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Abstract
During the course of the EU-funded Advanced-Creep Thematic Network, ECCC-WG1 reviewed the applicability and effectiveness of
a range of model equations to represent the accumulation of creep strain in various engineering alloys. In addition to considering the
experience of network members, the ability of several models to describe the deformation characteristics of large single and multi-cast
collations of e(t,T,s) creep curves have been evaluated in an intensive assessment inter-comparison activity involving three steels, 214CrMo
(P22), 9CrMoVNb (Steel-91) and 18Cr13NiMo (Type-316).
The choice of the most appropriate creep model equation for a given application depends not only on the high-temperature
deformation characteristics of the material under consideration, but also on the characteristics of the dataset, the number of casts for
which creep curves are available and on the strain regime for which an analytical representation is required. The paper focuses on the
factors which can influence creep model selection and model-fitting approach for multi-source, multi-cast datasets.
r 2007 Elsevier Ltd. All rights reserved.
0308-0161/$ - see front matter r 2007 Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijpvp.2007.06.009
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S.R. Holdsworth et al. / International Journal of Pressure Vessels and Piping 85 (2008) 80–88 81
H1 (continuous)
1E+2
H2 (continuous)
600°C 165 164 140 120 H3 (continuous)
150
170 140 115100 H4 (continuous)
H5 (interrupted)
180
1E+1 H6 (interrupted)
STRAIN, %
90
80
1E+0
80
72
56
50
1E-1
1E-2
1E+0 1E+1 1E+2 1E+3 1E+4 1E+5
TIME, h
Fig. 1. Continuous and interrupted measurement creep curves available for 6 casts of Steel-91 at 600 1C (curves with data points are the result of
interrupted measurement tests; labels are test stresses in MPa).
(X100 kh) strength values for standards. More recently, Many different model equations are used to represent creep
attention has moved to the assessment of creep strain data strain accumulation characteristics ranging from simple
[2,3]. The requirement for a representative description of a phenomenological to complex constitutive (e.g. [2–26]). Their
material’s ef(t,T,s) creep strain behaviour is no longer just effectiveness to model primary, secondary, and/or tertiary
for scientific interest and metallurgical understanding.1 The creep deformation for specific applications can vary with
creep deformation behaviour of engineering components is material characteristics and source data distribution. For
now routinely evaluated using PC-based finite-element example, not all model equations and fitting procedures are
analysis tools. Design engineers require the parameters for suitable for the prediction of mean long time creep strength
model equations to describe the long-time creep behaviour behaviour. Assessment inter-comparisons have been per-
of a specified alloy (not simply the characteristics of a formed on large multi-source, multi-cast, multi-temperature
single cast), typically in the primary and secondary datasets to establish the most effective approaches for the
deformation regimes. In contrast, remaining life assessment description of mean-alloy (rather than single cast) creep
engineers are more likely to require the best model deformation behaviour in evaluations based on working
description for a single cast of material, in the secondary datasets established for Steel-91 and Type-316.
and tertiary creep regimes. Prior to the start of the large multi-cast dataset evaluation
activity, a first creep data assessment inter-comparison
1
A list of nomenclature is given in Nomenclature. The terminology used examined a single-cast 214CrMo (P22) dataset [2,3]. The T,s
is as recommended in the ECCC Recommendations volume 2 [1b]. conditions for the creep curves in this dataset were uniformly
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82 S.R. Holdsworth et al. / International Journal of Pressure Vessels and Piping 85 (2008) 80–88
75 100 90 80 78
1E+2 125 123 63 125
98
700°C 190 165
98 50
90 62
49
62
1E+1
STRAIN, %
40
1E+0
1E-1 123b
123e
123m
123o
1E-2
1E-1 1E+0 1E+1 1E+2 1E+3 1E+4 1E+5
TIME, h
Fig. 2. Interrupted measurement creep curves available for 4 casts of Type-316 at 700 1C (low-strain sections of curves without data points determined by
continuous measurement; labels are test stresses in MPa).
Table 2
Summary of Z values associated with model-fits to Steel-91 dataset
many individual ef(t) co-ordinates and some with only a secutively for individual deformation regimes) to
small number of ep(t) co-ordinates (e.g. Fig. 1). establish the model parameters for specific conditions
of T and s.
2.2. Type-316 (ii) Determination of the temperature and stress depen-
dence of the selected model parameters to define the
Type-316 steel is a 18Cr13NiMo austenitic stainless steel. material mean master equation for all ef(t,T,s).
The Type-316 dataset used in the third WG1 creep strain
assessment inter-comparison comprised a total of 98 ep(t,T,s) Approach 2:
interrupted creep test records representing the behaviour of 4
casts at 6 temperatures in the range 500–700 1C (e.g. Fig. 2). (i) Determination of specific tf ðt; sÞ co-ordinates from
A wide variation in strength between the four casts was individual experimental creep curves either directly
observed. The maximum test duration exceeded 130 kh. In (unconstrained by a formal model description) or as a
lower temperature, higher stress tests in particular, the result of model fitting (with a model different to that
magnitude of instantaneous plastic strain was a significant used for final fitting).
proportion of the total plastic strain. (ii) Parametric model fitting of the specific co-ordinates to
establish parameters to define mean master equation
3. Creep strain data assessment for material in the form of e(,,s) or tf ðT; sÞ:
A wide range of creep model equations are in use today (i) Derivation of mean s ðt; TÞ relationships from specific
to represent the high-temperature time-dependent defor- observed tf ðT; sÞ co-ordinates from individual experi-
mation behaviour of engineering materials (e.g. [2–16], mental creep curves.
Appendix A). Many of these comprise components (ii) Model fitting with derived s ðt; TÞ to establish para-
originating from a small number of classical representa- meters for selected model to define mean master
tions of primary, secondary, and/or tertiary creep deforma- equation for material.
tion (e.g. [17–26], Table 1).
The multi-cast creep data assessment inter-comparisons
involved the application of 10 models by 10 different 3.3. Steel-91
analysts. These models are listed in Appendix A.3
Approach 1 was used to fit models A.1, A.2, A.4, and
3.2. Model fitting A.9 to the Steel-91 dataset (Table 2). In addition,
Approach 2 was used to fit models A.8 and A.10, with
Different approaches may be adopted to model-fit Approach 3 being used to fit models A.5 and A.7. The Z
ef(t,T,s) creep strain behaviour. values achieved with the 8 assessments are summarised in
Table 2. The lowest values achieved for the Steel-91 multi-
source, multi-cast dataset are significantly higher than
Approach 1:
those achieved during the assessment of the 214CrMo single-
(i) Model-fitting individual experimental creep curves with cast dataset [2,3]. The inherent cast-to-cast variability in
the selected model equation (simultaneously or con- the Steel-91 data led to best Z values typically in the range
6–7 for times to creep in the primary and secondary
3
The model equations used in the single-cast creep data assessment regimes. This compares with an achievable target of 2 for
inter-comparison are given elsewhere [2,3]. times in the same regimes for a single-cast dataset of creep
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84 S.R. Holdsworth et al. / International Journal of Pressure Vessels and Piping 85 (2008) 80–88
curves generated for a uniform distribution of tempera- establish the parameters for model A.10 (Table 3). This
tures and stresses. The best Z values for the multi-source proved to be a difficult dataset to assess and the activity is
multi-cast dataset were achieved using model-fitting still incomplete. Where available, the Z values associated
approaches 2 or 3 (italicised in Table 2). with the assessments of the multi-cast Type-316 dataset are
Examples of the A.5, A.7, and A.8 model fits determined generally larger than those reported for Steel-91 in Table 2.
by these approaches are compared with experimental creep These are undoubtedly a consequence of the significant
measurements in Fig. 3. Z values of 6–7 may have to be variation in strength between the four casts and uncertain-
regarded as acceptable for model equations representing ties associated with the determination of ei, in particular, at
alloy mean behaviour determined from the results of large higher stresses and lower application temperatures in the
multi-source, multi-cast datasets. creep range for the austenitic stainless steel.
Predicted 10 and 100 kh strength values for (a) 0.2% The lowest Z values obtained in the multi-cast Type-316
and (b) 1.0% creep strain determined using the A.1, creep strain data assessment inter-comparison were
A.5, A.7, and A.8 model equations are given in Fig. 4. achieved by employing an Approach 2 model fitting
There is good agreement for the creep strength values procedure (Table 3).
determined using model-fitting procedures involving Ap-
proach 2 or 3.
4. Creep model selection
3.4. Type-316
The selection of creep model and model-fitting approach
Approach 1 was used to fit models A.2, A.3, and A.6 to can depend on several factors including material char-
the Type-316 dataset, while Approach 2 was used to acteristics, data distribution, and practical application.
100 100
H3 (continuous) H2 (continuous)
H5 (interrupted) H4 (continuous)
H6 (interrupted) Bolton model fit
10 Bolton model fit 10 MHG model fit
MHG model fit Modified Graham-Walles
Mod Graham Walles
STRAIN, %
STRAIN, %
1 1
0.1 0.1
100 10
H1 (continuous) H4 (continuous)
H5 (interrupted) H6 (interrupted)
H6 (interrupted) Bolton model fit
10 Bolton model fit
MHG model fit
1 Modified Graham-Walles
MHG model fit
STRAIN, %
STRAIN, %
Modified Graham-Walles
0.1
0.1
Fig. 3. Comparison of creep curve fits to Steel-91 experimental data for (a) 550 1C/170 MPa tests (casts H3, H5 and H6), (b) 600 1C/150 MPa tests (casts
H2 and H4), (c) 600 1C/120 MPa tests (casts H1, H5 and H6), and (d) 600 1C/80 MPa tests (casts H4 and H6).
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400 400
Modified Theta (A1,1) Modified Theta (A1,1)
PREDICTED 0.2% CREEP STRENGTH, MPa
10kh
200 200
50 50
0 0
450 500 550 600 650 450 500 550 600 650
TEMPERATURE, °C TEMPERATURE, °C
Fig. 4. Comparison of predicted 10 and 100 kh strength values, were determined for all casts of Steel-91, (a) R0.2/t(T) and (b) R1.0/t(T) (open points are
predicted strength values for 10 kh; solid points are predicted strength values for 100 kh; the number following the model equation designation in the
legend label parentheses refers to the employed model-fitting approach as defined in Section 3.2).
Table 3
Summary of Z values associated with model-fits to Type-316 dataset
1.0 1.0
450C, 520MPa
450C, 430MPa
650C, 120MPa
0.6 0.6
0.4 0.4
2¼CrMo
540°C
0.2 Steel-91 0.2
600°C
0.0 0.0
0.0 0.2 0.4 0.6 0.8 1.0 0.0 0.2 0.4 0.6 0.8 1.0
NORMALISED TIME NORMALISED TIME
Fig. 5. Examples of creep curve shape variations for (a) 214CrMo, Steel-91 and Type-316 at typical application temperatures and (b) Steel-91 over a wide
T,s regime.
of observations in each regime. In such circumstances, it is mean creep behaviour for well-specified alloys from large
necessary to redress the balance of e(t) data points or to multi-source, multi-cast strain-time datasets.
model fit each regime independently [2,3]. As a generality, specific model equations are better
In contrast, the multi-cast Steel-91 dataset comprised 90 suited to representing creep strain accumulation character-
creep curves for 6 casts of the steel. The temperatures and istics of a given material in either the primary/secondary
stresses for which the creep curves were generated were not regime or the secondary/tertiary regime, although some
uniformly distributed and the number of e(t) observations models can be suitable for both.
per curve ranged between 2 and 250, the creep curves Certain model-fitting approaches are more applicable to
having been generated by interrupted and continuous large datasets, in particular, those involving a mixture of
measurement testing. For such datasets, Approach 2 or 3 continuous and interrupted measurement creep test records
appears to be the most appropriate procedures for model with a wide spectrum of ef(t,T,s) data points per unit time.
fitting (Tables 2 and 3), both approaches effectively Such approaches effectively average the multi-cast ef(t,T,s)
averaging the multi-cast ef(t,T,s) data in a balanced way data in a balanced way prior to model fitting.
prior to final model fitting. Whereas values for the model-fitting effectiveness para-
meter of Z-2 are achievable for single-cast creep strain
4.3. Practical application datasets which are well distributed in terms of (T,s), Z
values of 6–7 may have to be regarded as acceptable for
Model selection can also depend on the purpose for model equations representing alloy mean behaviour
which the materials creep strain description is required. determined from the results of large multi-source, multi-
Typically, the priority of the scientist is for a creep model cast datasets.
equation to have a sound physical basis in the primary,
secondary, and tertiary regimes. As a generality, it is more
Appendix A. Creep strain equations adopted in assessment
important for design and assessment engineers for the
inter-comparisons
model equation to be simple to implement and effective in
its description of creep deformation at long times (e.g. A.7
A.1. Modified theta model [4]
[10]). For design engineers, effective modelling is more
important in the relatively low-strain primary/secondary
creep regimes whereas for remaining life assessment f ¼ y1 ð1 expðy2 tÞÞ þ y5 t þ y3 ðexpðy4 tÞ 1Þ,
engineers, the priority is more likely to be an accurate where logðyi Þ ¼ ai þ bi T þ ci s þ d i Ts
knowledge of secondary/tertiary behaviour.
and y5 ¼ Asm expðQ=RTÞ. ðA:1Þ
5. Summary
A.2. BJF model [5]
Results are reviewed of an ECCC work programme to
investigate procedures for the practical representation of f ¼ n1 ð1 expðtÞb þ n2 tÞ,
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Z
the P91 case F(e,s) is of the form: a0 þ a1 log s2 þ
where t ¼ ðseff =A1 Þn expðQ=RT Þ dt
a2 log 3 :
s s m
seff ¼ and o _ ¼B . ðA:2Þ
1o 1o A.9. Modified omega model [14,15]
1 1
A.3. Modified Garofalo [6] f ¼ ð lnðtu tÞ þ lnðtu ÞÞ
O 2C tr
þ C tr ð1 expðmtr tÞÞ. ðA:9Þ
per ¼ i þ f1max ½1 expðDðt=t12 Þu Þ
þ _ p;min t þ c23 ðt=t23 Þf . ðA:3Þ
A.10. Modified Sandström [16]
Pnpol
A.4. Li-Akuluv model [7,8] ðF ð;sÞþf 2 ðTÞ=f 1 ðTÞð1=f 1 ðTÞÞ ajþ1 log sj Þ
t ¼ 10 j¼0 , (A.10)
where F ð; sÞ ¼ b1 log 4 þ b2 log 2 þ b3 T log s þ b4 T þ
_f;min _i _f;min
f ¼ ln 1 þ ð1 expðktÞÞ þ _s t b5 log s and any time temperature parameter satisfying
k _ f;min TTPðt; TÞ ¼ f 1 ðTÞ log t þ f 2 ðTÞ can be used.
þ T ðexpðt=tt Þ 1Þ. ðA:4Þ
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