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Geomech. Geophys. Geo-energ. Geo-resour.

(2024) 10:43
https://doi.org/10.1007/s40948-024-00751-3

ORIGINAL ARTICLE

Damage and hardening evolution characteristics


of sandstone under multilevel creep–fatigue loading
Zhang Bichuan · Liang Yunpei · Zou Quanle ·
Ning Yanhao · Kong Fanjie

Received: 11 January 2022 / Accepted: 10 January 2024


© The Author(s) 2024

Abstract During the operation of artificial under- trends under this loading path, and the evolution of the
ground structures, the surrounding rock experiences Mohr–Coulomb envelope is discussed. The proposed
fatigue and creep damage caused by several types of model can be used to describe the test data and the
disturbances under long-term constant loading. To evolution of the creep–fatigue process. With increas-
quantify the mechanical response of sandstone under ing creep–fatigue number, the acoustic emission ampli-
creep–fatigue loading, a damage–hardening evolution tude, energy, and cumulative counts increase. How-
model based on the linear superposition concept is ever, the amplitude is more sensitive than the energy,
proposed. In the model, coupling is applied to repre- indicating that it is more suitable for describing creep–
sent the synergistic effect of creep and fatigue. Creep– fatigue loading. Furthermore, the peak frequencies of
fatigue tests of sandstone specimens are conducted the AE signals are mostly distributed in the 0–15 kHz,
under multilevel loading. The damage and hardening 15–30 kHz, 30–45 kHz, and 45–55 kHz regions. The
effects of sandstone under creep–fatigue loading are signal proportion in the 45–55 kHz zone decreases
complex. Hardening is the dominant effect under low with the creep–fatigue number. However, other fre-
creep–fatigue loads, and damage is the dominant effect quency zones increase with the creep–fatigue number.
under high creep–fatigue loads. The strength of the This phenomenon illustrates that the crack scale of the
rock specimens undergoes increasing and decreasing specimens increases with the creep–fatigue number.

Highlights
Z. Bichuan
Key Laboratory of In‑Situ Property‑Improving
Mining of Ministry of Education, Taiyuan University • Damage and hardening effects are competitive
of Technology, Taiyuan 030024, China under multiple creep–fatigue cyclic loads.
• Low and high creep–fatigue loads dominate the
L. Yunpei (*) · Z. Quanle (*) · N. Yanhao · K. Fanjie
State Key Laboratory of Coal Mine Disaster Dynamics hardening and damage effects, respectively.
and Control, Chongqing University, Chongqing 400044, • Acoustic emission signals are obvious during
China cyclic loading.
e-mail: liangyunpei@cqu.edu.cn
Z. Quanle
e-mail: 756873156@qq.com Keywords Damage–hardening model · Rock
L. Yunpei · Z. Quanle · N. Yanhao · K. Fanjie damage · Acoustic emission · Mohr‒Coulomb circle
School of Resources and Safety Engineering, Chongqing evolution · Crack propagation
University, Chongqing 400044, China

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1 Introduction (Zhang et al. 2019). The crack closure, elastic, stable


crack propagation, and unstable propagation stages
Sandstone is a geological material widely used in can be identified through AE count curves (Ranjith
many fields, such as coal mining (Chen et al. 2023; et al. 2004). For one or more preexisting flaws in
Ran et al. 2023b), tunnel design (Xue et al. 2020), and specimens, the AE count can describe the relation-
blasting engineering (Cerfontaine and Collin 2018). ship between fracture propagation and the AE count
In these engineering applications, the sandstone expe- (Huang et al. 2018). A transition of the failure from
riences long-term static loading and periodic distur- the shear mode to the tensile mode can be obtained
bance (Yang and Hu 2018; Zhao et al. 2021; Liang through the RA (rise angle) –AF (average frequency)
et al. 2023). These environmental and human-induced distribution (Liu et al. 2020). AE technology can
loadings are essentially cyclic and time-depend- determine the accurate damage location through 6 or
ent (Cerfontaine and Collin 2018). Therefore, the more acoustic emission sensors (Yang et al. 2012).
creep–fatigue mechanical properties of this rock have The AE energy and amplitude can reveal the mechan-
attracted the attention of many researchers because ical characteristics under true triaxial compression
they are crucial for designing and constructing syn- conditions. However, only limited studies on the AE
thetically manufactured projects. characteristics under creep–fatigue conditions have
Numerous scholars have investigated the strength, been conducted.
deformation, and failure behaviors of rocks under dif- Several creep or damage models have been pro-
ferent loading paths (Zhang et al. 2021; Wang et al. posed to describe the time-dependent behavior of
2015; Liang et al. 2023; Ye et al. 2022). Mechanical rock under certain conditions. These models involve
characteristics are good signs of damage and harden- the initial damage (Hou et al. 2019), energy dissi-
ing effects. The changes in the mechanical parameters pation (Liu et al. 2016), strain hardening (He et al.
of a specimen are closely related to the loading envi- 2013), strain rate (Hajiabadi and Nick 2020), and gas-
ronment (Ran et al. 2023a; Ye et al. 2023; Zou et al. containing state. Previous models have been applied
2023). For example, the peak strength and elastic mainly to certain pure loading conditions. Sandstone
modulus of sandstone are highly reliant on the confin- in engineering structures experiences creep–fatigue
ing pressure (Zhang et al. 2015). Sandstone exhibits loading. The effects of creep and cyclic on rock fail-
brittle and ductile behaviors at low and high confin- ure are different. The coupled hardening and dam-
ing pressures, respectively (Wasantha et al. 2012). In age of sandstone are essential to the stability and
addition, low–high–low and high–low–high loading safety of underground engineering, but information
paths significantly affect the creep behavior of sand- about the coupled effect and evolution characteris-
stone (Chen et al. 2019). Heap et al. (2009) reported tics of these processes is scarce. To establish a suit-
that after long-term loading that leads to corrosion, able creep–fatigue model, the first steps are to con-
sandstone fails at stresses lower than the uniaxial sider cyclic fatigue and to identify the parameters
compressive strength (UCS). The creep behavior of that affect the damage process (Eftekhari and Fatemi
sandstone is relatively sensitive to dynamic distur- 2016). Then, the creep damage evolution charac-
bances under a high creep load; a higher energy dis- teristics should be developed. These approaches
turbance results in a shorter failure time and a more can describe the creep procedure macroscopically
significant strain rate (Zhu et al. 2019). In addition, and do not require many parameters. In addition,
the fracture system and propagation characteristics creep–fatigue loading can produce a hardening effect
under creep–fatigue loading are more complicated on rock materials. Finally, by taking the factors and
than those under multistage creep loading (Xu and coupling influences into consideration, a constitutive
Yang 2016). model can be proposed to describe the comprehensive
Acoustic emission (AE) behaviors have been behaviors of materials under certain loading condi-
proven to be an auxiliary tool for investigating dam- tions (Chaboche 2008).
age and hardening evolution characteristics in rock In this paper, a damage–hardening evolution model
and concrete materials (Liu et al. 2020). The AE tech- is proposed to describe the comprehensive effect of
nique mainly involves the AE time series, spectrum, creep–fatigue loading on sandstone. To verify this
spatial distribution, and fracture propagation mode model, multilevel creep–fatigue tests are conducted

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under load control modes. Then, the deformation and that creep damage and fatigue damage exhibit vis-
AE signal characteristics are analyzed. The results of ible coupling effects. Thus, the total damage D can be
this research can enrich the understanding of mining- divided into Dc and Df (Eftekhari and Fatemi 2016).
induced boundary evolution and may be helpful for Creep deformation is associated with the material.
identifying stable regions for gas drainage. When the strain reaches a critical value, the material
fails. Thus, the creep damage variable can be defined
as follows:
2 Damage–hardening evolution model t

∫0 𝜀∗C
𝜀̇
Dc = dt (1)
Herein, the damage and hardening evolution behav-
iors of multilevel creep–fatigue cycles are investi-
The damage process begins at the initial load-
gated. Each sandstone specimen needs to be cycli-
ing and ends when the material fails. The Dc value
cally and constantly loaded until failure. To simplify
ranges from 0 to 1. t is the duration time for con-
the damage–hardening model and facilitate the calcu-
stant stress. 𝜀∗C is the multiaxial creep ductility,
lation of the parameters, the softening and hardening
which can be defined as the uniaxial creep fracture
effects can reach zero at the beginning of the tests.
strain.
Two kinds of effects are considered separately. First,
the proposed model is based on the ductility exhaus- 𝜀̇ = Ce𝛽𝜎 (2)
tion theory. Second, the damage and hardening effects
are considered in creep or cyclic loading processes. where C and 𝛽 denote the material constant and creep

Finally, a nonlinear summation method is derived by exponent, respectively, 𝜎 denotes the deviatoric stress,
and 𝜀̇ is the strain rate, which can be calculated by the
Norton power law (Heap et al. 2009).
𝜀C
𝜀∗C = [ ] (3)
sin[2h(p − 0.5)∕3(p + 0.5)]∕ sin 2h𝜎m (p − 0.5)∕𝜎eq (p + 0.5)

the damage–hardening model to include creep and where 𝜀C is the uniaxial creep fracture strain; 𝜎m is the
cyclic loading. This model can describe the mechani- mean stress; 𝜎eq is the equivalent stress; h is the ratio
cal behaviors of rock under creep and cyclic loading of 𝜎m and 𝜎eq ; and p is the power law exponent.
conditions. The following assumptions are made: 𝜎m 𝜎 + 𝜎2 + 𝜎3
h= = 1 (4)
𝜎eq 3𝜎eq
Rock specimens do not contain any defects at the
beginning of creep–fatigue testing.
The damage and hardening effects are functions of [ ( )2 ( )2 ( )2 ]1∕2
1
𝜎eq = 𝜎 1 − 𝜎 2 + 𝜎 2 − 𝜎3 + 𝜎 3 − 𝜎 1
the cycle number during cyclic loading. In addi- 2
tion, the time effect is ignored in this procedure. (5)
The damage and hardening effects can be super- where 𝜎1, 𝜎2 and 𝜎3 represent the maximum, interme-
imposed linearly through normalized damage diate, and minimum principal stresses, respectively.
and hardening parameters; thus, the full effects of Under the creep–fatigue loading test, creep dam-
creep and cyclic loading can be described. age accumulates during the loading time. There-
fore, the creep damage is calculated only during the
2.1 Damage evolution model creep process, and the cyclic loading stage can be
ignored.
When creep damage (caused by the loading duration) The accumulation of damage characterizes
and fatigue damage (caused by relatively high-level fatigue. During the cyclic loading process, the
cyclic loading) occur simultaneously, it is assumed ductility of the material decreases, and energy

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dissipates during the fatigue procedure. Equa- Hc


tion (6) can be used to calculate the fatigue damage He� = (9)
𝜎mon + Hc
variable.
During the cyclic loading process, the strength of
( ( )1−c )1− b+1
f
the rock material increases, especially during low-
N (6)
DF = 1 − 1− cyclic loading. When the maximum cyclic stress
NF
exceeds 𝜎l , the hardening effect is obvious. Similar
to fatigue damage, the cyclic hardening effect can
where b and f are material constants and Nf is the
be described by Hf′.
number of cycles and failure cycles, respectively,
at a specific deviatoric stress. The value of DF is 0 � � f �
⎧ � �1−c �1− b+1
when the cycle number is 0. When the cycle number ⎪𝜆 1− 1− N
𝜎 ≤ 𝜎l
reaches NF, the specimen fails. During the fatigue Hf� = ⎨ NF (10)

process, the creep effect is ignored. Determining NF ⎩ 0 𝜎 > 𝜎l
is a challenging task. Thus, the relationship between
NF and the maximum cyclic stress can be expressed where 𝜆 is the cyclic hardening effect parameter, and
by Eq. (7) (Cerfontaine and Collin 2018). 𝜆 > 1.
𝜎max
𝜎mon
= −0.0278 log10 NF + 0.9455 (7) 2.3 Creep–fatigue interaction model

where 𝜎max and 𝜎mon represent the maximum cyclic When creep damage, cyclic damage, creep hardening
stress and monotonic strength 𝜎mon, respectively. and cyclic hardening occur simultaneously, the inter-
action effect can be represented by introducing a cou-
pling as follows (Eftekhari and Fatemi 2016):
2.2 Hardening evolution model
� � ⎫
dDc =
� fc 𝜎, Dc , Df , … dt� ⎪
When creep hardening (caused by the loading dura- dDf = ff 𝜎max , 𝜎m , Dc , Df , … dN ⎪
tion) and cyclic hardening (caused by low-level � ⎬ (11)
� c = fc (𝜎, …)dt
dH � ⎪
cyclic loading) occur simultaneously, it is assumed �
dHf = ff 𝜎max , 𝜎m , Dc , Df , … dN ⎪
that two kinds of loading can increase the strength ⎭
of the material. Thus, the total hardening H can be
divided into Hc and Hf . To simplify and make predictions from pure creep
During the steady creep procedure, the mate- and pure fatigue, it is assumed that creep and cyclic
rial experiences a creep-hardening effect. When the loading have a dual effect. The total dual effect of the
yield strength reaches the long-term strength (𝜎l ), two kinds of loading can be expressed as follows:
the strength of the rock does not increase, and the dF = 𝛼1 dDc + 𝛽1 + 𝛼2 dDf + 𝛽2 − 𝛼3 dHc� − 𝛽3 − 𝛼4 dHf� − 𝛽4
hardening effect approaches zero. With increasing (12)
time, the hardening effect narrows. This phenom-
enon can be described by the hardening function Hc where 𝛼1, 𝛼2, 𝛼3, 𝛼4, 𝛽1, 𝛽2, 𝛽3, and 𝛽4 are fitting param-
(Yongjun and Xiangke 2012): eters, and it is assumed that a = 𝛽1 + 𝛽2 − 𝛽3 − 𝛽4.
Thus, the comprehensive effect can be expressed by
C𝜎 t 𝜎 ≤ 𝜎l
{ 𝛾 1−𝛽
the following equation:
Hc =
0𝜎 > 𝜎l (8)
dF = 𝛼1 dDc1 + 𝛼2 dDf 2 − 𝛼3 dHc� − 𝛼4 dHf� + a (13)
where C , 𝛾 and 𝛽 are material constants, and 0 < 𝛾 < 1
,0 < 𝛽 < 1. The nonlinear accumulation and interaction can be
To minimize the hardening effect between 0 and derived by substituting Eqs. (6), (9), and Eq. (10) into
1, H ′ can be expressed through Eq. (9).

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Eq. (13). The time-dependent damage and hardening abbreviated as CFT. A PCI-2 system was used to col-
model can be reconstituted as follows: lect the AE signals in multilevel creep–fatigue load-

� � f �
⎧ � �1−c �1− b+1
⎪ (1 − 𝜆) 1 − 1 − N + ∫0 H 𝜀𝜀∗̇ dt − C𝜎 𝛾 t1−𝛽
+ a 𝜎 ≤ 𝜎l
t
⎪ N 𝜎mon +C𝜎 𝛾 t1−𝛽
(14)
F C
F=⎨ � �1− f
� �
+ ∫0 H 𝜀𝜀∗̇ dt + a
⎪ 1−c b+1
t
⎪ 1 − 1 − NN 𝜎 > 𝜎l
⎩ F C

Equation (14) is a piecewise function that is ing tests. The AE signals detected by the sensor were
divided by the long-term strength (𝜎l ) of a particular reamplified to more than 40 dB. Two AE sensors
rock. When the applied stress exceeds the long-term were assigned on the cylindrical surface of the rock
strength, the softening effect dominates the whole specimen in a symmetric position.
procedure, and the hardening effect is negligible. In The bottom and top surfaces of the specimens
contrast, we take both softening and hardening effects were ground flat to minimize the effect of the reac-
into consideration because their gaps are relatively tion. Three specimens in total were prepared for
small. creep–fatigue testing. The P-wave velocity was
measured in the axial direction. Closely packed
P-wave velocity samples were chosen for P-wave
3 Experimental material and test procedure experiments because they are good indicators of
specimen peak strength (Table 1). The upper and
Three sandstone specimens were used in these tests. lower loads of the cycles in this experiment were
These specimens were processed into standard speci- determined by the UCS value of the sandstone.
mens according to the instructions recommended by
the International Society for Molecular Medicine
(ISRM). The sample dimensions were 𝜙 50 mm × Table 1  P-wave velocity and density distribution
100 mm for the multilevel creep–fatigue loading tests. No P wave velocity (km/s) Mass (kg)
Multilevel creep–fatigue loading tests were con-
ducted using a rock compression system (Fig. 1) with #1 2.114 0.430
a flat cylinder striker that could produce cyclic load- #2 2.118 0.432
ing stress and long-term stable stress. The system is #3 2.114 0.431

Fig. 1  Experimental
system Acquisition System
Central control system
Dynamic strain gauge
Compression system

Electro-hydraulic
Rock sample servo system

Signal amplifier Oil pump


system
Acoustic emission
monitoring system

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Fig. 2  Stress‒time curves for multilevel CF tests: a 1st creep–fatigue cycle; b 3rd creep–fatigue cycle; and c 5th creep–fatigue cycle

Therefore, uniaxial compression tests were con- residual strength value. Finally, the CF tests were
ducted to determine these parameters. Then, the stopped.
upper stresses of the 1st, 3rd, and 5th creep–fatigue
cycles were set. Figure 2 shows the loading paths
of the CF tests, which consisted of different stages. 4 Results and discussion
The axial stress 𝜎1 was applied to the sandstone
specimens at a loading rate of 200 N/s during the 4.1 Verification of the proposed model under
cyclic loading and failure stage. A sinusoidal wave- different creep–fatigue loads
form was adopted to simulate cyclic loading. The
incremental cyclic loading stress was the same in 4.1.1 Prediction ability of the proposed model
each creep–fatigue stage. The axial stress remained
constant during every creep stage. When the sand- Three samples are used to verify the proposed dam-
stone specimens failed, the stress dropped to the age–hardening evolution model. The predicted results

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match well with the test data despite some fluctua- In the 1st and 3rd creep–fatigue procedure, the
tions at specific points. This result indicates that the damage–hardening evolution values are − 0.04929
proposed comprehensive impact model can describe and − 0.1886, respectively. This finding suggests
the comprehensive evolution characteristics of sand- that the hardening effect dominates in the 1st and
stone rock under creep–fatigue loading. 3rd creep–fatigue procedure. The hardening effect is
In the first creep–fatigue cycle, the comprehen- more obvious after 3 creep–fatigue cycles. The UCS
sive effect of sandstone is dominated by hardening. of the specimen increases from 48.7 to 53 MPa,
The compaction and closure of microcracks and the verifying the evolution of the damage–hardening
growth of new cracks increase the value of the dam- value. However, when the rock specimens experi-
age variable. However, this process results in relative ence additional creep–fatigue loads, the damage
hardening. Cyclic and creep hardening effects can be effect dominates, and the damage–hardening evolu-
calculated by Eqs. (9) and (10), respectively, which tion value is 0.7559. This finding indicates that the
show similar increasing trends with respect to the softening effect is dominant when specimens expe-
elastic modulus. Thus, the creep–fatigue hardening rience additional creep–fatigue loading procedures.
model can be used to describe the hardening effect A decrease in the peak strength to 45.6 MPa veri-
well. fies that additional creep–fatigue procedures occur
After three creep–fatigue cycles, because the (Figs. 3, 4 and 5).
microcracks are closed under the applied loading,
the rate of new crack generation stabilizes. Moreo- 4.1.2 Mohr circle variation with respect
ver, the matrix of the sandstone is compacted, and to the creep–fatigue model
damage accumulates during this stage. The elas-
tic moduli reach their maximum values when the The creep–fatigue model is used to describe the
creep–fatigue stress reaches a point close to the rock mechanical behavior near the mining-induced
long-term strength of the rock. Additionally, the boundary. After coal excavation, the minimum prin-
hardening effect dominates the process when the cipal stress 𝜎3 of the rock reaches approximately zero,
creep–fatigue stress is lower than this value. depending on the position (Fig. 6a). At locations far
In the fifth creep–fatigue procedure, the matrix from the excavation site, the rock experiences a lower
of sandstone produces new cracks. At this time, the stress disturbance and undergoes a long-term creep
damage variable increases rapidly. When the dam- procedure; subsequently, the strength of the rock
age accumulates to the critical value, macroscopic increases under low creep–fatigue loads (Fig. 6b).
cracks form in the sandstone. The comprehensive effect F is less than zero. In
contrast, the strength of rock decreases under high
creep–fatigue loads (Fig. 6c). The F value is greater
0.05 than zero.
Test results
Proposed model
The CF model is a coupling model that simulates
0.04
the time-dependent increases and decreases in the
deformation and strength characteristics of brittle
Fatigue damage variable

rocks. The increase and decrease rates are related to


0.03
the accumulated strain. However, the model is on a
small scale. It is impossible to describe the defor-
0.02
mation characteristics of rocks that contain obvi-
ous joints. In contrast, the stress and strain values
0.01
obtained from the in-situ environment are different.
As a result, this model is designed to improve the
0.00
0 2 4 6 8 10 12 14 16 18 20 22
understanding of multilevel CF conditions, and only
Cycle number qualitative conclusions are drawn.

Fig. 3  Comparison of the proposed model and cyclic damage


data from the 1st creep–fatigue cycle

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0.5 0.13
(a) 1 CF (b) Test results
2 CFs Proposed model
3 CFs
0.4
0.12

Fatigue damage variable


Fatigue damage variable

0.3

0.11

0.2

0.10
0.1

0.0 0.09
0 10 20 30 40 50 60 70 0 2 4 6 8 10 12 14 16 18 20 22
Cycle number Cycle number
0.30 0.44
Test results (d) Test results
(c)
Proposed model Proposed model
0.42

0.28
Fatigue damage variable

Fatigue damage variable


0.40

0.38
0.26

0.36

0.24 0.34

0.32

0.22
0 2 4 6 8 10 12 14 16 18 20 22 0.30
0 2 4 6 8 10 12 14 16 18 20 22
Cycle number
Cycle number

Fig. 4  Comparison of the proposed model and damage evolution characteristics in the 3rd creep–fatigue cycle. a Damage distribu-
tion in the 3rd creep–fatigue cycle. b, c, and d Comparisons of the proposed model and test data

4.2 Mechanical and AE characteristics of sandstone The spacing of the hysteresis loop is the largest during
under different creep–fatigue loads and the cyclic loading. In the middle cyclic loading stage, the
corresponding relationships with damage and axial deformation steadily and slowly increases. The
hardening effects elastic characteristics of the sandstone matrix dominate
this phenomenon. The spacing of the hysteresis loop
4.2.1 Mechanical behaviors of sandstone decreases with increasing creep–fatigue number. In the
under different creep–fatigue loads high-stress cyclic loading stage, the strain rate increases
rapidly until the specimen fails. The spacing of the
The stress‒strain curves and peak stresses of sand- hysteresis loop changes with increasing creep–fatigue
stone after multiple creep–fatigue cycles are plotted, level. The peak strength first increases from 48.7 MPa
as shown in Fig. 7. The cyclic loading characteristics to 53 MPa and then decreases to 45.6 MPa.
at different stress stages show noticeable differences. The deformation cannot recover when the extra
In the low cyclic loading stage, the axial strain devel- stress is removed. In this work, the calculation method
ops rapidly, and the deformation accumulates quickly. for the irreversible strain of the samples is illustrated in
This phenomenon may arise due to the compression of Fig. 8. The irreversible strain of each cycle can be cal-
the microcrack. The deformation of sandstone includes culated through Eq. (15).
the deformation of the sandstone matrix and crack.

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0.8 0.065
(a) 1 CF Test results
(b)
0.7 2 CFs Proposed model
3 CFs
0.060
4 CFs
0.6

Fatigue damage variable


Fatigue damage variable

5 CFs
0.5
0.055

0.4

0.050
0.3

0.2
0.045
0.1

0.040
0 20 40 60 80 100 120 0 2 4 6 8 10 12 14 16 18 20 22
Cycle number Cycle number
0.19 0.36
Test results Test results
(c) (d)
Proposed model Proposed model
0.34
0.18

Fatigue damage variable


Fatigue damage variable

0.32

0.17

0.30

0.16
0.28

0.15 0.26
0 2 4 6 8 10 12 14 16 18 20 22 0 2 4 6 8 10 12 14 16 18 20 22
Cycle number Cycle number
0.52 0.70
Test results
(e) Test results (f)
Proposed model Proposed model

0.68
0.50
Fatigue damage variable
Fatigue damage variable

0.66

0.48

0.64

0.46
0.62

0.44 0.60
0 2 4 6 8 10 12 14 16 18 20 22 0 2 4 6 8 10 12 14 16 18 20 22
Cycle number Cycle number

Fig. 5  Comparison of the proposed model and cyclic damage evolution characteristics in the 5th creep–fatigue cycle. a Damage dis-
tribution in the 5th creep–fatigue cycle. b–f Comparisons of the proposed model and test data


N

N
( n ) where 𝜀irr and 𝜀nirr denote the changes in irreversible
𝜀irr = 𝜀nirr = 𝜀total − 𝜀nelastic (15) axial strain during all the cycles and in a single cycle,
n=1 n=1 respectively, and n represents the number of cycles.

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per cycle in the cyclic loading stage. AE counts in


the lower cycle stress stage first show a considerable
increase. The number approaches 0 (Figs. 9, 10a and
11b). This phenomenon may first result from micro-
crack compression. In addition, new fractures may
not form under low loads. Thus, the irreversible
strain increases slowly. In the middle-stress stage,
the AE counts exhibit a steady trend (Fig. 10b and
c and Fig. 11b, c, and d), corresponding well with
the plastic deformation evolution. This phenomenon
may indicate that the fracture propagation speed can
remain constant. Under high loads, the AE count
decreases. This decrease may occur due to the large
fractures that rift through. The number of large frac-
tures is less than the number of small fractures. Thus,
the AE count is much lower than that in the middle
stress stage.

4.2.2 Variations in the AE count, amplitude,


and energy with creep–fatigue time

The variations in the AE parameters, such as ampli-


tude, energy, and count, and the fracture process are
evaluated under different creep–fatigue conditions to
describe the damage and hardening characteristics.
The AE counts can be used to describe the damage
accumulation and fracture propagation. As shown in
Fig. 12, at the beginning of the creep–fatigue proce-
dure, the initial AE signals have lower amplitudes and
energies than during failure. This phenomenon may
result from crack closure, which can produce some
signs of instantaneous strain when the upward pres-
sure head of the experimental machine touches the
rock specimens. However, there are few AE signals
Fig. 6  Strength evolution during the CF test. a Excavation in the creep procedure, especially when the creep
effect of rock near the mining-induced boundary; b increasing pressure is low (Fig. 12a). This finding suggests that
trend in strength under low-CF loads; and c strength degrada- relatively less damage is produced in this stage, and
tion under high-CF loads hardening may dominate the process. However, as the
creep pressure increases, the AE count increases. The
Furthermore, 𝜀ntotal and 𝜀nelastic indicate the final and AE energy increases noticeably with cumulative count
initial strains after n loading and unloading cycles. due to the generation and growth of large fractures.
The irreversible strain (plastic deformation) Microcrack generation and propagation may produce
increases with increasing number of cycles (Figs. 9, few AE signals. This finding suggests that the dam-
10 and 11). An increase in irreversible strain denotes age effect increases during this stress stage, and the
the amount of energy dissipated, which indicates the hardening effect may reach zero. Thus, an increase in
accumulation of damage per cycle (Liu et al. 2014). the AE count under constant stress is a good indicator
The sandstone specimens in the creep–fatigue test of accumulated rock damage. For rock specimens that
fail at a stress lower than the UCS. These phenom- experience additional creep–fatigue cycles, micro-
ena arise due to the accumulated irreversible strain cracks may fully develop. In the failure process, the

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Fig. 7  Curves describing the mechanical characteristics of sandstone specimens after multiple creep–fatigue cycles. a, b and c rela-
tionships between the stress and strain under different uniaxial creep–fatigue loads

AE waves may superimpose, leading to a significant


number of AE signals. Moreover, the shape of the
cumulative counts changes as the creep–fatigue time
increases. However, the AE amplitude is more sensi-
tive than the AE count under creep–fatigue loads. The
AE amplitude is a good indicator for distinguishing
between low and high stress creep–fatigue conditions.
AE signals can hardly be observed under low creep
loads. However, these signals can be detected under
high creep loads.

4.2.3 RA–AF distribution and its relationship


with fracture mode

Fig. 8  Schematic of the calculation of irreversible deformation The reciprocal gradient of the AE signal wave-
form can be described by the RA value, as shown
in Fig. 13. RA is a valuable tool for describing
AE signal characteristics (Sagar and Prasad 2012).
500
A combination of RA and AF is commonly used
6 450
to analyze the failure modes of rock and concrete
5
400
materials (Wang et al. 2016; Han et al. 2019). A low
350
RA and high AF indicate that the tension dominates
Irreversible strain (10-3)

The number of counts

4 300 fracture generation or propagation. This kind of


3
250 energy release is often initiated by fast longitudinal
200 waves. In contrast, a high RA and low AF suggest
2 150 that shear constitutes the main fracture evolution
100 mechanism and produces slow shear waves. The
1
50 ratio of the AF to RA values increases with increas-
0
0 ing creep–fatigue cycles, showing that the failure
-50 characteristics evolve from the tensile mode to the
0 2 4 6 8 10 12 14 16 18 20
Cycle loading and unloading times shear mode under this loading procedure. The evo-
lution of this signal reflects the damage accumula-
Fig. 9  Irreversible strain evolution in the 1st creep–fatigue tion characteristics.
cycle

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6 6.4 20
(a) 8000
(b)
5 7000 6.2 15

6000
Irreversible strain (10-3)

Irreversible strain (10-3)


The number of counts
4

The number of counts


6 10
5000
3
4000
5.8 5
2 3000

5.6 0
2000
1
1000
5.4 -5
0
0

0 2 4 6 8 10 12 14 16 18 20 5.2 -10
0 2 4 6 8 10 12 14 16 18 20
Cycle loading and unloading times
Cycle loading and unloading times

6.55 20
(c)
6.50
16
6.45
Irreversible strain (10-3)

The number of counts


12
6.40

6.35 8

6.30
4
6.25
0
6.20

6.15 -4
0 2 4 6 8 10 12 14 16 18 20

Cycle loading and unloading times

Fig. 10  Irreversible strain evolution in the 3rd creep–fatigue cycle. a, b, c irreversible strain after 1, 2, and 3 creep–fatigue cycles,
respectively

Figure 13 shows the typical variations in the RA the final fault plane. With the continuation of the
and AF values with time at different creep–fatigue creep–fatigue loading process, the gap enlarges
procedure. During one creep–fatigue test, AE sig- again, and the fracture mode changes back to ten-
nals are produced at the beginning of cyclic load- sion, which becomes the dominant failure mode
ing. In the later cyclic loading and creep process, again.
no apparent signals are produced. In the failure Another method for quantifying fracture behav-
stage, increases in the RA value are associated with ior is to employ the RA–AF distribution. Tensile
a decrease in the AF value, which can be attrib- cracks may produce AE signals with low RA val-
uted to the occurrence of the shear mode. Impor- ues and high AF values. The shear cracks exhibit
tantly, as shown in Fig. 13b, the gap between the the opposite trend. As shown in Fig. 14, the RA–AF
RA value and the AF value is narrow. This finding values are primarily distributed along the Y-axis
indicates a transition from tensile to shear fracture. during one creep–fatigue test, which indicates that
In the three creep–fatigue tests, the shear and ten- tensile cracking is the dominant fracture mode.
sile fracture generation speeds and propagations However, with increasing creep–fatigue cycles, the
are approximately equal. As the stress increases to RA–AF values tend to be evenly distributed along
a specific value, the fracture propagates and forms the X-axis and Y-axis, indicating that the tensile

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7 7.1 40
600
(a) (b)
6 7.0 35
500
6.9 30
5
Irreversible strain (10-3)

Irreversible strain (10-3)


The number of counts

The number of counts


400 25
6.8
4
300 6.7 20
3
6.6 15
200
2
6.5 10
100
1
6.4 5

0 0
6.3 0

-1 -100 6.2 -5
0 2 4 6 8 10 12 14 16 18 20 0 2 4 6 8 10 12 14 16 18 20

Cycle loading and unloading times Cycle loading and unloading times

7.6 40 8.6 60
(c) (d)
7.5
50
8.4
30
7.4
Irreversible strain (10-3)

Irreversible strain (10-3)


40
The number of counts

The number of counts


8.2
7.3
20
30
7.2 8
20
7.1 10
7.8
10
7
0 7.6
6.9 0

6.8 7.4
0 2 4 6 8 10 12 14 16 18 20 0 2 4 6 8 10 12 14 16 18 20

Cycle loading and unloading times Cycle loading and unloading times

9.6 50
(e)
40
9.4
Irreversible strain (10-3)

30
The number of counts

9.2

20
9
10

8.8
0

8.6 -10

8.4 -20
0 2 4 6 8 10 12 14 16 18 20

Cycle loading and unloading times

Fig. 11  Irreversible strain evolution in the 5th creep–fatigue cycle. a b, c, d and e represent irreversible strains after 1, 2, 3, 4 and 5
creep–fatigue cycles, respectively

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Fig. 12  Curves of the AE count, amplitude, and energy with


time at different creep–fatigue cycles under uniaxial compres-
sion and impact loading. a, b and c Results of uniaxial com-
pression tests after 1, 3, and 5 creep–fatigue procedure

and shear cracking modes are equal. Finally, when Fig. 13  Trends in the mean RA and AF parameters under uni-
axial compression and impact loading in sandstone. a, b and
the creep–fatigue process continues, tensile crack- c Uniaxial compression after 1, 3, and 5 creep–fatigue proce-
ing gradually dominates, suggesting that tensile dure, respectively
cracking dominates the failure mode after 4 and
5 creep–fatigue cycles. After one creep–fatigue
procedure, the cracks propagate along the radial 4.2.4 Peak frequency and acoustic emission counts
direction of the rock sample, resulting in split frag- in different creep–fatigue stages
ments. With increasing creep–fatigue cycles, there
is enough time for the microcracks to develop and The frequency is another parameter used to describe
propagate. The main crack tends to propagate along the source type of AE signals. This parameter can be
the weak planes. With increasing creep–fatigue pro- used to describe the internal state and the associated
cedure, the radial cracks may connect, and the ten- fracture mechanism of a rock. The different fracture
sile failure mode can dominate the process again. modes may release energy at different frequencies.

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(a) (b) (c)


1.0 1.0 1.0
Tensile mode
Tensile mode Tensile mode
0.8

Normalized AF value
0.8 0.8

Normalized AF value
Normalized AF value

0.6 0.6 0.6


Shear mode Shear mode
0.4 Shear mode 0.4 0.4

0.2 0.2 0.2

0.0 0.0 0.0


0.0 0.2 0.4 0.6 0.8 1.0 0.0 0.2 0.4 0.6 0.8 1.0 0.0 0.2 0.4 0.6 0.8 1.0

Normalized RA value Normalized RA value Normalized RA value

Fig. 14  Distribution of RA–AF values in granite during different creep–fatigue cycles under uniaxial compression. a, b and c Uni-
axial compression tests after 1, 3, and 5 creep–fatigue cycles, respectively

Large cracks may release low-frequency components, To analyze the variations in the counts with dif-
while small cracks may produce high-frequency com- ferent creep–fatigue procedure, the distribution per-
ponents. The peak frequency can be regarded as the centages of different creep–fatigue tests are plot-
main frequency of the signal, and the source type can ted, as shown in Fig. 16. At the early creep–fatigue
be classified. As shown in Fig. 15, the distribution of stage, the counts increase (Fig. 16b, c), and microc-
the peak frequency exhibits prominent zonal features, racks may be produced or propagated. However, at
and the frequency is located in the ranges of 0–15 low creep–fatigue loads, cyclic and creep loading
kHz, 15–30 kHz, 30–45 kHz, and 45–55 kHz. are insufficient for producing fatigue. Thus, when the
As the creep–fatigue time increases, the signal dis- cyclic or creep loading levels increase, the rates of
tributions at the beginning and failure stage exhibit crack production and propagation increase, thereby
a significant scale peak frequency. However, in the increasing the count. However, when the loading
middle creep–fatigue stage, the AE signals are con- increases, the energy may be concentrated in the
centrated at a relatively low frequency. On the one microcrack propagation process, which consumes
hand, a short creep–fatigue test shortens the crack relatively little energy. An increase in the speed of
propagation process in the early stage. Creep–fatigue counts may not be obvious (Fig. 16c).
increases, especially under relatively high creep In this paper, a damage hardening evolution model
stresses. The cracks produced during the previous is proposed based on the synergistic effect of creep
loading may continue to propagate during the creep and fatigue. In the future, when evaluating the dam-
process. These cracks are relatively small because the age and hardening characteristics in real situations
final fault plane has not formed. On the other hand, with complex loads, this model may be applied
45–55 kHz accounts for 54.6% of the frequency, to predict the lifetime of rocks. In addition, we can
which indicates that small-scale fracture propaga- obtain the damage–hardening values of a specific
tion occurs during one creep–fatigue cycle. With rock and can use then to determine the effects of these
increasing creep–fatigue cycles, the propagation of processes. It is difficult to quantify the relationship
large-scale fracture exceeds that of small-scale frac- between the damage–hardening evolution value and
ture. A larger fracture scale indicates greater dam- the strength of rock; this relationship may need to be
age. This trend can be used to describe the large studied further in the future.
damage accumulation effect. The proportion of low-
peak frequency (0–30 kHz) signals in the specimens
increases from 9.3 to 91.8% and to 92% after 1, 3, and 5 Conclusions
5 creep–fatigue procedure, respectively. This finding
indicates that relatively large crack propagation may Most artificial underground structures in a com-
occur in the late stages of creep–fatigue loading. pressed mechanical system are affected by

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Fig. 15  Peak frequencies under different creep–fatigue cycles. a Peak frequency versus time, b levels of five distinct peak frequency
bands, and c corresponding density cloud map

disturbances. Due to these disturbances, the rock sur- (1) A damage–hardening evolution model consider-
rounding these structures experiences creep–fatigue ing the damage and hardening effect is derived.
loading, and its deformation needs to be investigated. This model uses the nonlinear method to consider
In this study, creep–fatigue loading tests are con- creep and cyclic loading. The proposed model
ducted in a controlled manner with different numbers matches well with the test data and reflects the
of procedure. Several conclusions can be drawn:

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12000 187000 158400


(a) 11115 (b) (c)
186800 186678 158200 158152
10000 186600
158000
186400
12090
8000 186200
12000
186000
AE counts

AE counts

AE counts
6000 11800
30800 30713
800
4413 704
30600 658
608
4000
30400 600 558
30200 400
2000 279
30000
200 87 200

0 0
0
1 creep-fatigue stage destruction stage 1 creep-fatigue 2 creep-fatigue 3 creep-fatigue destruction stage 1 creep-fatigue 2 creep-fatigue 3 creep-fatigue 4 creep-fatigue 5 creep-fatigue destruction stage

Fig. 16  Variations in different stages after 1, 3, and 5 creep–fatigue procedure

comprehensive evolution characteristics of the included in the article’s Creative Commons licence and your
three deformation phases in sandstone. intended use is not permitted by statutory regulation or exceeds
the permitted use, you will need to obtain permission directly
(2) The creep–fatigue loading process affects the from the copyright holder. To view a copy of this licence, visit
UCS of sandstone. In creep–fatigue tests 1, 3, http://creativecommons.org/licenses/by/4.0/.
and 5, the damage–hardening evolution value
changes. A low creep–fatigue load increases the
peak strength of specimen, and a high creep–
fatigue load decreases it.
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