 0.38 Sb ppm 272 Yb ppm 0.42
Ga ppm 31.8 Sc ppm 4.50 Zn ppm 2130
Gd ppm 1.70 Se ppm <5 Zr ppm 120
Hf ppm 3.40 Sm ppm 1.94
Borate Fusion XRF
Al2O3 wt.% 10.80 Fe2O3 wt.% 5.54 Pb ppm 1430
As ppm 1620 K2O wt.% 1.31 SiO2 wt.% 59.57
Ba ppm 13700 MgO wt.% 0.100 Sn ppm 12.5
CaO wt.% 0.400 MnO wt.% 0.020 SO3 wt.% 21.00
Co ppm 110 Na2O wt.% 0.810 TiO2 wt.% 0.303
Cr ppm 30.0 Ni ppm 1515 U ppm 20.0
Cu ppm 50850 P2O5 wt.% 0.128 Zn ppm 2080
Thermogravimetry
LOI1000 wt.% 11.82
Table 4. Pooled-Lab Performance Gates for OREAS 605
Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Constituent
Value 1SD 2SD Low 2SD High 3SD Low 3SD High 1RSD 2RSD 3RSD Low
Pb Fire Assay
Ag, ppm 965 25 915 1015 889 1041 2.61% 5.22% 7.84% 917
Au, ppm 1.67 0.086 1.49 1.84 1.41 1.93 5.18% 10.36% 15.54% 1.58
4-Acid Digestion
Ag, ppm 972 28 917 1028 889 1055 2.86% 5.72% 8.57% 923
Al, wt.% 5.43 0.149 5.13 5.73 4.98 5.87 2.74% 5.49% 8.23% 5.16
As, ppm 1602 102 1398 1806 1297 1908 6.35% 12.71% 19.06% 1522
Be, ppm 0.67 0.08 0.52 0.82 0.45 0.90 11.13% 22.27% 33.40% 0.64
Bi, ppm 16.3 2.7 10.9 21.7 8.2 24.4 16.60% 33.20% 49.79% 15.5
Ca, wt.% 0.276 0.009 0.258 0.295 0.249 0.304 3.36% 6.73% 10.09% 0.263
Cd, ppm 12.5 0.97 10.6 14.5 9.6 15.4 7.75% 15.50% 23.25% 11.9
Ce, ppm 21.4 4.0 13.4 29.4 9.3 33.4 18.78% 37.55% 56.33% 20.3
Co, ppm 90 6.0 78 102 72 108 6.62% 13.23% 19.85% 86
Cr, ppm 30.4 4.2 22.1 38.8 18.0 42.9 13.65% 27.29% 40.94% 28.9
Cs, ppm 1.57 0.107 1.36 1.79 1.25 1.90 6.81% 13.62% 20.43% 1.49
Cu, wt.% 5.02 0.152 4.71 5.32 4.56 5.47 3.03% 6.05% 9.08% 4.77
Dy, ppm 1.02 0.083 0.86 1.19 0.77 1.27 8.12% 16.24% 24.36% 0.97
Er, ppm 0.39 0.037 0.32 0.46 0.28 0.50 9.37% 18.75% 28.12% 0.37
Fe, wt.% 3.76 0.260 3.24 4.28 2.98 4.54 6.93% 13.86% 20.79% 3.57
Ga, ppm 30.3 2.29 25.7 34.9 23.4 37.2 7.56% 15.12% 22.68% 28.8
Gd, ppm 1.60 0.094 1.41 1.79 1.32 1.88 5.87% 11.75% 17.62% 1.52
Ge, ppm <5 IND IND IND IND IND IND IND IND IND
Hf, ppm 2.58 0.174 2.23 2.93 2.06 3.10 6.73% 13.46% 20.18% 2.45
Ho, ppm 0.15 0.03 0.10 0.20 0.07 0.23 17.44% 34.89% 52.33% 0.14
In, ppm 3.78 0.346 3.09 4.48 2.75 4.82 9.14% 18.28% 27.43% 3.60
K, wt.% 1.04 0.055 0.93 1.15 0.87 1.20 5.29% 10.57% 15.86% 0.99
La, ppm < 20 IND IND IND IND IND IND IND IND IND
Li, ppm 21.7 2.13 17.5 26.0 15.3 28.1 9.81% 19.61% 29.42% 20.7
Lu, ppb 54 5 45 64 40 69 8.83% 17.66% 26.50% 52
Mg, ppm 476 42 392 559 350 601 8.82% 17.64% 26.45% 452
Mn, ppm 91 5.3 81 102 75 107 5.83% 11.66% 17.49% 87
Mo, ppm 4.82 0.70 3.43 6.21 2.74 6.91 14.42% 28.85% 43.27% 4.58
Na, wt.% 0.580 0.022 0.536 0.625 0.514 0.647 3.82% 7.64% 11.46% 0.551
Nb, ppm 6.92 0.557 5.80 8.03 5.24 8.59 8.05% 16.11% 24.16% 6.57
Nd, ppm 10.7 1.7 7.3 14.0 5.7 15.6 15.56% 31.12% 46.69% 10.1
Ni, ppm 1522 65 1392 1652 1327 1717 4.27% 8.54% 12.81% 1446
P, ppm 507 36 436 579 400 615 7.08% 14.16% 21.23% 482
Pb, ppm 1297 136 1024 1569 888 1705 10.50% 21.00% 31.50% 1232
Pr, ppm 2.97 0.38 2.22 3.73 1.84 4.10 12.68% 25.37% 38.05% 2.82
Rb, ppm 29.2 3.3 22.6 35.9 19.2 39.2 11.42% 22.85% 34.27% 27.8
S, wt.% 8.34 0.571 7.19 9.48 6.62 10.05 6.85% 13.69% 20.54% 7.92
Sb, ppm 294 16 262 325 246 341 5.37% 10.74% 16.12% 279
Sc, ppm 5.03 0.66 3.71 6.36 3.04 7.02 13.17% 26.34% 39.51% 4.78
Se, ppm 76 7.2 62 91 55 98 9.44% 18.89% 28.33% 73
Sm, ppm 2.09 0.138 1.81 2.36 1.67 2.50 6.62% 13.25% 19.87% 1.98
Sn, ppm 2.73 0.29 2.15 3.30 1.87 3.59 10.50% 21.00% 31.51% 2.59
Sr, ppm 373 73 227 520 153 593 19.65% 39.30% 58.94% 355
Ta, ppm <1 IND IND IND IND IND IND IND IND IND
Tb, ppm 0.20 0.02 0.16 0.25 0.13 0.27 11.74% 23.48% 35.22% 0.19
Te, ppm 31.8 4.8 22.2 41.4 17.3 46.3 15.15% 30.30% 45.46% 30.2
Th, ppm 5.12 0.82 3.48 6.75 2.67 7.56 15.94% 31.89% 47.83% 4.86
Ti, wt.% 0.177 0.012 0.152 0.201 0.140 0.214 6.94% 13.89% 20.83% 0.168
Tl, ppm 15.0 1.22 12.5 17.4 11.3 18.6 8.18% 16.36% 24.54% 14.2
U, ppm 2.79 0.167 2.46 3.13 2.30 3.29 5.96% 11.91% 17.87% 2.66
V, ppm 39.9 1.81 36.3 43.5 34.5 45.3 4.53% 9.07% 13.60% 37.9
W, ppm 27.0 3.2 20.5 33.5 17.2 36.7 12.02% 24.04% 36.06% 25.6
Y, ppm 4.26 0.320 3.62 4.90 3.30 5.22 7.50% 15.01% 22.51% 4.05
Yb, ppm 0.37 0.05 0.27 0.48 0.21 0.54 14.44% 28.88% 43.32% 0.36
Zn, wt.% 0.216 0.009 0.198 0.234 0.189 0.243 4.17% 8.34% 12.51% 0.205
Zr, ppm 84 6.0 72 96 66 102 7.18% 14.35% 21.53% 80
Ag, ppm 984 29 925 1042 896 1071 2.97% 5.94% 8.91% 934
Al, wt.% 0.730 0.123 0.485 0.975 0.362 1.098 16.80% 33.60% 50.40% 0.694
As, ppm 1613 131 1352 1875 1221 2005 8.10% 16.21% 24.31% 1533
Au, ppm 1.66 0.081 1.49 1.82 1.41 1.90 4.89% 9.79% 14.68% 1.57
B, ppm < 10 IND IND IND IND IND IND IND IND IND
Be, ppm 0.16 0.03 0.09 0.22 0.06 0.25 19.92% 39.84% 59.76% 0.15
Bi, ppm 16.7 3.0 10.6 22.7 7.5 25.8 18.27% 36.54% 54.82% 15.8
Ca, wt.% 0.182 0.013 0.157 0.208 0.145 0.220 6.92% 13.83% 20.75% 0.173
Cd, ppm 12.9 1.5 9.9 15.8 8.5 17.3 11.42% 22.83% 34.25% 12.2
Co, ppm 93 6.9 79 107 72 114 7.42% 14.85% 22.27% 88
Cr, ppm 27.5 3.1 21.3 33.7 18.2 36.8 11.27% 22.55% 33.82% 26.1
Cs, ppm 0.48 0.07 0.34 0.62 0.26 0.69 15.01% 30.01% 45.02% 0.45
Cu, wt.% 4.98 0.157 4.67 5.29 4.51 5.45 3.15% 6.30% 9.45% 4.73
Dy, ppm 0.52 0.051 0.42 0.62 0.37 0.67 9.87% 19.74% 29.61% 0.49
Er, ppm 0.15 0.03 0.09 0.21 0.06 0.24 19.45% 38.90% 58.35% 0.14
Eu, ppm 0.21 0.04 0.13 0.29 0.09 0.33 18.38% 36.75% 55.13% 0.20
Fe, wt.% 3.75 0.181 3.39 4.11 3.21 4.29 4.83% 9.66% 14.50% 3.56
Ga, ppm 6.66 0.86 4.95 8.38 4.09 9.23 12.87% 25.74% 38.60% 6.33
Gd, ppm 0.87 0.17 0.54 1.21 0.37 1.38 19.40% 38.80% 58.19% 0.83
Hf, ppm 0.55 0.11 0.33 0.77 0.21 0.88 20.31% 40.63% 60.94% 0.52
Hg, ppm <4 IND IND IND IND IND IND IND IND IND
Ho, ppb 73 12 49 97 37 109 16.43% 32.87% 49.30% 69
In, ppm 3.75 0.51 2.72 4.78 2.20 5.29 13.73% 27.46% 41.19% 3.56
K, wt.% 0.134 0.024 0.086 0.181 0.062 0.205 17.82% 35.65% 53.47% 0.127
La, ppm 3.95 0.86 2.24 5.67 1.38 6.53 21.68% 43.35% 65.03% 3.76
Li, ppm 5.17 0.99 3.19 7.15 2.20 8.14 19.14% 38.28% 57.42% 4.91
Lu, ppb 11 1 8 14 7 16 13.15% 26.30% 39.45% 11
Mg, ppm 289 52 185 394 132 446 18.08% 36.16% 54.24% 275
Mn, ppm 86 4.8 76 95 71 100 5.65% 11.30% 16.95% 81
Mo, ppm 4.75 0.424 3.90 5.60 3.48 6.02 8.93% 17.87% 26.80% 4.51
Na, ppm 328 60 209 448 149 507 18.18% 36.37% 54.55% 312
Nb, ppm 0.45 0.06 0.34 0.56 0.28 0.62 12.49% 24.97% 37.46% 0.43
Nd, ppm 6.10 1.15 3.80 8.40 2.65 9.55 18.83% 37.67% 56.50% 5.80
Ni, ppm 1538 64 1411 1665 1348 1729 4.13% 8.26% 12.38% 1461
P, ppm 116 24 68 163 44 187 20.57% 41.14% 61.71% 110
Pb, ppm 856 40 775 937 735 977 4.71% 9.42% 14.13% 813
Pr, ppm 1.74 0.24 1.25 2.22 1.01 2.46 13.93% 27.86% 41.80% 1.65
Rb, ppm 5.75 0.96 3.83 7.67 2.87 8.63 16.72% 33.43% 50.15% 5.46
S, wt.% 7.86 0.491 6.88 8.84 6.39 9.34 6.25% 12.50% 18.75% 7.47
Sb, ppm 228 46 137 319 92 365 19.94% 39.89% 59.83% 217
Sc, ppm 1.05 0.12 0.81 1.28 0.70 1.39 11.01% 22.03% 33.04% 0.99
Se, ppm 75 11 53 97 42 108 14.52% 29.03% 43.55% 71
Sm, ppm 1.16 0.20 0.77 1.55 0.57 1.75 16.88% 33.77% 50.65% 1.10
Sn, ppm 1.92 0.22 1.47 2.37 1.25 2.59 11.69% 23.37% 35.06% 1.82
Sr, ppm 28.1 5.5 17.0 39.1 11.5 44.6 19.65% 39.30% 58.96% 26.7
Tb, ppm 0.11 0.02 0.06 0.15 0.04 0.17 20.34% 40.67% 61.01% 0.10
Te, ppm 33.1 2.60 27.9 38.3 25.3 40.9 7.87% 15.74% 23.61% 31.4
Th, ppm <3 IND IND IND IND IND IND IND IND IND
Ti, ppm 100 12 75 125 63 137 12.29% 24.58% 36.87% 95
Tl, ppm 15.3 1.6 12.0 18.5 10.4 20.1 10.51% 21.02% 31.53% 14.5
U, ppm 0.95 0.13 0.69 1.21 0.56 1.34 13.71% 27.41% 41.12% 0.90
V, ppm 8.33 1.08 6.17 10.49 5.10 11.56 12.94% 25.88% 38.82% 7.91
W, ppm 5.90 1.16 3.57 8.22 2.41 9.38 19.71% 39.43% 59.14% 5.60
Y, ppm 1.91 0.34 1.24 2.58 0.90 2.91 17.61% 35.23% 52.84% 1.81
Yb, ppm 0.099 0.017 0.065 0.133 0.047 0.151 17.39% 34.77% 52.16% 0.094
Zn, wt.% 0.217 0.010 0.197 0.236 0.187 0.246 4.56% 9.12% 13.67% 0.206
Zr, ppm 19.0 2.7 13.6 24.3 11.0 27.0 14.04% 28.08% 42.11% 18.0
Infrared Combustion
S, wt.% 8.79 0.330 8.13 9.45 7.81 9.78 3.75% 7.50% 11.25% 8.35
5% window
High
1013
1.75
1021
5.70
1682
0.71
17.1
0.290
13.1
22.5
95
32.0
1.65
5.27
1.07
0.41
3.95
31.8
1.68
IND
2.71
0.16
3.97
1.09
IND
22.8
57
499
96
5.06
0.609
7.26
11.2
1598
533
1361
3.12
30.7
8.75
309
5.28
80
2.19
2.86
392
IND
0.21
33.4
5.37
0.186
15.7
2.93
41.9
28.3
4.48
0.39
0.227
88
1033
0.767
1694
1.74
IND
0.17
17.5
0.192
13.5
98
28.9
0.50
5.23
0.55
0.16
0.22
3.94
7.00
0.92
0.58
IND
76
3.93
0.140
4.15
5.43
12
304
90
4.99
345
0.47
6.41
1615
121
899
1.82
6.04
8.25
240
1.10
79
1.22
2.01
29.5
0.11
34.7
IND
105
16.0
1.00
8.75
6.19
2.00
0.104
0.228
19.9
9.23
Analytical results for Ag in OREAS 605 (Certified Value 965 ppm)
Ag Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 03 05 07 08 10
FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*OES
40g 30g 30g 30g 30g 30g
1 1 888 953 1030 954 960 978
1 2 894 951 1015 952 962 978
1 3 899 954 1015 954 914 978
1 4 884 970 1015 958 928 981
1 5 892 956 999 993 957 974
1 6 888 957 1035 982 967 982
Mean 891 957 1018 966 948 979
Median 890 955 1015 956 959 978
Std Dev. 5 7 13 18 22 3
Rel.Std.Dev. 0.60% 0.71% 1.26% 1.81% 2.28% 0.29%
PDM3 -7.69% -0.84% 5.52% 0.06% -1.75% 1.41%
Z-Score (Absolute) 3.13 0.09 2.73 0.05 0.50 0.90
Analytical results for Au in OREAS 605 (Certified Value 1.67 ppm)

Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 00 01 02 03 04 05
INAA FA*AAS FA*AAS FA*OES FA*AAS FA*AAS
1.0g 40g 25g 30g 30g 30g
1 1 1.67 1.51 1.67 1.79 1.70 1.73
1 2 1.68 1.61 1.67 1.77 1.67 1.62
1 3 1.68 1.51 1.72 1.74 1.78 1.61
1 4 1.69 1.52 1.70 1.79 1.69 1.73
1 5 1.68 1.50 1.70 1.73 1.59 1.63
1 6 1.66 1.57 1.71 1.77 1.68 1.75
7 1.60
8 1.59
9 1.66
10 1.61
11 1.64
12 1.64
13 1.58
14 1.56
15 1.62
16 1.66
17 1.66
18 1.68
19 1.63
20 1.67
Mean 1.64 1.54 1.69 1.76 1.68 1.68
Median 1.66 1.51 1.70 1.77 1.69 1.68
Std Dev. 0.038 0.043 0.021 0.024 0.060 0.064
Rel.Std.Dev. 2.32% 2.81% 1.22% 1.36% 3.54% 3.84%
PDM3 -1.44% -7.87% 1.68% 5.68% 0.98% 0.58%
Z-Score (Absolute) NA 2.26 0.24 1.20 0.07 0.02
Analytical results for Pd in OREAS 605 (Indicative Value 13.43 ppm)

Pd Round Replicate Lab Lab
No No 22 25
FA*OES FA*OES
30g 40g
1 1 15.00 12.70
1 2 12.90 13.30
1 3 12.50
1 4 13.20
1 5 12.70
1 6 13.10
Mean 13.95 12.92
Median 13.95 12.90
Std Dev. 1.485 0.325
Rel.Std.Dev. 10.64% 2.52%
PDM3 3.85% -3.85%
Z-Score (Absolute) 0.67 0.67
Analytical results for Pt in OREAS 605 (Indicative Value 2.21 ppm)

Pt Round Replicate Lab Lab
No No 22 25
FA*OES FA*OES
30g 40g
1 1 2.39 2.13
1 2 2.06 2.26
1 3 2.16
1 4 2.26
1 5 2.14
1 6 2.24
Mean 2.23 2.20
Median 2.23 2.20
Std Dev. 0.233 0.061
Rel.Std.Dev. 10.49% 2.80%
PDM3 0.60% -0.60%
Lab Lab Lab Lab Lab Lab Lab
11 12 16 17 19 20 23
FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*GRAV
30g 30g 30g 30g 30g 40g 30g
957 969 958 663 991 977 918
956 764 946 720 953 975 944
966 822 961 649 971 948 868
963 830 964 694 970 970 924
963 988 951 741 968 984 911
962 798 973 753 988 963 927
961 862 959 703 974 969 915
963 826 960 707 971 973 921
4 94 10 42 14 13 26
0.40% 10.85% 1.00% 5.97% 1.44% 1.30% 2.81%
-0.39% -10.68% -0.63% -27.11% 0.89% 0.47% -5.14%
0.11 4.46 0.00 11.75 0.67 0.49 1.56
Lab Lab Lab Lab Lab Lab Lab Lab Lab

06 07 08 09 10 11 12 13 14
FA*AAS FA*AAS FA*AAS FA*AAS FA*GRAV FA*AAS FA*AAS FA*AAS FA*OES
30g 30g 30g 30g 30g 30g 30g 30g 25g
1.67 1.69 1.62 1.58 1.23 1.72 1.68 1.48 1.62
1.77 1.68 1.62 1.58 1.25 1.72 1.75 1.52 1.64
1.75 1.71 1.64 1.58 1.21 1.70 1.54 1.50 1.59
1.72 1.73 1.61 1.59 1.26 1.71 1.71 1.49 1.69
1.75 1.73 1.63 1.57 1.28 1.68 2.02 1.45 1.63
1.68 1.73 1.67 1.58 1.34 1.70 1.71 1.48 1.61
1.72 1.71 1.63 1.58 1.26 1.70 1.73 1.48 1.63

1.73 1.72 1.63 1.58 1.26 1.70 1.71 1.48 1.63
0.042 0.022 0.022 0.006 0.045 0.015 0.156 0.024 0.034
2.41% 1.31% 1.33% 0.40% 3.59% 0.89% 8.97% 1.64% 2.09%
3.28% 2.38% -2.22% -5.04% -24.32% 2.11% 4.05% -10.93% -2.22%
0.63 0.41 0.69 1.37 6.00 0.35 0.00 2.79 0.69
15 16 17 18 19 20 21 22 23
FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*GRAV FA*AAS FA*OES FA*AAS
30g 30g 30g 30g 30g 40g 30g 30g 30g
1.53 1.67 1.65 1.79 1.64 1.70 1.63 1.88 1.63
1.45 1.66 1.84 1.78 1.64 1.70 1.59 1.70 1.58
1.51 1.65 1.68 1.78 1.61 1.60 1.62 1.65
1.50 1.71 1.66 1.75 1.60 1.60 1.57 1.66
1.50 1.67 1.76 1.77 1.65 1.60 1.62 1.60
1.64 1.71 1.74 1.74 1.65 1.70 1.53 1.66
1.52 1.68 1.72 1.77 1.63 1.65 1.59 1.79 1.63

1.51 1.67 1.71 1.78 1.64 1.65 1.60 1.79 1.64
0.064 0.024 0.073 0.019 0.019 0.055 0.040 0.127 0.031
4.19% 1.46% 4.23% 1.10% 1.18% 3.32% 2.50% 7.11% 1.92%
-8.72% 0.66% 3.28% 6.08% -2.11% -1.02% -4.52% 7.38% -2.22%
2.60 0.00 0.63 1.30 0.67 0.41 1.25 1.61 0.69
Lab Lab Lab Lab
24 25 26 27
FA*AAS FA*OES FA*AAS FA*AAS
20g 40g 40g 20g
1.78 1.64 1.72 1.74
1.74 1.73 1.71 1.71
1.76 1.69 1.71 1.64
1.78 1.71 1.73 1.89
1.78 1.65 1.74 1.74
1.80 1.72 1.74 1.63
1.77 1.69 1.72 1.72

1.78 1.70 1.73 1.72
0.021 0.037 0.014 0.094
1.16% 2.21% 0.80% 5.46%
6.38% 1.38% 3.48% 3.18%
1.37 0.17 0.67 0.60
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
965
7
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.67
8.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
13.43
7.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
2.21
7.00
No No 01 02 04 05 06 07
AR*OES AR*MS AR*AAS AR*OES/AAS
AR*OES/AAS
AR*OES/AAS
0.5g 40g 01g 0.5g 0.5g 0.5g
1 1 1005 > 250 982 992 1010 987
1 2 1002 > 250 993 997 1010 984
1 3 999 > 250 986 997 1020 972
1 4 1004 > 250 984 1005 947 978
1 5 1002 > 250 983 993 951 985
1 6 1008 > 250 970 1005 954 992
Mean 1003 983 998 982 983
Median 1003 984 997 982 985
Std Dev. 3 7 6 35 7
Rel.Std.Dev. 0.31% 0.76% 0.57% 3.52% 0.72%
PDM3 2.00% -0.07% 1.47% -0.17% -0.07%
Z-Score (Absolute) 0.67 NA 0.00 0.50 0.03 0.00
Analytical results for Al in OREAS 605 (Certified Value 0.73 wt.%)

Al Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES
0.5g 40g 01g 01g 01g 01g
1 1 0.980 0.906 0.760 0.680 0.730 0.720
1 2 0.950 0.902 0.760 0.680 0.730 0.700
1 3 0.967 0.892 0.750 0.680 0.720 0.660
1 4 0.967 0.889 0.760 0.680 0.700 0.670
1 5 0.973 0.878 0.750 0.630 0.710 0.670
1 6 0.957 0.883 0.770 0.640 0.730 0.660
Mean 0.966 0.892 0.758 0.665 0.720 0.680
Median 0.967 0.891 0.760 0.680 0.725 0.670
Std Dev. 0.011 0.011 0.008 0.023 0.013 0.024
Rel.Std.Dev. 1.13% 1.21% 0.99% 3.53% 1.76% 3.60%
PDM3 32.27% 22.17% 3.88% -8.90% -1.37% -6.85%
Z-Score (Absolute) 1.75 1.25 0.34 0.29 0.08 0.19
Analytical results for As in OREAS 605 (Certified Value 1613 ppm)

As Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
AR*OES AR*MS AR*OES AR*OES AR*OES AR*OES
0.5g 40g 01g 01g 01g 01g
1 1 1848 1401 1650 1700 1730 1685
1 2 1850 1444 1720 1710 1740 1625
1 3 1855 1407 1710 1730 1715 1620
1 4 1851 1389 1710 1710 1700 1645
1 5 1842 1485 1700 1610 1700 1635
1 6 1859 1446 1700 1600 1720 1620
Mean 1851 1429 1698 1677 1718 1638
Median 1850 1426 1705 1705 1718 1630
Std Dev. 6 36 25 56 16 25
Rel.Std.Dev. 0.32% 2.53% 1.46% 3.37% 0.93% 1.52%
PDM3 14.73% -11.44% 5.28% 3.94% 6.47% 1.56%
Z-Score (Absolute) 1.69 1.53 0.60 0.36 0.67 0.00
Analytical results for Au in OREAS 605 (Certified Value 1.66 ppm)

Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 00 01 02 05 06 07
INAA AR*AAS AR*MS AR*MS AR*MS AR*MS
1.0g 30g 25g 25g 25g 25g
1 1 1.67 1.52 1.55 1.67 1.51 1.71
1 2 1.68 1.54 1.55 1.61 1.40 1.69
1 3 1.68 1.45 1.51 1.58 1.48 1.68
1 4 1.69 1.56 1.51 1.68 1.38 1.70
1 5 1.68 1.57 1.57 1.64 1.34 1.74
1 6 1.66 1.56 1.56 1.63 1.66 1.76
7 1.60
8 1.59
9 1.66
10 1.61
11 1.64
12 1.64
13 1.58
14 1.56
15 1.62
16 1.66
17 1.66
18 1.68
19 1.63
20 1.67
Mean 1.64 1.53 1.54 1.63 1.46 1.71
Median 1.66 1.55 1.55 1.63 1.44 1.71
Std Dev. 0.038 0.043 0.024 0.037 0.116 0.031
Rel.Std.Dev. 2.32% 2.81% 1.54% 2.28% 7.94% 1.80%
PDM3 -0.75% -7.36% -6.79% -1.23% -11.70% 3.50%
Analytical results for B in OREAS 605 (Certified Value < 10 ppm)

B Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 06 07 08 09 14
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES
01g 01g 01g 01g 20g 0.5g
1 1 < 10 < 10 < 10 < 10 < 10 <5
1 2 < 10 < 10 < 10 < 10 < 10 <5
1 3 < 10 < 10 < 10 < 10 < 10 <5
1 4 < 10 < 10 < 10 < 10 < 10 <5
1 5 < 10 < 10 < 10 < 10 < 10 <5
1 6 < 10 < 10 < 10 < 10 < 10 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA NA NA NA NA
Analytical results for Ba in OREAS 605 (Indicative Value 25.3 ppm)

Ba Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 6.1 34.0 20.0 20.0 10.0 20.0
1 2 6.3 32.0 20.0 20.0 10.0 20.0
1 3 6.2 26.0 20.0 20.0 10.0 20.0
1 4 6.2 39.0 20.0 20.0 10.0 20.0
1 5 6.6 36.0 20.0 20.0 10.0 30.0
1 6 5.8 37.0 10.0 20.0 10.0 20.0
Mean 6.2 34.0 18.3 20.0 10.0 21.7
Median 6.2 35.0 20.0 20.0 10.0 20.0
Std Dev. 0.2 4.6 4.1 0.0 0.0 4.1
Rel.Std.Dev. 3.91% 13.54% 22.27% 0.00% 0.00% 18.84%
PDM3 -75.56% 34.14% -27.67% -21.10% -60.55% -14.52%
Z-Score (Absolute) 0.89 0.69 0.20 0.10 0.67 0.01
Analytical results for Be in OREAS 605 (Certified Value 0.16 ppm)

Be Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 <1 0.14 < 0.5 < 0.5 < 0.5 < 0.5
1 2 <1 0.13 < 0.5 < 0.5 < 0.5 < 0.5
1 3 <1 0.14 < 0.5 < 0.5 < 0.5 < 0.5
1 4 <1 0.15 < 0.5 < 0.5 < 0.5 < 0.5
1 5 <1 0.14 < 0.5 < 0.5 < 0.5 < 0.5
1 6 <1 0.14 < 0.5 < 0.5 < 0.5 < 0.5
Mean 0.14
Median 0.14
Std Dev. 0.006
Rel.Std.Dev. 4.52%
PDM3 -11.13%
Z-Score (Absolute) NA 0.53 NA NA NA NA
Analytical results for Bi in OREAS 605 (Certified Value 16.7 ppm)

Bi Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 <5 17.7 15.0 25.0 12.0 11.0
1 2 <5 17.2 14.0 19.0 19.0 7.0
1 3 <5 17.8 15.0 16.0 25.0 10.0
1 4 <5 17.8 12.0 22.0 16.0 19.0
1 5 <5 16.2 15.0 23.0 19.0 19.0
1 6 <5 17.4 9.0 19.0 18.0 14.0
Mean 17.3 13.3 20.7 18.2 13.3
Median 17.6 14.5 20.5 18.5 12.5
Std Dev. 0.6 2.4 3.3 4.3 4.9
Rel.Std.Dev. 3.46% 18.17% 15.80% 23.46% 36.95%
PDM3 4.12% -19.95% 24.08% 9.07% -19.95%
Analytical results for Ca in OREAS 605 (Certified Value 0.182 wt.%)

Ca Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 0.153 0.190 0.180 0.190 0.190 0.200
1 2 0.153 0.180 0.180 0.190 0.190 0.190
1 3 0.160 0.190 0.180 0.190 0.190 0.190
1 4 0.157 0.180 0.190 0.200 0.190 0.190
1 5 0.153 0.180 0.180 0.180 0.190 0.190
1 6 0.153 0.190 0.190 0.180 0.200 0.190
Mean 0.155 0.185 0.183 0.188 0.192 0.192
Median 0.153 0.185 0.180 0.190 0.190 0.190
Std Dev. 0.003 0.005 0.005 0.008 0.004 0.004
Rel.Std.Dev. 1.80% 2.96% 2.82% 4.00% 2.13% 2.13%
PDM3 -15.03% 1.41% 0.50% 3.24% 5.07% 5.07%
Z-Score (Absolute) 2.29 0.13 0.00 0.40 0.67 0.67
Analytical results for Cd in OREAS 605 (Certified Value 12.9 ppm)

Cd Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 27.5 11.2 13.4 13.6 13.7 13.6
1 2 27.6 11.3 13.6 13.7 13.7 13.3
1 3 27.9 11.2 13.3 13.7 13.5 13.2
1 4 27.3 11.2 13.3 13.8 13.2 13.2
1 5 27.4 11.7 13.3 12.7 13.3 13.2
1 6 27.5 11.4 13.3 13.0 13.3 12.9
Mean 27.6 11.3 13.4 13.4 13.4 13.2
Median 27.5 11.3 13.3 13.6 13.4 13.2
Std Dev. 0.2 0.2 0.1 0.5 0.2 0.2
Rel.Std.Dev. 0.79% 1.98% 0.91% 3.38% 1.61% 1.70%
PDM3 113.81% -12.09% 3.73% 4.12% 4.38% 2.70%
Z-Score (Absolute) 7.65 1.06 0.07 0.10 0.12 0.00
Analytical results for Ce in OREAS 605 (Indicative Value 12.3 ppm)

Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 13 14 15
AR*MS AR*OES/MS AR*OES AR*MS AR*MS AR*OES/MS
40g 20g 0.15g 01g 0.5g 01g
1 1 14.6 16.3 14.0 8.2 11.3 17.4
1 2 14.1 16.6 14.0 7.7 10.8 17.2
1 3 14.7 15.6 13.0 8.1 10.8 17.2
1 4 14.9 16.3 15.0 8.6 11.0 16.3
1 5 14.4 17.2 15.0 8.3 10.9 17.3
1 6 14.1 15.6 14.0 8.1 11.3 17.0
Mean 14.5 16.3 14.2 8.2 11.0 17.1
Median 14.5 16.3 14.0 8.2 10.9 17.2
Std Dev. 0.3 0.6 0.8 0.3 0.2 0.4
Rel.Std.Dev. 2.27% 3.62% 5.31% 3.71% 2.14% 2.35%
PDM3 17.89% 32.49% 15.35% -33.37% -10.53% 38.85%
Z-Score (Absolute) 0.67 1.07 0.61 0.72 0.10 1.28
Analytical results for Co in OREAS 605 (Certified Value 93 ppm)

Co Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 81 72 95 96 98 97
1 2 80 73 96 96 99 94
1 3 82 71 95 96 98 93
1 4 82 72 95 96 97 94
1 5 82 71 94 90 96 94
1 6 81 71 96 91 97 92
Mean 81 72 95 94 98 94
Median 81 72 95 96 98 94
Std Dev. 0.6 0.9 0.8 2.9 1.0 1.7
Rel.Std.Dev. 0.72% 1.28% 0.79% 3.03% 1.08% 1.78%
PDM3 -12.52% -22.68% 2.44% 1.36% 4.95% 1.18%
Z-Score (Absolute) 1.71 3.01 0.21 0.18 0.53 0.05
Analytical results for Cr in OREAS 605 (Certified Value 27.5 ppm)

Cr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 30.3 30.0 26.0 27.0 32.0 29.0
1 2 29.8 28.0 27.0 26.0 31.0 31.0
1 3 30.5 30.0 35.0 25.0 30.0 30.0
1 4 31.0 30.0 27.0 26.0 31.0 27.0
1 5 30.1 32.0 27.0 25.0 28.0 28.0
1 6 29.7 28.0 27.0 23.0 31.0 26.0
Mean 30.2 29.7 28.2 25.3 30.5 28.5
Median 30.2 30.0 27.0 25.5 31.0 28.5
Std Dev. 0.5 1.5 3.4 1.4 1.4 1.9
Rel.Std.Dev. 1.57% 5.07% 11.97% 5.39% 4.52% 6.56%
PDM3 9.92% 7.88% 2.42% -7.88% 10.91% 3.64%
Z-Score (Absolute) 0.90 0.67 0.45 1.03 1.00 0.22
Analytical results for Cs in OREAS 605 (Certified Value 0.48 ppm)

Cs Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 17
AR*MS AR*OES/MS AR*MS AR*MS AR*OES/MSAR*OES/MS
40g 20g 01g 0.5g 01g 0.25g
1 1 0.49 0.54 0.62 0.49 0.67 0.43
1 2 0.48 0.54 0.57 0.48 0.68 0.52
1 3 0.46 0.52 0.61 0.48 0.64 0.52
1 4 0.48 0.57 0.65 0.48 0.72 0.44
1 5 0.51 0.53 0.62 0.49 0.66 0.46
1 6 0.46 0.51 0.59 0.50 0.65 0.45
Mean 0.48 0.53 0.61 0.49 0.67 0.47
Median 0.48 0.53 0.61 0.49 0.67 0.46
Std Dev. 0.019 0.022 0.029 0.008 0.028 0.040
Rel.Std.Dev. 3.95% 4.09% 4.80% 1.68% 4.22% 8.51%
PDM3 0.27% 11.18% 27.43% 1.67% 39.96% -1.82%
Z-Score (Absolute) 0.00 0.67 1.68 0.09 2.45 0.13
Analytical results for Cu in OREAS 605 (Certified Value 4.98 wt.%)

Cu Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 07
AR*OES AR*OES AR*AAS AR*OES/AAS
AR*OES/AAS
AR*OES/AAS
0.5g 40g 01g 0.5g 0.5g 0.5g
1 1 4.81 > 10000 5.01 5.02 5.37 4.66
1 2 4.81 > 10000 5.04 5.00 5.36 4.61
1 3 4.81 > 10000 5.02 5.01 5.40 4.63
1 4 4.81 > 10000 4.95 5.01 4.98 4.64
1 5 4.81 > 10000 4.96 5.04 5.02 4.65
1 6 4.81 > 10000 4.95 5.01 5.09 4.62
Mean 4.81 4.99 5.02 5.20 4.64
Median 4.81 4.99 5.01 5.23 4.64
Std Dev. 0.002 0.037 0.014 0.194 0.019
Rel.Std.Dev. 0.04% 0.75% 0.27% 3.72% 0.40%
PDM3 -3.46% 0.15% 0.70% 4.48% -6.93%
Z-Score (Absolute) 1.84 NA 0.00 0.28 2.21 3.62
Analytical results for Dy in OREAS 605 (Certified Value 0.52 ppm)

Dy Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
AR*MS AR*OES/MS AR*MS AR*MS AR*OES/MS AR*MS
40g 20g 01g 0.5g 01g 40g
1 1 0.55 0.58 0.46 0.46 0.59 0.37
1 2 0.55 0.56 0.45 0.45 0.51 0.34
1 3 0.56 0.54 0.49 0.47 0.56 0.35
1 4 0.57 0.58 0.48 0.45 0.48 0.35
1 5 0.55 0.59 0.49 0.44 0.58 0.35
1 6 0.55 0.52 0.48 0.47 0.58 0.35
Mean 0.56 0.56 0.47 0.46 0.55 0.35
Median 0.55 0.57 0.48 0.46 0.57 0.35
Std Dev. 0.008 0.027 0.016 0.012 0.045 0.010
Rel.Std.Dev. 1.51% 4.78% 3.36% 2.65% 8.13% 2.80%
PDM3 6.75% 8.34% -8.71% -12.17% 5.79% -32.36%
Z-Score (Absolute) 0.61 0.73 0.54 0.80 0.54 2.37
Analytical results for Er in OREAS 605 (Certified Value 0.15 ppm)

Er Round Replicate Lab Lab Lab Lab Lab
No No 02 09 14 15 25
AR*MS AR*OES/MS AR*MS AR*OES/MS AR*MS
40g 20g 0.5g 01g 40g
1 1 0.17 0.17 0.14 0.18 0.12
1 2 0.16 0.18 0.13 0.17 0.10
1 3 0.17 0.17 0.14 0.19 0.10
1 4 0.17 0.17 0.14 0.19 0.10
1 5 0.17 0.17 0.14 0.15 0.09
1 6 0.17 0.18 0.14 0.20 0.12
Mean 0.17 0.17 0.14 0.18 0.11
Median 0.17 0.17 0.14 0.19 0.10
Std Dev. 0.004 0.005 0.004 0.018 0.012
Rel.Std.Dev. 2.43% 2.81% 2.95% 9.94% 11.66%
PDM3 10.31% 12.29% -9.35% 17.95% -31.19%
Z-Score (Absolute) 0.00 0.17 1.73 0.67 3.66
Analytical results for Eu in OREAS 605 (Certified Value 0.21 ppm)

Eu Round Replicate Lab Lab Lab Lab Lab
No No 02 09 14 15 25
40g 20g 0.5g 01g 40g
1 1 0.23 0.25 0.19 0.23 0.16
1 2 0.22 0.25 0.19 0.26 0.14
1 3 0.23 0.24 0.18 0.26 0.14
1 4 0.23 0.24 0.19 0.25 0.15
1 5 0.23 0.26 0.18 0.24 0.15
1 6 0.23 0.22 0.20 0.25 0.15
Mean 0.23 0.24 0.19 0.25 0.15
Median 0.23 0.24 0.19 0.25 0.15
Std Dev. 0.004 0.013 0.008 0.012 0.007
Rel.Std.Dev. 1.79% 5.17% 4.00% 4.71% 4.74%
PDM3 8.02% 14.61% -10.91% 17.48% -29.20%
Z-Score (Absolute) 0.00 0.47 1.35 0.67 2.65
Analytical results for Fe in OREAS 605 (Certified Value 3.75 wt.%)

Fe Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 3.58 3.74 3.56 3.72 3.59 3.65
1 2 3.62 3.73 3.58 3.71 3.61 3.58
1 3 3.62 3.75 3.59 3.74 3.56 3.50
1 4 3.66 3.69 3.55 3.72 3.53 3.55
1 5 3.58 3.73 3.53 3.47 3.53 3.54
1 6 3.60 3.74 3.60 3.52 3.58 3.50
Mean 3.61 3.73 3.57 3.65 3.57 3.55
Median 3.61 3.74 3.57 3.72 3.57 3.55
Std Dev. 0.030 0.021 0.026 0.119 0.033 0.056
Rel.Std.Dev. 0.82% 0.56% 0.74% 3.26% 0.92% 1.59%
PDM3 -3.69% -0.54% -4.85% -2.76% -4.89% -5.25%
Z-Score (Absolute) 0.50 0.03 0.67 0.22 0.68 0.73
Analytical results for Ga in OREAS 605 (Certified Value 6.66 ppm)

Ga Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 13 14
AR*OES AR*MS AR*OES/MS AR*OES AR*MS AR*MS
0.5g 40g 20g 0.15g 01g 0.5g
1 1 7.78 6.29 7.54 8.00 7.78 6.16
1 2 7.79 6.32 7.88 10.00 7.61 6.16
1 3 8.18 6.39 7.29 9.00 8.11 6.36
1 4 7.77 6.40 7.59 9.00 8.01 6.24
1 5 7.95 6.18 7.48 9.00 8.01 6.23
1 6 8.10 6.29 7.17 9.00 7.79 6.49
Mean 7.93 6.31 7.49 9.00 7.88 6.27
Median 7.87 6.31 7.51 9.00 7.90 6.24
Std Dev. 0.178 0.080 0.248 0.632 0.188 0.129
Rel.Std.Dev. 2.25% 1.27% 3.32% 7.03% 2.38% 2.06%
PDM3 18.99% -5.27% 12.42% 35.08% 18.32% -5.85%
Z-Score (Absolute) 1.65 0.22 1.14 2.89 1.60 0.26
Analytical results for Gd in OREAS 605 (Certified Value 0.87 ppm)

Gd Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
40g 20g 01g 0.5g 01g 40g
1 1 0.95 0.98 0.77 0.81 1.17 0.66
1 2 0.95 1.04 0.73 0.80 1.19 0.63
1 3 0.97 0.89 0.73 0.82 1.04 0.62
1 4 0.96 0.99 0.75 0.82 1.05 0.62
1 5 0.96 0.98 0.79 0.81 1.14 0.65
1 6 0.91 0.91 0.74 0.84 1.17 0.61
Mean 0.95 0.97 0.75 0.82 1.13 0.63
Median 0.96 0.98 0.75 0.82 1.15 0.62
Std Dev. 0.021 0.055 0.021 0.014 0.065 0.021
Rel.Std.Dev. 2.21% 5.68% 2.84% 1.67% 5.80% 3.31%
PDM3 8.60% 10.39% -14.00% -6.64% 28.80% -28.07%
Z-Score (Absolute) 0.45 0.50 0.85 0.45 1.51 1.63
Analytical results for Ge in OREAS 605 (Indicative Value 0.41 ppm)

Ge Round Replicate Lab Lab Lab Lab
No No 11 15 17 19
AR*OES AR*OES/MSAR*OES/MSAR*OES/MS
0.15g 01g 0.25g 0.25g
1 1 < 10 0.57 0.20 0.43
1 2 < 10 0.54 0.40 0.41
1 3 < 10 0.62 < 0.1 0.38
1 4 < 10 0.61 0.20 0.36
1 5 < 10 0.66 0.40 0.32
1 6 < 10 0.56 0.30 0.35
Mean 0.59 0.30 0.37
Median 0.59 0.30 0.37
Std Dev. 0.045 0.100 0.042
Rel.Std.Dev. 7.51% 33.33% 11.36%
PDM3 45.50% -26.43% -8.86%
Z-Score (Absolute) NA 1.32 0.67 0.00
Analytical results for Hf in OREAS 605 (Certified Value 0.55 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 17
40g 20g 01g 0.5g 01g 0.25g
1 1 0.74 0.68 0.56 0.50 0.70 0.43
1 2 0.71 0.63 0.58 0.51 0.67 0.49
1 3 0.76 0.59 0.56 0.52 0.56 0.34
1 4 0.76 0.67 0.56 0.51 0.61 0.50
1 5 0.71 0.65 0.57 0.51 0.60 0.48
1 6 0.73 0.61 0.56 0.51 0.60 0.42
Mean 0.74 0.64 0.57 0.51 0.62 0.44
Median 0.74 0.64 0.56 0.51 0.61 0.45
Std Dev. 0.023 0.037 0.006 0.006 0.052 0.060
Rel.Std.Dev. 3.07% 5.75% 1.06% 1.24% 8.28% 13.58%
PDM3 34.10% 16.25% 3.17% -6.95% 13.72% -19.12%
Z-Score (Absolute) 1.48 0.75 0.21 0.21 0.64 0.71
Analytical results for Hg in OREAS 605 (Certified Value < 4 ppm)

Hg Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 06 07 08 09 11
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES
01g 01g 01g 01g 20g 0.15g
1 1 1.00 3.00 2.00 1.00 1.76 2.00
1 2 1.00 3.00 2.00 1.00 1.79 2.00
1 3 2.00 2.00 1.00 2.00 1.65 2.00
1 4 1.00 2.00 2.00 2.00 1.74 2.00
1 5 1.00 2.00 2.00 1.00 1.71 2.00
1 6 1.00 2.00 2.00 1.00 1.76 2.00
Mean 1.17 2.33 1.83 1.33 1.74 2.00
Median 1.00 2.00 2.00 1.00 1.75 2.00
Std Dev. 0.408 0.516 0.408 0.516 0.051 0.000
Rel.Std.Dev. 34.99% 22.13% 22.27% 38.73% 2.96% 0.00%
PDM3
Z-Score (Absolute) 1.69 1.28 0.00 1.27 0.24 0.43
Analytical results for Ho in OREAS 605 (Certified Value 73 ppb)

Ho Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
40g 20g 01g 0.5g 01g 40g
1 1 80 83 82 70 < 100 60
1 2 80 75 74 70 < 100 50
1 3 80 77 78 70 < 100 45
1 4 80 77 83 70 < 100 50
1 5 80 80 72 70 100 50
1 6 80 72 79 70 < 100 60
Mean 80 77 78 70 100 53
Median 80 77 78 70 100 50
Std Dev. 0 4 4 0 6
Rel.Std.Dev. 0.00% 4.90% 5.46% 0.00% 11.66%
PDM3 10.01% 6.24% 7.28% -3.74% 37.51% -27.81%
Z-Score (Absolute) 0.80 0.46 0.55 0.46 1.92 2.65
Analytical results for In in OREAS 605 (Certified Value 3.75 ppm)

In Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 13 14
AR*OES AR*MS AR*OES/MS AR*OES AR*MS AR*MS
0.5g 40g 20g 0.15g 01g 0.5g
1 1 <5 3.43 3.74 < 10 4.51 3.81
1 2 <5 3.24 3.88 < 10 4.45 3.76
1 3 <5 3.23 3.89 < 10 4.40 3.81
1 4 <5 3.33 3.81 < 10 4.65 3.86
1 5 <5 3.35 3.79 < 10 4.58 3.78
1 6 <5 3.38 3.92 < 10 4.49 3.86
Mean 3.33 3.84 4.52 3.81
Median 3.34 3.85 4.50 3.81
Std Dev. 0.079 0.070 0.089 0.041
Rel.Std.Dev. 2.36% 1.82% 1.97% 1.07%
PDM3 -11.23% 2.43% 20.48% 1.75%
Z-Score (Absolute) NA 0.67 0.03 NA 0.96 0.00
Analytical results for K in OREAS 605 (Certified Value 0.134 wt.%)

K Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 0.160 0.181 0.130 0.120 0.130 0.130
1 2 0.160 0.181 0.140 0.130 0.130 0.130
1 3 0.170 0.181 0.140 0.130 0.130 0.120
1 4 0.170 0.179 0.140 0.130 0.130 0.120
1 5 0.170 0.173 0.140 0.120 0.130 0.120
1 6 0.170 0.168 0.140 0.120 0.130 0.120
Mean 0.167 0.177 0.138 0.125 0.130 0.123
Median 0.170 0.180 0.140 0.125 0.130 0.120
Std Dev. 0.005 0.006 0.004 0.005 0.000 0.005
Rel.Std.Dev. 3.10% 3.13% 2.95% 4.38% 0.00% 4.19%
PDM3 24.64% 32.60% 3.45% -6.52% -2.78% -7.76%
Z-Score (Absolute) 1.39 1.81 0.29 0.23 0.03 0.29
Analytical results for La in OREAS 605 (Certified Value 3.95 ppm)

La Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 2.48 7.13 < 10 < 10 < 10 < 10
1 2 2.92 7.07 < 10 < 10 < 10 < 10
1 3 2.96 7.06 < 10 < 10 < 10 < 10
1 4 3.00 7.01 < 10 < 10 < 10 < 10
1 5 2.95 7.03 < 10 < 10 < 10 < 10
1 6 3.07 7.10 < 10 < 10 < 10 < 10
Mean 2.90 7.07
Median 2.96 7.06
Std Dev. 0.211 0.044
Rel.Std.Dev. 7.30% 0.62%
PDM3 -26.77% 78.68%
Z-Score (Absolute) 1.13 3.39 NA NA NA NA
Analytical results for Li in OREAS 605 (Certified Value 5.17 ppm)

Li Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 13 14
AR*OES AR*MS AR*OES/MS AR*OES AR*OES AR*OES
0.5g 40g 20g 0.15g 01g 0.5g
1 1 6.66 4.90 6.95 <5 4.38 5.00
1 2 6.73 4.90 7.11 5.00 4.49 5.00
1 3 6.75 4.80 6.38 <5 4.77 5.00
1 4 6.79 5.20 7.01 5.00 4.62 5.00
1 5 6.70 5.10 6.87 5.00 4.71 5.00
1 6 6.76 4.80 6.30 5.00 4.55 5.00
Mean 6.73 4.95 6.77 5.00 4.59 5.00
Median 6.74 4.90 6.91 5.00 4.59 5.00
Std Dev. 0.049 0.164 0.342 0.000 0.145 0.000
Rel.Std.Dev. 0.73% 3.32% 5.05% 0.00% 3.16% 0.00%
PDM3 30.23% -4.24% 30.99% -3.27% -11.25% -3.27%
Z-Score (Absolute) 1.75 0.05 1.79 0.00 0.42 0.00
Analytical results for Lu in OREAS 605 (Certified Value 11 ppb)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 14 15 17 19
AR*MS AR*OES/MS AR*MS AR*OES/MSAR*OES/MSAR*OES/MS
40g 20g 0.5g 01g 0.25g 0.25g
1 1 20 12 12 < 100 10 16
1 2 20 10 13 < 100 10 13
1 3 20 10 13 < 100 20 13
1 4 20 9 12 < 100 10 13
1 5 20 14 13 < 100 10 12
1 6 20 11 13 < 100 10 13
Mean 20 11 13 12 13
Median 20 11 13 10 13
Std Dev. 0 2 1 4 1
Rel.Std.Dev. 0.00% 16.34% 4.08% 34.99% 10.25%
PDM3 76.51% -1.27% 11.79% 2.96% 17.67%
Z-Score (Absolute) 3.89 0.36 0.36 NA 0.93 0.42
Analytical results for Mg in OREAS 605 (Certified Value 289 ppm)

Mg Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 300 300 300 300 300 300
1 2 267 300 300 300 300 200
1 3 300 300 300 300 300 200
1 4 300 300 300 300 300 200
1 5 300 300 300 200 300 300
1 6 300 300 300 200 300 200
Mean 294 300 300 267 300 233
Median 300 300 300 300 300 200
Std Dev. 14 0 0 52 0 52
Rel.Std.Dev. 4.62% 0.00% 0.00% 19.36% 0.00% 22.13%
PDM3 1.78% 3.70% 3.70% -7.82% 3.70% -19.34%
Z-Score (Absolute) 0.00 0.00 0.00 2.08 0.00 4.17
Analytical results for Mn in OREAS 605 (Certified Value 86 ppm)

Mn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 81 85 80 86 88 84
1 2 84 85 83 88 86 81
1 3 81 87 84 89 85 84
1 4 85 85 85 88 84 83
1 5 82 83 83 81 84 88
1 6 82 85 84 81 86 81
Mean 83 85 83 86 86 84
Median 82 85 84 87 86 84
Std Dev. 1.7 1.3 1.7 3.6 1.5 2.6
Rel.Std.Dev. 2.03% 1.49% 2.07% 4.23% 1.77% 3.10%
PDM3 -3.53% -0.81% -2.95% -0.23% -0.23% -2.56%
Z-Score (Absolute) 0.69 0.12 0.57 0.00 0.00 0.49
Analytical results for Mo in OREAS 605 (Certified Value 4.75 ppm)

Mo Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 4.51 4.50 5.00 8.00 5.00 5.00
1 2 4.78 4.60 5.00 7.00 5.00 5.00
1 3 4.50 4.60 5.00 7.00 4.00 5.00
1 4 4.59 4.40 5.00 8.00 4.00 5.00
1 5 4.68 4.10 5.00 7.00 4.00 5.00
1 6 4.52 4.20 5.00 7.00 4.00 5.00
Mean 4.60 4.40 5.00 7.33 4.33 5.00
Median 4.56 4.45 5.00 7.00 4.00 5.00
Std Dev. 0.112 0.210 0.000 0.516 0.516 0.000
Rel.Std.Dev. 2.43% 4.77% 0.00% 7.04% 11.92% 0.00%
PDM3 -3.27% -7.39% 5.24% 54.35% -8.79% 5.24%
Z-Score (Absolute) 0.78 1.49 0.67 9.07 1.73 0.67
Analytical results for Na in OREAS 605 (Certified Value 328 ppm)

Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 233 300 200 400 300 300
1 2 233 300 200 400 300 300
1 3 233 300 200 400 300 300
1 4 233 300 200 400 300 300
1 5 233 300 200 400 300 300
1 6 233 300 200 400 300 300
Mean 233 300 200 400 300 300
Median 233 300 200 400 300 300
Std Dev. 0 0 0 0 0 0
Rel.Std.Dev. 0.00% 0.00% 0.00% 0.00% 0.00% 0.00%
PDM3 -28.90% -8.58% -39.06% 21.89% -8.58% -8.58%
Z-Score (Absolute) 0.67 0.00 1.01 1.01 0.00 0.00
Analytical results for Nb in OREAS 605 (Certified Value 0.45 ppm)

Nb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 14 15
AR*OES AR*MS AR*OES/MS AR*OES AR*MS AR*OES/MS
0.5g 40g 20g 0.15g 0.5g 01g
1 1 <5 0.46 0.48 < 10 0.44 0.84
1 2 <5 0.45 0.52 < 10 0.44 0.78
1 3 <5 0.52 0.45 < 10 0.45 0.86
1 4 <5 0.48 0.50 < 10 0.44 0.71
1 5 <5 0.50 0.52 < 10 0.44 0.83
1 6 <5 0.48 0.46 < 10 0.47 0.84
Mean 0.48 0.49 0.45 0.81
Median 0.48 0.49 0.44 0.84
Std Dev. 0.026 0.030 0.012 0.056
Rel.Std.Dev. 5.32% 6.18% 2.71% 6.90%
PDM3 7.35% 8.80% -0.45% 80.52%
Analytical results for Nd in OREAS 605 (Certified Value 6.1 ppm)

Nd Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
40g 20g 01g 0.5g 01g 40g
1 1 6.61 7.42 5.26 6.00 7.27 4.63
1 2 6.47 7.77 5.11 5.83 7.20 4.02
1 3 6.68 7.27 5.27 5.87 6.86 4.07
1 4 6.62 7.69 5.67 5.89 7.12 4.15
1 5 6.61 7.81 5.45 5.86 7.27 4.30
1 6 6.45 7.46 5.26 5.85 6.62 4.35
Mean 6.57 7.57 5.34 5.88 7.06 4.25
Median 6.61 7.58 5.27 5.87 7.16 4.23
Std Dev. 0.092 0.216 0.196 0.061 0.263 0.225
Rel.Std.Dev. 1.40% 2.86% 3.66% 1.03% 3.72% 5.28%
PDM3 7.74% 24.06% -12.52% -3.57% 15.66% -30.28%
Z-Score (Absolute) 0.26 1.01 0.72 0.26 0.63 1.49
Analytical results for Ni in OREAS 605 (Certified Value 1538 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 1552 1521 1540 1610 1590 1600
1 2 1583 1512 1590 1600 1600 1560
1 3 1570 1524 1600 1630 1590 1540
1 4 1539 1509 1570 1590 1560 1560
1 5 1568 1526 1570 1510 1560 1550
1 6 1571 1512 1580 1530 1590 1530
Mean 1564 1517 1575 1578 1582 1557
Median 1569 1516 1575 1595 1590 1555
Std Dev. 16 7 21 48 17 24
Rel.Std.Dev. 1.01% 0.48% 1.32% 3.01% 1.09% 1.56%
PDM3 1.67% -1.37% 2.38% 2.60% 2.82% 1.19%
Z-Score (Absolute) 0.40 0.33 0.57 0.62 0.67 0.29
Analytical results for P in OREAS 605 (Certified Value 116 ppm)

P Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 122 1222 100 100 100 100
1 2 121 1699 110 100 100 100
1 3 118 1050 100 100 110 100
1 4 119 946 110 100 100 100
1 5 120 1410 100 90 100 100
1 6 119 1661 100 90 110 100
Mean 120 1331 103 97 103 100
Median 119 1316 100 100 100 100
Std Dev. 1 313 5 5 5 0
Rel.Std.Dev. 1.23% 23.51% 5.00% 5.34% 5.00% 0.00%
PDM3 3.49% 1050.55% -10.70% -16.46% -10.70% -13.58%
Z-Score (Absolute) 0.00 42.45 0.58 0.81 0.58 0.69
Analytical results for Pb in OREAS 605 (Certified Value 856 ppm)

Pb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 804 842 856 848 852 864
1 2 807 825 868 853 857 853
1 3 804 846 861 855 849 827
1 4 814 844 862 856 835 838
1 5 815 870 857 801 836 841
1 6 810 867 865 807 850 825
Mean 809 849 862 837 847 841
Median 808 845 862 851 850 840
Std Dev. 5 17 5 26 9 15
Rel.Std.Dev. 0.60% 1.98% 0.53% 3.05% 1.06% 1.79%
PDM3 -5.48% -0.82% 0.65% -2.25% -1.11% -1.71%
Z-Score (Absolute) 1.14 0.10 0.49 0.28 0.02 0.14
Analytical results for Pd in OREAS 605 (Indicative Value 11.83 ppm)

Pd Round Replicate Lab Lab Lab
No No 09 14 25
AR*OES/MS AR*MS AR*MS
20g 0.5g 40g
1 1 11.67 12.70 11.40
1 2 12.05 12.53 11.10
1 3 11.78 12.66 10.90
1 4 11.62 12.55 11.00
1 5 11.74 12.50 11.00
1 6 12.03 12.67 11.10
Mean 11.82 12.60 11.08
Median 11.76 12.60 11.05
Std Dev. 0.182 0.082 0.172
Rel.Std.Dev. 1.54% 0.65% 1.55%
PDM3 -0.15% 6.49% -6.34%
Z-Score (Absolute) 0.00 0.72 0.67
Analytical results for Pr in OREAS 605 (Certified Value 1.74 ppm)

Pr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
40g 20g 01g 0.5g 01g 40g
1 1 1.87 1.92 1.46 1.50 2.00 1.01
1 2 1.80 1.99 1.51 1.48 1.96 0.87
1 3 1.87 1.83 1.40 1.47 2.02 0.87
1 4 1.89 1.92 1.44 1.45 1.94 0.91
1 5 1.82 2.03 1.47 1.47 2.10 0.95
1 6 1.82 1.75 1.36 1.53 2.04 0.96
Mean 1.85 1.91 1.44 1.48 2.01 0.93
Median 1.85 1.92 1.45 1.48 2.01 0.93
Std Dev. 0.036 0.102 0.052 0.028 0.058 0.054
Rel.Std.Dev. 1.96% 5.34% 3.64% 1.89% 2.87% 5.87%
PDM3 6.20% 9.82% -17.09% -14.62% 15.70% -46.66%
Z-Score (Absolute) 0.52 0.70 0.65 0.52 1.00 2.13
Analytical results for Pt in OREAS 605 (Indicative Value 2.22 ppm)

Pt Round Replicate Lab Lab Lab
No No 09 14 25
20g 0.5g 40g
1 1 2.18 2.20 2.30
1 2 2.35 2.19 2.23
1 3 2.13 2.17 2.21
1 4 2.25 2.19 2.23
1 5 2.28 2.19 2.24
1 6 2.17 2.22 2.27
Mean 2.23 2.19 2.25
Median 2.22 2.19 2.24
Std Dev. 0.080 0.015 0.033
Rel.Std.Dev. 3.58% 0.68% 1.45%
PDM3 0.26% -1.34% 1.08%
Z-Score (Absolute) 0.00 1.31 0.67
Analytical results for Rb in OREAS 605 (Certified Value 5.75 ppm)

Rb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 17
40g 20g 01g 0.5g 01g 0.25g
1 1 5.98 6.41 5.24 5.11 7.47 5.60
1 2 5.88 6.41 5.54 4.88 7.48 6.90
1 3 5.70 6.03 5.20 4.89 7.22 7.70
1 4 6.10 6.32 5.39 4.92 7.30 5.90
1 5 5.96 6.65 5.63 4.95 7.38 6.30
1 6 5.71 5.99 5.15 5.04 7.39 6.00
Mean 5.89 6.30 5.36 4.96 7.37 6.40
Median 5.92 6.36 5.31 4.94 7.39 6.15
Std Dev. 0.159 0.251 0.197 0.091 0.100 0.775
Rel.Std.Dev. 2.69% 3.98% 3.67% 1.84% 1.36% 12.10%
PDM3 2.44% 9.66% -6.79% -13.62% 28.28% 11.35%
Z-Score (Absolute) 0.00 0.53 0.67 1.17 1.89 0.65
Analytical results for Re in OREAS 605 (Indicative Value 1 ppb)

Re Round Replicate Lab Lab Lab Lab Lab
No No 02 09 11 14 15
AR*MS AR*OES/MS AR*OES AR*MS AR*OES/MS
40g 20g 0.15g 0.5g 01g
1 1 1 <1 < 5000 2 10
1 2 2 <1 < 5000 2 < 10
1 3 2 <1 < 5000 1 10
1 4 1 <1 < 5000 1 10
1 5 1 <1 < 5000 1 10
1 6 2 <1 < 5000 1 < 10
Mean 2 1 10
Median 2 1 10
Std Dev. 1 1 0
Rel.Std.Dev. 36.51% 38.73% 0.00%
PDM3 5.88% -5.88% 605.88%
Z-Score (Absolute) 0.00 NA NA 0.67 27.65
Analytical results for Ru in OREAS 605 (Indicative Value < 2 ppb)

Ru Round Replicate Lab
No No 14
AR*MS
0.5g
1 1 <2
1 2 <2
1 3 <2
1 4 <2
1 5 <2
1 6 <2
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA
Analytical results for S in OREAS 605 (Certified Value 7.86 wt.%)

S Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 8.14 6.85 8.50 8.23 8.46 8.08
1 2 8.12 6.86 8.60 8.22 8.51 7.96
1 3 8.23 6.83 8.48 8.24 8.42 7.85
1 4 8.27 6.54 8.53 8.21 8.29 7.95
1 5 8.24 6.99 8.41 7.72 8.29 7.87
1 6 8.23 6.83 8.44 7.87 8.41 7.69
Mean 8.21 6.82 8.49 8.08 8.40 7.90
Median 8.23 6.84 8.49 8.22 8.42 7.91
Std Dev. 0.060 0.149 0.067 0.227 0.090 0.131
Rel.Std.Dev. 0.73% 2.18% 0.79% 2.81% 1.07% 1.66%
PDM3 4.38% -13.29% 8.04% 2.80% 6.81% 0.49%
Z-Score (Absolute) 0.56 2.00 1.11 0.46 0.93 0.03
Analytical results for Sb in OREAS 605 (Certified Value 228 ppm)

Sb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 180 206 268 238 275 300
1 2 179 206 269 239 280 293
1 3 181 200 266 239 280 293
1 4 181 198 265 239 276 294
1 5 179 208 270 229 270 295
1 6 181 205 269 233 272 285
Mean 180 204 268 236 276 293
Median 180 205 269 239 276 294
Std Dev. 1 4 2 4 4 5
Rel.Std.Dev. 0.47% 1.97% 0.72% 1.78% 1.48% 1.65%
PDM3 -21.13% -10.75% 17.33% 3.46% 20.69% 28.50%
Z-Score (Absolute) 1.22 0.78 0.43 0.14 0.57 0.91
Analytical results for Sc in OREAS 605 (Certified Value 1.05 ppm)

Sc Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 1.04 1.00 1.00 1.00 1.00 1.00
1 2 1.06 0.90 1.00 1.00 1.00 1.00
1 3 1.06 0.90 1.00 1.00 1.00 1.00
1 4 1.06 1.00 1.00 1.00 1.00 1.00
1 5 1.06 1.00 1.00 1.00 1.00 1.00
1 6 1.05 0.90 1.00 1.00 1.00 1.00
Mean 1.05 0.95 1.00 1.00 1.00 1.00
Median 1.06 0.95 1.00 1.00 1.00 1.00
Std Dev. 0.010 0.055 0.000 0.000 0.000 0.000
Rel.Std.Dev. 0.90% 5.77% 0.00% 0.00% 0.00% 0.00%
PDM3 0.83% -9.10% -4.32% -4.32% -4.32% -4.32%
Z-Score (Absolute) 1.45 1.35 0.00 0.00 0.00 0.00
Analytical results for Se in OREAS 605 (Certified Value 75 ppm)

Se Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 14 15
0.5g 40g 20g 0.15g 0.5g 01g
1 1 87 67 78 72 72 91
1 2 86 66 80 74 72 88
1 3 88 64 76 73 73 90
1 4 87 67 78 74 72 89
1 5 87 64 82 76 73 89
1 6 86 66 73 72 72 88
Mean 87 66 78 74 72 89
Median 87 66 78 74 72 89
Std Dev. 1 1 3 2 0 1
Rel.Std.Dev. 0.75% 2.08% 4.19% 2.06% 0.67% 1.34%
PDM3 15.86% -12.61% 3.36% -2.19% -4.08% 18.63%
Z-Score (Absolute) 0.87 0.75 0.16 0.16 0.27 1.03
Analytical results for Sm in OREAS 605 (Certified Value 1.16 ppm)

Sm Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 25
40g 20g 01g 0.5g 01g 40g
1 1 1.26 1.37 1.05 1.07 1.29 0.93
1 2 1.23 1.45 1.00 1.06 1.46 0.80
1 3 1.25 1.31 1.09 1.02 1.53 0.81
1 4 1.23 1.45 1.08 1.05 1.30 0.86
1 5 1.24 1.41 1.08 1.05 1.32 0.85
1 6 1.24 1.20 1.09 1.08 1.27 0.90
Mean 1.24 1.37 1.07 1.06 1.36 0.86
Median 1.24 1.39 1.08 1.06 1.31 0.86
Std Dev. 0.012 0.096 0.035 0.021 0.107 0.050
Rel.Std.Dev. 0.94% 7.05% 3.31% 1.97% 7.85% 5.87%
PDM3 7.03% 17.75% -8.19% -9.06% 17.37% -26.01%
Z-Score (Absolute) 0.36 0.91 0.36 0.46 0.89 1.33
Analytical results for Sn in OREAS 605 (Certified Value 1.92 ppm)

Sn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 14 15
0.5g 40g 20g 0.15g 0.5g 01g
1 1 <5 1.77 2.06 < 10 2.10 2.41
1 2 <5 1.67 2.15 < 10 2.10 2.19
1 3 <5 1.74 1.93 < 10 2.10 2.25
1 4 <5 1.73 2.03 < 10 2.10 2.29
1 5 <5 1.71 2.05 < 10 2.10 2.39
1 6 <5 1.69 1.97 < 10 2.10 2.26
Mean 1.72 2.03 2.10 2.30
Median 1.72 2.04 2.10 2.28
Std Dev. 0.036 0.077 0.000 0.085
Rel.Std.Dev. 2.10% 3.77% 0.00% 3.72%
PDM3 -10.43% 5.91% 9.47% 19.80%
Analytical results for Sr in OREAS 605 (Certified Value 28.1 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 22.7 45.5 34.0 29.0 28.0 35.0
1 2 22.5 44.1 34.0 30.0 29.0 34.0
1 3 23.1 42.9 34.0 32.0 29.0 31.0
1 4 23.7 45.5 33.0 32.0 28.0 34.0
1 5 23.7 43.9 33.0 31.0 28.0 34.0
1 6 23.6 40.8 34.0 30.0 29.0 29.0
Mean 23.2 43.8 33.7 30.7 28.5 32.8
Median 23.3 44.0 34.0 30.5 28.5 34.0
Std Dev. 0.5 1.8 0.5 1.2 0.5 2.3
Rel.Std.Dev. 2.34% 4.10% 1.53% 3.95% 1.92% 7.06%
PDM3 -17.33% 56.04% 19.96% 9.27% 1.55% 16.99%
Z-Score (Absolute) 0.69 1.98 0.67 0.28 0.00 0.56
Analytical results for Ta in OREAS 605 (Indicative Value < 0.01 ppm)
Ta Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 14 15 17 19
AR*MS AR*OES/MS AR*MS AR*OES/MSAR*OES/MSAR*OES/MS
40g 20g 0.5g 01g 0.25g 0.25g
1 1 0.090 < 0.01 < 0.01 < 0.1 0.080 < 0.05
1 2 0.090 < 0.01 < 0.01 < 0.1 0.090 < 0.05
1 3 0.080 < 0.01 < 0.01 < 0.1 0.140 < 0.05
1 4 0.090 < 0.01 < 0.01 < 0.1 0.140 < 0.05
1 5 0.090 < 0.01 < 0.01 < 0.1 0.090 < 0.05
1 6 0.090 < 0.01 < 0.01 < 0.1 0.090 < 0.05
Mean 0.088 0.105
Median 0.090 0.090
Std Dev. 0.004 0.027
Rel.Std.Dev. 4.62% 26.08%
PDM3
Analytical results for Tb in OREAS 605 (Certified Value 0.11 ppm)

Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 17
40g 20g 01g 0.5g 01g 0.25g
1 1 0.12 0.14 0.11 0.11 0.12 0.08
1 2 0.12 0.15 0.11 0.11 0.13 0.08
1 3 0.13 0.13 0.11 0.11 0.14 0.09
1 4 0.13 0.14 0.11 0.11 0.18 0.09
1 5 0.12 0.15 0.12 0.11 0.12 0.07
1 6 0.12 0.12 0.10 0.12 0.15 0.07
Mean 0.12 0.14 0.11 0.11 0.14 0.08
Median 0.12 0.14 0.11 0.11 0.14 0.08
Std Dev. 0.005 0.010 0.006 0.004 0.023 0.009
Rel.Std.Dev. 4.19% 6.92% 5.42% 3.25% 16.29% 11.18%
PDM3 13.74% 27.54% 1.01% 0.98% 29.11% -26.22%
Z-Score (Absolute) 0.50 1.04 0.00 0.00 0.82 1.07
Analytical results for Te in OREAS 605 (Certified Value 33.1 ppm)

Te Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 14 15 17
AR*MS AR*OES/MS AR*OES AR*MS AR*OES AR*OES/MS
40g 20g 0.15g 0.5g 01g 0.25g
1 1 33.7 29.8 29.0 33.0 41.0 22.8
1 2 33.4 31.1 31.0 32.9 36.0 23.2
1 3 32.9 30.3 32.0 33.0 40.0 30.8
1 4 32.1 29.9 30.0 33.0 40.0 21.6
1 5 34.1 29.9 30.0 32.5 36.0 21.4
1 6 33.9 31.0 31.0 33.4 35.0 20.3
Mean 33.3 30.3 30.5 33.0 38.0 23.4
Median 33.5 30.1 30.5 33.0 38.0 22.2
Std Dev. 0.711 0.571 1.049 0.291 2.608 3.795
Rel.Std.Dev. 2.13% 1.88% 3.44% 0.88% 6.86% 16.25%
PDM3 0.79% -8.34% -7.81% -0.35% 14.86% -29.42%
Z-Score (Absolute) 0.12 1.31 1.23 0.06 2.33 5.32
Analytical results for Th in OREAS 605 (Certified Value < 3 ppm)

Th Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 05 06 07 08 09
AR*MS AR*OES AR*OES AR*OES AR*OES AR*OES/MS
40g 01g 01g 01g 01g 20g
1 1 2.82 < 20 < 20 < 20 < 20 2.16
1 2 2.76 < 20 < 20 < 20 < 20 2.15
1 3 2.76 < 20 < 20 < 20 < 20 2.04
1 4 2.86 < 20 < 20 < 20 < 20 2.10
1 5 2.85 < 20 < 20 < 20 < 20 2.11
1 6 2.95 < 20 < 20 < 20 < 20 1.91
Mean 2.83 2.08
Median 2.84 2.11
Std Dev. 0.071 0.090
Rel.Std.Dev. 2.52% 4.34%
PDM3
Z-Score (Absolute) 1.73 NA NA NA NA 0.42
Analytical results for Ti in OREAS 605 (Certified Value 100 ppm)

Ti Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 105 116 100 100 100 100
1 2 105 115 100 100 100 100
1 3 105 114 100 100 100 100
1 4 105 112 100 100 100 100
1 5 105 111 100 100 100 100
1 6 105 109 100 100 100 100
Mean 105 113 100 100 100 100
Median 105 113 100 100 100 100
Std Dev. 0 3 0 0 0 0
Rel.Std.Dev. 0.00% 2.34% 0.00% 0.00% 0.00% 0.00%
PDM3 4.97% 12.80% -0.03% -0.03% -0.03% -0.03%
Analytical results for Tl in OREAS 605 (Certified Value 15.3 ppm)

Tl Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
AR*OES AR*MS AR*OES/MS AR*OES AR*OES AR*MS
0.5g 40g 20g 0.15g 0.5g 01g
1 1 10.3 17.5 14.8 15.0 12.0 11.1
1 2 9.7 17.2 15.4 15.0 13.0 10.9
1 3 10.0 17.8 13.9 16.0 12.0 11.3
1 4 9.5 17.7 14.5 16.0 14.0 10.6
1 5 9.7 16.8 14.3 16.0 13.0 11.1
1 6 9.5 17.4 14.1 16.0 16.0 10.7
Mean 9.8 17.4 14.5 15.7 13.3 11.0
Median 9.7 17.4 14.4 16.0 13.0 11.0
Std Dev. 0.3 0.4 0.5 0.5 1.5 0.3
Rel.Std.Dev. 3.21% 2.04% 3.78% 3.30% 11.29% 2.38%
PDM3 -35.92% 14.04% -4.75% 2.71% -12.59% -28.21%
Z-Score (Absolute) 4.19 2.30 0.11 0.85 1.11 3.11
Analytical results for Tm in OREAS 605 (Indicative Value 0.018 ppm)

Tm Round Replicate Lab Lab Lab Lab Lab
No No 02 09 14 15 25
40g 20g 0.5g 01g 40g
1 1 0.020 0.017 0.020 < 0.1 0.015
1 2 0.020 0.021 0.020 < 0.1 0.015
1 3 0.020 0.017 0.020 < 0.1 0.015
1 4 0.020 0.014 0.020 < 0.1 0.015
1 5 0.020 0.016 0.020 < 0.1 0.015
1 6 0.020 0.015 0.020 < 0.1 0.015
Mean 0.020 0.017 0.020 0.015
Median 0.020 0.016 0.020 0.015
Std Dev. 0.000 0.002 0.000 0.000
Rel.Std.Dev. 0.00% 13.95% 0.00% 0.00%
PDM3 11.60% -6.90% 11.60% -16.30%
Z-Score (Absolute) 0.67 0.67 0.67 NA 1.36
Analytical results for U in OREAS 605 (Certified Value 0.95 ppm)

U Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 05 07 08 09 11
AR*MS AR*OES AR*OES AR*OES AR*OES/MS AR*OES
40g 01g 01g 01g 20g 0.15g
1 1 1.14 < 10 < 10 < 10 1.03 < 10
1 2 1.12 < 10 < 10 < 10 1.04 < 10
1 3 1.15 < 10 < 10 < 10 0.92 < 10
1 4 1.17 < 10 < 10 < 10 0.97 < 10
1 5 1.10 < 10 < 10 < 10 0.96 < 10
1 6 1.11 < 10 < 10 < 10 0.89 < 10
Mean 1.13 0.97
Median 1.13 0.96
Std Dev. 0.026 0.061
Rel.Std.Dev. 2.33% 6.26%
PDM3 19.29% 2.00%
Z-Score (Absolute) 1.14 NA NA NA 0.02 NA
Analytical results for V in OREAS 605 (Certified Value 8.33 ppm)

V Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 10.63 10.00 9.00 8.00 8.00 8.00
1 2 10.47 10.00 10.00 8.00 8.00 7.00
1 3 10.90 10.00 9.00 8.00 8.00 7.00
1 4 10.94 9.00 9.00 8.00 8.00 7.00
1 5 10.89 9.00 10.00 8.00 8.00 7.00
1 6 10.85 9.00 10.00 7.00 8.00 7.00
Mean 10.78 9.50 9.50 7.83 8.00 7.17
Median 10.87 9.50 9.50 8.00 8.00 7.00
Std Dev. 0.186 0.548 0.548 0.408 0.000 0.408
Rel.Std.Dev. 1.72% 5.77% 5.77% 5.21% 0.00% 5.70%
PDM3 29.42% 14.05% 14.05% -5.96% -3.96% -13.96%
Z-Score (Absolute) 1.97 0.98 0.98 0.31 0.19 0.83
Analytical results for W in OREAS 605 (Certified Value 5.9 ppm)

W Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 <5 6.59 < 10 < 10 < 10 10.00
1 2 <5 7.26 < 10 < 10 < 10 10.00
1 3 <5 7.10 < 10 < 10 < 10 10.00
1 4 <5 7.17 < 10 < 10 < 10 10.00
1 5 <5 7.84 < 10 < 10 < 10 10.00
1 6 <5 7.46 < 10 < 10 < 10 10.00
Mean 7.24 10.00
Median 7.22 10.00
Std Dev. 0.414 0.000
Rel.Std.Dev. 5.72% 0.00%
PDM3 22.74% 69.61%
Z-Score (Absolute) NA 0.52 NA NA NA 2.56
Analytical results for Y in OREAS 605 (Certified Value 1.91 ppm)

Y Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 13 14
AR*OES AR*MS AR*OES/MS AR*OES AR*MS AR*OES
0.5g 40g 20g 0.15g 01g 0.5g
1 1 2.39 1.73 2.05 2.00 2.58 2.00
1 2 2.39 1.69 2.02 2.00 2.21 2.00
1 3 2.39 1.68 2.08 2.00 2.35 2.00
1 4 2.49 1.79 2.01 2.00 2.37 2.00
1 5 2.48 1.78 2.00 2.00 2.36 2.00
1 6 2.44 1.70 1.82 2.00 2.28 2.00
Mean 2.43 1.73 2.00 2.00 2.36 2.00
Median 2.42 1.71 2.01 2.00 2.35 2.00
Std Dev. 0.046 0.047 0.092 0.000 0.125 0.000
Rel.Std.Dev. 1.90% 2.72% 4.59% 0.00% 5.28% 0.00%
PDM3 27.40% -9.36% 4.70% 4.88% 23.65% 4.88%
Z-Score (Absolute) 1.18 0.74 0.09 0.00 0.98 0.00
Analytical results for Yb in OREAS 605 (Certified Value 0.099 ppm)

Yb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 14 15 19
40g 20g 01g 0.5g 01g 0.25g
1 1 0.110 0.107 0.114 0.100 < 0.1 < 0.1
1 2 0.110 0.118 0.110 0.100 < 0.1 < 0.1
1 3 0.100 0.099 0.117 0.100 < 0.1 < 0.1
1 4 0.110 0.114 0.115 0.100 < 0.1 < 0.1
1 5 0.120 0.106 0.108 0.100 < 0.1 < 0.1
1 6 0.100 0.092 0.111 0.100 < 0.1 < 0.1
Mean 0.108 0.106 0.112 0.100
Median 0.110 0.107 0.112 0.100
Std Dev. 0.008 0.009 0.003 0.000
Rel.Std.Dev. 6.95% 8.88% 2.95% 0.00%
PDM3 9.44% 7.07% 13.44% 1.02%
Z-Score (Absolute) 0.26 0.00 0.71 0.67 NA NA
Analytical results for Zn in OREAS 605 (Certified Value 0.217 wt.%)

Zn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
0.5g 40g 01g 01g 01g 01g
1 1 0.226 0.220 0.217 0.221 0.225 0.223
1 2 0.228 0.223 0.223 0.218 0.226 0.219
1 3 0.229 0.220 0.224 0.225 0.222 0.214
1 4 0.233 0.217 0.221 0.219 0.221 0.217
1 5 0.227 0.212 0.220 0.207 0.220 0.217
1 6 0.232 0.217 0.221 0.208 0.222 0.212
Mean 0.229 0.218 0.221 0.216 0.223 0.217
Median 0.229 0.219 0.221 0.219 0.222 0.217
Std Dev. 0.003 0.004 0.002 0.007 0.002 0.004
Rel.Std.Dev. 1.22% 1.81% 1.11% 3.35% 1.05% 1.77%
PDM3 5.76% 0.72% 1.99% -0.16% 2.76% 0.14%
Z-Score (Absolute) 1.24 0.00 0.31 0.22 0.50 0.14
Analytical results for Zr in OREAS 605 (Certified Value 19 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
AR*OES AR*MS AR*OES/MS AR*OES AR*OES AR*OES
0.5g 40g 20g 0.15g 0.5g 01g
1 1 21.8 18.4 20.9 16.0 21.0 20.9
1 2 21.9 18.2 21.2 17.0 20.0 20.8
1 3 21.9 17.4 19.4 17.0 20.0 20.7
1 4 21.8 17.8 21.1 17.0 19.0 20.3
1 5 21.9 18.4 21.5 17.0 19.0 20.8
1 6 22.0 18.0 20.7 16.0 20.0 20.1
Mean 21.9 18.0 20.8 16.7 19.8 20.6
Median 21.9 18.1 21.0 17.0 20.0 20.7
Std Dev. 0.1 0.4 0.7 0.5 0.8 0.3
Rel.Std.Dev. 0.34% 2.15% 3.48% 3.10% 3.80% 1.59%
PDM3 15.29% -4.95% 9.65% -12.16% 4.53% 8.56%
Z-Score (Absolute) 0.96 0.42 0.67 0.92 0.23 0.50
08 09 10 11 12 13 14 15 16
AR*OES/AAS
AR*OES/MS AR*OES AR*AAS AR*OES AR*MS AR*OES AR*OES AR*OES
0.5g 20g 01g 0.5g 0.5g 01g 0.5g 01g 10g
1000 1018 978 928 > 100 990 > 200 997 > 100
996 1053 934 960 > 100 989 > 200 1001 > 100
944 1042 1006 959 > 100 986 > 200 982 > 100
991 1022 963 940 > 100 1022 > 200 971 > 100
984 1026 946 927 > 100 992 > 200 986 > 100
997 1043 938 956 > 100 1015 > 200 973 > 100
985 1034 961 945 999 985
993 1034 955 948 991 984
21 14 28 15 15 12
2.13% 1.34% 2.87% 1.63% 1.53% 1.24%
0.17% 5.12% -2.32% -3.93% 1.56% 0.14%
0.35 1.69 0.73 1.26 NA 0.53 NA 0.07 NA

09 10 11 12 13 14 15 16 17
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
0.949 0.630 0.670 0.740 0.823 0.700 0.920 0.630 0.810
0.845 0.660 0.690 0.740 0.829 0.690 0.920 0.610 0.820
0.940 0.640 0.680 0.730 0.837 0.700 0.890 0.600 0.830
0.952 0.620 0.690 0.720 0.828 0.700 0.840 0.600 0.850
0.839 0.610 0.690 0.710 0.822 0.690 0.890 0.600 0.810
0.830 0.610 0.700 0.760 0.824 0.700 0.880 0.610 0.830
0.892 0.628 0.687 0.733 0.827 0.697 0.890 0.608 0.825
0.892 0.625 0.690 0.735 0.826 0.700 0.890 0.605 0.825
0.060 0.019 0.010 0.018 0.005 0.005 0.030 0.012 0.015
6.73% 3.09% 1.50% 2.39% 0.66% 0.74% 3.33% 1.92% 1.84%
22.25% -13.93% -5.94% 0.46% 13.34% -4.57% 21.92% -16.67% 13.01%
1.25 0.54 0.14 0.17 0.81 0.08 1.23 0.67 0.79

09 10 11 12 13 14 15 16 17
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES/MS
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
1614 1670 1618 1477 1842 1662 1737 1502 1100
1668 1660 1659 1482 1844 1669 1736 1539 1165
1636 1680 1625 1486 1891 1654 1710 1502 1596
1669 1660 1649 1453 1870 1665 1664 1482 1190
1623 1630 1645 1446 1925 1670 1700 1504 1060
1661 1640 1660 1455 1847 1678 1702 1535 980
1645 1657 1643 1467 1870 1666 1708 1511 1182
1648 1660 1647 1466 1859 1667 1706 1503 1133
24 19 18 17 33 8 27 22 216
1.46% 1.12% 1.07% 1.17% 1.76% 0.50% 1.58% 1.45% 18.31%
1.98% 2.70% 1.83% -9.09% 15.90% 3.30% 5.89% -6.35% -26.74%
0.12 0.21 0.10 1.24 1.83 0.28 0.60 0.90 4.04
Lab Lab Lab Lab Lab Lab Lab Lab

09 14 15 18 24 25 26 27
AR*OES/MS AR*MS AR*AAS AR*AAS AR*MS AR*MS AR*AAS AR*AAS
20g 25g 30g 50g 40g 40g 40g 40g
1.71 1.53 1.73 1.63 1.74 1.74 1.68 1.83
1.77 1.54 1.69 1.49 1.67 1.74 1.69 1.72
1.60 1.60 1.65 1.72 1.83 1.72 1.67 1.73
1.68 1.51 1.68 1.64 1.69 1.74 1.69 1.80
1.68 1.52 1.65 1.68 < 1.69 1.74 1.69 1.67
1.66 1.47 1.64 1.69 1.69 1.74 1.68 1.75
1.69 1.53 1.67 1.64 1.72 1.74 1.68 1.75

1.68 1.52 1.67 1.66 1.69 1.74 1.69 1.74
0.057 0.042 0.034 0.082 0.065 0.008 0.008 0.059
3.36% 2.78% 2.02% 5.02% 3.75% 0.47% 0.49% 3.34%
1.83% -7.75% 1.08% -1.02% 4.14% 4.91% 1.69% 5.76%
0.21 2.46 0.00 0.07 0.41 1.07 0.17 1.30
Lab Lab Lab Lab

18 19 21 23
AR*OES AR*OES/MS AR*OES AR*OES
10g 0.25g 0.25g 0.5g
< 10 25.1 11.0 < 20
< 10 24.6 12.0 < 20
< 10 25.3 10.0 < 20
< 10 24.2 < 10 < 20
< 10 24.0 < 10 < 20
< 10 23.7 < 10 < 20
24.5 11.0
24.4 11.0
0.7 1.0
2.66% 9.09%
NA NA NA NA

09 11 12 13 14 16 17 18 21
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES
20g 0.15g 0.5g 01g 0.5g 10g 0.25g 10g 0.25g
18.9 187.0 35.0 58.1 11.0 36.0 28.0 44.0 125.0
18.8 179.0 37.0 60.0 10.0 37.0 28.0 45.0 123.0
20.7 174.0 30.0 59.0 11.0 44.0 31.0 49.0 129.0
21.9 199.0 26.0 59.9 12.0 51.0 29.0 48.0 126.0
20.7 207.0 30.0 61.0 10.0 55.0 32.0 45.0 153.0
19.1 427.0 30.0 60.8 11.0 43.0 31.0 41.0 128.0
20.0 228.8 31.3 59.8 10.8 44.3 29.8 45.3 130.7
19.9 193.0 30.0 59.9 11.0 43.5 30.0 45.0 127.0
1.3 97.9 4.0 1.1 0.8 7.5 1.7 2.9 11.1
6.30% 42.76% 12.71% 1.80% 6.95% 16.98% 5.77% 6.34% 8.53%
-20.90% 802.79% 23.62% 135.91% -57.26% 74.90% 17.70% 78.85% 415.51%
0.10 9.54 0.54 2.16 0.63 1.28 0.46 1.34 5.95

09 11 13 14 15 16 17 18 19
AR*OES/MS AR*OES AR*MS AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS
20g 0.15g 01g 0.5g 01g 10g 0.25g 10g 0.25g
0.19 < 0.5 0.18 0.23 < 0.5 < 0.5 0.10 <1 < 0.1
0.18 < 0.5 0.17 0.20 < 0.5 < 0.5 0.20 <1 0.14
0.19 < 0.5 0.19 0.14 < 0.5 < 0.5 0.20 <1 0.14
0.18 < 0.5 0.19 0.17 < 0.5 < 0.5 0.10 <1 0.11
0.18 < 0.5 0.18 0.14 < 0.5 < 0.5 0.10 <1 0.13
0.17 < 0.5 0.17 0.20 < 0.5 < 0.5 < 0.1 <1 0.14
0.18 0.18 0.18 0.14 0.13
0.18 0.18 0.19 0.10 0.14
0.006 0.010 0.036 0.055 0.013
3.31% 5.57% 20.18% 39.12% 9.88%
15.39% 15.17% 14.26% -11.13% -16.21%
0.95 NA 0.94 0.53 NA NA 0.53 NA 0.82

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
16.8 20.0 14.0 23.0 9.3 17.2 18.0 < 10 10.9
17.3 20.0 14.0 22.0 18.7 17.0 16.0 < 10 10.7
14.5 20.0 15.0 31.0 10.4 17.1 20.0 < 10 10.4
15.9 20.0 15.0 28.0 20.7 17.0 15.0 < 10 12.0
16.0 20.0 15.0 26.0 0.1 17.0 15.0 < 10 9.7
15.3 20.0 15.0 27.0 30.8 17.4 17.0 < 10 9.2
15.9 20.0 14.7 26.2 15.0 17.1 16.8 10.5
15.9 20.0 15.0 26.5 14.6 17.1 16.5 10.6
1.0 0.0 0.5 3.3 10.7 0.2 1.9 1.0
6.26% 0.00% 3.52% 12.66% 71.33% 0.97% 11.53% 9.47%
-4.26% 20.07% -11.95% 57.10% -9.89% 2.76% 1.06% -37.11%
0.15 1.51 0.67 4.03 0.63 0.33 0.21 NA 2.39

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
0.212 0.190 0.190 0.200 0.168 0.180 0.210 0.170 0.180
0.222 0.190 0.200 0.190 0.162 0.177 0.210 0.170 0.180
0.214 0.200 0.190 0.200 0.169 0.180 0.210 0.170 0.190
0.228 0.190 0.200 0.190 0.166 0.177 0.200 0.160 0.190
0.242 0.190 0.200 0.190 0.168 0.177 0.200 0.170 0.180
0.222 0.190 0.190 0.210 0.167 0.183 0.200 0.170 0.180
0.223 0.192 0.195 0.197 0.167 0.179 0.205 0.168 0.183
0.222 0.190 0.195 0.195 0.167 0.179 0.205 0.170 0.180
0.011 0.004 0.005 0.008 0.002 0.002 0.005 0.004 0.005
4.80% 2.13% 2.81% 4.15% 1.39% 1.37% 2.67% 2.43% 2.82%
22.34% 5.07% 6.90% 7.81% -8.58% -1.88% 12.38% -7.72% 0.50%
3.22 0.67 0.94 1.08 1.34 0.35 1.75 1.21 0.00

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
14.6 16.0 14.0 13.4 11.7 13.7 12.7 12.0 11.0
15.2 16.0 14.0 13.4 12.0 13.3 12.8 12.0 10.5
14.2 16.0 14.0 13.3 12.3 13.0 12.9 11.0 13.8
14.9 16.0 14.0 13.1 12.1 13.4 12.4 12.0 12.0
15.0 16.0 14.0 13.2 12.2 13.2 12.6 12.0 9.4
14.3 16.0 14.0 13.7 11.6 13.5 12.6 12.0 9.0
14.7 16.0 14.0 13.4 12.0 13.4 12.7 11.8 11.0
14.8 16.0 14.0 13.4 12.0 13.4 12.6 12.0 10.8
0.4 0.0 0.0 0.2 0.3 0.2 0.2 0.4 1.8
2.78% 0.00% 0.00% 1.55% 2.31% 1.82% 1.38% 3.45% 15.99%
14.13% 24.17% 8.64% 3.60% -7.10% 3.60% -1.70% -8.17% -14.92%
0.79 1.48 0.41 0.06 0.67 0.06 0.30 0.75 1.21
Lab Lab Lab

17 19 25
AR*OES/MSAR*OES/MS AR*MS
0.25g 0.25g 40g
11.2 10.5 6.4
11.2 11.2 5.3
14.0 10.3 5.1
12.9 10.0 5.5
9.8 10.1 6.0
9.4 10.6 6.0
11.4 10.5 5.7
11.2 10.4 5.8
1.8 0.4 0.5
15.33% 3.86% 8.74%
-6.93% -14.90% -53.40%
0.00 0.22 1.26

09 10 11 12 13 14 15 16 17
AR*OES/MS AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES AR*OES/MS
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
91 109 91 101 89 93 100 86 83
94 109 93 101 89 94 100 88 80
88 110 90 101 88 94 99 88 99
92 108 91 99 89 94 97 88 93
95 108 92 99 89 93 99 88 73
88 109 91 103 88 94 97 88 69
91 109 91 101 89 94 99 88 83
91 109 91 101 89 94 99 88 81
2.9 0.8 1.0 1.5 0.4 0.5 1.5 0.8 11.4
3.17% 0.69% 1.13% 1.50% 0.45% 0.55% 1.51% 0.93% 13.75%
-1.78% 17.15% -1.69% 8.36% -4.69% 0.82% 6.09% -5.64% -10.77%
0.33 2.09 0.32 0.96 0.71 0.00 0.67 0.83 1.11

09 10 11 12 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES/MS AR*OES
20g 01g 0.15g 0.5g 0.5g 01g 10g 0.25g 10g
25.8 29.0 31.0 31.0 30.2 30.0 25.0 24.0 24.0
29.1 29.0 32.0 31.0 32.2 28.0 25.0 22.0 24.0
25.0 29.0 28.0 30.0 27.7 29.0 27.0 26.0 23.0
28.8 28.0 28.0 33.0 25.0 30.0 26.0 24.0 25.0
31.1 29.0 29.0 31.0 24.1 30.0 25.0 24.0 25.0
25.8 29.0 30.0 28.0 28.5 29.0 31.0 24.0 26.0
27.6 28.8 29.7 30.7 28.0 29.3 26.5 24.0 24.5
27.3 29.0 29.5 31.0 28.1 29.5 25.5 24.0 24.5
2.4 0.4 1.6 1.6 3.1 0.8 2.3 1.3 1.0
8.78% 1.42% 5.50% 5.32% 10.97% 2.78% 8.85% 5.27% 4.28%
0.33% 4.85% 7.88% 11.51% 1.64% 6.67% -3.64% -12.73% -10.91%
0.14 0.35 0.67 1.07 0.00 0.54 0.92 1.55 1.36
Lab Lab Lab

19 24 25
0.25g 40g 40g
0.44 0.40 0.40
0.44 0.50 0.36
0.42 0.50 0.36
0.41 0.40 0.36
0.42 0.50 0.38
0.43 0.40 0.38
0.43 0.45 0.37
0.43 0.45 0.37
0.011 0.055 0.016
2.50% 12.17% 4.37%
-10.73% -5.99% -22.01%
0.68 0.39 1.38

08 09 10 11 12 13 14 15 16
AR*OES/AAS
AR*OES/MS AR*OES AR*AAS AR*AAS AR*OES AR*OES AR*OES AR*OES
0.5g 20g 01g 0.5g 01g 01g 0.5g 01g 10g
4.98 5.02 4.53 5.24 4.96 4.71 > 10000 5.02 > 10000
5.00 4.95 4.46 5.25 4.97 4.67 > 10000 5.10 > 10000
5.09 4.98 4.56 5.30 5.01 4.67 > 10000 4.99 > 10000
5.09 4.86 4.50 5.20 4.96 4.72 > 10000 4.94 > 10000
5.06 4.88 4.45 5.24 4.96 4.68 > 10000 5.01 > 10000
5.08 4.91 4.46 5.25 4.94 4.81 4.89 4.97 > 10000
5.05 4.94 4.49 5.25 4.97 4.71 4.89 5.00
5.07 4.93 4.48 5.24 4.96 4.69 4.89 5.00
0.048 0.060 0.045 0.032 0.024 0.055 0.056
0.95% 1.22% 0.99% 0.62% 0.48% 1.16% 1.12%
1.40% -0.91% -9.78% 5.32% -0.30% -5.44% -1.76% 0.49%
0.64 0.54 5.08 2.64 0.23 2.86 0.98 0.17 NA
09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
3.91 3.98 3.96 3.82 3.78 3.68 3.98 3.59 3.66
4.04 3.97 4.17 3.89 3.78 3.75 3.99 3.49 3.65
4.07 3.97 3.96 3.98 3.87 3.71 3.95 3.48 3.97
4.04 3.91 4.06 3.80 3.84 3.75 3.83 3.60 3.94
4.10 3.86 4.02 3.84 3.94 3.75 3.93 3.49 3.84
4.02 3.89 3.75 3.96 3.77 3.79 3.89 3.60 3.73
4.03 3.93 3.99 3.88 3.83 3.74 3.93 3.54 3.80
4.04 3.94 3.99 3.87 3.81 3.75 3.94 3.54 3.79
0.067 0.050 0.140 0.075 0.070 0.039 0.060 0.060 0.139
1.66% 1.28% 3.50% 1.93% 1.82% 1.05% 1.53% 1.71% 3.67%
7.47% 4.79% 6.31% 3.51% 2.15% -0.37% 4.75% -5.56% 1.28%
1.28 0.78 1.00 0.58 0.38 0.00 0.77 0.78 0.25
Lab Lab Lab Lab Lab Lab

15 17 19 23 24 25
AR*OES AR*OES/MSAR*OES/MS AR*OES AR*MS AR*MS
01g 0.25g 0.25g 0.5g 40g 40g
6.00 6.60 5.60 <5 5.80 7.00
6.00 7.30 5.52 <5 5.90 6.20
6.00 8.70 5.44 <5 5.70 6.20
5.00 6.70 5.32 <5 5.80 6.40
7.00 6.70 5.53 <5 6.20 6.40
7.00 6.00 5.58 <5 6.10 6.80
6.17 7.00 5.50 5.92 6.50
6.00 6.70 5.53 5.85 6.40
0.753 0.930 0.104 0.194 0.329
12.21% 13.28% 1.88% 3.28% 5.06%
-7.45% 5.06% -17.48% -11.20% -2.44%
0.39 0.18 1.16 NA 0.67 0.00
Lab Lab
19 25
AR*OES/MS AR*MS
0.25g 40g
0.47 0.40
0.47 0.40
0.47 0.40
0.47 0.40
0.48 0.40
0.50 0.40
0.48 0.40
0.47 0.40
0.012 0.000
2.60% 0.00%
-13.28% -27.02%
0.50 1.03

12 14 16 17 19 23 24 25
AR*OES AR*MS AR*OES AR*OES/MSAR*OES/MS AR*OES AR*MS AR*MS
0.5g 0.5g 10g 0.25g 0.25g 0.5g 40g 40g
3.00 1.58 <5 2.90 1.50 2.00 1.50 1.75
<3 1.56 <5 3.03 1.36 2.00 1.50 1.77
<3 1.56 <5 3.53 1.54 2.00 1.50 1.81
<3 1.58 <5 3.08 1.41 2.00 1.50 1.81
<3 1.56 <5 2.79 1.50 2.00 2.00 1.99
<3 1.56 <5 2.61 1.47 2.00 1.50 1.86
3.00 1.57 2.99 1.46 2.00 1.58 1.83
3.00 1.56 2.97 1.48 2.00 1.50 1.81
0.010 0.314 0.066 0.000 0.204 0.086
0.66% 10.51% 4.54% 0.00% 12.89% 4.71%
2.97 0.67 NA 2.95 0.94 0.43 0.63 0.00
Lab Lab Lab Lab Lab

15 17 19 24 25
AR*OES/MSAR*OES/MSAR*OES/MS AR*MS AR*MS
01g 0.25g 0.25g 40g 40g
4.61 3.31 3.23 4.00 3.41
4.41 3.17 3.23 4.00 3.32
4.42 3.62 3.19 4.00 3.31
4.34 3.46 3.17 4.00 3.29
4.40 2.84 3.21 4.50 3.27
4.49 2.73 3.15 4.00 3.33
4.45 3.19 3.20 4.08 3.32
4.42 3.24 3.20 4.00 3.32
0.094 0.348 0.030 0.204 0.048
2.11% 10.93% 0.95% 5.00% 1.46%
18.61% -14.92% -14.71% 8.96% -11.37%
0.87 0.86 0.85 0.37 0.67

09 11 12 13 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES
20g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g 10g
0.163 0.130 0.150 0.140 0.140 0.160 0.120 0.150 0.110
0.177 0.130 0.150 0.142 0.130 0.160 0.120 0.150 0.100
0.182 0.130 0.150 0.148 0.130 0.150 0.120 0.160 0.100
0.183 0.130 0.150 0.146 0.130 0.150 0.120 0.160 0.100
0.180 0.140 0.140 0.153 0.130 0.150 0.120 0.150 0.110
0.170 0.130 0.160 0.146 0.130 0.150 0.120 0.140 0.110
0.176 0.132 0.150 0.146 0.132 0.153 0.120 0.152 0.105
0.178 0.130 0.150 0.146 0.130 0.150 0.120 0.150 0.105
0.008 0.004 0.006 0.005 0.004 0.005 0.000 0.008 0.005
4.50% 3.10% 4.22% 3.10% 3.10% 3.37% 0.00% 4.96% 5.22%
31.47% -1.53% 12.18% 9.08% -1.53% 14.67% -10.26% 13.43% -21.47%
1.75 0.03 0.75 0.58 0.03 0.88 0.42 0.81 1.00

09 11 12 13 14 16 17 18 19
AR*OES/MS AR*OES AR*OES AR*MS AR*MS AR*OES AR*OES/MS AR*OES AR*OES/MS
20g 0.15g 0.5g 01g 0.5g 10g 0.25g 10g 0.25g
6.86 6.00 4.00 3.26 3.78 4.10 3.60 < 10 4.21
6.84 6.00 4.00 3.10 3.50 4.00 3.70 < 10 4.58
6.67 6.00 4.00 3.29 3.52 4.20 10.00 < 10 4.06
6.92 6.00 4.00 3.54 3.62 4.20 4.30 < 10 3.90
6.54 6.00 4.00 3.43 3.55 5.00 3.10 < 10 3.88
6.44 6.00 4.00 3.30 3.67 3.90 2.60 < 10 4.25
6.71 6.00 4.00 3.32 3.61 4.23 4.55 4.15
6.76 6.00 4.00 3.30 3.59 4.15 3.65 4.14
0.193 0.000 0.000 0.150 0.106 0.393 2.731 0.262
2.88% 0.00% 0.00% 4.53% 2.94% 9.29% 60.02% 6.31%
69.73% 51.71% 1.14% -16.05% -8.80% 7.04% 15.05% 4.85%
3.00 2.21 0.00 0.75 0.43 0.09 0.60 NA 0.16

15 16 17 18 19 21 25
AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS
01g 10g 0.25g 10g 0.25g 0.25g 40g
4.00 5.00 6.00 5.00 5.97 4.00 4.50
4.00 5.00 6.00 6.00 5.95 5.00 4.20
4.00 4.00 6.00 5.00 5.90 4.00 4.30
3.00 5.00 7.00 5.00 5.60 4.00 4.20
4.00 4.00 6.00 5.00 5.67 4.00 4.20
3.00 5.00 6.00 6.00 5.86 4.00 4.60
3.67 4.67 6.17 5.33 5.83 4.17 4.33
4.00 5.00 6.00 5.00 5.88 4.00 4.25
0.516 0.516 0.408 0.516 0.152 0.408 0.175
14.08% 11.07% 6.62% 9.68% 2.61% 9.80% 4.04%
-29.07% -9.72% 19.30% 3.18% 12.69% -19.39% -16.17%
1.35 0.34 1.18 0.34 0.83 0.84 0.67
Lab
25
AR*MS
40g
10
10
10
10
10
10
10
10
0
0.00%
-11.74%
0.93

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
287 300 300 400 228 300 300 200 300
299 300 300 400 227 300 300 300 300
273 300 300 400 232 200 300 200 300
301 300 300 400 232 300 300 200 300
306 300 300 400 231 200 300 200 300
269 300 300 400 234 300 300 200 300
289 300 300 400 231 267 300 217 300
293 300 300 400 231 300 300 200 300
15 0 0 0 2 52 0 41 0
5.36% 0.00% 0.00% 0.00% 1.08% 19.36% 0.00% 18.84% 0.00%
-0.03% 3.70% 3.70% 38.27% -20.24% -7.82% 3.70% -25.10% 3.70%
0.67 0.00 0.00 6.25 4.33 2.08 0.00 5.21 0.00

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
89 91 80 87 86 91 97 77 81
93 92 83 87 85 88 96 76 83
92 92 80 87 89 89 98 76 83
91 90 80 85 88 88 93 76 85
93 89 81 83 89 87 96 76 83
88 89 81 88 86 89 96 76 82
91 91 81 86 87 89 96 76 83
92 91 81 87 87 89 96 76 83
2.1 1.4 1.2 1.8 1.6 1.4 1.4 0.4 1.3
2.25% 1.52% 1.45% 2.13% 1.84% 1.54% 1.46% 0.54% 1.60%
6.37% 5.61% -5.67% 0.55% 1.66% 3.47% 11.70% -11.12% -3.34%
1.39 1.23 1.25 0.32 0.40 0.78 2.51 2.29 0.65

09 10 11 12 13 14 15 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES/MS AR*OES
20g 01g 0.15g 0.5g 01g 0.5g 01g 0.25g 10g
4.78 5.00 5.00 4.00 4.34 5.00 5.00 2.40 7.00
4.91 5.00 5.00 4.00 4.29 5.00 5.00 2.35 7.00
4.74 5.00 5.00 4.00 4.62 5.00 5.00 3.12 8.00
4.87 5.00 5.00 4.00 4.61 5.00 4.00 2.59 8.00
4.85 5.00 5.00 4.00 4.69 5.00 5.00 2.12 7.00
4.60 5.00 4.00 4.00 4.57 5.00 4.00 2.03 7.00
4.79 5.00 4.83 4.00 4.52 5.00 4.67 2.44 7.33
4.82 5.00 5.00 4.00 4.59 5.00 5.00 2.38 7.00
0.110 0.000 0.408 0.000 0.163 0.000 0.516 0.391 0.516
2.30% 0.00% 8.45% 0.00% 3.60% 0.00% 11.07% 16.06% 7.04%
0.86% 5.24% 1.73% -15.81% -4.85% 5.24% -1.78% -48.75% 54.35%
0.07 0.67 0.07 2.93 1.05 0.67 0.53 8.56 9.07

09 11 12 13 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES
20g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g 10g
370 300 400 329 300 300 300 400 400
373 300 400 317 300 300 300 400 300
352 300 400 324 300 300 300 400 400
369 300 400 320 300 300 300 400 400
392 300 400 326 300 300 300 400 400
346 300 400 324 300 300 300 400 400
367 300 400 323 300 300 300 400 383
370 300 400 324 300 300 300 400 400
16 0 0 4 0 0 0 0 41
4.47% 0.00% 0.00% 1.32% 0.00% 0.00% 0.00% 0.00% 10.65%
11.86% -8.58% 21.89% -1.49% -8.58% -8.58% -8.58% 21.89% 16.81%
0.68 0.00 1.01 0.24 0.00 0.00 0.00 1.01 0.84
Lab Lab Lab

17 19 25
AR*OES/MSAR*OES/MS AR*MS
0.25g 0.25g 40g
0.34 0.53 0.40
0.38 0.51 0.40
2.71 0.51 0.40
0.43 0.48 0.40
0.37 0.49 0.40
0.31 0.55 0.20
0.76 0.51 0.37
0.38 0.51 0.40
0.958 0.025 0.082
126.58% 4.93% 22.27%
68.64% 13.59% -18.28%
2.23 0.54 1.57

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
1633 1770 1578 1618 1356 1515 1556 1437 1145
1684 1770 1613 1590 1345 1537 1565 1426 1140
1563 1760 1562 1593 1343 1526 1532 1424 1228
1671 1740 1578 1563 1342 1541 1507 1435 1190
1640 1710 1599 1548 1366 1516 1545 1426 1035
1659 1730 1539 1647 1381 1529 1525 1435 985
1642 1747 1578 1593 1356 1527 1538 1431 1121
1650 1750 1578 1592 1351 1528 1539 1431 1143
43 24 26 36 15 11 21 6 93
2.63% 1.39% 1.66% 2.26% 1.14% 0.70% 1.38% 0.40% 8.28%
6.72% 13.54% 2.59% 3.56% -11.88% -0.72% 0.00% -7.01% -27.16%
1.61 3.24 0.62 0.85 2.84 0.17 0.00 1.68 6.50

09 11 12 13 14 16 17 18 19
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS
20g 0.15g 0.5g 01g 0.5g 10g 0.25g 10g 0.25g
119 101 344 1087 107 200 120 < 100 107
123 99 344 1083 104 100 130 < 100 186
117 97 330 1019 102 100 130 < 100 < 50
137 100 338 1023 103 200 130 < 100 89
119 100 325 1039 103 200 140 < 100 313
109 98 337 1032 105 < 100 130 < 100 231
121 99 336 1047 104 160 130 185
119 100 338 1035 104 200 130 186
9 1 8 30 2 55 6 92
7.75% 1.48% 2.26% 2.88% 1.72% 34.23% 4.87% 49.56%
4.26% -14.30% 190.66% 804.74% -10.12% 38.27% 12.35% 60.06%
0.09 0.72 7.59 32.48 0.55 1.41 0.36 NA 0.27

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
920 930 902 956 861 857 904 825 752
955 910 922 954 860 848 911 824 904
919 920 912 959 868 840 894 834 810
921 920 916 937 869 833 874 838 899
920 890 918 936 868 834 899 835 823
940 910 891 975 871 863 884 831 756
929 913 910 953 866 846 894 831 824
920 915 914 955 868 844 897 833 817
15 14 12 15 5 12 14 6 66
1.62% 1.50% 1.27% 1.54% 0.56% 1.45% 1.51% 0.68% 8.06%
8.54% 6.70% 6.33% 11.32% 1.22% -1.19% 4.48% -2.90% -3.73%
2.42 2.10 2.00 3.32 0.64 0.00 1.51 0.45 0.67
Lab Lab Lab
19 24 25
0.25g 40g 40g
4.63 6.40 5.10
4.73 6.50 4.45
4.50 6.30 4.40
4.33 6.20 4.45
4.58 7.00 4.55
4.61 6.50 4.65
4.56 6.48 4.60
4.60 6.45 4.50
0.136 0.279 0.261
2.99% 4.30% 5.67%
-20.61% 12.80% -19.97%
1.68 0.62 1.76
09 10 11 13 14 15 16 17 19
AR*OES/MS AR*OES AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES/MSAR*OES/MS
20g 01g 0.15g 01g 0.5g 01g 10g 0.25g 0.25g
8.19 7.99 7.91 7.81 6.54 7.64 >5 - >5
8.13 7.91 8.16 7.79 6.43 7.69 >5 - >5
8.07 8.00 7.86 7.88 6.57 7.59 >5 - >5
8.04 7.93 7.96 7.72 6.50 7.38 >5 - >5
7.92 7.81 8.13 7.75 6.48 7.56 >5 - >5
7.96 7.84 7.66 7.64 6.57 7.51 >5 - >5
8.05 7.91 7.95 7.77 6.52 7.56
8.06 7.92 7.94 7.77 6.52 7.58
0.101 0.077 0.185 0.082 0.055 0.111
1.26% 0.97% 2.32% 1.05% 0.85% 1.47%
2.39% 0.66% 1.08% -1.22% -17.13% -3.81%
0.26 0.00 0.06 0.28 2.68 0.67 NA NA NA

09 10 11 12 13 14 15 16 17
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
198 210 245 250 175 251 295 240 119
205 200 256 250 176 250 303 242 138
184 200 248 251 173 258 297 250 204
200 200 255 244 175 257 291 263 131
202 190 254 253 173 251 302 256 130
199 200 242 242 171 257 297 252 117
198 200 250 248 174 254 298 251 140
199 200 251 250 174 254 297 251 131
7 6 6 4 2 4 4 9 32
3.71% 3.16% 2.33% 1.74% 1.03% 1.53% 1.50% 3.44% 23.17%
-13.20% -12.38% 9.52% 8.79% -23.71% 11.24% 30.33% 9.74% -38.74%
0.83 0.85 0.09 0.06 1.33 0.16 0.98 0.10 2.22

09 11 12 13 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*MS AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES
20g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g 10g
1.21 2.00 1.00 0.98 0.90 1.20 0.50 1.20 <3
1.17 2.00 1.00 1.08 0.91 1.26 0.50 1.30 <3
1.10 2.00 1.00 0.99 0.92 1.34 0.50 1.50 <3
1.22 2.00 1.00 0.98 0.88 1.32 0.50 1.40 <3
1.24 2.00 1.00 1.04 0.91 1.20 0.50 1.20 <3
1.11 2.00 1.00 1.06 0.92 1.15 0.50 1.20 <3
1.17 2.00 1.00 1.02 0.91 1.25 0.50 1.30
1.19 2.00 1.00 1.02 0.91 1.23 0.50 1.25
0.057 0.000 0.000 0.043 0.015 0.075 0.000 0.126
4.88% 0.00% 0.00% 4.25% 1.66% 6.01% 0.00% 9.73%
12.30% 91.36% -4.32% -2.11% -13.25% 19.12% -52.16% 24.38%
4.69 26.97 0.00 0.62 2.52 6.61 13.49 8.09 NA

17 18 19 21 24 25
AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS AR*MS
0.25g 10g 0.25g 0.25g 40g 40g
89 58 62 84 85 69
86 55 61 81 87 68
120 60 61 75 84 68
96 67 61 82 82 67
75 47 61 81 91 67
71 52 59 82 86 68
90 57 61 81 86 68
88 57 61 82 85 68
18 7 1 3 3 1
19.59% 12.20% 1.61% 3.79% 3.42% 1.11%
19.10% -24.81% -19.03% 7.57% 14.00% -9.73%
0.59 1.45 1.09 0.49 0.77 0.59
16 17 18 19 21 24 25
AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS AR*MS
10g 0.25g 10g 0.25g 0.25g 40g 40g
< 10 1.60 < 10 1.65 < 10 2.00 1.90
< 10 2.00 < 10 1.65 < 10 2.00 1.80
< 10 1.60 < 10 1.63 < 10 2.00 1.80
< 10 1.70 < 10 1.62 < 10 2.00 1.80
< 10 1.90 < 10 1.62 < 10 2.00 1.80
< 10 1.70 < 10 1.62 < 10 2.00 1.80
1.75 1.63 2.00 1.82
1.70 1.63 2.00 1.80
0.164 0.016 0.000 0.041
9.39% 0.95% 0.00% 2.25%
-8.78% -14.92% 4.25% -5.30%
NA 0.61 NA 1.07 NA 0.35 0.35

09 11 12 13 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES
20g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g 10g
40.6 47.0 28.0 28.7 26.9 19.8 27.5 32.1 23.0
39.8 49.0 28.0 28.0 25.1 20.9 25.5 33.9 22.0
38.5 48.0 28.0 28.2 25.3 20.8 27.9 35.3 23.0
40.8 48.0 27.0 28.7 26.5 18.3 28.6 34.5 22.0
41.2 49.0 28.0 29.1 25.8 19.0 28.9 33.8 23.0
40.0 50.0 28.0 28.2 26.6 20.5 27.5 32.7 21.0
40.2 48.5 27.8 28.5 26.0 19.9 27.7 33.7 22.3
40.3 48.5 28.0 28.4 26.1 20.2 27.7 33.8 22.5
1.0 1.0 0.4 0.4 0.7 1.0 1.2 1.2 0.8
2.39% 2.16% 1.47% 1.42% 2.85% 5.26% 4.34% 3.46% 3.66%
43.09% 72.82% -0.82% 1.48% -7.24% -29.09% -1.48% 20.14% -20.42%
1.51 2.59 0.09 0.00 0.32 1.11 0.11 0.68 0.80
Lab
25
AR*MS
40g
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
NA
Lab Lab
19 25
AR*OES/MS AR*MS
0.25g 40g
0.09 0.09
0.10 0.08
0.10 0.08
0.09 0.08
0.09 0.08
0.10 0.08
0.09 0.08
0.09 0.08
0.002 0.005
2.62% 6.85%
-12.55% -26.22%
0.53 1.07
Lab Lab
19 25
AR*OES/MS AR*MS
0.25g 40g
34.2 33.8
33.3 33.1
33.4 33.0
32.5 33.3
32.9 33.0
32.9 33.2
33.2 33.2
33.1 33.2
0.594 0.301
1.79% 0.91%
0.40% 0.45%
0.06 0.07

13 14 15 17 18 19 23 24 25
AR*MS AR*MS AR*OES/MSAR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS AR*MS
01g 0.5g 01g 0.25g 10g 0.25g 0.5g 40g 40g
1.56 1.53 2.69 1.80 < 10 1.88 <2 1.35 0.86
1.49 1.47 2.85 2.00 < 10 1.99 <2 1.40 0.82
1.50 1.46 2.64 2.20 < 10 1.85 <2 1.40 0.80
1.52 1.50 2.64 1.90 < 10 1.78 2.00 1.30 0.86
1.55 1.46 2.73 1.80 < 10 1.74 2.00 1.45 0.90
1.51 1.54 2.82 1.70 < 10 1.91 2.00 1.40 0.96
1.52 1.49 2.73 1.90 1.86 2.00 1.38 0.87
1.51 1.48 2.71 1.85 1.87 2.00 1.40 0.86
0.028 0.036 0.090 0.179 0.091 0.000 0.052 0.058
1.82% 2.38% 3.29% 9.42% 4.92% 0.00% 3.73% 6.64%
0.65 0.70 1.54 0.04 NA 0.04 0.22 0.90 1.84

09 11 12 14 15 16 17 18 19
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS
20g 0.15g 0.5g 0.5g 01g 10g 0.25g 10g 0.25g
123 < 100 < 100 85 100 < 100 100 < 100 110
122 < 100 < 100 82 100 < 100 100 < 100 110
114 < 100 < 100 83 100 < 100 100 < 100 110
125 < 100 < 100 83 100 < 100 100 < 100 100
125 < 100 < 100 82 100 < 100 100 < 100 100
115 100 < 100 85 100 < 100 100 < 100 110
121 100 83 100 100 107
122 100 83 100 100 110
5 1 0 0 5
4.06% 1.64% 0.00% 0.00% 4.84%
20.82% -0.03% -16.69% -0.03% -0.03% 6.64%
NA NA NA NA NA NA NA NA NA

14 15 17 18 19 23 24 25
AR*MS AR*OES/MSAR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS AR*MS
0.5g 01g 0.25g 10g 0.25g 0.5g 40g 40g
15.4 18.2 13.8 11.0 15.2 15.0 14.7 14.5
15.3 18.3 15.9 11.0 15.3 13.0 15.2 14.4
15.3 18.2 16.0 < 10 14.9 13.0 15.0 14.2
15.2 17.7 14.3 11.0 14.9 11.0 14.0 14.5
15.2 18.3 14.6 < 10 14.8 16.0 16.2 14.4
15.1 17.8 14.1 < 10 14.8 18.0 15.3 14.3
15.3 18.1 14.8 11.0 15.0 14.3 15.1 14.4
15.2 18.2 14.5 11.0 14.9 14.0 15.1 14.4
0.1 0.3 0.9 0.0 0.2 2.5 0.7 0.1
0.73% 1.58% 6.37% 0.00% 1.37% 17.47% 4.82% 0.81%
-0.01% 18.49% -3.08% -27.89% -1.83% -6.03% -1.23% -5.71%
0.50 2.87 0.11 3.07 0.27 0.27 0.34 0.23

13 14 15 17 18 19 24 25
AR*MS AR*MS AR*OES/MSAR*OES/MS AR*OES AR*OES/MS AR*MS AR*MS
01g 0.5g 01g 0.25g 10g 0.25g 40g 40g
0.88 0.87 1.09 0.87 < 10 0.96 1.00 0.78
0.79 0.86 1.13 1.04 < 10 0.97 1.05 0.70
0.84 0.85 1.03 1.14 < 10 0.93 1.10 0.68
0.85 0.86 1.02 0.90 < 10 0.91 1.00 0.70
0.85 0.85 1.03 0.96 < 10 0.93 1.10 0.72
0.82 0.85 1.08 0.88 < 10 0.97 1.05 0.74
0.84 0.86 1.06 0.97 0.95 1.05 0.72
0.84 0.86 1.06 0.93 0.94 1.05 0.71
0.033 0.008 0.044 0.107 0.024 0.045 0.036
3.92% 0.95% 4.11% 11.04% 2.55% 4.26% 4.97%
-11.63% -9.70% 12.09% 1.72% -0.37% 10.68% -24.10%
0.87 0.74 0.67 0.00 NA 0.14 0.58 1.68

09 11 12 13 14 15 16 17 18
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
20g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g 10g
9.50 8.00 8.00 7.62 9.00 8.32 15.00 13.00 7.00
9.72 8.00 8.00 7.36 9.00 9.19 14.00 12.00 7.00
8.97 8.00 8.00 6.95 8.00 7.38 13.00 13.00 7.00
10.00 8.00 8.00 7.10 8.00 8.65 16.00 13.00 7.00
10.30 8.00 7.00 7.76 9.00 9.21 14.00 13.00 7.00
9.00 9.00 8.00 7.42 8.00 9.04 14.00 12.00 7.00
9.58 8.17 7.83 7.37 8.50 8.63 14.33 12.67 7.00
9.61 8.00 8.00 7.39 8.50 8.84 14.00 13.00 7.00
0.535 0.408 0.408 0.305 0.548 0.704 1.033 0.516 0.000
5.58% 5.00% 5.21% 4.15% 6.44% 8.15% 7.21% 4.08% 0.00%
15.04% -1.95% -5.96% -11.54% 2.05% 3.63% 72.08% 52.07% -15.96%
1.04 0.06 0.31 0.67 0.20 0.30 4.72 3.43 0.96

09 11 13 14 15 17 18 19 21
AR*OES/MS AR*OES AR*MS AR*MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
20g 0.15g 01g 0.5g 01g 0.25g 10g 0.25g 0.25g
6.48 13.00 5.60 6.06 < 10 6.20 < 10 6.99 17.00
6.85 < 10 5.62 5.85 < 10 6.60 < 10 7.01 15.00
6.20 10.00 5.55 5.82 < 10 7.00 < 10 6.94 17.00
6.57 13.00 5.86 5.83 < 10 6.60 < 10 6.79 19.00
6.59 10.00 5.75 5.92 < 10 6.30 < 10 6.88 18.00
6.54 13.00 5.61 6.06 < 10 5.80 < 10 7.02 19.00
6.54 11.80 5.67 5.92 6.42 6.94 17.50
6.56 13.00 5.62 5.89 6.45 6.96 17.50
0.209 1.643 0.117 0.111 0.412 0.088 1.517
3.19% 13.93% 2.07% 1.88% 6.42% 1.27% 8.67%
10.92% 100.14% -3.88% 0.47% 8.84% 17.68% 196.82%
0.00 3.89 0.67 0.46 NA 0.09 NA 0.29 8.10

15 16 17 18 19 21 25
AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS
01g 10g 0.25g 10g 0.25g 0.25g 40g
2.00 <5 1.14 <1 1.77 2.00 1.63
2.00 <5 1.33 <1 1.78 2.00 1.44
2.00 <5 1.70 <1 1.75 2.00 1.43
2.00 <5 1.28 <1 1.72 2.00 1.46
2.00 <5 1.21 <1 1.75 2.00 1.46
2.00 <5 1.12 <1 1.76 2.00 1.50
2.00 1.30 1.75 2.00 1.49
2.00 1.25 1.75 2.00 1.46
0.000 0.213 0.021 0.000 0.074
0.00% 16.44% 1.20% 0.00% 4.99%
4.88% -32.00% -8.02% 4.88% -22.04%
0.00 NA 2.15 NA 0.67 0.00 1.49
Lab
25
AR*MS
40g
0.080
0.070
0.070
0.060
0.060
0.070
0.068
0.070
0.008
11.02%
-30.97%
4.24

09 10 11 12 13 14 15 16 17
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*MS AR*OES/MS AR*OES AR*OES/MS
20g 01g 0.15g 0.5g 01g 0.5g 01g 10g 0.25g
0.220 0.235 0.224 0.238 0.179 > 0.2 0.219 0.202 0.212
0.227 0.227 0.226 0.234 0.179 > 0.2 0.219 0.201 0.203
0.218 0.227 0.222 0.234 0.185 > 0.2 0.229 0.201 0.217
0.225 0.225 0.225 0.230 0.183 > 0.2 0.228 0.205 0.218
0.225 0.225 0.229 0.227 0.185 > 0.2 0.223 0.201 0.222
0.221 0.224 0.220 0.239 0.179 0.205 0.208 0.207 0.215
0.223 0.227 0.224 0.234 0.181 0.205 0.221 0.203 0.215
0.223 0.226 0.225 0.234 0.181 0.205 0.221 0.202 0.216
0.004 0.004 0.003 0.005 0.003 0.008 0.003 0.006
1.73% 1.77% 1.34% 1.93% 1.64% 3.53% 1.26% 2.94%
2.78% 4.84% 3.46% 7.81% -16.27% -5.25% 1.95% -6.39% -0.95%
0.51 0.84 0.67 1.74 4.18 1.47 0.30 1.75 0.41

14 15 16 17 18 19 25
AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*MS
0.5g 01g 10g 0.25g 10g 0.25g 40g
19.4 21.1 16.8 18.8 16.0 24.4 15.0
19.1 20.8 16.5 18.3 16.0 23.7 13.0
19.3 20.5 16.2 19.7 16.0 23.5 13.0
19.1 20.0 15.7 19.9 16.0 22.3 14.0
18.8 20.5 16.2 18.9 17.0 23.4 14.0
19.7 20.9 15.9 18.4 16.0 24.0 14.0
19.2 20.6 16.2 19.0 16.2 23.5 13.8
19.2 20.6 16.2 18.9 16.0 23.6 14.0
0.3 0.4 0.4 0.7 0.4 0.7 0.8
1.66% 1.86% 2.45% 3.49% 2.53% 3.03% 5.44%
1.23% 8.63% -14.53% 0.14% -14.79% 24.05% -27.09%
0.00 0.51 1.08 0.07 1.10 1.56 1.94
17 18 19 21 23 24 25
AR*OES/MS AR*OES AR*OES/MS
AR*OES/AAS AR*AAS AR*OES AR*MS
0.25g 10g 0.25g 02.5g 01g 40g 40g
- 326 > 100 913 930 N.A. 36
- 322 > 100 915 929 N.A. 39
- 347 > 100 914 880 N.A. 38
- 366 > 100 889 937 N.A. 36
- 309 > 100 894 935 N.A. 36
- 237 > 100 922 954 N.A. 34
318 908 928 36
324 914 933 36
44 13 25 2
13.98% 1.44% 2.69% 4.45%
-67.69% -7.71% -5.71% -96.30%
NA 21.51 NA 2.49 1.52 NA 31.38

18 19 21 23 24 25
AR*OES AR*OES/MS AR*OES AR*OES AR*OES AR*OES
10g 0.25g 0.25g 0.5g 40g 40g
0.570 0.737 0.500 0.660 0.870 0.600
0.550 0.738 0.520 0.650 0.860 0.570
0.550 0.724 0.490 0.670 0.830 0.570
0.550 0.683 0.510 0.680 0.820 0.580
0.560 0.653 0.490 0.660 0.810 0.600
0.580 0.712 0.500 0.690 0.830 0.600
0.560 0.708 0.502 0.668 0.837 0.587
0.555 0.718 0.500 0.665 0.830 0.590
0.013 0.034 0.012 0.015 0.023 0.015
2.26% 4.75% 2.33% 2.20% 2.79% 2.57%
-23.29% -3.04% -31.28% -8.45% 14.61% -19.63%
1.00 0.00 1.40 0.27 0.87 0.82

18 19 21 23 24 25
AR*OES AR*OES/MS AR*OES AR*OES AR*MS AR*MS
10g 0.25g 0.25g 0.5g 40g 40g
1470 1515 1557 1603 1350 1570
1457 1530 1609 1619 1370 1550
1482 1514 1540 1631 1330 1510
1507 1493 1574 1612 1310 1530
1499 1517 1557 1606 1430 1540
1478 1522 1582 1627 1390 1540
1482 1515 1570 1616 1363 1540
1480 1516 1566 1616 1360 1540
18 12 24 11 43 20
1.24% 0.82% 1.54% 0.70% 3.17% 1.30%
-8.12% -6.07% -2.69% 0.20% -15.49% -4.54%
1.12 0.87 0.45 0.10 2.02 0.68
Lab Lab
23 25
AR*OES AR*MS
0.5g 40g
7.0 19.0
6.0 19.0
7.0 20.0
7.0 23.0
7.0 25.0
6.0 25.0
6.7 21.8
7.0 21.5
0.5 2.9
7.75% 13.09%
-73.70% -13.86%
0.86 0.00
Lab
21
AR*OES
0.25g
<2
<2
<2
<2
<2
<2
NA
Lab Lab Lab Lab

19 21 24 25
AR*OES/MS AR*OES AR*MS AR*MS
0.25g 0.25g 40g 40g
16.1 13.0 16.8 17.4
16.1 12.0 17.1 17.8
16.0 9.0 17.2 17.2
15.9 7.0 15.1 17.8
16.0 10.0 15.2 17.8
15.7 <1 16.5 17.7
16.0 10.2 16.3 17.6
16.0 10.0 16.7 17.8
0.1 2.4 0.9 0.3
0.86% 23.41% 5.74% 1.45%
-4.08% -38.76% -2.04% 5.76%
0.14 2.50 0.00 0.53

18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
0.170 0.179 0.170 0.180 0.190 0.190
0.160 0.183 0.180 0.180 0.190 0.180
0.170 0.183 0.170 0.180 0.180 0.190
0.160 0.176 0.170 0.180 0.180 0.180
0.170 0.178 0.170 0.180 0.180 0.190
0.170 0.177 0.170 0.180 0.180 0.190
0.167 0.179 0.172 0.180 0.183 0.187
0.170 0.179 0.170 0.180 0.180 0.190
0.005 0.003 0.004 0.000 0.005 0.005
3.10% 1.68% 2.38% 0.00% 2.82% 2.77%
-8.64% -1.69% -5.90% -1.33% 0.50% 2.33%
1.35 0.32 0.94 0.27 0.00 0.27

18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
4.0 11.1 15.0 12.7 10.7 12.4
5.0 11.2 15.0 12.9 10.7 12.0
4.0 11.0 14.0 13.0 10.5 12.0
4.0 11.0 15.0 12.8 10.0 11.7
5.0 11.0 15.0 12.7 11.3 11.8
4.0 10.9 15.0 12.8 10.6 12.0
4.3 11.0 14.8 12.8 10.6 12.0
4.0 11.0 15.0 12.8 10.6 12.0
0.5 0.1 0.4 0.1 0.4 0.2
11.92% 1.06% 2.75% 0.91% 3.93% 2.00%
-66.37% -14.53% 15.11% -0.54% -17.48% -7.01%
4.76 1.19 0.86 0.22 1.39 0.67

18 19 21 23 24 25
AR*OES AR*OES/MS AR*OES AR*OES AR*MS AR*OES
10g 0.25g 0.25g 0.5g 40g 40g
86 81 95 97 85 98
87 83 99 97 87 96
87 85 95 98 83 99
88 84 97 97 83 97
88 84 96 97 92 98
88 86 96 98 87 99
87 84 96 97 86 98
88 84 96 97 86 98
0.8 1.8 1.5 0.5 3.1 1.2
0.93% 2.09% 1.56% 0.53% 3.59% 1.19%
-5.99% -9.70% 3.69% 4.77% -7.18% 5.31%
0.87 1.35 0.37 0.50 1.02 0.57
Lab Lab Lab Lab

21 23 24 25
AR*OES AR*OES AR*OES AR*OES
0.25g 0.5g 40g 40g
25.0 30.0 30.0 20.0
29.0 28.0 30.0 20.0
26.0 25.0 30.0 20.0
25.0 23.0 30.0 20.0
32.0 25.0 30.0 20.0
24.0 28.0 30.0 20.0
26.8 26.5 30.0 20.0
25.5 26.5 30.0 20.0
3.1 2.6 0.0 0.0
11.41% 9.77% 0.00% 0.00%
-2.42% -3.64% 9.09% -27.27%
0.44 0.57 0.81 3.12

17 18 19 21 23 24 25
AR*OES/MS AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES
0.25g 10g 0.5g 0.25g 01g 40g 40g
> 10000 > 10000 5.07 4.76 4.95 N.A. 5.15
> 10000 -- 5.08 4.93 5.15 N.A. 5.01
> 10000 > 10000 5.01 4.69 4.93 N.A. 5.02
> 10000 > 10000 5.05 4.79 4.99 N.A. 5.02
> 10000 > 10000 4.99 4.73 4.93 N.A. 5.10
> 10000 > 10000 5.03 4.79 5.15 N.A. 5.02
5.04 4.78 5.02 5.05
5.04 4.77 4.97 5.02
0.032 0.080 0.105 0.058
0.64% 1.67% 2.10% 1.14%
1.18% -4.01% 0.70% 1.47%
NA NA 0.53 2.12 0.28 NA 0.67
18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
3.54 4.04 3.44 3.73 3.94 3.91
3.45 4.03 3.56 3.65 3.96 3.81
3.51 4.02 3.42 3.77 3.83 3.82
3.50 3.92 3.47 3.68 3.72 3.81
3.55 3.87 3.45 3.70 3.80 3.87
3.55 3.86 3.47 3.78 3.86 3.83
3.52 3.96 3.47 3.72 3.85 3.84
3.53 3.97 3.46 3.72 3.85 3.83
0.039 0.081 0.049 0.051 0.090 0.040
1.10% 2.05% 1.41% 1.38% 2.32% 1.05%
-6.23% 5.49% -7.52% -0.85% 2.71% 2.44%
0.88 0.88 1.08 0.07 0.46 0.42
Lab Lab Lab Lab Lab
19 21 23 24 25
AR*OES/MS AR*OES AR*OES AR*OES AR*OES
0.25g 0.25g 0.5g 40g 40g
0.119 0.090 0.110 0.140 0.110
0.121 0.100 0.110 0.130 0.100
0.115 0.090 0.110 0.110 0.100
0.110 0.090 0.110 0.120 0.100
0.113 0.090 0.110 0.140 0.100
0.114 0.090 0.120 0.130 0.100
0.115 0.092 0.112 0.128 0.102
0.114 0.090 0.110 0.130 0.100
0.004 0.004 0.004 0.012 0.004
3.50% 4.45% 3.66% 9.11% 4.02%
-13.75% -31.45% -16.49% -4.02% -23.97%
0.60 1.52 0.75 0.10 1.13
Lab Lab
23 25
AR*OES AR*MS
0.5g 40g
4.00 1.63
4.00 1.26
4.00 1.22
4.00 1.35
4.00 1.47
4.00 1.49
4.00 1.40
4.00 1.41
0.000 0.155
0.00% 11.05%
1.14% -64.52%
0.00 2.87
18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
200 320 200 300 400 300
300 330 300 300 400 300
300 330 200 300 400 300
200 320 200 300 300 300
200 320 200 300 400 300
300 310 200 300 400 300
250 322 217 300 383 300
250 320 200 300 400 300
55 8 41 0 41 0
21.91% 2.34% 18.84% 0.00% 10.65% 0.00%
-13.58% 11.19% -25.10% 3.70% 32.51% 3.70%
3.12 1.35 5.21 0.00 5.21 0.00

18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
< 100 92 100 83 80 88
< 100 94 102 88 80 86
< 100 95 < 100 84 80 87
< 100 90 < 100 82 80 87
< 100 90 < 100 82 80 88
< 100 92 < 100 85 80 88
92 101 84 80 87
92 101 84 80 88
1.9 1.4 2.3 0.0 0.8
2.03% 1.40% 2.71% 0.00% 0.93%
7.54% 17.86% -1.98% -6.65% 1.91%
NA 1.63 3.81 0.37 1.35 0.45
Lab Lab Lab Lab Lab

19 21 23 24 25
AR*OES/MS AR*OES AR*OES AR*MS AR*MS
0.25g 0.25g 0.5g 40g 40g
4.71 4.00 5.00 5.00 5.60
4.81 5.00 5.00 4.80 5.60
4.89 5.00 5.00 4.60 5.60
4.58 4.00 5.00 4.60 5.60
4.54 5.00 4.00 5.20 5.60
4.63 5.00 5.00 4.80 5.60
4.69 4.67 4.83 4.83 5.60
4.67 5.00 5.00 4.80 5.60
0.136 0.516 0.408 0.234 0.000
2.89% 11.07% 8.45% 4.84% 0.00%
-1.23% -1.78% 1.73% 1.73% 17.87%
0.43 0.53 0.07 0.07 2.83
Lab Lab Lab Lab

19 21 23 25
AR*OES/MS AR*OES AR*OES AR*OES
0.25g 0.25g 0.5g 40g
490 400 300 500
520 400 300 400
480 400 300 400
470 400 300 400
420 400 300 400
500 400 300 400
480 400 300 417
485 400 300 400
34 0 0 41
7.10% 0.00% 0.00% 9.80%
46.27% 21.89% -8.58% 26.97%
1.82 1.01 0.00 1.01

18 19 21 23 24 25
AR*OES AR*OES/MS AR*OES AR*OES AR*MS AR*OES
10g 0.25g 0.25g 0.5g 40g 40g
1398 1547 1469 1592 1460 1530
1384 1539 1520 1593 1480 1500
1394 1538 1466 1608 1450 1510
1401 1484 1488 1574 1400 1520
1415 1512 1488 1568 1550 1530
1427 1539 1487 1596 1510 1530
1403 1527 1486 1589 1475 1520
1400 1539 1488 1593 1470 1525
15 24 19 15 52 13
1.10% 1.56% 1.30% 0.93% 3.50% 0.83%
-8.79% -0.76% -3.38% 3.26% -4.12% -1.19%
2.10 0.05 0.81 0.78 0.99 0.29
Lab Lab Lab Lab

21 23 24 25
AR*OES AR*OES AR*OES AR*OES
0.25g 0.5g 40g 40g
147 < 10 120 100
< 100 < 10 120 100
342 < 10 120 100
< 100 < 10 120 100
157 < 10 100 120
113 < 10 120 100
190 117 103
152 120 100
103 8 8
54.40% 7.00% 7.90%
63.98% 0.82% -10.70%
0.67 NA 0.01 0.69

18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
751 803 753 856 808 751
753 807 775 859 848 750
755 801 745 869 850 731
758 794 765 860 780 743
775 791 765 859 909 752
776 795 772 871 829 758
761 799 763 862 837 748
757 798 765 860 839 751
11 6 11 6 44 9
1.47% 0.79% 1.50% 0.71% 5.24% 1.26%
-11.05% -6.69% -10.92% 0.74% -2.18% -12.67%
2.62 1.46 2.58 0.51 0.26 3.05
Lab Lab Lab
23 24 25
AR*OES AR*OES AR*OES
0.5g 40g 40g
6.99 8.73 7.36
7.05 8.76 7.22
7.18 8.38 7.20
7.11 8.12 7.30
7.05 8.24 7.29
7.12 8.34 7.37
7.08 8.43 7.29
7.08 8.36 7.30
0.067 0.261 0.070
0.94% 3.10% 0.96%
-9.90% 7.21% -7.27%
1.59 0.99 1.20
Lab Lab Lab Lab Lab

18 19 21 23 25
AR*OES AR*OES/MS AR*OES AR*OES AR*MS
10g 0.25g 0.25g 0.5g 40g
243 192 154 271 251
246 188 160 274 243
251 190 153 275 243
251 189 154 271 243
247 187 152 272 243
241 185 156 271 240
247 189 155 272 244
247 188 154 272 243
4 2 3 2 4
1.66% 1.31% 1.85% 0.64% 1.52%
7.99% -17.40% -32.17% 19.30% 6.82%
0.03 1.06 1.72 0.51 0.03
Lab Lab Lab Lab

19 23 24 25
AR*OES/MS AR*OES AR*OES AR*MS
0.25g 0.5g 40g 40g
0.95 <5 1.00 1.00
1.02 <5 2.00 1.00
0.98 <5 1.00 1.00
1.03 <5 1.00 1.00
1.05 <5 1.00 1.00
1.12 <5 2.00 1.00
1.03 1.33 1.00
1.03 1.00 1.00
0.059 0.516 0.000
5.75% 38.73% 0.00%
-1.93% 27.57% -4.32%
0.67 NA 0.00 0.00
Lab Lab Lab Lab Lab
19 21 23 24 25
AR*OES/MS AR*OES AR*OES AR*MS AR*MS
0.25g 0.25g 0.5g 40g 40g
30.3 30.0 20.0 19.0 8.2
35.1 31.0 20.0 21.0 6.8
29.5 30.0 21.0 19.0 6.6
27.6 32.0 21.0 20.0 7.3
27.1 31.0 21.0 22.0 8.1
30.1 32.0 21.0 22.0 8.7
30.0 31.0 20.7 20.5 7.6
29.8 31.0 21.0 20.5 7.7
2.8 0.9 0.5 1.4 0.8
9.49% 2.89% 2.50% 6.72% 11.06%
6.75% 10.46% -26.36% -26.95% -72.86%
0.19 0.33 1.01 1.04 2.71
Lab Lab Lab
21 23 25
AR*OES AR*OES AR*OES
0.25g 0.5g 40g
< 100 70 < 50
< 100 70 < 50
< 100 70 < 50
< 100 70 < 50
< 100 70 < 50
< 100 80 < 50
72
70
4
5.70%
-28.35%
NA NA NA
Lab Lab Lab Lab
19 21 23 25
AR*OES/MS AR*OES AR*OES AR*OES
0.25g 0.25g 0.5g 40g
8.68 8.00 7.00 8.00
8.31 9.00 7.00 8.00
8.06 8.00 7.00 10.00
8.02 9.00 7.00 8.00
8.10 8.00 7.00 8.00
8.27 9.00 7.00 8.00
8.24 8.50 7.00 8.33
8.19 8.50 7.00 8.00
0.245 0.548 0.000 0.816
2.97% 6.44% 0.00% 9.80%
-1.09% 2.05% -15.96% 0.05%
0.00 0.20 0.96 0.19
Lab Lab
23 25
AR*OES AR*MS
0.5g 40g
5.00 4.20
3.00 4.20
4.00 4.00
4.00 4.20
6.00 4.20
4.00 4.10
4.33 4.15
4.00 4.20
1.033 0.084
23.83% 2.02%
-26.50% -29.61%
1.63 1.77
18 19 21 23 24 25
10g 0.25g 0.25g 0.5g 40g 40g
0.202 0.244 0.200 0.217 0.215 0.207
0.201 0.251 0.207 0.220 0.216 0.201
0.200 0.251 0.198 0.221 0.213 0.203
0.204 0.242 0.202 0.219 0.217 0.203
0.205 0.239 0.201 0.217 0.216 0.205
0.202 0.237 0.201 0.221 0.221 0.202
0.202 0.244 0.201 0.219 0.216 0.204
0.202 0.243 0.201 0.220 0.216 0.203
0.002 0.006 0.003 0.002 0.003 0.002
0.80% 2.44% 1.38% 0.82% 1.23% 1.07%
-6.59% 12.64% -7.04% 1.14% -0.16% -6.09%
1.80 2.93 1.91 0.10 0.22 1.68
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
984
67
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.730
68.000
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1613
69
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.66
70.00
Certified
1.00
ppm
1.00
1.00
1.0
3.0
16.0
< 10
71.0
Indicative
1.00
ppm
1.00
1.00
1.0
4.0
16.0
25.3
12.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.16
72.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
16.7
73.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.182
74.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
12.9
75.0
Indicative
1.00
ppm
1.00
1.00
1.0
7.0
16.0
12.3
13.0
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
93
76
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
27.5
77.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.48
78.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
4.98
79.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.52
80.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.15
81.00
Certified
1.00
ppm
2.00
2.00
1.00
3.00
16.00
0.21
82.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.75
83.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
6.66
84.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.87
85.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
0.41
14.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.55
86.00
Certified
1.00
ppm
2.00
2.00
1.00
4.00
16.00
<4
87.00
Certified
1.00
ppb
0.00
0.00
1
#N/A
16
73
88
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
3.75
89.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.134
90.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
3.95
91.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.17
92.00
Certified
1.00
ppb
0.00
0.00
1
#N/A
16
11
93
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
289
94
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
86
95
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.75
96.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
328
97
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.45
98.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
6.10
99.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1538
100
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
116
101
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
856
102
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
11.83
12.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.74
103.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
2.22
13.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.75
104.00
Indicative
1.00
ppb
0.00
0.00
1
8
16
1
14
Indicative
1.00
ppb
0.00
0.00
1
6
16
<2
12
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
7.86
105.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
228
106
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.05
107.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
75
108
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.16
109.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.92
110.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
28.1
111.0
Indicative
1.00
ppm
3.00
3.00
1.000
7.000
16.000
< 0.01
13.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.11
112.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
33.1
113.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
<3
114.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
100
115
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
15.3
116.0
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.018
14.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.95
117.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
8.33
118.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.90
119.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.91
120.00
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.099
121.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.217
122.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
19.0
123.0
Analytical results for Ag in OREAS 605 (Indicative Value 989 ppm)
Ag Round Replicate Lab
No No 01
ABL*MS
1 1 1010
1 2 967
Mean 989
Median 989
Std Dev. 30
Rel.Std.Dev. 3.08%
PDM3 0.00%
Analytical results for As in OREAS 605 (Indicative Value 1615 ppm)

As Round Replicate Lab
No No 01
ABL*MS
1 1 1660
1 2 1570
Mean 1615
Median 1615
Std Dev. 64
Rel.Std.Dev. 3.94%
PDM3 0.00%
Analytical results for Ba in OREAS 605 (Indicative Value 13150 ppm)

Ba Round Replicate Lab
No No 01
ABL*MS
1 1 13300
1 2 13000
Mean 13150
Median 13150
Std Dev. 212
Rel.Std.Dev. 1.61%
PDM3 0.00%
Analytical results for Be in OREAS 605 (Indicative Value 0.9 ppm)

Be Round Replicate Lab
No No 01
ABL*MS
1 1 0.80
1 2 1.00
Mean 0.90
Median 0.90
Std Dev. 0.141
Rel.Std.Dev. 15.71%
PDM3 0.00%
Analytical results for Bi in OREAS 605 (Indicative Value 16.6 ppm)
Bi Round Replicate Lab
No No 01
ABL*MS
1 1 17.0
1 2 16.2
Mean 16.6
Median 16.6
Std Dev. 0.6
Rel.Std.Dev. 3.41%
PDM3 0.00%
Analytical results for Cd in OREAS 605 (Indicative Value 13.9 ppm)

Cd Round Replicate Lab
No No 01
ABL*MS
1 1 13.5
1 2 14.2
Mean 13.9
Median 13.9
Std Dev. 0.5
Rel.Std.Dev. 3.57%
PDM3 0.00%
Analytical results for Ce in OREAS 605 (Indicative Value 31.4 ppm)

Ce Round Replicate Lab
No No 01
ABL*MS
1 1 32.0
1 2 30.8
Mean 31.4
Median 31.4
Std Dev. 0.8
Rel.Std.Dev. 2.70%
PDM3 0.00%
Analytical results for Co in OREAS 605 (Indicative Value 94 ppm)

Co Round Replicate Lab
No No 01
ABL*MS
1 1 95
1 2 94
Mean 94
Median 94
Std Dev. 1
Rel.Std.Dev. 1.12%
PDM3 0.00%
Analytical results for Cr in OREAS 605 (Indicative Value 35 ppm)
Cr Round Replicate Lab
No No 01
ABL*MS
1 1 35.0
1 2 35.0
Mean 35.0
Median 35.0
Std Dev. 0.0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Cs in OREAS 605 (Indicative Value 1.61 ppm)

Cs Round Replicate Lab
No No 01
ABL*MS
1 1 1.58
1 2 1.64
Mean 1.61
Median 1.61
Std Dev. 0.042
Rel.Std.Dev. 2.64%
PDM3 0.00%
Analytical results for Cu in OREAS 605 (Indicative Value 47800 ppm)

Cu Round Replicate Lab
No No 01
ABL*MS
1 1 48900
1 2 46700
Mean 47800
Median 47800
Std Dev. 1556
Rel.Std.Dev. 3.25%
PDM3 0.00%
Analytical results for Dy in OREAS 605 (Indicative Value 1.11 ppm)

Dy Round Replicate Lab
No No 01
ABL*MS
1 1 1.18
1 2 1.03
Mean 1.11
Median 1.11
Std Dev. 0.106
Rel.Std.Dev. 9.60%
PDM3 0.00%
Analytical results for Er in OREAS 605 (Indicative Value 0.44 ppm)
Er Round Replicate Lab
No No 01
ABL*MS
1 1 0.39
1 2 0.49
Mean 0.44
Median 0.44
Std Dev. 0.071
Rel.Std.Dev. 16.07%
PDM3 0.00%
Analytical results for Eu in OREAS 605 (Indicative Value 0.38 ppm)

Eu Round Replicate Lab
No No 01
ABL*MS
1 1 0.38
1 2 0.37
Mean 0.38
Median 0.38
Std Dev. 0.007
Rel.Std.Dev. 1.89%
PDM3 0.00%
Analytical results for Ga in OREAS 605 (Indicative Value 31.8 ppm)

Ga Round Replicate Lab
No No 01
ABL*MS
1 1 33.0
1 2 30.6
Mean 31.8
Median 31.8
Std Dev. 1.7
Rel.Std.Dev. 5.34%
PDM3 0.00%
Analytical results for Gd in OREAS 605 (Indicative Value 1.7 ppm)

Gd Round Replicate Lab
No No 01
ABL*MS
1 1 1.80
1 2 1.59
Mean 1.70
Median 1.70
Std Dev. 0.148
Rel.Std.Dev. 8.76%
PDM3 0.00%
Analytical results for Hf in OREAS 605 (Indicative Value 3.4 ppm)
Hf Round Replicate Lab
No No 01
ABL*MS
1 1 3.34
1 2 3.45
Mean 3.40
Median 3.40
Std Dev. 0.078
Rel.Std.Dev. 2.29%
PDM3 0.00%
Analytical results for Ho in OREAS 605 (Indicative Value 0.2 ppm)

Ho Round Replicate Lab
No No 01
ABL*MS
1 1 0.22
1 2 0.17
Mean 0.20
Median 0.20
Std Dev. 0.035
Rel.Std.Dev. 18.13%
PDM3 0.00%
Analytical results for In in OREAS 605 (Indicative Value 3.75 ppm)

In Round Replicate Lab
No No 01
ABL*MS
1 1 3.80
1 2 3.70
Mean 3.75
Median 3.75
Std Dev. 0.071
Rel.Std.Dev. 1.89%
PDM3 0.00%
Analytical results for La in OREAS 605 (Indicative Value 19.4 ppm)

La Round Replicate Lab
No No 01
ABL*MS
1 1 19.4
1 2 19.4
Mean 19.4
Median 19.4
Std Dev. 0.0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Lu in OREAS 605 (Indicative Value 0.05 ppm)
Lu Round Replicate Lab
No No 01
ABL*MS
1 1 0.050
1 2 0.050
Mean 0.050
Median 0.050
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Mn in OREAS 605 (Indicative Value 0.009 wt.%)

Mn Round Replicate Lab
No No 01
ABL*MS
1 1 0.009
1 2 0.010
Mean 0.009
Median 0.009
Std Dev. 0.000
Rel.Std.Dev. 1.50%
PDM3 0.00%
Analytical results for Mo in OREAS 605 (Indicative Value 4.9 ppm)

Mo Round Replicate Lab
No No 01
ABL*MS
1 1 4.60
1 2 5.20
Mean 4.90
Median 4.90
Std Dev. 0.424
Rel.Std.Dev. 8.66%
PDM3 0.00%
Analytical results for Nb in OREAS 605 (Indicative Value 7.22 ppm)

Nb Round Replicate Lab
No No 01
ABL*MS
1 1 7.20
1 2 7.23
Mean 7.22
Median 7.22
Std Dev. 0.021
Rel.Std.Dev. 0.29%
PDM3 0.00%
Analytical results for Nd in OREAS 605 (Indicative Value 12.1 ppm)
Nd Round Replicate Lab
No No 01
ABL*MS
1 1 12.5
1 2 11.6
Mean 12.1
Median 12.1
Std Dev. 0.6
Rel.Std.Dev. 5.28%
PDM3 0.00%
Analytical results for Ni in OREAS 605 (Indicative Value 1415 ppm)

Ni Round Replicate Lab
No No 01
ABL*MS
1 1 1420
1 2 1410
Mean 1415
Median 1415
Std Dev. 7
Rel.Std.Dev. 0.50%
PDM3 0.00%
Analytical results for Pb in OREAS 605 (Indicative Value 1390 ppm)

Pb Round Replicate Lab
No No 01
ABL*MS
1 1 1420
1 2 1360
Mean 1390
Median 1390
Std Dev. 42
Rel.Std.Dev. 3.05%
PDM3 0.00%
Analytical results for Pr in OREAS 605 (Indicative Value 3.7 ppm)

Pr Round Replicate Lab
No No 01
ABL*MS
1 1 3.80
1 2 3.59
Mean 3.70
Median 3.70
Std Dev. 0.148
Rel.Std.Dev. 4.02%
PDM3 0.00%
Analytical results for Rb in OREAS 605 (Indicative Value 31.6 ppm)
Rb Round Replicate Lab
No No 01
ABL*MS
1 1 32.0
1 2 31.1
Mean 31.6
Median 31.6
Std Dev. 0.6
Rel.Std.Dev. 2.02%
PDM3 0.00%
Analytical results for Re in OREAS 605 (Indicative Value 0.013 ppm)

Re Round Replicate Lab
No No 01
ABL*MS
1 1 0.020
1 2 < 0.01
Mean 0.020
Median 0.020
Std Dev.
Rel.Std.Dev.
PDM3 60.00%
Analytical results for Sb in OREAS 605 (Indicative Value 272 ppm)

Sb Round Replicate Lab
No No 01
ABL*MS
1 1 279
1 2 265
Mean 272
Median 272
Std Dev. 10
Rel.Std.Dev. 3.64%
PDM3 0.00%
Analytical results for Sc in OREAS 605 (Indicative Value 4.5 ppm)

Sc Round Replicate Lab
No No 01
ABL*MS
1 1 4.90
1 2 4.10
Mean 4.50
Median 4.50
Std Dev. 0.566
Rel.Std.Dev. 12.57%
PDM3 0.00%
Analytical results for Se in OREAS 605 (Indicative Value < 5 ppm)
Se Round Replicate Lab
No No 01
ABL*MS
1 1 <5
1 2 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Sm in OREAS 605 (Indicative Value 1.94 ppm)

Sm Round Replicate Lab
No No 01
ABL*MS
1 1 1.99
1 2 1.89
Mean 1.94
Median 1.94
Std Dev. 0.071
Rel.Std.Dev. 3.64%
PDM3 0.00%
Analytical results for Sn in OREAS 605 (Indicative Value 3.1 ppm)

Sn Round Replicate Lab
No No 01
ABL*MS
1 1 3.20
1 2 3.00
Mean 3.10
Median 3.10
Std Dev. 0.141
Rel.Std.Dev. 4.56%
PDM3 0.00%
Analytical results for Sr in OREAS 605 (Indicative Value 548 ppm)

Sr Round Replicate Lab
No No 01
ABL*MS
1 1 554
1 2 542
Mean 548
Median 548
Std Dev. 8
Rel.Std.Dev. 1.55%
PDM3 0.00%
Analytical results for Ta in OREAS 605 (Indicative Value 0.61 ppm)
Ta Round Replicate Lab
No No 01
ABL*MS
1 1 0.61
1 2 0.60
Mean 0.61
Median 0.61
Std Dev. 0.007
Rel.Std.Dev. 1.17%
PDM3 0.00%
Analytical results for Tb in OREAS 605 (Indicative Value 0.19 ppm)

Tb Round Replicate Lab
No No 01
ABL*MS
1 1 0.19
1 2 0.18
Mean 0.19
Median 0.19
Std Dev. 0.007
Rel.Std.Dev. 3.82%
PDM3 0.00%
Analytical results for Te in OREAS 605 (Indicative Value 36.7 ppm)

Te Round Replicate Lab
No No 01
ABL*MS
1 1 36.2
1 2 37.2
Mean 36.7
Median 36.7
Std Dev. 0.7
Rel.Std.Dev. 1.93%
PDM3 0.00%
Analytical results for Th in OREAS 605 (Indicative Value 6.78 ppm)

Th Round Replicate Lab
No No 01
ABL*MS
1 1 6.84
1 2 6.72
Mean 6.78
Median 6.78
Std Dev. 0.085
Rel.Std.Dev. 1.25%
PDM3 0.00%
Analytical results for Ti in OREAS 605 (Indicative Value 0.182 wt.%)
Ti Round Replicate Lab
No No 01
ABL*MS
1 1 0.181
1 2 0.182
Mean 0.182
Median 0.182
Std Dev. 0.001
Rel.Std.Dev. 0.39%
PDM3 0.00%
Analytical results for Tl in OREAS 605 (Indicative Value 16 ppm)

Tl Round Replicate Lab
No No 01
ABL*MS
1 1 16.6
1 2 15.4
Mean 16.0
Median 16.0
Std Dev. 0.8
Rel.Std.Dev. 5.30%
PDM3 0.00%

Tm Round Replicate Lab
No No 01
ABL*MS
1 1 0.040
1 2 0.040
Mean 0.040
Median 0.040
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for U in OREAS 605 (Indicative Value 2.69 ppm)

U Round Replicate Lab
No No 01
ABL*MS
1 1 2.68
1 2 2.69
Mean 2.69
Median 2.69
Std Dev. 0.007
Rel.Std.Dev. 0.26%
PDM3 0.00%
Analytical results for V in OREAS 605 (Indicative Value 39.4 ppm)
V Round Replicate Lab
No No 01
ABL*MS
1 1 39.2
1 2 39.6
Mean 39.4
Median 39.4
Std Dev. 0.3
Rel.Std.Dev. 0.72%
PDM3 0.00%
Analytical results for W in OREAS 605 (Indicative Value 25.8 ppm)

W Round Replicate Lab
No No 01
ABL*MS
1 1 25.9
1 2 25.7
Mean 25.8
Median 25.8
Std Dev. 0.1
Rel.Std.Dev. 0.55%
PDM3 0.00%
Analytical results for Y in OREAS 605 (Indicative Value 4.99 ppm)

Y Round Replicate Lab
No No 01
ABL*MS
1 1 5.20
1 2 4.78
Mean 4.99
Median 4.99
Std Dev. 0.297
Rel.Std.Dev. 5.95%
PDM3 0.00%
Analytical results for Yb in OREAS 605 (Indicative Value 0.42 ppm)

Yb Round Replicate Lab
No No 01
ABL*MS
1 1 0.43
1 2 0.41
Mean 0.42
Median 0.42
Std Dev. 0.014
Rel.Std.Dev. 3.37%
PDM3 0.00%
Analytical results for Zn in OREAS 605 (Indicative Value 2130 ppm)
Zn Round Replicate Lab
No No 01
ABL*MS
1 1 2220
1 2 2040
Mean 2130
Median 2130
Std Dev. 127
Rel.Std.Dev. 5.98%
PDM3 0.00%
Analytical results for Zr in OREAS 605 (Indicative Value 120 ppm)

Zr Round Replicate Lab
No No 01
ABL*MS
1 1 122
1 2 118
Mean 120
Median 120
Std Dev. 3
Rel.Std.Dev. 2.36%
PDM3 0.00%
Indicative
1.00
ppm
0.00
0.00
1
1
16
989
7
Indicative
1.00
ppm
0.00
0.00
1
2
16
1615
8
Indicative
1.00
ppm
0.00
0.00
1
3
16
13150
9
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
0.90
10.00
Indicative
1.00
ppm
1.00
1.00
1.0
5.0
16.0
16.6
11.0
Indicative
1.00
ppm
1.00
1.00
1.0
6.0
16.0
13.9
12.0
Indicative
1.00
ppm
1.00
1.00
1.0
7.0
16.0
31.4
13.0
Indicative
1.00
ppm
0.00
0.00
1
8
16
94
14
Indicative
1.00
ppm
1.00
1.00
1.0
9.0
16.0
35.0
15.0
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
1.61
16.00
Indicative
1.00
ppm
0.00
0.00
1
11
16
47800
17
Indicative
1.00
ppm
2.00
2.00
1.00
12.00
16.00
1.11
18.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.44
19.00
Indicative
1.00
ppm
2.00
2.00
1.00
14.00
16.00
0.38
20.00
Indicative
1.00
ppm
1.00
1.00
1.0
15.0
16.0
31.8
21.0
Indicative
1.00
ppm
2.00
2.00
1.00
16.00
16.00
1.70
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
17.00
16.00
3.40
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
0.20
7.00
Indicative
1.00
ppm
2.00
2.00
1.00
2.00
16.00
3.75
8.00
Indicative
1.00
ppm
1.00
1.00
1.0
3.0
16.0
19.4
9.0
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.050
10.000
Indicative
1.00
wt.%
3.00
3.00
1.000
5.000
16.000
0.009
11.000
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
4.90
12.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
7.22
13.00
Indicative
1.00
ppm
1.00
1.00
1.0
8.0
16.0
12.1
14.0
Indicative
1.00
ppm
0.00
0.00
1
9
16
1415
15
Indicative
1.00
ppm
0.00
0.00
1
10
16
1390
16
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
3.70
17.00
Indicative
1.00
ppm
1.00
1.00
1.0
12.0
16.0
31.6
18.0
Indicative
1.00
ppm
3.00
3.00
1.000
13.000
16.000
0.013
19.000
Indicative
1.00
ppm
0.00
0.00
1
14
16
272
20
Indicative
1.00
ppm
2.00
2.00
1.00
15.00
16.00
4.50
21.00
Indicative
1.00
ppm
2.00
2.00
1.00
16.00
16.00
<5
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
17.00
16.00
1.94
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
3.10
7.00
Indicative
1.00
ppm
0.00
0.00
1
2
16
548
8
Indicative
1.00
ppm
2.00
2.00
1.00
3.00
16.00
0.61
9.00
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
0.19
10.00
Indicative
1.00
ppm
1.00
1.00
1.0
5.0
16.0
36.7
11.0
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
6.78
12.00
Indicative
1.00
wt.%
3.00
3.00
1.000
7.000
16.000
0.182
13.000
Indicative
1.00
ppm
1.00
1.00
1.0
8.0
16.0
16.0
14.0
Indicative
1.00
ppm
3.00
3.00
1.000
9.000
16.000
0.040
15.000
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
2.69
16.00
Indicative
1.00
ppm
1.00
1.00
1.0
11.0
16.0
39.4
17.0
Indicative
1.00
ppm
1.00
1.00
1.0
12.0
16.0
25.8
18.0
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
4.99
19.00
Indicative
1.00
ppm
2.00
2.00
1.00
14.00
16.00
0.42
20.00
Indicative
1.00
ppm
0.00
0.00
1
15
16
2130
21
Indicative
1.00
ppm
0.00
0.00
1
16
16
120
22
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Analytical results for Al2O3 in OREAS 605 (Indicative Value 10.8 wt.%)
Al2O3 Round Replicate Lab
No No 01
BF*XRF
1 1 10.79
1 2 10.80
Mean 10.80
Median 10.80
Std Dev. 0.007
Rel.Std.Dev. 0.07%
PDM3 0.00%
Analytical results for As in OREAS 605 (Indicative Value 1620 ppm)

As Round Replicate Lab
No No 01
BF*XRF
1 1 1610
1 2 1630
Mean 1620
Median 1620
Std Dev. 14
Rel.Std.Dev. 0.87%
PDM3 0.00%

Ba Round Replicate Lab
No No 01
BF*XRF
1 1 13700
1 2 13700
Mean 13700
Median 13700
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for CaO in OREAS 605 (Indicative Value 0.4 wt.%)
CaO Round Replicate Lab
No No 01
BF*XRF
1 1 0.400
1 2 0.400
Mean 0.400
Median 0.400
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Co in OREAS 605 (Indicative Value 110 ppm)
Co Round Replicate Lab
No No 01
BF*XRF
1 1 110
1 2 110
Mean 110
Median 110
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Cr in OREAS 605 (Indicative Value 30 ppm)

Cr Round Replicate Lab
No No 01
BF*XRF
1 1 30.0
1 2 30.0
Mean 30.0
Median 30.0
Std Dev. 0.0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Cu in OREAS 605 (Indicative Value 50850 ppm)

Cu Round Replicate Lab
No No 01
BF*XRF
1 1 50800
1 2 50900
Mean 50850
Median 50850
Std Dev. 71
Rel.Std.Dev. 0.14%
PDM3 0.00%
Analytical results for Fe2O3 in OREAS 605 (Indicative Value 5.54 wt.%)
Fe2O3 Round Replicate Lab
No No 01
BF*XRF
1 1 5.54
1 2 5.53
Mean 5.54
Median 5.54
Std Dev. 0.007
Rel.Std.Dev. 0.13%
PDM3 0.00%
Analytical results for K2O in OREAS 605 (Indicative Value 1.31 wt.%)
K2O Round Replicate Lab
No No 01
BF*XRF
1 1 1.30
1 2 1.31
Mean 1.31
Median 1.31
Std Dev. 0.007
Rel.Std.Dev. 0.54%
PDM3 0.00%
Analytical results for MgO in OREAS 605 (Indicative Value 0.1 wt.%)
MgO Round Replicate Lab
No No 01
BF*XRF
1 1 0.100
1 2 0.100
Mean 0.100
Median 0.100
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for MnO in OREAS 605 (Indicative Value 0.02 wt.%)
MnO Round Replicate Lab
No No 01
BF*XRF
1 1 0.020
1 2 0.020
Mean 0.020
Median 0.020
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Na2O in OREAS 605 (Indicative Value 0.81 wt.%)
Na2O Round Replicate Lab
No No 01
BF*XRF
1 1 0.810
1 2 0.810
Mean 0.810
Median 0.810
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Ni in OREAS 605 (Indicative Value 1515 ppm)

Ni Round Replicate Lab
No No 01
BF*XRF
1 1 1510
1 2 1520
Mean 1515
Median 1515
Std Dev. 7
Rel.Std.Dev. 0.47%
PDM3 0.00%
Analytical results for P2O5 in OREAS 605 (Indicative Value 0.128 wt.%)
P2O5 Round Replicate Lab
No No 01
BF*XRF
1 1 0.127
1 2 0.128
Mean 0.128
Median 0.128
Std Dev. 0.001
Rel.Std.Dev. 0.55%
PDM3 0.00%
Analytical results for Pb in OREAS 605 (Indicative Value 1430 ppm)

Pb Round Replicate Lab
No No 01
BF*XRF
1 1 1420
1 2 1440
Mean 1430
Median 1430
Std Dev. 14
Rel.Std.Dev. 0.99%
PDM3 0.00%
Analytical results for SiO2 in OREAS 605 (Indicative Value 59.57 wt.%)
SiO2 Round Replicate Lab
No No 01
BF*XRF
1 1 59.51
1 2 59.62
Mean 59.57
Median 59.57
Std Dev. 0.078
Rel.Std.Dev. 0.13%
PDM3 0.00%
Analytical results for Sn in OREAS 605 (Indicative Value 12.5 ppm)

Sn Round Replicate Lab
No No 01
BF*XRF
1 1 20.0
1 2 < 10
Mean 20.0
Median 20.0
Std Dev.
Rel.Std.Dev.
PDM3 60.00%
Analytical results for SO3 in OREAS 605 (Indicative Value 21 wt.%)

SO3 Round Replicate Lab
No No 01
BF*XRF
1 1 20.98
1 2 21.02
Mean 21.00
Median 21.00
Std Dev. 0.028
Rel.Std.Dev. 0.13%
PDM3 0.00%
Analytical results for TiO2 in OREAS 605 (Indicative Value 0.303 wt.%)
TiO2 Round Replicate Lab
No No 01
BF*XRF
1 1 0.301
1 2 0.305
Mean 0.303
Median 0.303
Std Dev. 0.003
Rel.Std.Dev. 0.93%
PDM3 0.00%
Analytical results for U in OREAS 605 (Indicative Value 20 ppm)

U Round Replicate Lab
No No 01
BF*XRF
1 1 20.0
1 2 20.0
Mean 20.0
Median 20.0
Std Dev. 0.0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Zn in OREAS 605 (Indicative Value 2080 ppm)

Zn Round Replicate Lab
No No 01
BF*XRF
1 1 2080
1 2 2080
Mean 2080
Median 2080
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Indicative
1.00
wt.%
2.00
2.00
1.00
19.00
16.00
10.80
25.00
Indicative
1.00
ppm
0.00
0.00
1
2
16
1620
26
Indicative
1.00
ppm
0.00
0.00
1
3
16
13700
27
Indicative
1.00
wt.%
3.00
3.00
1.000
22.000
16.000
0.400
28.000
Indicative
1.00
ppm
0.00
0.00
1
8
16
110
29
Indicative
1.00
ppm
1.00
1.00
1.0
9.0
16.0
30.0
30.0
Indicative
1.00
ppm
0.00
0.00
1
11
16
50850
31
Indicative
1.00
wt.%
2.00
2.00
1.00
19.00
16.00
5.54
25.00
Indicative
1.00
wt.%
2.00
2.00
1.00
20.00
16.00
1.31
26.00
Indicative
1.00
wt.%
3.00
3.00
1.000
21.000
16.000
0.100
27.000
Indicative
1.00
wt.%
3.00
3.00
1.000
22.000
16.000
0.020
28.000
Indicative
1.00
wt.%
3.00
3.00
1.000
23.000
16.000
0.810
29.000
Indicative
1.00
ppm
0.00
0.00
1
9
16
1515
30
Indicative
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.128
31.000
Indicative
1.00
ppm
0.00
0.00
1
10
16
1430
25
Indicative
1.00
wt.%
2.00
2.00
1.00
20.00
16.00
59.57
26.00
Indicative
1.00
ppm
1.00
1.00
1.0
1.0
16.0
12.5
27.0
Indicative
1.00
wt.%
2.00
2.00
1.00
22.00
16.00
21.00
28.00
Indicative
1.00
wt.%
3.00
3.00
1.000
23.000
16.000
0.303
29.000
Indicative
1.00
ppm
1.00
1.00
1.0
10.0
16.0
20.0
30.0
Indicative
1.00
ppm
0.00
0.00
1
15
16
2080
31
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Indicative
Analytical results for LOI1000 in OREAS 605 (Indicative Value 11.82 wt.%)
LOI1000 Round Replicate Lab
No No 01
at 1000°C
1 1 11.79
1 2 11.84
Mean 11.82
Median 11.82
Std Dev. 0.035
Rel.Std.Dev. 0.30%
PDM3 0.00%
Indicative
1.00
wt.%
2.00
2.00
1.00
27.00
16.00
11.82
33.00
Indicative
No No 01 02 04 05 06 07
4A*OES 4A*OES 4A*AAS 4A*OES/AAS
4A*OES/AAS
4A*OES/AAS
1 1 1001 980 966 1030 1010 999

1 2 1004 968 984 1030 1000 978
1 3 999 1000 996 1010 1005 987
1 4 1008 950 985 1010 999 985
1 5 1009 966 967 1010 996 977
1 6 999 969 979 1010 983 972
Mean 1003 972 980 1017 999 983
Median 1002 969 982 1010 1000 982
Std Dev. 4 17 12 10 9 10
Rel.Std.Dev. 0.44% 1.72% 1.17% 1.02% 0.92% 0.97%
PDM3 3.21% 0.01% 0.76% 4.59% 2.75% 1.12%
Z-Score (Absolute) 0.95 0.00 0.22 1.35 0.81 0.33
Analytical results for Al in OREAS 605 (Certified Value 5.43 wt.%)

Al Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES
1 1 5.26 5.34 5.28 5.29 5.20 5.20

1 2 5.51 5.40 5.37 5.43 5.14 5.28
1 3 5.47 5.39 5.27 5.35 5.21 5.38
1 4 5.48 5.37 5.34 5.26 5.30 5.24
1 5 5.43 5.31 5.19 5.34 5.34 5.07
1 6 5.45 5.40 5.19 5.52 5.16 5.33
Mean 5.43 5.37 5.27 5.36 5.23 5.25
Median 5.46 5.38 5.28 5.35 5.21 5.26
Std Dev. 0.087 0.035 0.074 0.096 0.079 0.109
Rel.Std.Dev. 1.61% 0.65% 1.41% 1.78% 1.51% 2.07%
PDM3 0.02% -1.11% -2.85% -1.16% -3.74% -3.28%
Z-Score (Absolute) 0.21 0.21 0.62 0.22 0.83 0.73
Analytical results for As in OREAS 605 (Certified Value 1602 ppm)

As Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
4A*OES 4A*MS 4A*OES 4A*OES 4A*OES 4A*OES
1 1 1691 1487 1640 1690 1645 1670

1 2 1684 1519 1660 1700 1625 1700
1 3 1713 1538 1640 1700 1650 1740
1 4 1720 1518 1640 1640 1670 1700
1 5 1695 1547 1590 1665 1685 1630
1 6 1694 1524 1610 1735 1645 1730
Mean 1700 1522 1630 1688 1653 1695
Median 1694 1522 1640 1695 1648 1700
Std Dev. 14 21 25 33 21 40
Rel.Std.Dev. 0.81% 1.36% 1.55% 1.93% 1.28% 2.38%
PDM3 6.09% -4.99% 1.74% 5.38% 3.20% 5.80%
Z-Score (Absolute) 0.62 1.00 0.02 0.52 0.20 0.58
Analytical results for B in OREAS 605 (Indicative Value < 20 ppm)

B Round Replicate Lab
No No 25
PF*OES
1 1 < 20
1 2 < 20
1 3 < 20
1 4 < 20
1 5 < 20
1 6 < 20
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3

Ba Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 05 06 07 08 09
4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS
1 1 3444 1720 30 120 200 9447

1 2 3672 1600 30 120 210 9505
1 3 3513 1470 30 100 200 9537
1 4 3714 1950 30 130 130 9576
1 5 3486 2800 30 130 210 9503
1 6 3791 2770 30 70 200 9563
Mean 3603 2052 30 112 192 9522
Median 3593 1835 30 120 200 9521
Std Dev. 141 590 0 23 31 47
Rel.Std.Dev. 3.92% 28.74% 0.00% 20.75% 15.97% 0.49%
PDM3 -35.16% -63.08% -99.46% -97.99% -96.55% 71.34%
Z-Score (Absolute) 2.74 1.24 0.72 0.63 0.55 8.45
Analytical results for Be in OREAS 605 (Certified Value 0.67 ppm)

Be Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.69 0.63 0.60 0.70 0.70 0.60

1 2 0.72 0.64 0.70 0.70 0.70 0.70
1 3 0.71 0.63 0.60 0.70 0.70 0.70
1 4 0.71 0.65 0.70 0.70 0.70 0.70
1 5 0.71 0.64 0.60 0.70 0.70 0.60
1 6 0.72 0.64 0.70 0.70 0.70 0.70
Mean 0.71 0.64 0.65 0.70 0.70 0.67
Median 0.71 0.64 0.65 0.70 0.70 0.70
Std Dev. 0.009 0.008 0.055 0.000 0.000 0.052
Rel.Std.Dev. 1.28% 1.18% 8.43% 0.00% 0.00% 7.75%
PDM3 4.92% -5.39% -3.66% 3.75% 3.75% -1.19%
Z-Score (Absolute) 0.09 0.71 0.58 0.00 0.00 0.39
Analytical results for Bi in OREAS 605 (Certified Value 16.3 ppm)

Bi Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 16.4 17.8 27.0 15.0 26.0 13.0

1 2 11.4 18.5 28.0 30.0 25.0 13.0
1 3 14.9 17.8 29.0 25.0 27.0 22.0
1 4 11.5 18.2 27.0 18.0 13.0 8.0
1 5 15.1 18.5 28.0 12.0 22.0 26.0
1 6 10.3 18.3 30.0 27.0 28.0 11.0
Mean 13.3 18.2 28.2 21.2 23.5 15.5
Median 13.2 18.3 28.0 21.5 25.5 13.0
Std Dev. 2.5 0.3 1.2 7.2 5.5 6.9
Rel.Std.Dev. 18.83% 1.79% 4.15% 33.99% 23.58% 44.84%
PDM3 -18.53% 11.66% 72.88% 29.92% 44.24% -4.86%
Z-Score (Absolute) 1.55 0.85 5.72 0.51 4.46 0.46
Analytical results for Ca in OREAS 605 (Certified Value 0.276 wt.%)

Ca Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.325 0.272 0.270 0.280 0.290 0.280

1 2 0.365 0.274 0.280 0.290 0.280 0.280
1 3 0.345 0.275 0.270 0.280 0.280 0.280
1 4 0.355 0.273 0.280 0.280 0.290 0.280
1 5 0.320 0.269 0.270 0.290 0.290 0.270
1 6 0.330 0.276 0.270 0.290 0.290 0.280
Mean 0.340 0.273 0.273 0.285 0.287 0.278
Median 0.337 0.273 0.270 0.285 0.290 0.280
Std Dev. 0.018 0.002 0.005 0.005 0.005 0.004
Rel.Std.Dev. 5.26% 0.85% 1.89% 1.92% 1.80% 1.47%
PDM3 22.97% -1.28% -1.14% 3.08% 3.68% 0.66%
Z-Score (Absolute) 6.47 0.31 0.27 0.91 1.08 0.24
Analytical results for Cd in OREAS 605 (Certified Value 12.5 ppm)
Cd Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 29.7 11.8 13.1 13.7 13.4 12.7

1 2 31.3 11.5 13.1 13.7 13.3 12.9
1 3 30.6 11.9 13.1 13.8 13.5 12.9
1 4 30.5 12.0 12.8 13.3 13.5 12.8
1 5 31.0 11.8 13.1 13.4 13.7 12.3
1 6 29.9 12.0 12.8 13.9 13.3 13.0
Mean 30.5 11.8 13.0 13.6 13.5 12.8
Median 30.6 11.9 13.1 13.7 13.5 12.9
Std Dev. 0.608 0.179 0.155 0.234 0.152 0.250
Rel.Std.Dev. 1.99% 1.52% 1.19% 1.71% 1.13% 1.96%
PDM3 143.47% -5.48% 3.82% 8.88% 7.42% 1.96%
Z-Score (Absolute) 17.14 1.00 0.14 0.75 0.57 0.00
Analytical results for Ce in OREAS 605 (Certified Value 21.4 ppm)

Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 12 13 15
4A*MS 4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*MS
1 1 20.9 30.5 20.0 17.3 28.6 32.9

1 2 22.5 30.9 18.0 15.3 28.8 32.1
1 3 22.0 29.9 20.0 15.8 29.2 32.8
1 4 21.3 30.3 21.0 16.0 28.8 32.8
1 5 20.6 30.0 20.0 15.7 29.8 32.7
1 6 20.7 31.3 19.0 15.8 30.4 32.0
Mean 21.3 30.5 19.7 16.0 29.3 32.5
Median 21.1 30.4 20.0 15.8 29.0 32.8
Std Dev. 0.8 0.5 1.0 0.7 0.7 0.4
Rel.Std.Dev. 3.60% 1.70% 5.25% 4.12% 2.42% 1.23%
PDM3 -0.32% 42.48% -8.08% -25.31% 36.78% 52.12%
Z-Score (Absolute) 0.11 2.01 0.50 1.41 1.73 2.49
Analytical results for Co in OREAS 605 (Certified Value 90 ppm)

Co Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 89 87 93 100 95 89
1 2 93 86 95 101 93 91
1 3 91 85 93 100 95 92
1 4 90 89 94 98 95 92
1 5 93 86 93 99 97 88
1 6 92 88 92 102 95 92
Mean 91 87 93 100 95 91
Median 91 87 93 100 95 92
Std Dev. 1.6 1.3 1.0 1.4 1.3 1.8
Rel.Std.Dev. 1.73% 1.54% 1.11% 1.41% 1.33% 1.93%
PDM3 1.34% -3.61% 3.51% 10.90% 5.36% 0.55%
Z-Score (Absolute) 0.11 0.58 0.41 1.45 0.67 0.00
Analytical results for Cr in OREAS 605 (Certified Value 30.4 ppm)

Cr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 32.3 25.0 29.0 30.0 30.0 33.0

1 2 31.9 26.0 31.0 30.0 32.0 29.0
1 3 32.8 26.0 32.0 28.0 31.0 31.0
1 4 33.7 27.0 27.0 35.0 37.0 33.0
1 5 33.7 26.0 29.0 30.0 34.0 30.0
1 6 34.8 32.0 27.0 29.0 33.0 32.0
Mean 33.2 27.0 29.2 30.3 32.8 31.3
Median 33.3 26.0 29.0 30.0 32.5 31.5
Std Dev. 1.1 2.5 2.0 2.4 2.5 1.6
Rel.Std.Dev. 3.27% 9.37% 7.00% 7.99% 7.56% 5.21%
PDM3 9.02% -11.32% -4.21% -0.38% 7.84% 2.91%
Z-Score (Absolute) 0.67 0.93 0.22 0.17 0.59 0.26
Analytical results for Cs in OREAS 605 (Certified Value 1.57 ppm)

Cs Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 12 13 14 15
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*MS
1 1 1.44 1.60 1.87 1.63 1.70 1.62

1 2 1.43 1.60 1.62 1.66 1.60 1.52
1 3 1.45 1.51 1.87 1.55 1.60 1.55
1 4 1.47 1.50 1.67 1.80 1.60 1.51
1 5 1.47 1.59 1.79 1.59 1.60 1.51
1 6 1.54 1.51 1.71 1.75 1.70 1.56
Mean 1.47 1.55 1.76 1.66 1.63 1.55
Median 1.46 1.55 1.75 1.65 1.60 1.54
Std Dev. 0.039 0.048 0.105 0.094 0.052 0.042
Rel.Std.Dev. 2.68% 3.08% 5.98% 5.67% 3.16% 2.74%
PDM3 -6.79% -1.35% 11.53% 5.79% 3.80% -1.81%
Z-Score (Absolute) 0.66 0.03 1.67 0.94 0.69 0.03
Analytical results for Cu in OREAS 605 (Certified Value 5.02 wt.%)

Cu Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 07
4A*OES 4A*OES 4A*AAS 4A*OES/AAS
4A*OES/AAS
4A*OES/AAS
1 1 4.80 5.14 5.10 5.18 5.21 5.03

1 2 4.85 5.25 5.18 5.16 5.17 4.99
1 3 4.80 5.15 5.22 5.05 5.13 5.01
1 4 4.85 5.03 5.25 5.09 5.14 4.95
1 5 4.79 5.15 5.26 5.08 5.14 4.91
1 6 4.83 5.16 5.22 5.08 5.06 4.99
Mean 4.82 5.14 5.21 5.11 5.14 4.98
Median 4.82 5.15 5.22 5.09 5.14 4.99
Std Dev. 0.028 0.067 0.058 0.051 0.050 0.043
Rel.Std.Dev. 0.58% 1.31% 1.12% 1.00% 0.96% 0.87%
PDM3 -3.91% 2.53% 3.75% 1.78% 2.48% -0.74%
Z-Score (Absolute) 1.15 0.97 1.38 0.73 0.96 0.11
Analytical results for Dy in OREAS 605 (Certified Value 1.02 ppm)

Dy Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*OES/MS 4A*MS
1 1 1.02 1.09 0.92 1.03 0.92 1.00

1 2 1.08 1.11 0.94 1.13 0.93 1.00
1 3 1.07 1.06 0.94 1.09 0.91 1.05
1 4 1.02 1.12 0.93 1.16 0.93 1.05
1 5 1.06 1.10 0.95 1.13 0.88 0.95
1 6 1.06 1.12 0.91 1.13 0.92 1.00
Mean 1.05 1.10 0.93 1.11 0.92 1.01
Median 1.06 1.11 0.93 1.13 0.92 1.00
Std Dev. 0.026 0.025 0.017 0.046 0.019 0.038
Rel.Std.Dev. 2.44% 2.26% 1.81% 4.12% 2.04% 3.73%
PDM3 2.86% 7.51% -8.83% 8.73% -10.50% -1.37%
Z-Score (Absolute) 0.17 0.56 0.79 0.79 0.93 0.17
Analytical results for Er in OREAS 605 (Certified Value 0.39 ppm)

Er Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 0.40 0.41 0.11 0.42 0.34 0.35

1 2 0.43 0.44 0.11 0.36 0.37 0.40
1 3 0.42 0.41 0.11 0.40 0.36 0.35
1 4 0.42 0.41 0.12 0.39 0.37 0.35
1 5 0.42 0.41 0.11 0.46 0.35 0.40
1 6 0.40 0.44 0.12 0.36 0.36 0.30
Mean 0.42 0.42 0.11 0.40 0.36 0.36
Median 0.42 0.41 0.11 0.40 0.36 0.35
Std Dev. 0.012 0.016 0.004 0.038 0.012 0.038
Rel.Std.Dev. 2.95% 3.72% 3.46% 9.58% 3.26% 10.50%
PDM3 6.39% 7.78% -71.12% 2.11% -8.14% -8.14%
Z-Score (Absolute) 0.87 1.00 6.32 0.48 0.48 0.48
Analytical results for Eu in OREAS 605 (Indicative Value 0.43 ppm)
Eu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 0.37 0.44 - 0.45 0.79 0.55

1 2 0.37 0.44 - 0.35 1.22 0.60
1 3 0.38 0.41 - 0.42 0.89 0.60
1 4 0.37 0.40 - 0.37 0.96 0.50
1 5 0.35 0.40 - 0.50 1.20 0.50
1 6 0.35 0.44 - 0.37 1.18 0.50
Mean 0.37 0.42 0.41 1.04 0.54
Median 0.37 0.42 0.40 1.07 0.53
Std Dev. 0.012 0.019 0.058 0.184 0.049
Rel.Std.Dev. 3.36% 4.57% 14.05% 17.68% 9.08%
PDM3 -16.00% -3.01% -5.65% 139.34% 24.66%
Z-Score (Absolute) 0.67 0.00 NA 0.14 7.39 1.44
Analytical results for Fe in OREAS 605 (Certified Value 3.76 wt.%)

Fe Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 3.65 3.73 3.73 3.71 3.64 3.60

1 2 3.76 3.81 3.78 3.76 3.59 3.62
1 3 3.67 3.83 3.72 3.74 3.65 3.66
1 4 3.67 3.84 3.75 3.67 3.69 3.60
1 5 3.75 3.76 3.67 3.69 3.72 3.46
1 6 3.73 3.89 3.66 3.84 3.62 3.65
Mean 3.70 3.81 3.72 3.74 3.65 3.60
Median 3.70 3.82 3.73 3.73 3.65 3.61
Std Dev. 0.049 0.058 0.046 0.061 0.047 0.072
Rel.Std.Dev. 1.31% 1.51% 1.24% 1.63% 1.29% 2.01%
PDM3 -1.42% 1.37% -1.06% -0.62% -2.84% -4.26%
Z-Score (Absolute) 0.09 0.24 0.05 0.00 0.26 0.34
Analytical results for Ga in OREAS 605 (Certified Value 30.3 ppm)

Ga Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 33.3 29.6 30.0 30.0 30.0 30.0

1 2 33.5 30.7 30.0 30.0 30.0 30.0
1 3 33.2 30.9 30.0 30.0 30.0 30.0
1 4 33.5 30.8 30.0 30.0 30.0 30.0
1 5 33.0 29.6 30.0 30.0 30.0 30.0
1 6 33.3 30.5 30.0 30.0 30.0 30.0
Mean 33.3 30.3 30.0 30.0 30.0 30.0
Median 33.3 30.6 30.0 30.0 30.0 30.0
Std Dev. 0.166 0.595 0.000 0.000 0.000 0.000
Rel.Std.Dev. 0.50% 1.96% 0.00% 0.00% 0.00% 0.00%
PDM3 9.88% 0.00% -1.03% -1.03% -1.03% -1.03%
Z-Score (Absolute) 0.98 0.05 0.05 0.05 0.05 0.05
Analytical results for Gd in OREAS 605 (Certified Value 1.6 ppm)

Gd Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 1.61 2.31 1.55 1.70 1.53 1.40

1 2 1.63 2.24 1.62 1.73 1.56 1.40
1 3 1.62 2.19 1.61 1.73 1.54 1.60
1 4 1.66 2.11 1.69 1.69 1.60 1.60
1 5 1.57 2.10 1.54 1.85 1.50 1.60
1 6 1.57 2.16 1.69 1.76 1.59 1.40
Mean 1.61 2.19 1.62 1.74 1.55 1.50
Median 1.62 2.18 1.61 1.73 1.55 1.50
Std Dev. 0.035 0.081 0.066 0.058 0.038 0.110
Rel.Std.Dev. 2.19% 3.71% 4.09% 3.32% 2.43% 7.30%
PDM3 0.61% 36.67% 0.97% 8.94% -2.93% -6.26%
Z-Score (Absolute) 0.02 4.59 0.02 0.87 0.48 0.90
Analytical results for Ge in OREAS 605 (Certified Value < 5 ppm)

Ge Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 12 14 15
4A*MS 4A*OES/MS 4A*OES 4A*MS 4A*MS 4A*MS
1 1 2.84 3.93 < 10 2.31 3.60 1.72

1 2 2.85 3.99 < 10 2.02 3.90 1.88
1 3 2.89 3.89 < 10 1.71 3.90 2.01
1 4 2.95 3.81 < 10 1.95 3.50 1.97
1 5 2.93 3.91 < 10 2.22 3.70 2.18
1 6 2.76 3.96 < 10 1.93 3.70 1.96
Mean 2.87 3.91 2.02 3.72 1.95
Median 2.87 3.92 1.98 3.70 1.96
Std Dev. 0.069 0.062 0.216 0.160 0.151
Rel.Std.Dev. 2.40% 1.60% 10.67% 4.31% 7.76%
PDM3
Analytical results for Hf in OREAS 605 (Certified Value 2.58 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 12 13 14 15
1 1 2.73 2.78 2.50 2.44 2.80 2.53

1 2 2.76 2.62 2.20 2.45 2.80 2.64
1 3 2.71 2.67 2.50 2.43 3.00 2.56
1 4 2.84 2.55 2.20 2.55 2.80 2.57
1 5 2.71 2.54 2.30 2.40 2.90 2.59
1 6 2.79 2.73 2.30 2.35 2.90 2.55
Mean 2.76 2.65 2.33 2.44 2.87 2.57
Median 2.75 2.65 2.30 2.44 2.85 2.57
Std Dev. 0.051 0.097 0.137 0.067 0.082 0.038
Rel.Std.Dev. 1.86% 3.67% 5.86% 2.73% 2.85% 1.49%
PDM3 6.75% 2.53% -9.64% -5.60% 11.01% -0.35%
Z-Score (Absolute) 1.06 0.44 1.35 0.75 1.69 0.02
Analytical results for Hg in OREAS 605 (Indicative Value < 1 ppm)

Hg Round Replicate Lab
No No 11
4A*OES
1 1 <1
1 2 <1
1 3 <1
1 4 1.00
1 5 <1
1 6 <1
Mean 1.00
Median 1.00
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Ho in OREAS 605 (Certified Value 0.15 ppm)

Ho Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 0.17 0.18 0.11 0.18 0.13 0.14

1 2 0.18 0.17 0.11 0.19 0.15 0.14
1 3 0.18 0.16 0.11 0.17 0.13 0.14
1 4 0.18 0.15 0.12 0.19 0.14 0.14
1 5 0.17 0.18 0.10 0.15 0.13 0.14
1 6 0.18 0.17 0.11 0.18 0.14 0.14
Mean 0.18 0.17 0.11 0.18 0.14 0.14
Median 0.18 0.17 0.11 0.18 0.14 0.14
Std Dev. 0.005 0.009 0.005 0.015 0.008 0.000
Rel.Std.Dev. 2.92% 5.45% 4.64% 8.52% 5.97% 0.00%
PDM3 16.68% 11.73% -27.80% 16.68% -9.74% -7.54%
Z-Score (Absolute) 0.74 0.49 1.53 0.74 0.60 0.49
Analytical results for In in OREAS 605 (Certified Value 3.78 ppm)
In Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
4A*OES 4A*MS 4A*OES/MS 4A*OES 4A*MS 4A*MS
1 1 <5 3.57 3.98 < 10 4.25 3.57

1 2 <5 3.60 4.00 < 10 3.76 3.52
1 3 <5 3.55 3.88 < 10 4.29 3.75
1 4 <5 3.61 3.99 < 10 3.88 3.68
1 5 <5 3.68 3.80 < 10 4.16 3.51
1 6 <5 3.56 4.01 < 10 4.03 3.62
Mean 3.59 3.94 4.06 3.61
Median 3.59 3.99 4.10 3.60
Std Dev. 0.048 0.086 0.211 0.096
Rel.Std.Dev. 1.33% 2.17% 5.19% 2.65%
PDM3 -5.01% 4.22% 7.32% -4.71%
Analytical results for K in OREAS 605 (Certified Value 1.04 wt.%)

K Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.97 1.03 1.00 1.07 1.00 0.98

1 2 1.02 1.07 1.02 1.10 0.99 1.00
1 3 1.02 1.08 1.00 1.07 1.00 1.02
1 4 1.03 1.08 1.02 1.06 1.01 1.01
1 5 1.00 1.06 0.98 1.08 1.01 0.97
1 6 1.01 1.10 0.98 1.11 1.00 0.99
Mean 1.01 1.07 1.00 1.08 1.00 1.00
Median 1.01 1.07 1.00 1.08 1.00 0.99
Std Dev. 0.019 0.021 0.018 0.019 0.008 0.019
Rel.Std.Dev. 1.91% 2.00% 1.79% 1.79% 0.75% 1.88%
PDM3 -3.27% 2.94% -3.75% 4.11% -3.59% -4.23%
Z-Score (Absolute) 0.65 0.46 0.88 0.69 0.85 0.98
Analytical results for La in OREAS 605 (Certified Value < 20 ppm)

La Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 16.3 13.2 10.0 10.0 10.0 10.0

1 2 16.1 14.2 10.0 10.0 10.0 10.0
1 3 16.1 13.9 10.0 10.0 10.0 10.0
1 4 16.0 14.4 10.0 10.0 10.0 10.0
1 5 16.0 14.4 10.0 10.0 10.0 10.0
1 6 16.5 14.7 10.0 10.0 10.0 10.0
Mean 16.2 14.1 10.0 10.0 10.0 10.0
Median 16.1 14.3 10.0 10.0 10.0 10.0
Std Dev. 0.2 0.5 0.0 0.0 0.0 0.0
Rel.Std.Dev. 1.09% 3.73% 0.00% 0.00% 0.00% 0.00%
PDM3
Z-Score (Absolute) 1.18 0.79 0.00 0.00 0.00 0.00
Analytical results for Li in OREAS 605 (Certified Value 21.7 ppm)

Li Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
4A*OES 4A*MS 4A*OES/MS 4A*OES 4A*MS 4A*OES
1 1 19.8 20.8 26.4 23.0 20.3 24.3

1 2 20.8 20.9 25.7 22.0 16.8 24.8
1 3 20.4 20.8 25.9 23.0 22.9 24.6
1 4 21.6 20.0 26.1 23.0 19.7 24.3
1 5 21.1 20.9 26.6 24.0 17.3 24.7
1 6 20.6 20.7 26.9 23.0 16.3 24.7
Mean 20.7 20.7 26.3 23.0 18.9 24.6
Median 20.7 20.8 26.3 23.0 18.5 24.7
Std Dev. 0.594 0.343 0.454 0.632 2.543 0.214
Rel.Std.Dev. 2.87% 1.66% 1.73% 2.75% 13.47% 0.87%
PDM3 -4.73% -4.88% 20.87% 5.78% -13.16% 13.02%
Z-Score (Absolute) 0.60 0.55 1.99 0.47 1.45 1.20
Analytical results for Lu in OREAS 605 (Certified Value 54 ppb)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 15 17 19 25
4A*MS 4A*OES/MS 4A*MS 4A*OES/MS4A*OES/MS 4A*MS
1 1 50 61 < 100 50 58 60
1 2 50 50 < 100 50 59 80
1 3 50 59 < 100 50 57 60
1 4 50 54 < 100 50 52 60
1 5 50 46 < 100 50 61 60
1 6 50 56 < 100 50 57 60
Mean 50 55 50 57 63
Median 50 55 50 58 60
Std Dev. 0 6 0 3 8
Rel.Std.Dev. 0.00% 10.40% 0.00% 5.25% 12.89%
PDM3 -8.06% 0.36% -8.06% 5.43% 16.46%
Analytical results for Mg in OREAS 605 (Certified Value 476 ppm)

Mg Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 415 479 400 500 400 400

1 2 458 467 400 500 400 400
1 3 462 474 400 500 400 400
1 4 438 464 400 500 400 400
1 5 458 455 400 500 500 400
1 6 458 478 400 500 400 400
Mean 448 470 400 500 417 400
Median 458 471 400 500 400 400
Std Dev. 18 9 0 0 41 0
Rel.Std.Dev. 4.05% 1.97% 0.00% 0.00% 9.80% 0.00%
PDM3 -5.81% -1.26% -15.88% 5.15% -12.37% -15.88%
Z-Score (Absolute) 1.04 0.70 2.29 0.00 1.91 2.29
Analytical results for Mn in OREAS 605 (Certified Value 91 ppm)

Mn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 87 86 98 97 94 89
1 2 90 91 95 97 93 90
1 3 88 91 91 97 94 88
1 4 88 89 94 96 94 91
1 5 90 86 90 98 94 86
1 6 89 92 90 100 92 88
Mean 88 89 93 98 94 89
Median 88 90 93 97 94 89
Std Dev. 1.4 2.6 3.2 1.4 0.8 1.8
Rel.Std.Dev. 1.53% 2.96% 3.47% 1.41% 0.89% 1.98%
PDM3 -3.25% -2.46% 1.73% 6.65% 2.28% -3.01%
Z-Score (Absolute) 0.67 0.54 0.19 0.95 0.28 0.63
Analytical results for Mo in OREAS 605 (Certified Value 4.82 ppm)

Mo Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 6.07 4.30 4.00 5.00 3.00 4.00

1 2 6.17 4.30 4.00 5.00 3.00 5.00
1 3 6.17 4.30 4.00 5.00 4.00 4.00
1 4 6.39 4.40 4.00 5.00 4.00 5.00
1 5 5.95 4.00 4.00 5.00 4.00 4.00
1 6 6.42 4.50 4.00 5.00 4.00 5.00
Mean 6.19 4.30 4.00 5.00 3.67 4.50
Median 6.17 4.30 4.00 5.00 4.00 4.50
Std Dev. 0.180 0.167 0.000 0.000 0.516 0.548
Rel.Std.Dev. 2.90% 3.89% 0.00% 0.00% 14.08% 12.17%
PDM3 28.44% -10.84% -17.06% 3.68% -23.97% -6.69%
Z-Score (Absolute) 2.00 0.97 1.44 0.13 1.96 0.65
Analytical results for Na in OREAS 605 (Certified Value 0.58 wt.%)
Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.547 0.577 0.560 0.600 0.560 0.560

1 2 0.570 0.584 0.570 0.630 0.550 0.570
1 3 0.581 0.580 0.560 0.600 0.560 0.580
1 4 0.570 0.578 0.580 0.610 0.560 0.580
1 5 0.573 0.589 0.550 0.600 0.570 0.550
1 6 0.567 0.577 0.550 0.620 0.550 0.570
Mean 0.568 0.581 0.562 0.610 0.558 0.568
Median 0.570 0.579 0.560 0.605 0.560 0.570
Std Dev. 0.012 0.005 0.012 0.013 0.008 0.012
Rel.Std.Dev. 2.03% 0.86% 2.08% 2.07% 1.35% 2.06%
PDM3 -2.15% 0.04% -3.24% 5.09% -3.81% -2.09%
Z-Score (Absolute) 0.33 0.00 0.74 1.14 0.87 0.48
Analytical results for Nb in OREAS 605 (Certified Value 6.92 ppm)

Nb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 14
1 1 5.93 7.01 6.97 < 10 4.50 7.00

1 2 6.15 6.66 6.99 < 10 4.00 7.10
1 3 5.97 6.63 6.99 < 10 3.00 7.00
1 4 5.94 6.91 7.05 < 10 5.10 7.00
1 5 6.15 6.64 7.08 < 10 4.70 7.00
1 6 6.14 6.84 7.00 < 10 4.90 7.00
Mean 6.04 6.78 7.01 4.37 7.02
Median 6.05 6.75 7.00 4.60 7.00
Std Dev. 0.111 0.161 0.040 0.769 0.041
Rel.Std.Dev. 1.83% 2.38% 0.57% 17.60% 0.58%
PDM3 -12.61% -1.93% 1.41% -36.85% 1.47%
Z-Score (Absolute) 3.93 0.61 0.43 NA 11.47 0.45
Analytical results for Nd in OREAS 605 (Certified Value 10.7 ppm)

Nd Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 9.9 13.0 10.2 12.3 9.0 10.2

1 2 9.8 12.6 10.7 12.4 8.5 11.1
1 3 9.7 12.6 11.0 12.9 8.2 10.6
1 4 9.6 12.5 10.2 12.4 8.4 10.4
1 5 9.2 12.2 10.5 12.7 7.3 10.6
1 6 9.7 12.9 10.7 11.9 6.8 10.3
Mean 9.6 12.6 10.6 12.4 8.0 10.5
Median 9.7 12.6 10.6 12.4 8.3 10.5
Std Dev. 0.2 0.3 0.3 0.3 0.8 0.3
Rel.Std.Dev. 2.50% 2.07% 2.95% 2.75% 10.22% 3.04%
PDM3 -9.51% 18.59% -0.86% 16.69% -24.62% -1.16%
Z-Score (Absolute) 0.41 1.04 0.01 0.94 1.26 0.01
Analytical results for Ni in OREAS 605 (Certified Value 1522 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 1668 1582 1525 1530 1550 1490

1 2 1644 1585 1550 1560 1520 1520
1 3 1686 1601 1525 1550 1560 1540
1 4 1672 1595 1525 1510 1570 1520
1 5 1635 1542 1490 1520 1590 1450
1 6 1631 1588 1500 1570 1540 1530
Mean 1656 1582 1519 1540 1555 1508
Median 1656 1586 1525 1540 1555 1520
Std Dev. 23 21 21 24 24 33
Rel.Std.Dev. 1.36% 1.31% 1.40% 1.54% 1.56% 2.20%
PDM3 8.84% 3.99% -0.16% 1.21% 2.19% -0.87%
Z-Score (Absolute) 2.58 1.19 0.00 0.39 0.67 0.02
Analytical results for P in OREAS 605 (Certified Value 507 ppm)

P Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 496 1335 500 510 500 490

1 2 498 1850 510 510 500 490
1 3 504 1659 500 520 510 500
1 4 505 1208 510 500 520 520
1 5 507 1445 490 510 520 480
1 6 500 1802 500 530 510 500
Mean 502 1550 502 513 510 497
Median 502 1552 500 510 510 495
Std Dev. 4 261 8 10 9 14
Rel.Std.Dev. 0.82% 16.82% 1.50% 2.01% 1.75% 2.75%
PDM3 -1.10% 205.48% -1.12% 1.18% 0.52% -2.11%
Z-Score (Absolute) 0.21 21.67 0.21 0.03 0.03 0.31
Analytical results for Pb in OREAS 605 (Certified Value 1297 ppm)

Pb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 1043 1273 1420 1440 1420 1400

1 2 1064 1296 1430 1470 1395 1415
1 3 1046 1317 1405 1450 1420 1435
1 4 1036 1319 1420 1420 1430 1415
1 5 1051 1270 1405 1420 1440 1365
1 6 1086 1296 1400 1490 1405 1435
Mean 1055 1295 1413 1448 1418 1411
Median 1049 1296 1413 1445 1420 1415
Std Dev. 18 21 12 28 16 26
Rel.Std.Dev. 1.72% 1.61% 0.83% 1.92% 1.15% 1.85%
PDM3 -18.67% -0.11% 9.00% 11.70% 9.39% 8.81%
Z-Score (Absolute) 1.83 0.15 0.67 0.92 0.71 0.66
Analytical results for Pr in OREAS 605 (Certified Value 2.97 ppm)

Pr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 2.32 3.34 2.88 3.51 2.62 2.52

1 2 2.73 3.41 3.06 3.44 3.00 2.84
1 3 2.69 3.23 3.15 3.55 2.72 2.62
1 4 2.63 3.26 3.02 3.58 2.86 2.62
1 5 2.51 3.34 2.93 3.59 2.83 2.68
1 6 2.33 3.36 2.83 3.51 2.93 2.56
Mean 2.54 3.32 2.98 3.53 2.83 2.64
Median 2.57 3.34 2.98 3.53 2.84 2.62
Std Dev. 0.179 0.067 0.118 0.055 0.139 0.112
Rel.Std.Dev. 7.06% 2.02% 3.96% 1.57% 4.90% 4.26%
PDM3 -14.72% 11.84% 0.23% 18.75% -4.91% -11.19%
Z-Score (Absolute) 0.79 0.90 0.16 1.34 0.16 0.56
Analytical results for Rb in OREAS 605 (Certified Value 29.2 ppm)

Rb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 12 13 14 15
1 1 26.5 31.4 35.0 30.6 31.1 31.6

1 2 26.9 31.1 30.9 30.3 31.0 30.2
1 3 26.5 31.3 34.0 30.4 30.0 30.0
1 4 26.9 31.4 31.6 30.8 30.2 29.6
1 5 26.3 31.6 33.9 30.2 30.4 29.4
1 6 26.6 30.8 33.0 31.1 30.6 29.9
Mean 26.6 31.3 33.1 30.6 30.6 30.1
Median 26.5 31.3 33.5 30.5 30.5 30.0
Std Dev. 0.3 0.3 1.6 0.3 0.4 0.8
Rel.Std.Dev. 0.96% 0.93% 4.71% 1.06% 1.43% 2.55%
PDM3 -8.99% 6.94% 13.12% 4.53% 4.51% 3.04%
Z-Score (Absolute) 0.92 0.28 0.74 0.09 0.09 0.09
Analytical results for Re in OREAS 605 (Indicative Value 2 ppb)
Re Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 12 14 15
1 1 2 2 < 5000 4 < 50 10

1 2 2 <2 < 5000 2 < 50 20
1 3 <2 2 < 5000 3 < 50 20
1 4 2 3 < 5000 3 < 50 10
1 5 2 <2 < 5000 4 < 50 10
1 6 4 <2 < 5000 3 < 50 20
Mean 2 2 3 15
Median 2 2 3 15
Std Dev. 1 1 1 5
Rel.Std.Dev. 37.27% 29.59% 23.77% 36.51%
PDM3 10.16% -1.83% 45.35% 588.48%
Z-Score (Absolute) 0.58 0.77 NA 0.58 NA 10.57

No No 01 02 05 06 07 08
1 1 8.87 7.80 8.42 8.59 8.35 8.09

1 2 8.85 7.99 8.58 8.73 8.29 8.30
1 3 8.69 8.00 8.39 8.64 8.44 8.44
1 4 8.73 7.89 8.45 8.50 8.50 8.29
1 5 8.85 8.02 8.36 8.55 8.55 7.98
1 6 8.82 8.06 8.31 8.92 8.33 8.41
Mean 8.80 7.96 8.42 8.66 8.41 8.25
Median 8.83 7.99 8.41 8.62 8.40 8.30
Std Dev. 0.074 0.097 0.093 0.152 0.103 0.181
Rel.Std.Dev. 0.84% 1.22% 1.10% 1.75% 1.22% 2.20%
PDM3 5.55% -4.51% 0.99% 3.83% 0.89% -1.01%
Z-Score (Absolute) 0.72 0.83 0.02 0.45 0.00 0.29
Analytical results for Sb in OREAS 605 (Certified Value 294 ppm)

Sb Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 277 258 310 317 305 296

1 2 283 231 312 315 307 299
1 3 290 247 314 313 315 303
1 4 289 258 314 307 311 303
1 5 282 260 313 311 316 286
1 6 289 285 300 321 307 299
Mean 285 257 311 314 310 298
Median 286 258 313 314 309 299
Std Dev. 5 18 5 5 5 6
Rel.Std.Dev. 1.77% 6.84% 1.73% 1.55% 1.48% 2.12%
PDM3 -3.04% -12.68% 5.67% 6.86% 5.55% 1.30%
Z-Score (Absolute) 0.24 1.52 1.29 1.37 1.16 0.60
Analytical results for Sc in OREAS 605 (Certified Value 5.03 ppm)

Sc Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 3.60 3.90 5.00 6.00 5.00 5.00

1 2 4.24 4.10 5.00 6.00 5.00 5.00
1 3 4.16 4.00 5.00 6.00 5.00 5.00
1 4 4.10 4.00 5.00 5.00 5.00 5.00
1 5 4.13 4.10 5.00 6.00 5.00 5.00
1 6 4.32 4.40 5.00 6.00 5.00 5.00
Mean 4.09 4.08 5.00 5.83 5.00 5.00
Median 4.14 4.05 5.00 6.00 5.00 5.00
Std Dev. 0.254 0.172 0.000 0.408 0.000 0.000
Rel.Std.Dev. 6.21% 4.22% 0.00% 7.00% 0.00% 0.00%
PDM3 -18.73% -18.86% -0.64% 15.92% -0.64% -0.64%
Z-Score (Absolute) 0.96 1.16 0.00 0.98 0.00 0.00
Analytical results for Se in OREAS 605 (Certified Value 76 ppm)

Se Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 14
1 1 81 73 75 55 83 73
1 2 80 73 75 57 72 74
1 3 80 75 75 54 82 77
1 4 81 75 75 51 77 78
1 5 81 72 74 53 86 74
1 6 81 75 75 56 81 77
Mean 81 74 75 54 80 76
Median 81 74 75 55 82 76
Std Dev. 0.4 1.3 0.4 2.2 5.0 2.1
Rel.Std.Dev. 0.53% 1.72% 0.52% 3.98% 6.18% 2.75%
PDM3 5.62% -3.18% -1.80% -28.88% 4.93% -1.18%
Z-Score (Absolute) 0.75 0.22 0.07 3.06 0.67 0.00
Analytical results for Sm in OREAS 605 (Certified Value 2.09 ppm)

Sm Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 2.08 2.19 1.99 2.24 1.60 1.80

1 2 2.15 2.35 1.95 2.23 1.50 2.05
1 3 2.06 2.31 1.95 2.02 1.50 1.95
1 4 2.10 2.28 2.00 1.99 1.60 1.95
1 5 2.20 2.19 1.99 2.29 1.40 2.00
1 6 2.13 2.14 2.00 2.15 1.30 1.85
Mean 2.12 2.24 1.98 2.15 1.48 1.93
Median 2.12 2.24 1.99 2.19 1.50 1.95
Std Dev. 0.051 0.083 0.024 0.124 0.117 0.093
Rel.Std.Dev. 2.41% 3.69% 1.19% 5.75% 7.88% 4.82%
PDM3 1.62% 7.46% -4.96% 3.21% -28.90% -7.33%
Z-Score (Absolute) 0.42 1.17 0.42 0.62 3.48 0.72
Analytical results for Sn in OREAS 605 (Certified Value 2.73 ppm)

Sn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 14
1 1 <5 2.70 2.89 < 10 2.80 2.90

1 2 <5 2.80 3.01 < 10 2.50 2.80
1 3 <5 2.70 2.72 < 10 2.70 2.90
1 4 <5 2.80 2.72 < 10 2.50 2.90
1 5 <5 2.90 2.83 < 10 2.50 3.00
1 6 <5 2.90 2.79 < 10 2.40 2.80
Mean 2.80 2.83 2.57 2.88
Median 2.80 2.81 2.50 2.90
Std Dev. 0.089 0.112 0.151 0.075
Rel.Std.Dev. 3.19% 3.95% 5.87% 2.61%
PDM3 2.69% 3.70% -5.87% 5.75%
Analytical results for Sr in OREAS 605 (Certified Value 373 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 497 286 372 326 362 337

1 2 514 341 386 331 377 356
1 3 493 329 371 319 358 349
1 4 520 315 380 339 339 347
1 5 507 323 380 321 370 341
1 6 526 296 367 330 360 339
Mean 510 315 376 328 361 345
Median 510 319 376 328 361 344
Std Dev. 13 21 7 7 13 7
Rel.Std.Dev. 2.54% 6.54% 1.90% 2.23% 3.57% 2.08%
PDM3 36.53% -15.63% 0.76% -12.19% -3.26% -7.59%
Z-Score (Absolute) 1.91 0.63 0.17 0.46 0.03 0.24
Analytical results for Ta in OREAS 605 (Certified Value < 1 ppm)
Ta Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 12 14 15 17
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*OES/MS
1 1 0.69 0.51 0.24 0.55 0.76 1.15

1 2 0.59 0.52 0.19 0.55 0.74 0.80
1 3 0.63 0.49 0.15 0.54 0.74 0.47
1 4 0.71 0.48 0.26 0.55 0.72 0.46
1 5 0.65 0.49 0.22 0.54 0.73 0.95
1 6 0.67 0.48 0.26 0.54 0.72 0.66
Mean 0.66 0.50 0.22 0.55 0.74 0.75
Median 0.66 0.49 0.23 0.55 0.74 0.73
Std Dev. 0.043 0.015 0.043 0.005 0.015 0.273
Rel.Std.Dev. 6.58% 2.94% 19.71% 1.00% 2.06% 36.50%
PDM3
Z-Score (Absolute) 0.67 0.29 1.96 0.00 1.15 0.74
Analytical results for Tb in OREAS 605 (Certified Value 0.2 ppm)

Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 19
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*OES/MS4A*OES/MS
1 1 0.20 0.24 0.16 0.22 0.20 0.20

1 2 0.21 0.26 0.18 0.23 0.21 0.20
1 3 0.21 0.24 0.17 0.21 0.20 0.19
1 4 0.21 0.23 0.17 0.24 0.21 0.19
1 5 0.20 0.25 0.17 0.21 0.20 0.20
1 6 0.20 0.25 0.18 0.21 0.21 0.20
Mean 0.21 0.24 0.17 0.22 0.21 0.20
Median 0.21 0.24 0.17 0.22 0.21 0.20
Std Dev. 0.005 0.010 0.008 0.013 0.005 0.004
Rel.Std.Dev. 2.67% 4.09% 4.51% 5.75% 2.67% 2.07%
PDM3 0.85% 20.04% -16.35% 8.23% 0.85% -3.82%
Z-Score (Absolute) 0.00 1.75 1.57 0.67 0.00 0.43
Analytical results for Te in OREAS 605 (Certified Value 31.8 ppm)

Te Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 12 13 14
1 1 35.8 32.1 30.0 19.7 14.5 33.0

1 2 35.3 32.0 27.0 14.4 15.3 33.1
1 3 35.7 31.6 27.0 15.3 14.8 35.1
1 4 34.4 31.6 29.0 12.9 15.1 33.2
1 5 33.7 32.2 32.0 14.1 15.0 31.7
1 6 34.2 32.7 34.0 16.1 15.2 33.6
Mean 34.8 32.0 29.8 15.4 15.0 33.3
Median 34.8 32.0 29.5 14.8 15.1 33.2
Std Dev. 0.9 0.4 2.8 2.4 0.3 1.1
Rel.Std.Dev. 2.49% 1.23% 9.34% 15.43% 1.92% 3.30%
PDM3 9.59% 0.71% -6.19% -51.53% -52.81% 4.66%
Z-Score (Absolute) 0.67 0.18 0.20 2.88 2.80 0.40
Analytical results for Th in OREAS 605 (Certified Value 5.12 ppm)

Th Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 05 06 07 08 09
4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS
1 1 4.25 < 20 < 20 < 20 < 20 5.99

1 2 4.60 < 20 < 20 < 20 < 20 5.85
1 3 4.77 < 20 < 20 < 20 < 20 5.62
1 4 4.65 < 20 < 20 < 20 < 20 5.80
1 5 4.35 < 20 < 20 < 20 < 20 5.68
1 6 4.52 < 20 < 20 < 20 < 20 5.78
Mean 4.52 5.79
Median 4.56 5.79
Std Dev. 0.194 0.130
Rel.Std.Dev. 4.28% 2.25%
PDM3 -11.58% 13.10%
Z-Score (Absolute) 0.01 NA NA NA NA 1.38
Analytical results for Ti in OREAS 605 (Certified Value 0.177 wt.%)

Ti Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.170 0.182 0.180 0.180 0.180 0.180

1 2 0.170 0.178 0.180 0.190 0.180 0.180
1 3 0.165 0.180 0.180 0.190 0.180 0.180
1 4 0.175 0.180 0.180 0.180 0.180 0.180
1 5 0.170 0.176 0.180 0.180 0.180 0.170
1 6 0.170 0.181 0.170 0.190 0.180 0.170
Mean 0.170 0.180 0.178 0.185 0.180 0.177
Median 0.170 0.180 0.180 0.185 0.180 0.180
Std Dev. 0.003 0.002 0.004 0.005 0.000 0.005
Rel.Std.Dev. 1.86% 1.30% 2.29% 2.96% 0.00% 2.92%
PDM3 -3.81% 1.63% 0.91% 4.68% 1.85% -0.03%
Z-Score (Absolute) 0.53 0.28 0.17 0.73 0.31 0.03
Analytical results for Tl in OREAS 605 (Certified Value 15 ppm)

Tl Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
1 1 13.3 16.4 15.0 14.0 17.0 12.6

1 2 14.3 16.7 15.2 13.0 14.6 12.6
1 3 13.8 16.1 14.6 13.0 16.5 13.4
1 4 13.0 16.6 14.7 13.0 15.2 13.7
1 5 13.8 17.1 15.1 14.0 16.2 12.9
1 6 14.2 16.7 15.1 12.0 15.6 13.8
Mean 13.7 16.6 15.0 13.2 15.8 13.2
Median 13.8 16.6 15.1 13.0 15.9 13.1
Std Dev. 0.494 0.319 0.224 0.753 0.876 0.537
Rel.Std.Dev. 3.60% 1.92% 1.50% 5.72% 5.53% 4.08%
PDM3 -8.29% 10.81% -0.01% -12.05% 5.86% -12.09%
Z-Score (Absolute) 1.25 1.21 0.19 1.74 0.57 1.74

Tm Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 25
1 1 0.050 0.054 11.810 < 0.1 < 0.05 0.060

1 2 0.050 0.053 12.265 < 0.1 < 0.05 0.060
1 3 0.060 0.050 13.009 < 0.1 < 0.05 0.040
1 4 0.050 0.049 12.331 < 0.1 < 0.05 0.040
1 5 0.050 0.063 12.511 < 0.1 < 0.05 0.060
1 6 0.060 0.050 12.352 < 0.1 < 0.05 0.040
Mean 0.053 0.053 12.380 0.050
Median 0.050 0.052 12.342 0.050
Std Dev. 0.005 0.005 0.388 0.011
Rel.Std.Dev. 9.68% 9.43% 3.14% 21.91%
PDM3 3.46% 3.23% 23916.24% -3.00%
Z-Score (Absolute) 0.41 0.41 4987.51 NA NA 0.94
Analytical results for U in OREAS 605 (Certified Value 2.79 ppm)

U Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 11 12 13 14
1 1 2.81 2.69 < 10 3.20 2.88 2.73

1 2 2.87 2.68 < 10 2.70 2.89 2.74
1 3 2.89 2.62 < 10 3.00 2.97 2.77
1 4 2.78 2.59 < 10 2.80 2.96 2.69
1 5 2.83 2.65 < 10 3.00 2.96 2.73
1 6 2.83 2.72 < 10 3.00 3.01 2.73
Mean 2.83 2.66 2.95 2.95 2.73
Median 2.83 2.66 3.00 2.96 2.73
Std Dev. 0.040 0.048 0.176 0.049 0.026
Rel.Std.Dev. 1.41% 1.82% 5.97% 1.67% 0.94%
PDM3 1.44% -4.88% 5.55% 5.39% -2.26%
Analytical results for V in OREAS 605 (Certified Value 39.9 ppm)
V Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 41.6 38.0 38.0 42.0 39.0 38.0

1 2 43.1 38.0 39.0 43.0 39.0 38.0
1 3 42.1 39.0 38.0 42.0 40.0 39.0
1 4 41.9 38.0 38.0 40.0 40.0 39.0
1 5 42.9 37.0 38.0 41.0 40.0 37.0
1 6 42.0 38.0 37.0 43.0 39.0 39.0
Mean 42.3 38.0 38.0 41.8 39.5 38.3
Median 42.1 38.0 38.0 42.0 39.5 38.5
Std Dev. 0.597 0.632 0.632 1.169 0.548 0.816
Rel.Std.Dev. 1.41% 1.66% 1.66% 2.79% 1.39% 2.13%
PDM3 5.93% -4.74% -4.74% 4.87% -0.98% -3.90%
Z-Score (Absolute) 1.25 0.75 0.75 1.05 0.05 0.60
Analytical results for W in OREAS 605 (Certified Value 27 ppm)

W Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
1 1 19.7 28.3 27.1 31.0 52.8 21.8

1 2 21.5 28.8 27.7 35.0 48.8 21.3
1 3 21.0 28.0 26.7 30.0 53.9 22.4
1 4 20.2 29.2 26.8 32.0 53.9 22.9
1 5 21.4 28.1 27.7 31.0 52.1 22.2
1 6 19.7 28.9 27.6 32.0 51.1 22.6
Mean 20.6 28.6 27.3 31.8 52.1 22.2
Median 20.6 28.6 27.4 31.5 52.5 22.3
Std Dev. 0.8 0.5 0.5 1.7 1.9 0.6
Rel.Std.Dev. 3.91% 1.70% 1.66% 5.41% 3.73% 2.67%
PDM3 -23.63% 5.87% 1.20% 18.04% 93.19% -17.73%
Z-Score (Absolute) 2.09 0.02 0.31 0.89 6.25 1.66
Analytical results for Y in OREAS 605 (Certified Value 4.26 ppm)

Y Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
1 1 3.72 4.02 4.37 4.00 4.70 4.80

1 2 4.13 4.02 4.40 4.00 4.30 4.87
1 3 4.04 3.93 4.52 4.00 4.80 4.95
1 4 3.98 4.08 4.47 4.00 4.30 5.06
1 5 3.92 4.03 4.55 4.00 4.50 4.88
1 6 4.08 4.03 4.50 4.00 4.40 5.14
Mean 3.98 4.02 4.47 4.00 4.50 4.95
Median 4.01 4.03 4.49 4.00 4.45 4.92
Std Dev. 0.147 0.049 0.071 0.000 0.210 0.128
Rel.Std.Dev. 3.70% 1.21% 1.59% 0.00% 4.66% 2.59%
PDM3 -6.76% -5.77% 4.81% -6.20% 5.53% 16.14%
Z-Score (Absolute) 0.67 0.55 0.81 0.60 0.90 2.27
Analytical results for Yb in OREAS 605 (Certified Value 0.37 ppm)

Yb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 09 13 15 17 19
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*OES/MS4A*OES/MS
1 1 0.36 0.37 0.20 0.34 0.30 0.35

1 2 0.38 0.39 0.22 0.38 0.30 0.36
1 3 0.36 0.42 0.22 0.36 0.30 0.35
1 4 0.39 0.39 0.23 0.39 0.30 0.34
1 5 0.36 0.36 0.23 0.38 0.30 0.34
1 6 0.37 0.39 0.20 0.36 0.30 0.38
Mean 0.37 0.39 0.22 0.37 0.30 0.35
Median 0.37 0.39 0.22 0.37 0.30 0.35
Std Dev. 0.013 0.020 0.015 0.018 0.000 0.015
Rel.Std.Dev. 3.42% 5.27% 7.04% 4.98% 0.00% 4.26%
PDM3 -1.09% 3.21% -41.80% -1.53% -19.80% -5.54%
Z-Score (Absolute) 0.06 0.67 5.72 0.00 2.59 0.57
Analytical results for Zn in OREAS 605 (Certified Value 0.216 wt.%)

Zn Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 05 06 07 08
1 1 0.221 0.233 0.214 0.222 0.219 0.209

1 2 0.222 0.227 0.217 0.223 0.215 0.211
1 3 0.223 0.227 0.213 0.223 0.220 0.214
1 4 0.221 0.223 0.215 0.218 0.222 0.212
1 5 0.221 0.222 0.208 0.219 0.224 0.204
1 6 0.225 0.231 0.209 0.227 0.218 0.215
Mean 0.222 0.227 0.213 0.222 0.220 0.211
Median 0.221 0.227 0.214 0.223 0.220 0.212
Std Dev. 0.002 0.004 0.004 0.003 0.003 0.004
Rel.Std.Dev. 0.80% 1.87% 1.65% 1.45% 1.43% 1.88%
PDM3 2.90% 5.26% -1.46% 2.86% 1.78% -2.31%
Z-Score (Absolute) 0.58 1.08 0.34 0.57 0.34 0.52
Analytical results for Zr in OREAS 605 (Certified Value 84 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 09 11 12 13
1 1 90 82 93 87 80 85
1 2 89 79 92 85 70 82
1 3 90 81 91 88 81 85
1 4 92 82 90 85 71 86
1 5 90 80 91 85 76 87
1 6 91 86 92 86 74 86
Mean 90 82 91 86 75 85
Median 90 82 91 86 75 86
Std Dev. 1.2 2.4 0.8 1.3 4.5 1.5
Rel.Std.Dev. 1.36% 2.94% 0.90% 1.47% 5.95% 1.81%
PDM3 7.18% -2.80% 8.67% 2.29% -10.22% 1.40%
Z-Score (Absolute) 0.68 0.65 0.88 0.03 1.64 0.00
08 09 11 12 13 14 15 16 17
4A*OES 4A*OES/MS 4A*AAS 4A*MS 4A*MS 4A*OES 4A*OES 4A*AAS 4A*OES/MS
> 100 1048 943 > 100 996 928 951 N.A. -
> 100 1059 966 > 100 990 956 956 N.A. -
> 100 1061 945 > 100 983 951 947 N.A. -
> 100 1053 951 > 100 1021 947 949 N.A. -
> 100 1055 951 > 100 1000 952 947 N.A. -
> 100 1058 970 > 100 986 955 950 N.A. -
1056 954 996 948 950
1056 951 993 952 950
5 11 14 10 3
0.45% 1.17% 1.39% 1.09% 0.36%
8.60% -1.83% 2.45% -2.46% -2.27%
NA 2.54 0.54 NA 0.72 0.73 0.67 NA NA

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS
6.07 6.70 5.51 4.10 5.59 5.43 5.64 4.86 5.61

6.01 6.67 5.47 3.73 5.64 5.38 5.73 4.85 5.44
6.06 7.24 5.52 3.77 5.69 5.39 5.71 4.51 5.57
6.07 6.66 5.58 3.91 5.51 5.45 5.71 4.78 5.45
6.08 6.71 5.48 4.58 5.56 5.35 5.67 4.86 5.47
6.04 6.69 5.49 4.17 5.67 5.42 5.69 4.54 5.38
6.06 6.78 5.51 4.04 5.61 5.40 5.69 4.73 5.49
6.07 6.70 5.50 4.01 5.62 5.40 5.70 4.81 5.46
0.027 0.227 0.040 0.316 0.071 0.037 0.033 0.164 0.086
0.44% 3.35% 0.72% 7.80% 1.26% 0.68% 0.57% 3.47% 1.57%
11.58% 24.88% 1.48% -25.51% 3.36% -0.48% 4.86% -12.80% 1.08%
2.80 5.55 0.40 6.00 0.85 0.06 1.20 2.98 0.31

09 10 11 12 14 15 16 17 18
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES
1743 1650 1677 302 1703 1667 1498 1908 1501

1738 1660 1654 270 1712 1700 1522 1530 1505
1736 1680 1643 293 1734 1693 1502 1521 1519
1742 1650 1635 276 1715 1700 1521 1638 1479
1760 1680 1645 323 1674 1706 1459 1647 1521
1776 1690 1674 306 1727 1707 1477 1539 1512
1749 1668 1655 295 1711 1696 1497 1631 1506
1743 1670 1650 297 1714 1700 1500 1589 1509
16 17 17 20 21 15 25 147 15
0.89% 1.03% 1.04% 6.73% 1.24% 0.88% 1.66% 9.01% 1.02%
9.19% 4.14% 3.28% -81.59% 6.79% 5.83% -6.59% 1.77% -5.99%
1.08 0.34 0.21 12.25 0.73 0.59 1.24 0.52 1.15

11 12 13 14 16 17 18 21 23
4A*OES 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES
986 1972 685 2655 83 837 359 322 66

739 1705 703 2179 142 833 323 133 60
814 1181 701 2265 99 849 431 621 73
2700 2697 691 3511 86 841 321 423 52
1289 2522 711 2116 93 850 219 553 58
874 2145 699 2015 84 864 303 459 47
1234 2037 698 2457 98 846 326 419 59
930 2059 700 2222 90 845 322 441 59
744 553 9 561 22 11 69 174 9
60.28% 27.15% 1.34% 22.85% 22.98% 1.32% 21.31% 41.60% 15.80%
-77.80% -63.34% -87.43% -55.79% -98.24% -84.78% -94.13% -92.47% -98.93%
0.16 1.22 0.07 1.42 0.66 0.07 0.43 0.34 0.69

09 11 12 13 14 15 16 17 18
4A*OES/MS 4A*OES 4A*MS 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES
0.76 0.80 0.79 0.63 0.70 0.75 0.70 1.20 <3

0.71 0.80 0.69 0.61 0.60 0.77 0.60 1.10 <3
0.76 0.80 0.78 0.62 0.60 0.77 0.60 1.10 <3
0.72 1.00 0.71 0.66 0.60 0.76 0.70 1.10 <3
0.74 0.80 0.78 0.62 0.50 0.74 0.70 1.10 <3
0.72 0.80 0.78 0.61 0.60 0.71 0.60 1.10 <3
0.73 0.83 0.76 0.63 0.60 0.75 0.65 1.12
0.73 0.80 0.78 0.62 0.60 0.76 0.65 1.10
0.024 0.082 0.043 0.017 0.063 0.023 0.055 0.041
3.21% 9.80% 5.73% 2.75% 10.54% 3.04% 8.43% 3.66%
8.93% 23.51% 11.90% -7.24% -11.07% 11.16% -3.66% 65.51%
0.40 1.16 0.64 0.93 1.16 0.58 0.58 4.82 NA

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS
16.0 20.0 16.0 19.2 15.4 16.4 17.0 < 30 15.4

16.5 < 10 15.0 16.4 15.5 16.5 15.0 < 30 13.5
16.5 < 10 15.0 18.6 16.0 16.6 20.0 < 30 13.4
16.3 < 10 8.0 16.8 16.2 16.6 16.0 < 30 14.0
16.5 < 10 14.0 18.2 15.5 16.3 18.0 < 30 12.8
16.3 20.0 15.0 17.5 15.5 16.8 17.0 < 30 11.6
16.4 20.0 13.8 17.8 15.7 16.5 17.2 13.5
16.4 20.0 15.0 17.9 15.5 16.5 17.0 13.5
0.2 0.0 2.9 1.1 0.3 0.2 1.7 1.3
1.20% 0.00% 21.16% 5.97% 1.99% 1.23% 10.03% 9.38%
0.39% 22.76% -15.09% 9.04% -3.71% 1.49% 5.37% -17.45%
0.04 1.73 0.71 0.64 0.42 0.04 0.35 NA 1.46

09 10 11 12 13 14 15 16 17
0.272 0.430 0.270 0.280 0.276 0.278 0.290 0.250 0.290

0.275 0.440 0.270 0.260 0.277 0.277 0.290 0.250 0.270
0.271 0.460 0.270 0.290 0.279 0.273 0.280 0.240 0.280
0.284 0.420 0.290 0.260 0.271 0.280 0.290 0.250 0.280
0.268 0.420 0.270 0.270 0.271 0.275 0.290 0.240 0.280
0.271 0.420 0.270 0.270 0.277 0.277 0.290 0.230 0.270
0.273 0.432 0.273 0.272 0.275 0.277 0.288 0.243 0.278
0.271 0.425 0.270 0.270 0.276 0.277 0.290 0.245 0.280
0.006 0.016 0.008 0.012 0.003 0.002 0.004 0.008 0.008
2.13% 3.71% 2.99% 4.30% 1.22% 0.82% 1.42% 3.36% 2.70%
-1.09% 56.12% -1.14% -1.75% -0.48% 0.11% 4.28% -11.99% 0.66%
0.25 15.75 0.27 0.44 0.08 0.08 1.25 3.30 0.24
09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES/MS
13.5 20.0 13.0 14.6 12.3 13.2 13.1 12.0 10.2

13.3 22.0 13.0 13.0 12.0 13.1 13.4 13.0 11.2
13.8 21.0 13.0 14.9 12.0 12.9 13.2 12.0 10.6
13.2 21.0 12.0 13.4 12.8 13.1 13.8 12.0 11.0
13.7 20.0 13.0 14.1 12.3 12.8 13.2 12.0 9.5
13.6 19.0 13.0 13.7 12.0 13.3 13.2 12.0 9.3
13.5 20.5 12.8 14.0 12.2 13.1 13.3 12.2 10.3
13.6 20.5 13.0 13.9 12.1 13.1 13.2 12.0 10.4
0.247 1.049 0.408 0.751 0.298 0.175 0.271 0.408 0.785
1.83% 5.12% 3.18% 5.38% 2.44% 1.33% 2.04% 3.36% 7.63%
7.88% 63.72% 2.49% 11.42% -2.31% 4.45% 6.30% -2.83% -17.77%
0.63 7.43 0.03 1.06 0.61 0.21 0.34 0.67 2.29
Lab Lab Lab

17 19 25
4A*OES/MS4A*OES/MS 4A*MS
19.4 18.7 22.7

23.6 18.9 26.1
20.5 17.8 23.5
21.8 19.3 22.8
22.5 20.2 23.6
23.1 18.7 22.7
21.8 18.9 23.6
22.2 18.8 23.2
1.6 0.8 1.3
7.35% 4.11% 5.54%
1.96% -11.62% 10.14%
0.00 0.67 0.29

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS
96 86 92 66 95 94 94 83 103
96 91 91 57 95 94 96 84 83
96 89 89 47 95 93 96 82 83
97 90 92 58 94 93 96 84 87
97 88 89 72 94 92 95 81 89
97 88 88 64 94 94 95 81 83
97 89 90 61 94 93 95 83 88
97 89 90 61 94 93 96 83 85
0.5 1.8 1.7 8.6 0.3 0.8 0.8 1.4 7.9
0.51% 1.98% 1.91% 14.24% 0.30% 0.89% 0.86% 1.67% 8.94%
7.21% -1.67% 0.00% -32.79% 4.64% 3.29% 5.72% -8.51% -2.50%
0.94 0.31 0.08 4.68 0.57 0.38 0.73 1.27 0.90

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES/MS
29.9 34.0 30.0 21.0 48.4 32.0 34.1 58.0 17.0

27.4 32.0 28.0 21.0 48.9 54.0 30.7 35.0 20.0
27.4 34.0 32.0 22.0 51.1 42.0 34.3 32.0 17.0
30.0 33.0 29.0 22.0 45.9 33.0 32.4 42.0 18.0
30.4 33.0 31.0 20.0 45.0 58.0 34.0 36.0 19.0
31.3 35.0 31.0 21.0 46.5 55.0 32.5 35.0 16.0
29.4 33.5 30.2 21.2 47.6 45.7 33.0 39.7 17.8
30.0 33.5 30.5 21.0 47.4 48.0 33.3 35.5 17.5
1.6 1.0 1.5 0.8 2.3 11.6 1.4 9.6 1.5
5.60% 3.13% 4.88% 3.56% 4.75% 25.34% 4.19% 24.11% 8.25%
-3.42% 10.03% -0.92% -30.48% 56.45% 49.98% 8.44% 30.28% -41.43%
0.17 0.74 0.00 2.00 3.89 3.45 0.64 1.30 2.75
Lab Lab Lab Lab

17 19 24 25
4A*OES/MS4A*OES/MS 4A*MS 4A*MS
1.42 1.24 1.60 1.50

1.50 1.23 1.50 1.50
1.44 1.23 1.60 1.50
1.49 1.21 1.60 1.50
1.43 1.24 1.60 1.50
1.49 1.20 1.60 1.50
1.46 1.22 1.58 1.50
1.46 1.23 1.60 1.50
0.035 0.017 0.041 0.000
2.43% 1.40% 2.58% 0.00%
-7.11% -22.18% 0.62% -4.67%
0.70 2.62 0.28 0.39

08 09 10 11 12 13 14 15 16
4A*OES/AAS4A*OES/MS 4A*OES 4A*AAS 4A*AAS 4A*OES 4A*OES 4A*MS PF*OES
5.31 4.99 4.93 5.23 4.93 4.86 4.77 4.90 4.88

5.29 5.04 4.96 5.28 5.06 4.85 4.93 4.99 5.02
5.29 4.97 5.08 5.21 5.03 4.81 4.93 4.94 4.87
5.31 5.01 4.94 5.21 4.94 4.87 4.80 4.83 4.92
5.24 4.95 5.05 5.28 5.07 4.81 4.92 4.96 4.85
5.13 4.93 5.10 5.27 5.03 4.84 4.93 4.87 4.87
5.26 4.98 5.01 5.25 5.01 4.84 4.88 4.92 4.90
5.29 4.98 5.01 5.25 5.03 4.84 4.93 4.92 4.88
0.069 0.041 0.075 0.031 0.060 0.026 0.073 0.057 0.062
1.32% 0.82% 1.50% 0.60% 1.20% 0.53% 1.49% 1.16% 1.27%
4.87% -0.69% -0.15% 4.55% -0.15% -3.52% -2.70% -2.03% -2.31%
1.92 0.09 0.09 1.64 0.09 1.02 0.61 0.53 0.62
09 10 11 12 13 14 15 16 17
4.05 4.11 3.98 3.46 3.95 3.75 3.84 3.25 3.85

4.05 4.14 3.97 3.05 3.97 3.73 3.89 3.31 3.74
3.97 4.16 4.02 3.67 3.98 3.72 3.87 3.21 3.83
4.07 4.02 4.04 3.21 3.89 3.76 3.87 3.25 3.76
3.99 4.06 4.01 3.10 3.93 3.69 3.85 3.28 3.81
4.06 4.10 3.91 3.06 3.98 3.74 3.86 3.10 3.71
4.03 4.10 3.99 3.26 3.95 3.73 3.86 3.23 3.78
4.05 4.11 4.00 3.16 3.96 3.74 3.86 3.25 3.78
0.043 0.052 0.046 0.253 0.033 0.025 0.018 0.073 0.055
1.05% 1.26% 1.16% 7.77% 0.85% 0.67% 0.45% 2.27% 1.45%
7.29% 9.05% 6.12% -13.30% 5.09% -0.71% 2.79% -13.97% 0.66%
0.93 1.14 0.80 1.50 0.67 0.01 0.40 1.49 0.15

09 11 12 13 14 15 17 19 24
4A*OES/MS 4A*OES 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES/MS4A*OES/MS 4A*MS
33.3 38.0 27.6 27.6 33.7 30.0 28.2 27.5 30.6

33.3 38.0 24.9 27.9 33.1 32.0 28.3 27.1 30.4
33.2 37.0 23.9 27.4 32.9 31.0 27.0 26.7 30.8
32.7 38.0 25.7 28.0 33.1 32.0 28.4 26.7 32.6
33.7 37.0 29.9 28.0 32.8 31.0 27.6 27.1 32.6
33.5 38.0 27.1 27.7 34.1 30.0 28.5 26.3 31.2
33.3 37.7 26.5 27.8 33.3 31.0 28.0 26.9 31.4
33.3 38.0 26.4 27.8 33.1 31.0 28.3 26.9 31.0
0.337 0.516 2.146 0.250 0.508 0.894 0.583 0.390 0.991
1.01% 1.37% 8.10% 0.90% 1.53% 2.89% 2.08% 1.45% 3.16%
9.78% 24.26% -12.55% -8.36% 9.80% 2.27% -7.63% -11.28% 3.48%
0.97 2.34 1.14 0.74 0.97 0.26 0.61 1.02 0.38
Lab Lab
17 25
4A*OES/MS PF*MS
1.30 < 20
0.70 < 20
0.80 < 20
0.90 < 20
0.80 < 20
0.90 < 20
0.90
0.85
0.210
23.31%
1.24 NA
Lab Lab Lab Lab

17 19 24 25
2.76 2.74 2.40 2.40

2.57 2.66 2.60 2.40
2.36 2.61 2.60 2.60
2.51 2.66 2.60 2.40
2.58 2.69 2.60 2.40
2.42 2.68 2.60 2.40
2.53 2.67 2.57 2.43
2.54 2.67 2.60 2.40
0.140 0.041 0.082 0.082
5.54% 1.55% 3.18% 3.36%
-1.90% 3.57% -0.61% -5.77%
0.21 0.60 0.02 0.78
14 15 17 19 24 25
4A*MS 4A*MS 4A*OES/MS4A*OES/MS 4A*MS 4A*MS
4.08 4.11 3.14 3.00 3.95 3.52

3.95 4.31 3.49 2.98 3.75 3.48
4.01 4.22 3.24 2.97 3.95 3.50
4.01 4.10 3.41 2.92 4.15 3.46
3.95 4.24 2.93 2.97 4.05 3.44
4.00 4.31 2.85 2.96 3.95 3.40
4.00 4.22 3.18 2.97 3.97 3.47
4.01 4.23 3.19 2.97 3.95 3.47
0.048 0.093 0.255 0.026 0.133 0.043
1.20% 2.20% 8.03% 0.86% 3.35% 1.25%
5.69% 11.37% -16.06% -21.57% 4.81% -8.40%
0.59 1.18 1.68 2.26 0.50 0.88

09 11 12 13 14 15 16 17 18
4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES
1.04 1.06 1.15 1.08 1.03 1.01 0.95 1.13 1.21

1.02 1.08 1.02 1.09 1.02 1.04 0.94 1.08 1.22
1.01 1.07 1.17 1.08 1.02 1.04 0.92 1.10 1.14
1.04 1.03 1.05 1.05 1.05 1.04 0.92 1.08 1.15
1.02 1.06 1.07 1.06 1.02 1.04 0.95 1.08 1.13
1.02 1.05 1.07 1.07 1.03 1.03 0.89 1.06 1.05
1.03 1.06 1.09 1.07 1.03 1.03 0.93 1.09 1.15
1.02 1.06 1.07 1.08 1.03 1.04 0.93 1.08 1.15
0.011 0.017 0.059 0.012 0.010 0.012 0.023 0.024 0.062
1.05% 1.63% 5.40% 1.09% 0.95% 1.17% 2.50% 2.21% 5.36%
-1.34% 1.86% 4.75% 3.18% -0.87% -0.54% -10.65% 4.75% 10.69%
0.40 0.24 0.82 0.50 0.31 0.24 2.26 0.66 1.74

09 11 12 13 15 16 17 18 19
4A*OES/MS 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS
15.2 8.0 7.4 13.2 17.0 3.7 9.5 < 20 5.5

15.7 7.0 6.5 13.9 18.0 4.0 12.8 < 20 5.5
15.1 7.0 5.1 14.8 17.0 5.4 10.5 < 20 5.9
15.7 9.0 6.7 13.1 18.0 2.8 11.3 < 20 5.9
14.8 8.0 5.6 13.2 18.0 3.5 12.1 < 20 6.3
16.0 8.0 6.5 12.1 17.0 3.0 12.4 < 20 5.9
15.4 7.8 6.3 13.4 17.5 3.7 11.4 5.8
15.4 8.0 6.5 13.2 17.5 3.6 11.7 5.9
0.4 0.8 0.8 0.9 0.5 0.9 1.3 0.3
2.84% 9.61% 13.05% 6.68% 3.13% 24.88% 10.98% 5.00%
1.03 0.41 0.71 0.64 1.43 1.19 0.27 NA 0.79

14 15 16 17 18 19 21 24 25
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS
20.5 21.4 21.0 23.0 34.0 19.8 51.0 20.0 22.0

20.6 22.1 22.0 23.0 35.0 19.7 52.0 20.0 22.5
20.7 22.3 22.0 23.0 34.0 19.5 44.0 20.0 22.5
20.4 21.9 21.0 22.0 34.0 19.7 49.0 20.0 22.0
20.4 22.8 21.0 23.0 34.0 19.8 44.0 20.0 21.5
20.7 22.8 21.0 22.0 34.0 19.2 46.0 20.0 21.5
20.6 22.2 21.3 22.7 34.2 19.6 47.7 20.0 22.0
20.6 22.2 21.0 23.0 34.0 19.7 47.5 20.0 22.0
0.138 0.549 0.516 0.516 0.408 0.219 3.502 0.000 0.447
0.67% 2.47% 2.42% 2.28% 1.19% 1.12% 7.35% 0.00% 2.03%
-5.49% 2.22% -1.89% 4.24% 57.13% -9.77% 119.22% -8.02% 1.18%
0.67 0.11 0.31 0.31 5.66 1.11 11.94 0.93 0.00

09 10 11 12 13 14 15 16 17
472 700 500 600 511 455 500 500 500

464 700 500 500 517 457 500 500 500
468 700 500 600 513 457 500 500 500
473 700 500 500 507 460 500 500 500
478 700 500 500 513 456 500 500 500
476 700 500 500 518 458 500 500 500
472 700 500 533 513 457 500 500 500
472 700 500 500 513 457 500 500 500
5 0 0 52 4 2 0 0 0
1.09% 0.00% 0.00% 9.68% 0.73% 0.38% 0.00% 0.00% 0.00%
-0.81% 47.21% 5.15% 12.16% 7.89% -3.86% 5.15% 5.15% 5.15%
0.65 4.58 0.00 0.76 0.30 0.98 0.00 0.00 0.00

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES/MS
92 95 93 84 97 96 97 86 95
93 95 93 77 98 95 95 85 92
90 98 92 89 98 95 96 82 94
93 93 93 78 97 98 95 84 95
91 95 91 79 97 94 95 81 94
90 96 90 86 98 96 97 79 94
91 95 92 82 98 96 96 83 94
91 95 93 82 98 96 96 83 94
1.2 1.6 1.3 4.9 0.8 1.4 0.8 2.6 1.1
1.35% 1.71% 1.37% 5.93% 0.82% 1.43% 0.80% 3.19% 1.17%
-0.07% 4.28% 0.63% -10.12% 6.72% 4.65% 4.80% -9.39% 2.82%
0.12 0.63 0.00 1.86 1.06 0.70 0.72 1.74 0.38

09 10 11 12 14 15 17 18 19
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS
5.06 5.00 6.00 4.87 5.30 4.00 4.65 5.00 4.56

5.01 5.00 6.00 3.54 5.20 5.00 4.85 5.00 4.47
4.89 6.00 6.00 4.38 5.30 5.00 4.45 5.00 4.47
4.99 4.00 5.00 4.12 5.10 5.00 4.72 5.00 4.32
5.03 5.00 5.00 4.72 4.90 5.00 4.25 6.00 4.51
5.03 6.00 5.00 4.34 5.00 5.00 3.92 5.00 4.42
5.00 5.17 5.50 4.33 5.13 4.83 4.47 5.17 4.46
5.02 5.00 5.50 4.36 5.15 5.00 4.55 5.00 4.47
0.058 0.753 0.548 0.472 0.163 0.408 0.344 0.408 0.082
1.16% 14.57% 9.96% 10.91% 3.18% 8.45% 7.68% 7.90% 1.84%
3.72% 7.14% 14.05% -10.25% 6.44% 0.22% -7.24% 7.14% -7.56%
0.13 0.39 0.91 0.92 0.34 0.13 0.70 0.39 0.72
09 11 12 13 14 15 16 17 18
0.641 0.590 0.620 0.584 0.563 0.570 0.540 0.580 0.590

0.626 0.580 0.550 0.586 0.559 0.580 0.550 0.590 0.610
0.638 0.590 0.640 0.583 0.559 0.570 0.540 0.600 0.600
0.649 0.590 0.570 0.577 0.573 0.580 0.540 0.590 0.590
0.643 0.590 0.580 0.588 0.563 0.580 0.540 0.590 0.600
0.633 0.580 0.580 0.583 0.564 0.570 0.510 0.580 0.600
0.639 0.587 0.590 0.584 0.563 0.575 0.537 0.588 0.598
0.640 0.590 0.580 0.584 0.563 0.575 0.540 0.590 0.600
0.008 0.005 0.033 0.004 0.005 0.005 0.014 0.008 0.008
1.25% 0.88% 5.67% 0.64% 0.92% 0.95% 2.55% 1.28% 1.26%
10.01% 1.07% 1.64% 0.53% -2.94% -0.94% -7.55% 1.35% 3.08%
2.26 0.23 0.36 0.11 0.67 0.22 1.51 0.30 0.69
Lab Lab Lab Lab Lab

15 17 19 23 25
4A*OES 4A*OES/MS4A*OES/MS 4A*OES 4A*MS
7.00 7.00 6.96 7.00 8.00

7.00 7.00 6.97 6.00 8.00
6.00 6.00 7.21 7.00 8.00
7.00 5.90 7.10 7.00 8.00
7.00 6.90 7.25 8.00 8.00
7.00 6.50 7.00 7.00 7.50
6.83 6.55 7.08 7.00 7.92
7.00 6.70 7.05 7.00 8.00
0.408 0.501 0.125 0.632 0.204
5.97% 7.65% 1.77% 9.04% 2.58%
-1.18% -5.28% 2.41% 1.23% 14.48%
0.37 1.65 0.74 0.37 4.50
09 10 11 12 13 14 15 16 17
1492 1630 1481 1451 1486 1532 1533 1429 1728

1484 1650 1476 1301 1495 1532 1540 1445 1404
1504 1650 1470 1534 1501 1529 1555 1438 1395
1500 1590 1492 1348 1467 1543 1544 1471 1458
1520 1610 1493 1394 1478 1544 1537 1401 1485
1505 1640 1502 1405 1504 1534 1539 1388 1377
1501 1628 1486 1405 1488 1536 1541 1429 1475
1502 1635 1487 1399 1490 1533 1540 1434 1431
12 24 12 81 14 6 8 30 131
0.81% 1.47% 0.81% 5.78% 0.96% 0.41% 0.49% 2.12% 8.87%
-1.36% 7.01% -2.36% -7.63% -2.20% 0.92% 1.30% -6.11% -3.10%
0.34 2.05 0.63 1.75 0.58 0.31 0.42 1.70 1.79

09 11 12 14 16 17 18 19 21
4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
529 493 782 489 300 452 600 661 840

553 503 696 484 200 471 500 588 785
542 505 807 486 200 467 600 680 707
541 510 704 491 300 450 600 714 804
554 500 779 480 300 462 600 531 734
559 504 751 483 300 455 500 626 802
546 503 753 486 267 460 567 633 779
547 504 765 485 300 459 600 644 794
11 6 45 4 52 9 52 66 49
2.04% 1.13% 5.96% 0.83% 19.36% 1.85% 9.11% 10.46% 6.32%
7.67% -0.96% 48.45% -4.31% -47.44% -9.43% 11.69% 24.84% 53.48%
0.72 0.19 5.04 0.55 5.11 1.09 1.15 2.54 5.57

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES/MS
1230 930 1255 1488 1343 1059 1332 1201 1530

1288 890 1232 1342 1378 1096 1341 1180 1218
1262 800 1249 1622 1393 1112 1399 1143 1359
1243 800 1242 1390 1392 1171 1296 1160 1491
1250 1120 1212 1432 1398 995 1300 1162 1257
1272 810 1210 1376 1367 1129 1300 1156 1269
1257 892 1233 1442 1379 1094 1328 1167 1354
1256 850 1237 1411 1385 1104 1316 1161 1314
21 124 19 102 21 61 40 20 130
1.67% 13.92% 1.53% 7.06% 1.50% 5.56% 2.98% 1.75% 9.62%
-3.02% -31.23% -4.88% 11.19% 6.34% -15.65% 2.42% -10.00% 4.42%
0.41 3.28 0.58 0.87 0.43 1.56 0.08 1.04 0.26
Lab Lab Lab Lab

17 19 24 25
26.0 24.1 26.8 31.6

26.1 24.1 26.8 33.4
24.8 24.2 28.0 35.4
25.6 24.4 29.0 34.8
23.1 24.5 28.4 34.4
21.4 24.1 28.0 33.6
24.5 24.2 27.8 33.9
25.2 24.2 28.0 34.0
1.9 0.2 0.9 1.3
7.68% 0.72% 3.16% 3.95%
-16.18% -17.06% -4.78% 15.86%
1.47 1.53 0.61 0.95
Lab
25
4A*MS
< 100
< 100
< 100
< 100
< 100
< 100
NA

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES PF*OES 4A*OES/MS
8.39 8.74 7.76 7.65 7.64 8.14 8.24 9.47 -

8.60 8.79 7.60 6.80 7.72 8.15 8.34 9.62 -
8.49 8.88 7.55 8.29 7.80 8.10 8.31 9.24 -
8.56 8.64 7.54 7.06 7.69 8.22 8.33 9.77 -
8.43 8.76 7.44 8.36 7.71 8.05 8.29 9.44 -
8.57 8.83 7.42 7.43 7.74 8.18 8.28 9.56 -
8.51 8.77 7.55 7.60 7.71 8.14 8.30 9.52
8.53 8.78 7.55 7.54 7.71 8.15 8.30 9.52
0.086 0.082 0.123 0.635 0.053 0.060 0.034 0.180
1.01% 0.94% 1.63% 8.36% 0.69% 0.73% 0.42% 1.89%
2.05% 5.25% -9.41% -8.85% -7.46% -2.33% -0.46% 14.16%
0.18 0.67 1.59 1.51 1.29 0.50 0.21 2.05 NA

09 10 11 12 13 14 15 16 17
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES/MS
288 290 323 131 214 298 301 280 313

285 310 304 93 216 291 306 288 295
285 300 322 90 222 300 302 278 212
282 290 313 121 224 294 298 277 228
288 290 319 117 218 290 299 274 302
290 300 304 118 217 296 294 270 286
286 297 314 112 218 295 300 278 273
286 295 316 118 217 295 300 278 291
3 8 9 17 4 4 4 6 42
0.90% 2.75% 2.74% 14.77% 1.77% 1.32% 1.33% 2.19% 15.42%
-2.55% 0.96% 6.91% -61.96% -25.66% 0.31% 2.02% -5.45% -7.21%
0.16 0.41 1.38 9.79 3.90 0.31 0.59 0.63 0.54

09 11 12 13 14 15 16 17 18
4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*OES
5.47 5.00 4.80 5.60 5.00 4.90 4.20 5.50 <5

5.17 5.00 4.20 5.63 5.00 4.89 4.10 6.20 <5
5.45 5.00 5.10 5.71 5.00 4.99 3.70 5.80 <5
5.24 5.00 4.20 5.66 5.00 4.86 4.00 6.10 <5
5.38 5.00 4.40 5.47 5.00 5.01 4.00 5.90 <5
5.43 5.00 4.20 5.68 5.00 5.04 3.90 6.20 <5
5.36 5.00 4.48 5.63 5.00 4.95 3.98 5.95
5.40 5.00 4.30 5.65 5.00 4.95 4.00 6.00
0.121 0.000 0.382 0.085 0.000 0.074 0.172 0.274
2.25% 0.00% 8.51% 1.51% 0.00% 1.50% 4.32% 4.60%
6.45% -0.64% -10.91% 11.79% -0.64% -1.67% -20.84% 18.24%
0.42 0.00 0.61 0.74 0.00 0.06 1.20 1.12 NA

15 17 18 19 21 24 25
4A*MS 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
75 82 105 62 112 85 70
76 79 105 61 114 85 75
73 78 102 63 95 90 70
75 80 103 63 109 95 70
76 79 88 64 98 95 70
74 81 105 61 108 90 75
75 80 101 62 106 90 72
75 80 104 62 109 90 70
1.0 1.5 6.7 1.1 7.7 4.5 2.6
1.32% 1.84% 6.57% 1.84% 7.28% 4.97% 3.60%
-2.09% 4.49% 32.64% -18.39% 38.74% 17.80% -6.20%
0.10 0.63 4.12 1.90 4.41 2.10 0.55
15 16 17 18 19 23 24 25
4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
2.97 < 15 2.70 < 20 2.26 3.00 2.90 4.00

3.11 < 15 2.60 < 20 2.25 5.00 2.80 4.00
3.14 < 15 2.40 < 20 2.20 3.00 2.90 4.00
3.08 < 15 2.40 < 20 2.12 3.00 3.10 4.00
3.18 < 15 2.50 < 20 2.21 6.00 3.00 4.00
3.03 < 15 2.40 < 20 2.16 4.00 3.00 4.00
3.09 2.50 2.20 4.00 2.95 4.00
3.09 2.45 2.21 3.50 2.95 4.00
0.076 0.126 0.054 1.265 0.105 0.000
2.47% 5.06% 2.45% 31.62% 3.56% 0.00%
13.14% -8.31% -19.29% 46.70% 8.19% 46.70%
0.60 NA 0.92 NA 1.70 2.98 0.25 2.98

09 11 12 13 14 15 16 17 18
4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES
468 307 278 402 424 429 134 326 377

463 251 244 405 418 433 126 324 378
439 261 217 405 405 436 146 325 371
436 347 258 398 430 426 104 324 355
438 314 214 393 403 428 125 323 388
447 291 245 407 429 441 118 315 395
448 295 243 401 418 432 126 323 377
443 299 244 403 421 431 126 324 378
14 36 24 5 12 6 14 4 14
3.08% 12.04% 10.00% 1.35% 2.76% 1.34% 11.33% 1.23% 3.68%
20.15% -20.90% -34.98% 7.58% 12.06% 15.84% -66.37% -13.49% 1.11%
1.11 0.89 1.57 0.50 0.72 0.90 3.10 0.53 0.18
Lab Lab Lab
19 24 25
4A*OES/MS 4A*MS 4A*MS
0.71 0.40 0.50

0.70 0.40 0.50
0.74 0.40 0.50
0.72 0.40 0.50
0.74 0.50 0.50
0.75 0.50 0.50
0.73 0.43 0.50
0.73 0.40 0.50
0.020 0.052 0.000
2.72% 11.92% 0.00%
1.10 0.67 0.27
Lab
25
4A*MS
0.18
0.18
0.18
0.20
0.18
0.18
0.18
0.18
0.008
4.45%
-9.81%
0.97
Lab Lab Lab

15 17 25
4A*OES 4A*OES/MS 4A*MS
40.0 24.2 31.8

40.0 23.5 31.6
40.0 20.8 30.4
39.0 22.3 30.2
38.0 23.0 31.0
36.0 22.9 31.0
38.8 22.8 31.0
39.5 23.0 31.0
1.6 1.2 0.6
4.13% 5.10% 2.04%
22.11% -28.36% -2.52%
1.37 1.44 0.00

12 13 14 15 17 18 19 23 24
4A*MS 4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS
2.70 6.00 5.26 6.16 3.70 < 20 4.53 <2 4.70

2.30 6.50 5.02 6.25 4.40 < 20 4.50 2.00 5.10
2.40 6.37 4.99 6.19 3.50 < 20 4.34 2.00 4.70
2.50 6.19 5.24 6.34 4.00 < 20 4.59 <2 3.50
2.70 6.36 5.07 6.36 4.40 < 20 5.01 <2 4.00
2.40 6.13 5.30 6.15 4.40 < 20 4.24 <2 5.00
2.50 6.26 5.15 6.24 4.07 4.53 2.00 4.50
2.45 6.28 5.16 6.22 4.20 4.51 2.00 4.70
0.167 0.185 0.135 0.091 0.398 0.266 0.000 0.623
6.69% 2.95% 2.63% 1.46% 9.79% 5.88% 0.00% 13.84%
-51.13% 22.32% 0.61% 22.02% -20.50% -11.36% -60.90% -12.03%
2.24 1.90 0.67 1.88 0.52 NA 0.00 2.79 0.04

09 11 12 13 14 15 16 17 18
0.194 0.160 0.145 0.185 0.178 0.170 0.120 0.160 0.180

0.192 0.150 0.128 0.184 0.174 0.170 0.120 0.160 0.180
0.193 0.160 0.153 0.184 0.176 0.170 0.120 0.170 0.180
0.193 0.160 0.136 0.183 0.178 0.170 0.120 0.160 0.180
0.195 0.150 0.119 0.183 0.173 0.170 0.120 0.160 0.180
0.190 0.150 0.113 0.184 0.176 0.170 0.120 0.160 0.180
0.193 0.155 0.132 0.184 0.176 0.170 0.120 0.162 0.180
0.193 0.155 0.132 0.184 0.176 0.170 0.120 0.160 0.180
0.002 0.005 0.015 0.001 0.002 0.000 0.000 0.004 0.000
0.85% 3.53% 11.57% 0.47% 1.15% 0.00% 0.00% 2.53% 0.00%
9.08% -12.29% -25.12% 3.94% -0.44% -3.81% -32.10% -8.52% 1.85%
1.38 1.79 3.69 0.62 0.03 0.53 4.73 1.23 0.31

14 15 17 18 19 24 25
4A*MS 4A*MS 4A*OES/MS 4A*OES 4A*OES/MS 4A*MS 4A*MS
15.2 16.3 15.4 < 20 15.0 14.8 14.4

15.2 17.1 15.1 < 20 14.9 15.2 14.3
15.5 16.8 14.9 < 20 15.2 15.5 14.3
15.4 16.6 16.0 < 20 15.0 15.9 14.3
15.3 17.2 14.9 < 20 15.4 15.6 14.2
15.4 16.8 15.3 < 20 15.1 15.4 14.2
15.3 16.8 15.3 15.1 15.4 14.3
15.3 16.8 15.2 15.1 15.5 14.3
0.098 0.300 0.413 0.163 0.374 0.075
0.64% 1.78% 2.71% 1.08% 2.43% 0.53%
2.41% 12.21% 1.98% 0.89% 2.87% -4.59%
0.13 1.39 0.07 NA 0.07 0.19 0.78

15 17 18 19 23 24 25
4A*MS 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
2.84 2.20 < 20 2.60 < 20 3.10 2.60

3.03 2.09 < 20 2.66 < 20 2.80 2.60
2.89 2.14 < 20 2.67 < 20 3.00 2.60
3.00 2.21 < 20 2.61 < 20 3.10 2.60
2.99 2.12 < 20 2.65 < 20 2.60 2.60
2.87 2.13 < 20 2.59 < 20 2.60 2.60
2.94 2.15 2.63 2.87 2.60
2.94 2.14 2.63 2.90 2.60
0.079 0.047 0.034 0.234 0.000
2.70% 2.19% 1.30% 8.16% 0.00%
5.07% -23.13% -5.90% 2.57% -6.97%
0.67 2.79 NA 0.67 NA 0.37 0.81
09 11 12 13 14 15 16 17 18
4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*OES
43.7 42.0 36.0 37.9 37.0 41.9 40.0 46.0 40.0

43.3 42.0 31.0 38.5 39.0 42.2 40.0 45.0 39.0
42.3 42.0 36.0 39.6 38.0 42.2 39.0 45.0 39.0
43.0 43.0 32.0 38.4 40.0 42.8 40.0 44.0 40.0
44.0 41.0 34.0 39.7 38.0 43.2 43.0 45.0 41.0
43.0 41.0 33.0 38.5 39.0 41.5 39.0 45.0 41.0
43.2 41.8 33.7 38.8 38.5 42.3 40.2 45.0 40.0
43.2 42.0 33.5 38.5 38.5 42.2 40.0 45.0 40.0
0.596 0.753 2.066 0.718 1.049 0.634 1.472 0.632 0.894
1.38% 1.80% 6.14% 1.85% 2.72% 1.50% 3.66% 1.41% 2.24%
8.40% 4.87% -15.60% -2.82% -3.48% 6.00% 0.69% 12.81% 0.28%
1.71 1.05 2.79 0.39 0.52 1.26 0.00 2.54 0.19

14 15 16 17 18 19 23 24 25
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
28.3 26.7 74.0 48.6 < 20 29.0 26.0 28.0 27.0

28.3 27.2 75.0 44.9 < 20 29.6 24.0 29.0 27.5
28.9 26.2 73.0 41.6 < 20 29.8 24.0 30.0 27.0
28.4 26.1 75.0 45.1 < 20 29.0 26.0 29.5 27.0
28.3 26.1 72.0 45.7 < 20 30.1 27.0 30.0 27.0
28.3 25.8 74.0 42.4 < 20 29.0 27.0 30.0 27.0
28.4 26.4 73.8 44.7 29.4 25.7 29.4 27.1
28.3 26.2 74.0 45.0 29.3 26.0 29.8 27.0
0.2 0.5 1.2 2.5 0.5 1.4 0.8 0.2
0.85% 1.84% 1.58% 5.60% 1.61% 5.32% 2.72% 0.75%
5.37% -2.24% 173.78% 65.82% 9.03% -4.82% 9.08% 0.43%
0.02 0.60 11.99 4.29 NA 0.24 0.74 0.25 0.37

14 15 16 17 18 19 21 23 24
4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS
4.40 4.00 < 10 4.00 4.00 3.97 14.00 2.00 4.20

4.30 4.00 < 10 4.30 4.00 3.93 14.00 4.00 4.30
4.30 4.00 < 10 4.20 4.00 3.93 13.00 4.00 4.30
4.30 4.00 < 10 4.30 4.00 3.94 14.00 3.00 4.60
4.40 4.00 < 10 4.10 4.00 3.94 13.00 4.00 4.50
4.40 4.00 < 10 4.30 4.00 3.91 14.00 3.00 4.50
4.35 4.00 4.20 4.00 3.94 13.67 3.33 4.40
4.35 4.00 4.25 4.00 3.94 14.00 3.50 4.40
0.055 0.000 0.126 0.000 0.020 0.516 0.816 0.155
1.26% 0.00% 3.01% 0.00% 0.50% 3.78% 24.49% 3.52%
2.01% -6.20% -1.51% -6.20% -7.68% 220.48% -21.83% 3.18%
0.45 0.60 NA 0.00 0.60 0.79 28.54 2.61 0.60
Lab
25
4A*MS
0.50
0.50
0.45
0.50
0.45
0.40
0.47
0.48
0.041
8.75%
24.75%
3.73

09 10 11 12 13 14 15 16 17
0.226 0.208 0.223 0.242 0.214 0.210 0.218 0.196 0.209

0.225 0.207 0.219 0.217 0.215 0.208 0.223 0.200 0.209
0.225 0.204 0.221 0.256 0.215 0.208 0.221 0.196 0.209
0.227 0.200 0.223 0.222 0.210 0.211 0.221 0.197 0.209
0.228 0.202 0.216 0.231 0.212 0.206 0.219 0.194 0.207
0.229 0.204 0.215 0.226 0.215 0.210 0.219 0.190 0.209
0.227 0.204 0.219 0.233 0.213 0.209 0.220 0.196 0.209
0.226 0.204 0.220 0.229 0.214 0.209 0.220 0.196 0.209
0.002 0.003 0.003 0.014 0.002 0.002 0.002 0.003 0.001
0.73% 1.47% 1.58% 6.11% 1.02% 0.84% 0.88% 1.64% 0.40%
5.06% -5.40% 1.56% 7.78% -1.10% -3.18% 2.05% -9.41% -3.37%
1.04 1.18 0.30 1.16 0.27 0.71 0.40 2.02 0.75

14 15 16 17 18 19 23 24 25
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
91 90 86 84 84 92 72 81 74
90 92 80 84 84 88 75 81 75
89 92 76 83 86 90 76 82 77
90 90 78 85 86 88 73 86 75
90 90 79 83 86 90 76 85 74
91 90 77 82 89 88 78 86 74
90 91 79 83 86 89 75 84 75
90 90 79 84 86 89 76 84 75
0.8 1.2 3.6 1.1 1.8 1.6 2.2 2.4 1.2
0.83% 1.38% 4.49% 1.26% 2.14% 1.76% 2.92% 2.91% 1.56%
7.15% 7.77% -5.64% -0.76% 2.09% 6.20% -10.79% -0.68% -10.99%
0.67 0.76 1.24 0.38 0.00 0.55 1.72 0.37 1.75
18 19 21 22 23 24 25
4A*OES 4A*AAS 4A*OES 4A*MS 4A*AAS 4A*OES 4A*MS
912 --- 1001 971 964 970 793

914 --- 951 985 954 970 806
922 --- 826 959 950 807
913 --- 996 951 961 945 792
920 --- 932 962 960 811
920 --- 989 965 960 774
917 949 969 961 959 797
917 970 971 962 960 800
4 66 17 4 10 14
0.47% 6.99% 1.76% 0.41% 1.06% 1.73%
-5.68% -2.37% -0.32% -1.16% -1.33% -17.99%
1.68 NA 0.05 0.10 0.34 0.40 5.32
Lab Lab Lab Lab Lab

18 19 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES
5.27 5.56 3.06 5.45 5.64

5.31 5.46 4.92 5.46 5.61
5.25 5.46 4.95 5.46 5.55
5.24 5.46 4.05 5.35 5.57
5.29 5.54 4.84 5.43 5.61
5.33 5.30 4.45 5.43 5.64
5.28 5.46 4.38 5.43 5.60
5.28 5.46 4.65 5.44 5.61
0.035 0.091 0.733 0.041 0.037
0.66% 1.66% 16.73% 0.76% 0.65%
-2.70% 0.62% -19.34% 0.04% 3.23%
0.59 0.20 3.38 0.06 0.82
Lab Lab Lab Lab Lab

19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS
1415 1495 1502 1470 1580

1397 1435 1483 1460 1610
1447 1239 1523 1490 1640
1407 1500 1498 1550 1670
1395 1416 1467 1530 1700
1396 1498 1510 1460 1600
1410 1431 1497 1493 1633
1402 1465 1500 1480 1625
20 100 20 38 45
1.41% 7.02% 1.32% 2.56% 2.78%
-12.01% -10.71% -6.55% -6.79% 1.95%
2.10 1.49 1.23 1.27 0.02
Lab
25
PF*MS
14000
13700
13900
13900
13800
14000
13883
13900
117
0.84%
149.83%
12.67
Lab Lab Lab Lab Lab

19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS
0.59 2.00 <1 1.00 0.60

0.55 2.00 <1 1.00 0.60
0.56 2.00 <1 1.00 0.60
0.53 <2 <1 1.00 0.60
0.47 <2 <1 1.00 0.60
0.50 <2 <1 1.00 0.70
0.53 2.00 1.00 0.62
0.54 2.00 1.00 0.60
0.042 0.000 0.000 0.041
7.99% 0.00% 0.00% 6.62%
-21.20% 196.43% 48.22% -8.60%
1.95 15.03 NA 3.47 0.96

18 19 21 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS
53.0 15.7 7.0 6.0 15.1 17.2

50.0 15.8 4.0 11.0 15.2 16.9
55.0 16.0 6.0 8.0 15.7 16.6
47.0 15.4 12.0 10.0 16.4 16.7
52.0 15.8 6.0 6.0 15.7 16.4
53.0 15.7 17.0 13.0 15.7 16.4
51.7 15.7 8.7 9.0 15.6 16.7
52.5 15.8 6.5 9.0 15.7 16.7
2.8 0.2 4.9 2.8 0.5 0.3
5.43% 1.15% 56.37% 31.43% 2.96% 1.86%
217.12% -3.45% -46.81% -44.76% -4.05% 2.50%
17.18 0.35 4.61 3.63 0.40 0.12
Lab Lab Lab Lab Lab

18 19 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES
0.260 0.269 0.160 0.280 0.290

0.260 0.265 0.250 0.280 0.290
0.260 0.266 0.250 0.280 0.290
0.260 0.265 0.200 0.270 0.290
0.260 0.262 0.240 0.280 0.290
0.260 0.256 0.230 0.280 0.280
0.260 0.264 0.222 0.278 0.288
0.260 0.265 0.235 0.280 0.290
0.000 0.004 0.035 0.004 0.004
0.00% 1.69% 15.99% 1.47% 1.42%
-5.97% -4.58% -19.83% 0.66% 4.28%
1.62 1.23 5.49 0.24 1.25
18 19 21 23 24 25
35.0 11.9 12.0 12.3 11.0 12.5

36.0 11.7 11.0 12.4 11.0 13.0
36.0 11.8 9.0 12.4 11.0 12.5
35.0 11.8 12.0 12.4 11.5 13.0
36.0 11.6 10.0 12.3 11.5 12.5
36.0 11.7 11.0 12.2 11.0 12.5
35.7 11.8 10.8 12.3 11.2 12.7
36.0 11.8 11.0 12.4 11.0 12.5
0.516 0.090 1.169 0.082 0.258 0.258
1.45% 0.77% 10.79% 0.66% 2.31% 2.04%
184.85% -6.10% -13.48% -1.50% -10.82% 1.16%
22.18 1.07 1.61 0.51 1.65 0.19

18 19 21 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES
81 77 89 94 86 95
82 77 84 93 93 95
83 75 74 93 86 95
81 76 89 92 93 95
83 76 83 93 90 100
83 78 88 93 87 95
82 77 85 93 89 96
83 77 86 93 89 95
1.0 1.1 5.8 0.6 3.3 2.0
1.20% 1.38% 6.81% 0.68% 3.71% 2.13%
-8.88% -15.09% -6.29% 3.14% -1.11% 6.28%
1.32 2.19 0.96 0.36 0.23 0.67

18 19 21 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES PF*OES
15.0 25.8 37.0 28.0 20.0 50.0

17.0 24.9 36.0 31.0 30.0 < 50
13.0 29.1 32.0 28.0 30.0 50.0
11.0 31.1 39.0 27.0 30.0 < 50
11.0 28.3 36.0 34.0 30.0 < 50
14.0 26.7 37.0 31.0 30.0 < 50
13.5 27.6 36.2 29.8 28.3 50.0
13.5 27.5 36.5 29.5 30.0 50.0
2.3 2.3 2.3 2.6 4.1 0.0
17.37% 8.30% 6.41% 8.85% 14.41% 0.00%
-55.66% -9.21% 18.78% -2.02% -6.94% 64.22%
3.71 0.56 1.34 0.07 0.41 4.42

17 18 19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES/AAS 4A*OES 4A*OES 4A*OES
> 10000 > 10000 5.02 4.83 4.96 5.06 5.11

> 10000 -- 4.94 4.75 4.93 5.03 5.18
> 10000 > 10000 4.95 4.72 4.90 5.10 5.19
> 10000 > 10000 5.03 4.66 4.92 5.01 5.16
> 10000 > 10000 4.92 4.74 4.94 5.12 5.15
> 10000 > 10000 4.84 4.70 4.96 5.13 5.12
4.95 4.74 4.94 5.08 5.15
4.95 4.73 4.94 5.08 5.15
0.070 0.059 0.023 0.049 0.032
1.41% 1.24% 0.46% 0.97% 0.62%
-1.34% -5.61% -1.61% 1.15% 2.68%
NA NA 0.31 1.72 0.39 0.52 1.02
18 19 21 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES PF*OES
4.09 3.46 3.57 3.36 4.08 4.06

4.17 3.42 3.39 3.54 4.11 4.03
4.12 3.42 2.96 3.66 4.10 4.06
4.13 3.44 3.57 3.47 4.00 3.98
4.14 3.48 3.41 3.59 4.09 3.97
4.19 3.56 3.59 3.54 4.02 3.97
4.14 3.46 3.41 3.53 4.07 4.01
4.14 3.45 3.49 3.54 4.09 4.01
0.036 0.056 0.239 0.103 0.045 0.044
0.86% 1.61% 7.01% 2.92% 1.12% 1.09%
10.15% -7.85% -9.14% -6.16% 8.20% 6.74%
1.27 0.85 0.72 0.65 1.04 0.87
Lab
25
4A*MS
31.2
32.6
32.2
33.0
33.2
32.8
32.5
32.7
0.724
2.23%
7.22%
0.81
Lab Lab Lab Lab Lab
19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES PF*OES
1.05 1.24 0.93 1.04 1.00

1.03 1.41 0.96 1.09 1.10
1.02 1.47 0.97 1.08 1.10
1.03 1.14 0.93 1.09 1.10
1.04 2.15 0.96 1.08 1.00
0.99 1.47 0.96 1.09 1.10
1.02 1.48 0.95 1.08 1.07
1.03 1.44 0.96 1.09 1.10
0.020 0.354 0.017 0.019 0.052
1.95% 23.93% 1.81% 1.80% 4.84%
-1.36% 42.45% -8.40% 3.79% 2.67%
0.40 5.78 1.81 0.77 0.40
Lab Lab
23 25
4A*OES 4A*MS
3.0 12.3
6.0 15.1
5.0 13.3
4.0 12.0
6.0 12.1
5.0 11.9
4.8 12.8
5.0 12.2
1.2 1.2
24.19% 9.73%
0.98 0.44
Lab Lab Lab Lab Lab

18 19 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES PF*OES
500 500 300 500 700

500 490 500 500 600
500 480 500 500 600
500 480 400 500 700
500 490 500 500 600
500 460 400 500 600
500 483 433 500 633
500 485 450 500 600
0 14 82 0 52
0.00% 2.83% 18.84% 0.00% 8.15%
5.15% 1.65% -8.87% 5.15% 33.19%
0.00 0.38 0.92 0.00 3.05

18 19 21 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES
100 94 136 75 86 90
100 90 130 88 90 94
100 91 116 89 82 92
100 92 137 82 80 86
100 91 135 88 78 84
100 88 138 87 88 94
100 91 132 85 84 90
100 91 136 88 84 91
0.0 1.8 8.3 5.4 4.7 4.2
0.00% 1.99% 6.30% 6.39% 5.63% 4.66%
9.39% -0.37% 44.39% -7.20% -8.12% -1.55%
1.52 0.17 8.19 0.99 1.52 0.38
Lab Lab Lab

23 24 25
4A*OES 4A*MS 4A*MS
5.00 5.00 5.00

4.00 5.00 5.00
4.00 5.00 6.00
4.00 5.00 6.00
5.00 5.00 6.00
5.00 5.00 5.50
4.50 5.00 5.58
4.50 5.00 5.75
0.548 0.000 0.492
12.17% 0.00% 8.80%
-6.69% 3.68% 15.78%
0.65 0.13 1.05
Lab Lab Lab Lab
19 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES
0.572 0.510 0.600 0.620

0.563 0.510 0.620 0.620
0.564 0.510 0.620 0.610
0.569 0.500 0.600 0.620
0.568 0.520 0.590 0.620
0.551 0.530 0.620 0.610
0.565 0.513 0.608 0.617
0.566 0.510 0.610 0.620
0.007 0.010 0.013 0.005
1.31% 2.01% 2.18% 0.84%
-2.75% -11.57% 4.80% 6.24%
0.63 2.63 1.08 1.40
18 19 21 23 24 25
1332 1515 1299 1519 1580 1520

1336 1481 1230 1491 1570 1550
1345 1468 1071 1519 1580 1560
1333 1473 1296 1481 1540 1540
1343 1476 1194 1490 1550 1530
1388 1425 1284 1508 1580 1530
1346 1473 1229 1501 1567 1538
1340 1474 1257 1500 1575 1535
21 29 88 16 18 15
1.57% 1.97% 7.15% 1.08% 1.12% 0.96%
-11.53% -3.19% -19.23% -1.33% 2.96% 1.10%
3.41 0.87 5.46 0.34 0.89 0.36
Lab Lab Lab

23 24 25
4A*OES 4A*OES 4A*OES
440 550 500

490 550 550
450 500 550
470 550 500
460 550 500
410 550 500
453 542 517
455 550 500
27 20 26
6.03% 3.77% 5.00%
-10.65% 6.76% 1.84%
1.22 0.63 0.10

18 19 21 23 24 25
1196 1248 1106 1343 1290 1490

1191 1306 1037 1370 1290 1450
1201 1324 910 1368 1290 1460
1191 1255 1090 1343 1380 1460
1241 1313 985 1371 1330 1450
1207 1275 1058 1305 1320 1430
1205 1287 1031 1350 1317 1457
1199 1291 1048 1356 1305 1455
19 32 73 26 36 20
1.57% 2.47% 7.08% 1.90% 2.70% 1.35%
-7.11% -0.76% -20.49% 4.12% 1.54% 12.34%
0.83 0.21 1.99 0.23 0.00 0.98
Lab Lab Lab Lab
19 23 24 25
4A*OES/MS 4A*OES 4A*OES PF*OES
>5 7.40 8.72 8.70

>5 7.40 9.03 8.72
>5 7.50 8.98 8.54
>5 7.40 9.17 8.56
>5 7.50 9.03 8.68
>5 7.60 9.15 8.62
7.47 9.01 8.64
7.45 9.03 8.65
0.082 0.162 0.075
1.09% 1.80% 0.87%
-10.43% 8.13% 3.61%
NA 1.75 1.12 0.42
Lab Lab Lab Lab Lab

18 19 21 23 25
4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS
136 278 241 280 289

82 281 227 282 285
108 275 201 276 292
129 269 237 278 302
208 276 217 284 281
235 278 236 290 303
150 276 227 282 292
133 277 232 281 291
59 4 15 5 9
39.66% 1.41% 6.70% 1.76% 3.06%
-49.07% -6.04% -22.92% -4.15% -0.63%
7.70 0.72 3.46 0.41 0.16
Lab Lab Lab Lab

19 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES
4.30 4.00 6.00 6.00

4.41 5.00 6.00 6.00
4.35 5.00 6.00 6.00
4.29 5.00 6.00 6.00
4.44 5.00 6.00 6.00
4.36 5.00 6.00 6.00
4.36 4.83 6.00 6.00
4.36 5.00 6.00 6.00
0.061 0.408 0.000 0.000
1.40% 8.45% 0.00% 0.00%
-13.40% -3.95% 19.23% 19.23%
0.76 0.20 1.18 1.18
Lab Lab Lab Lab Lab
19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*MS PF*MS
408 373 157 404 510

371 325 263 443 500
403 334 272 436 510
333 367 219 441 500
330 369 262 423 500
348 381 262 457 510
365 358 239 434 505
359 368 262 439 505
34 23 44 18 5
9.39% 6.39% 18.56% 4.23% 1.08%
-2.08% -4.02% -35.91% 16.30% 35.33%
0.03 0.07 1.40 0.92 1.85
Lab
25
4A*MS
4.80
5.40
5.10
4.80
5.10
4.70
4.98
4.95
0.264
5.30%
-2.58%
0.49
Lab Lab Lab Lab Lab

19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES PF*OES
0.157 0.129 0.170 0.205 0.190

0.157 0.120 0.170 0.200 0.190
0.156 0.104 0.170 0.200 0.190
0.154 0.123 0.170 0.195 0.190
0.158 0.111 0.170 0.200 0.190
0.152 0.116 0.170 0.200 0.190
0.156 0.117 0.170 0.200 0.190
0.157 0.118 0.170 0.200 0.190
0.002 0.009 0.000 0.003 0.000
1.45% 7.61% 0.00% 1.58% 0.00%
-11.92% -33.70% -3.81% 13.17% 7.51%
1.73 4.97 0.53 1.99 1.15
Lab Lab Lab Lab Lab
19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES
39.1 41.0 39.0 40.0 40.0

38.3 39.0 38.0 40.0 40.0
37.3 34.0 39.0 40.0 40.0
37.0 40.0 38.0 40.0 40.0
38.3 38.0 38.0 40.0 40.0
37.7 40.0 38.0 40.0 40.0
37.9 38.7 38.3 40.0 40.0
38.0 39.5 38.0 40.0 40.0
0.780 2.503 0.516 0.000 0.000
2.06% 6.47% 1.35% 0.00% 0.00%
-4.88% -3.07% -3.90% 0.28% 0.28%
0.78 0.00 0.60 0.19 0.19
Lab
25
4A*MS
4.60
4.70
4.70
4.60
4.70
4.50
4.63
4.65
0.082
1.76%
8.65%
1.31

18 19 21 23 24 25
0.226 0.215 0.190 0.208 0.217 0.217

0.229 0.210 0.179 0.208 0.216 0.217
0.223 0.208 0.155 0.209 0.217 0.219
0.229 0.209 0.188 0.206 0.214 0.216
0.224 0.213 0.177 0.208 0.215 0.217
0.229 0.201 0.188 0.210 0.218 0.215
0.227 0.209 0.179 0.208 0.216 0.217
0.227 0.209 0.183 0.208 0.217 0.217
0.003 0.005 0.013 0.001 0.001 0.001
1.19% 2.39% 7.29% 0.54% 0.68% 0.61%
5.08% -3.03% -16.90% -3.57% 0.16% 0.47%
1.04 0.67 3.13 0.79 0.00 0.07
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
972
10
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.43
11.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1602
12
Indicative
1.00
ppm
1.00
1.00
1.0
3.0
16.0
< 20
9.0
Indicative
1.00
ppm
0.00
0.00
1
4
16
5557
10
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.67
13.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
16.3
14.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.276
15.000
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
12.5
16.0
Certified
1.00
ppm
1.00
1.00
1.0
7.0
16.0
21.4
17.0
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
90
18
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
30.4
19.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.57
20.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.02
21.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.02
22.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.39
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
3.00
16.00
0.43
9.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.76
24.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
30.3
25.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.60
26.00
Certified
1.00
ppm
2.00
2.00
1.00
8.00
16.00
<5
27.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.58
28.00
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
<1
10.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.15
29.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
3.78
30.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.04
31.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
< 20
32.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
21.7
33.0
Certified
1.00
ppb
0.00
0.00
1
#N/A
16
54
34
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
476
35
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
91
36
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.82
37.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.580
38.000
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
6.92
39.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
10.7
40.0
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1522
41
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
507
42
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1297
43
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
2.97
44.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
29.2
45.0
Indicative
1.00
ppb
0.00
0.00
1
8
16
2
9
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
8.34
46.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
294
47
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.03
48.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
76
49
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.09
50.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
2.73
51.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
373
52
Certified
1.00
ppm
2.00
2.00
1.00
7.00
16.00
<1
53.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.20
54.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
31.8
55.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.12
56.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.177
57.000
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
15.0
58.0
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.052
10.000
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.79
59.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
39.9
60.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
27.0
61.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.26
62.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.37
63.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.216
64.000
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
84
65
Analytical results for C in OREAS 605 (Indicative Value 0.043 wt.%)
C Round Replicate Lab Lab
No No 02 21
IRC IRC
1 1 0.050 0.038
1 2 0.060 0.036
1 3 0.050 0.033
1 4 0.040 0.037
1 5 0.050 0.036
1 6 0.050 0.035
Mean 0.050 0.036
Median 0.050 0.036
Std Dev. 0.006 0.002
Rel.Std.Dev. 12.65% 4.30%
PDM3 16.34% -16.34%

No No 01 05 06 07 09 11
IRC IRC IRC IRC IRC IRC
1 1 8.72 8.92 8.55 9.02 8.60 8.79

1 2 8.56 8.94 8.76 8.76 8.58 8.79
1 3 8.69 8.88 8.66 8.84 8.60 8.93
1 4 8.56 8.94 8.64 9.01 8.57 8.85
1 5 8.51 8.95 8.59 8.77 8.62 8.82
1 6 8.55 8.98 8.60 8.96 8.47 8.89
Mean 8.60 8.94 8.63 8.89 8.57 8.85
Median 8.56 8.94 8.62 8.90 8.59 8.84
Std Dev. 0.085 0.033 0.073 0.118 0.054 0.056
Rel.Std.Dev. 0.99% 0.37% 0.85% 1.33% 0.63% 0.64%
PDM3 -2.23% 1.60% -1.83% 1.13% -2.52% 0.58%
Z-Score (Absolute) 0.68 0.23 0.59 0.11 0.75 0.02
12 14 17 18 19 21 22 24 25
IRC IRC IRC IRC IRC IRC IRC IRC IRC
9.26 8.04 9.41 10.05 8.82 9.88 8.71 8.84 8.52

9.31 8.18 9.53 10.20 8.71 9.92 8.72 8.66
9.21 8.22 9.60 10.15 8.69 9.28 8.57 8.89 8.58
9.29 8.04 9.46 10.21 8.73 9.74 8.11 8.89 8.59
9.35 8.36 9.47 10.20 8.80 9.87 8.86 8.61
9.64 8.30 9.48 10.19 8.71 9.95 8.94 8.66
9.34 8.19 9.49 10.17 8.74 9.77 8.46 8.86 8.60
9.30 8.20 9.48 10.19 8.72 9.87 8.57 8.88 8.60
0.153 0.132 0.066 0.058 0.054 0.252 0.314 0.075 0.053
1.64% 1.61% 0.69% 0.57% 0.61% 2.58% 3.71% 0.85% 0.62%
6.24% -6.87% 7.93% 15.60% -0.58% 11.13% -3.76% 0.71% -2.17%
1.17 1.78 1.73 3.55 0.29 2.75 1.05 0.02 0.67
Lab
26
IRC
8.97
9.06
9.02
9.02
9.00
8.98
9.01
9.01
0.033
0.36%
2.44%
0.42
Indicative
1.00
wt.%
3.00
3.00
1.000
10.000
16.000
0.043
16.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
8.79
125.00
Table 2. Certified Values, SD's, 95% Confidence and Tolerance Limits for OREAS 605
95% Confidence 95% Tolerance
Certified
Constituent SD Limits Limits
Value Low High Low High
4-Acid Digestion
Ag, Silver (ppm) 972 28 958 986 960 985
Co, Cobalt (ppm) 90 6.0 87 93 88 93
Cu, Copper (wt.%) 5.02 0.152 4.95 5.09 4.94 5.09
Fe, Iron (wt.%) 3.76 0.260 3.64 3.88 3.67 3.85
Pb, Lead (ppm) 1297 136 1235 1358 1250 1343
Zn, Zinc (wt.%) 0.216 0.009 0.212 0.220 0.212 0.220
Ag, Silver (ppm) 984 29 967 1000 966 1002
Co, Cobalt (ppm) 93 6.9 90 96 91 95
Cu, Copper (wt.%) 4.98 0.157 4.90 5.06 4.92 5.04
Fe, Iron (wt.%) 3.75 0.181 3.67 3.83 3.67 3.83
Pb, Lead (ppm) 856 40 837 874 836 876
Zn, Zinc (wt.%) 0.217 0.010 0.212 0.221 0.211 0.222

OREAS 605 DataPack

Uploaded by

Document Information

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

OREAS 605 DataPack

Uploaded by

Copyright:

Available Formats

Table 1.

Abbreviations used for OREAS 605

Batch & Limits

one sigma standard deviation

4-acid (HF-HNO3-HClO4-HCl) digest with AAS finish

- Outlying individual values

- Outlying laboratory batch data sets and superfluous limit values

Laboratory Name and Location

Accurassay, Thunder Bay, Ontario, Canada

Constituent Unit Value Constituent Unit Value Constituent Unit Value

Constituent Unit Value Constituent Unit Value Constituent Unit Value

Laser Ablation ICP-MS

Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Analytical results for Au in OREAS 605 (Certified Value 1.67 ppm)

Analytical results for Pd in OREAS 605 (Indicative Value 13.43 ppm)

Analytical results for Pt in OREAS 605 (Indicative Value 2.21 ppm)

Lab Lab Lab Lab Lab Lab Lab Lab Lab

1.72 1.71 1.63 1.58 1.26 1.70 1.73 1.48 1.63

1.52 1.68 1.72 1.77 1.63 1.65 1.59 1.79 1.63

1.77 1.69 1.72 1.72

Analytical results for Al in OREAS 605 (Certified Value 0.73 wt.%)

Analytical results for As in OREAS 605 (Certified Value 1613 ppm)

Analytical results for Au in OREAS 605 (Certified Value 1.66 ppm)

Analytical results for B in OREAS 605 (Certified Value < 10 ppm)

Analytical results for Ba in OREAS 605 (Indicative Value 25.3 ppm)

Analytical results for Be in OREAS 605 (Certified Value 0.16 ppm)

Analytical results for Bi in OREAS 605 (Certified Value 16.7 ppm)

Analytical results for Ca in OREAS 605 (Certified Value 0.182 wt.%)

Analytical results for Cd in OREAS 605 (Certified Value 12.9 ppm)

Analytical results for Ce in OREAS 605 (Indicative Value 12.3 ppm)

Analytical results for Co in OREAS 605 (Certified Value 93 ppm)

Analytical results for Cr in OREAS 605 (Certified Value 27.5 ppm)

Analytical results for Cs in OREAS 605 (Certified Value 0.48 ppm)

Analytical results for Cu in OREAS 605 (Certified Value 4.98 wt.%)

Analytical results for Dy in OREAS 605 (Certified Value 0.52 ppm)

Analytical results for Er in OREAS 605 (Certified Value 0.15 ppm)

Analytical results for Eu in OREAS 605 (Certified Value 0.21 ppm)

Analytical results for Fe in OREAS 605 (Certified Value 3.75 wt.%)

Analytical results for Ga in OREAS 605 (Certified Value 6.66 ppm)

Analytical results for Gd in OREAS 605 (Certified Value 0.87 ppm)

Analytical results for Ge in OREAS 605 (Indicative Value 0.41 ppm)

Analytical results for Hf in OREAS 605 (Certified Value 0.55 ppm)

Analytical results for Hg in OREAS 605 (Certified Value < 4 ppm)

Analytical results for Ho in OREAS 605 (Certified Value 73 ppb)

Analytical results for In in OREAS 605 (Certified Value 3.75 ppm)

Analytical results for K in OREAS 605 (Certified Value 0.134 wt.%)

Analytical results for La in OREAS 605 (Certified Value 3.95 ppm)

Analytical results for Li in OREAS 605 (Certified Value 5.17 ppm)

Analytical results for Lu in OREAS 605 (Certified Value 11 ppb)

Analytical results for Mg in OREAS 605 (Certified Value 289 ppm)

Analytical results for Mn in OREAS 605 (Certified Value 86 ppm)

Analytical results for Mo in OREAS 605 (Certified Value 4.75 ppm)

Analytical results for Na in OREAS 605 (Certified Value 328 ppm)

Analytical results for Nb in OREAS 605 (Certified Value 0.45 ppm)

Analytical results for Nd in OREAS 605 (Certified Value 6.1 ppm)

Analytical results for Ni in OREAS 605 (Certified Value 1538 ppm)

Analytical results for P in OREAS 605 (Certified Value 116 ppm)

Analytical results for Pb in OREAS 605 (Certified Value 856 ppm)

Analytical results for Pd in OREAS 605 (Indicative Value 11.83 ppm)

Analytical results for Pr in OREAS 605 (Certified Value 1.74 ppm)

Analytical results for Pt in OREAS 605 (Indicative Value 2.22 ppm)

Analytical results for Rb in OREAS 605 (Certified Value 5.75 ppm)

Analytical results for Re in OREAS 605 (Indicative Value 1 ppb)

Analytical results for Ru in OREAS 605 (Indicative Value < 2 ppb)