Professional Documents
Culture Documents
Bulletin of DRDO
ADVANCED SEMICONDUCTOR
DEVICE TECHNOLOGIES
Technology Focus
VSDu¨ykWth Q¨dl
2 JUNE 2023
Technology Focus
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the IR sensor technology based on MCT, T2SL, and Si MEMS are at a mature
stage of development. The Dewar to house the sensors and Sterling Cooler
to hold the DEWAR at cryogenic temperatures have been transferred to
production. Si Read Out Integrated Circuit (ROIC) is under production in
SCL, Chandigarh.
Sensors for safe and arm devices, CBRN and snow avalanche prediction
have been developed and transferred for production to industry. Quantum
and THz are emerging technologies that are also being pursued for futuristic
applications in sensors, imaging and computing at SSPL. GAETEC & STARC
are the pilot production FAB foundries that not only absorb the technologies
developed at SSPL but also hold a symbolic partnership with SSPL in the
very establishment invigilation.
For easy understanding of the readers, this issue is focusing on device
concepts in simple terms including fabrication processes. The devices and
circuits developed by SSPL have already been successfully implemented
in a variety of defence and space missions. I am sure, that this issue will
allow readers to obtain up-to-date information about emerging trends and
future directions of essential critical semiconductor device technologies. Key
articles in each section present snap-shot and mini reviews of state-of-the-
art inhouse results making the issue a must read for engineers, scientists,
and students working on development of advanced and futuristic device
technologies.
Dr Seema Vinayak
OS & Director, SSPL
4 JUNE 2023
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50V drain bias and power densities of ~10 W/mm
in S/C band, 5 W/mm in X-band has been attained.
Recently, SSPL also demonstrated HEMT devices
with power density of 3.5 W/mm at Ku band.
unit processes that need to be integrated to realise the Depletion mode HEMT devices with 1 A/mm peak
device with desired reliable reproducible performance. drain current density, DC trans-conductance of ~230
SSPL has developed all the processes required for the mS/mm and extrapolated power output of 5. 0-6.0
fabrication of AlGaN/GaN HEMTs namely, ohmic W/mm up to X-band have been achieved at 28 V
and Schottky contacts, surface passivation, e-beam operation. The main process parameters are shown
lithography, RIE for device isolation and gate slit in Table 1.
etching, implant isolation, inter-connect formation Table 1. Process Parameters
by lift-off and electroplating. Devices with gate length
Unit Process Attained Results
of 0.4 µm and 0.25 µm with cut-off frequencies of 26
GHz and 34 GHz, respectively, have been fabricated. Mesa isolation by RIE/ ~40 nA@ 100 V
To achieve the maximum performance of a particular Implant isolation with
mesa to mesa leakage
GaN HEMT, the features that hold the maximum
importance are high off-state breakdown voltage, Repeatable ohmic con- 0.3-0.6 ohm-mm
current collapse suppression, low gate and buffer tacts with FOM
leakage and low on state resistance. Optimisation Schottky contacts with 0.9-1.2 V@ 1 mA/mm
of these features through simulations, process repeatable Vf
technology development and characterisation has Reverse Schottky break- -80 V @ 1 mA/mm
been achieved at SSPL. The processes have been down
integrated on indigenously grown material by Surface Passivation by Minimal knee walkout.
MOCVD and MBE as well as on imported material. PECVD and ICPCVD Minimal current collapse
The main technology breakthroughs include the
Packaged devices with gate width of 7.2 mm have
control over breakdown voltage and minimised knee
been measured with saturated output power of 30 W
walkout after device surface passivation. Field plates
in S-band at 3 GHz. The in-house developed bias tees
have been incorporated over the gates to improve the
have enabled the on-wafer load pull measurement of
device breakdown voltage. The technology has been
large periphery devices. 3 mm devices with fish bone
developed on 75 mm AlGaN/GaN on SiC substrates configuration could be measured in a wafer mode
(Figure 1). with saturated output power of 15 W (Figure 2).
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The via-hole interconnection technology is very
important for AlGaN/GaN HEMT devices at microwave
frequencies. These structures help in parasitic
reduction at higher frequencies. SSPL has developed
in-house via-hole technology and implemented in the
AlGaN/GaN HEMT-based devices/MMICs on SiC
substrate for source grounding. The back-side image
of fabricated device with via source grounds is shown
in the Figure 5. All the active and passive components
Fig 7 (a). Small Signal Performance of Power Amplifier
have been fabricated with vias.
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GaN MMICs Power Amplifiers, Low-noise and developing capabilities of controlling and making
Amplifiers, Switches and TR Chips use of natural phenomenon for the betterment of
GaN HEMT-based C and X band power amplifier mankind. In the history of mankind, several efforts
MMICs low noise amplifiers and switch circuits have have been made in this direction and a number of
been successfully developed (based on external PDK) different kinds of sensors have been developed that
and demonstrated. GaN MMIC power amplifiers in C aid the human sensing. The infrared sensors are
band (5.4-5.9 GHz) with 40 W Pout and X band (9-10 some of those that provide the capability of seeing the
GHz) with 13 W, 20 W, and 30 W Pout using UMS PDK wavelengths higher than the wavelength band that
have been designed, fabricated, and characterised. can be sensed by the biological eyes of human beings.
The team demonstrated GaN-based 10 W C-Ku band
and 10 W Ku band high power amplifiers, low noise Infrared systems are used in numerous applications
amplifiers, and switch MMIC, which are required in ranging from defence, space, law enforcement,
huge numbers for the development of next generation thermographic inspections, astronomers, and many
electronic warfare and seeker applications. (Figure 9) more. IR imaging enables seeing in dark as it senses
the thermal energy emitted by the scene/objects
themselves. This also ensures passive imaging which
is very important for defence applications to avoid
detection by enemy. Another important feature of
IR imaging is visibility in fog, dust, and smoke as
Fig 9. Ku band Switch, LNA and Power Amplifiers IR radiation can penetrate through them. They are
used in missions ranging from surveillance to high
For radar applications, indigenous S band 130 W and performance target search, track, acquisition and
X band MMICs including power amplifier, low noise guidance. High performance infrared sensors are
amplifiers, and have been designed, fabricated and the most important elements of the night vision
tested meeting designed specifications. (Figure 10) technology. The emerging trends in the battlefield
scenario, threat perception, low intensity conflicts/
counter insurgency have led to the rapid technological
advancement in the development of Infrared Focal
Plane Arrays (IRFPAs) consisting of a 2-D staring
array of micro-size infrared sensors which is placed at
Fig 10. (a) 130 W Power Bar (b) Power Amplifier (c) Low Noise the focal plane of optics in a thermal imaging camera.
Amplifier
IRFPAs allow operating in day & night.
Looking at the present requirements of future Cooled thermal imaging cameras are the most
electronic warfare systems and radars, GaN has turned sensitive type of cameras to differentiate small
out to be the technology-of-choice for RF electronics. differences in scene temperature. They are the ones
Therefore, establishing commercially viable GaN that are preferred during war scenarios or military
material and MMIC technology is an important goal environments. They can detect the smallest of
that SSPL and GAETEC are determined to meet. This temperature differences between objects. Enhanced
is SSPL’s contribution towards self-reliance in GaN performance limits and reduction in cost desired
technology for meeting all the future requirements of by the users for infrared surveillance, night vision
strategic systems. cameras, thermal imaging in medical diagnosis,
etc. call for continuous research & development in
IRFPA this vital field. Hence continuous improvement in
Sensing beyond the human capability has been material quality, detector technology and associated
very useful and attractive for exploring the nature electronics is required for realising the desired
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performance with lower cost. Uncooled IRFPAs are and various other astronomical applications, etc.
less sensitive and slower than high performance Out of various potential material systems suitable
cooled ones. They are, however, generally, much less for SWIR imaging, the ability of InGaAs photodiodes
expensive and have lower SWaP, i.e., size, weight, to operate at room temperature with high quantum
and power requirements than the cooled IRFPAs. efficiency for wavelengths from 920 nm to 1700 nm
These sensors can be manufactured in fewer steps (that may be extended to the band of 500 nm to 2800
with higher yields. They require less expensive nm wavelengths also) makes it an optimal material of
vacuum packaging as they do not require cryocoolers, choice for SWIR imaging applications.
which are very costly devices and deteriorate the
Two dimensional image sensor array kept at
long time reliability of cooled IRFPAs. They tend
the focal plane of the optics is called Focal Plane
to have much longer service lives under similar
Array (FPA). These FPAs are usually fabricated by
operating conditions. Security applications often
hybridizing two chips, one containing the detector
require continuous operation of cameras to avoid
array of desired format and other one containing
the possibility of missing any threats. IR imaging
the signal processing circuitry to collect the detected
markets are seeing continuously increasing demands
signals from all individual detector elements of
in cooled and uncooled sensor segments.
detector array. The two chips, i.e., detector array chip
SSPL is working on development of both cooled and readout chip are joined together using Indium
and uncooled IRFPAs for past several years. IRFPAs, bumps using flip chip process. For SWIR detectors,
a major thrust area of the laboratory, involves state InGaAs is the suitable material, while Si is the only
of art technology from material development to final material suitable for realising high performance
integrated device. mixed signal VLSI circuits. Therefore, the InGaAs
photo-detector array is integrated with Si Readout
SWIR FPA Integrated Circuit (ROIC) for realising SWIR FPAs as
Short Wave Infra-red (SWIR), nominally 1-3 µm shown in Figure 11.
wavelength range, lies between the visible (VIS, 0.4-
0.8 µm band of wavelengths) and the Mid-Wave
Infra-Red (MWIR, 3-5 µm band of wavelengths)
region of electromagnetic spectrum and therefore,
enjoys the benefits of both. On one hand, wavelength
being shorter than MWIR, it provides better
resolution than that provided by MWIR. On the
other hand longer wavelength of SWIR compared
to VIS gives better atmospheric transmission.
Another advantage of SWIR over MWIR is the use
of reflected light for imaging rather than emissive Fig 11. Schematic Cross-section of InGaAs-based SWIR FPA
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package and Thermoelectric Cooler (TEC) after a is mostly a Capacitive Trans-Impedance Amplifier
detailed design for mesa structured detector array (CTIA). The n+ common contact is connected to
along with complete process design prepared in- the common connection ring of ROIC using indium
house for minimum dark current and maximum bumps. The photographs of certain sections of the
photo-response for near zero bias operation. Each detector array are shown in Figure 13 after individual
unit process is under optimisation for effective process steps.
repeatability, reliability, and yield improvement.
The performance of the detector elements and the
The detector array was designed using 2D and 3D test structures have been evaluated by measuring
numerical simulations in industry standard ATLAS
device simulator as shown in Figure 12. Figure 12 (a)
shows the 3D model of 5×5 mini detector array. The
central pixel was simulated with incident SWIR flux
and the photo generated carriers were investigated in
2D cut-plane as shown in Figure 12 (b).
(a)
Fig 13 (a) Photographs of the Sections of Detector Array after Mesa
Etching, (b) SEM Pictures after Mesa Etching, (c) Photogrpagh after
Metallisation, (d) Photograpgh after Indium Bump Growth
(b)
Fig 12. 3D Model of 5×5 Mini Detector Array
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The SWIR FPAs have been tested for their (PV) infrared detector array fabricated on a thin
radiometric response at Space Application Center (~10µm) HgCdTe layer grow on a lattice matched
(SAC), ISRO, Ahmedabad by bonding them in Chip- CdZnTe (CZT) substrate, hybridized to Read-Out
on-Board (CoB) PCB as shown in Figure 15 (a). After Integrated Circuit (ROIC) and packaged in a suitable
showing good response to the SWIR flux, these FPAs Dewar assembly, integrated to a cryo-cooler. IRFPA
have also shown good SWIR image of the objects technology involves several sub-technologies, like
when focussed on to them using SWIR optics. The growth of CdZnTe (CZT) substrates, growth of
images of the hot object, such as soldering iron and HgCdTe epilayers on these substrates, fabrication
the hot air blower are shown in Figure 15 (b). of photodiode arrays, design and development of
compatible CMOS ROIC, flip chip hybridization of the
detector array and the ROIC resulting in the Sensor
Chip Assembly (SCA), development of tactical Dewar
and JT (Joule-Thomson) cooler and final integration
of SCA, Dewar and cooler called as Detector-Dewar
Cooler assembly (DDCA). SSPL has developed all of
these sub-technologies at laboratory level for MW
(a)
IRFPA format 320x256/30 μm as well as 384x288/15
μm, 640x512/15 μm and demonstrated thermal
images of human target.
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640x512 array has also been procured, along with the of temperature cycles. An all metal Dewar suitable
development of 384x288 ROIC in collaboration with for packaging IRFPAs has been developed that
SCL, Chandigarh. Test setups for testing of ROICs at involves design and assembly of various components
SSPL have been established. To realise a hybrid focal like, HTCC feed-through, detector carrier/header,
plane array ROIC and detector arrays are flip chip cold shield, inner Dewar tube, evacuation tube etc.,
bonded through indium bumps that are grown both followed by integration, degassing and vacuum
on detector array and ROIC chip. Since two different sealing of Dewars. SSPL is competent to design
materials are being joined, temperature cycling from Dewar components and seal it with leak rate < 10-12
room temperature to detector operating temperature, Std. cc/s. Since high performance MWIR detectors
i.e., 80K, will result in a shift in alignment. work at cryogenic temperatures, SSPL has also
developed cryogenic coolers for IRFPAs.
In general, the detector array will contract more
than the silicon ROIC by an amount that can be Various equipment are installed to establish these
calculated from the known thermal expansion technologies for 320x256/30μm, 640x512/15μm,
coefficients. Technology to grow indium bumps and and 384x288/15μm MWIR FPAs at laboratory level.
flip chip bonding process has been developed such Images of some of these equipment installed at SSPL
that these hybrid arrays can withstand large numbers are shown in Figure 16.
Fig 16. Showing Equipment (a) Ellipsometer for HgCdTe Surface Characterization, (b) Mask Aligner for Photolithography, (c) Vacuum
Coating Unit for Passivation & Metallization, (d) ICP RIE for Dry Etching, (e) Cryoprober for Detector Array Testing at 80 K, (f) Parallel Gap
Welding for Electrical Connection with Feedthrough, (g) UHV for Ultra High Vacuum Sealing of Dewar, (h) FPA Tester, (i) Wafer Prober,
(j) Indigenously Developed Lab Level IR Camera
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Figure of merit for these detectors is Noise
Equivalent Temperature Difference (NETD) that
represents the minimum temperature difference
that produces the signal in the detector equal to its
temporal noise. It is basically the sensitivity of the IR
imager; lesser the NETD, better is the detector.
(b)
Fig 18 (a) The Measured NETD (in Histogram form as well as 2D
Intensity map) of a Best FPA Fabricated at SSPL (b) MWIR Images
of Human Target
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Development of Laser Diode Module and at GAETEC and SSPL and mounted on F-mount
C/F-mounted Laser Diode (10W, CW) packages as per the user requirements
Laser fencing is a technology for monitoring and (Figure 21). Light-current characteristic of 10 W
sensing of unwanted or suspicious intrusion in the single stripe laser diode are shown in Figure 22. The
desired area. SSPL has developed modules for laser 10 W CW single emitter fiber coupled laser diodes
fencing systems. Laser diode module is the heart find application directly in initiation of explosives
of fencing system. It includes a 1-2 W CW infrared for detonation. C-mount laser diode are used in laser
wavelength laser diode on a c-mount package, laser fencing application.
collimation lens, a heat sink and a fan for air cooling of
the module. Laser fencing modules for 100 m fencing
range have been successfully tested and delivered to
LASTEC (Figure 19). c-mounted laser diode units
(Figure 20) were delivered to CEL, Sahibabad for
their upcoming requirements as per the specifications
listed in Table 2. Fig 22. Light Current Chara-
Fig 21. F-mount Laser Diodes cteristics of 10 W Laser Diode
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Blue/Green Laser Diode metal. Various metal schemes, viz. Ni-Au, Pd/Au etc.
Underwater communication is a key area for have been applied and further work is in progress to
defence applications. Traditionally most underwater achieve low resistive p-contacts.
communication systems have been acoustic and have
SSPL has recently started a research activity for
relatively low bandwidth. Sonar communication
the fabrication of InGaN/GaN based semiconductor
is used more often, but available modems and
lasers. Fabrication process includes stripe formation
transducers are too large and very expensive.
by mesa etching using Reactive Ion Etching (RIE)
High bandwidth, short range underwater optical process, low resistance Ohmic contact formation on p
communications have high potential to augment and n side, thinning of epitaxial structure by grinding,
acoustic methods. Blue-Green region of the optical lapping & polishing, cavity formation, facet coating,
spectrum has the minimum attenuation in sea water. and packaging.
Communication between various underwater entities
One of the major challenges in processing of GaN-
like submarine to Unmanned Underwater Vehicle
based laser diode is in laser cavity facet formation.
(UUV) as well as underwater optical sensors can be
Typically, laser cavity facets are made by cleaving the
realized using laser sources emitting in blue green
semiconductor material. For c-plane green lasers,
region. A free space laser communication system
m-plane cleaved-facets may be formed by cleaving, as
operating in the blue-green portion of the spectrum
the m-plane is favourable for cleavage propagation.
has the potential to transmit at very high data rates
However, for semi-polar orientations the choice of
under sea water.
stripe direction is limited and facet formation by
The most promising and viable route for developing cleaving is very difficult.
blue/green laser diode is to employ Gallium Nitride The optical gain
GaN-based material systems. InGaN/AlGaN/GaN in the InGaN QWs
based multiple quantum well laser structures are is relatively low.
being used for developing such laser diodes. By The total optical
choosing the indium content in InxGa1-xN quantum losses have to be
wells in the active region, it is possible to realise laser minimized to reach
diodes emitting in wavelength range 400 nm to 550 lasing conditions at
nm. moderate current
density. Both facets are
Major Challenges
required to be coated
GaN based laser structures are usually grown on with high reflection
c-plane. In addition to issues of spontaneous and films to reduce the
piezoelectric polarization, there are various growth optical losses and so
and fabrication challenges. Growth of green laser the threshold current,
diode requires increase in the Indium (In) content however the output
in the InGaN Multi Quantum Well (MQW) layers. power is reduced. In
Growth of high-quality Indium rich InGaN/GaN QWs order to maintain
is still the major technical challenge due to several a high Wall Plug
material related issues such as high lattice mismatch Efficiency (WPE) and
between InGaN and GaN, deterioration of the material obtain high output
due to low growth temperatures requirement, In- power, the reflectivity
segregation and phase separation and p type doping. of the front facet has
Further, p-ohmic contact fabrication is a major to be reduced to an
optimised value. Fig 24. Blue Green Laser Diode
challenge due to requirement of high work function
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At SSPL research is being pursued to address all
the processing related issues. Recently, GaN-based
single emitter laser diode has been fabricated and
lasing action has been realised (Fig 24) in CW and
pulse mode. Figure 25 & 26 show the spectrum and
Current (A)
SENSOR TECHNOLOGY
To make our Armed Forces better equipped to deal program. The e-Nasika system is a SAW-GC (gas
with any kind of battlefield situations where outbreak chromatography) based system which is capable of
of any chemical or biological agents or destructive detecting lethal CWA like Sarin, Soman, Tabun, VX,
radiations, there is need to develop and fabricate Lewisite (G Agents), Sulphur Mustard (H Agent),
sensors that push the limits of sensitivity and Phosgene (choking agent), Hydrogen Cyanide (blood
selectivity. Besides Chemical Biological Radiation agent) and other agents, with concentrations in low
and Nuclear (CBRN) sensors other physical sensors ppb and in less than a minute time. The developed
such as underwater acoustic sensors are need of the system has been tested and certified by TNO,
hour. Next generation sensors are expected to be more Netherlands, an independent testing and certification
sensitive and reliable, in addition to being small in agency in the field of NBC. The system has met
size and low power consumption. Future systems are the JSQR performance criterion laid down by the
expected to have much more situational awareness. Services. (Figure 27).
This necessitates improving the performance of
existing devices and exploration of new application
areas, which were previously not thought of.
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18 JUNE 2023
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Technology Breakthrough
The technology breakthrough was achieved with
the realisation of fast gas chromatography operation,
Fig 29. Sequential Sensing of Gases over Different Concentrations
(a) for NO2 and (b) for NH3 (c) Response of Sensor for Sensing of by reducing the conventional GC response time from
Ammonium Nitrate
about 20 minute to 30 seconds. Both products use
A complete hand held the miniaturized GC module with SAW device as
prototype for detection of NO2 detector.
and NH3 has been developed
Major technology achievements and their details
for on-field detection.
are:
This prototype n-Nasika
(Fig 30) has been • Compound Detection: All compounds are
demonstrated during detected as a whole and not by its constituent
various exhibitions elements.
as well as DefExpo • Simultaneous Detection: All the targeted com-
and Aero India. pounds simultaneously in one go. No mode change
needed. Single unit for G, H, B, C, and TIC/TIMs.
Fig 30. n-Nasika-Automated
Handheld CNT-based Gas Sensor • Insensitivity to Physical Changes: SAW e-Nasika
has temperature, pressure/flow controlled inter-
ACADA nally. External variations do not affect the response.
Humidity is detected as a separate compound.
SSPL has also developed Automatic Chemical
Agent Monitor and Alarm (ACADA) system, modified • Saturation Proof: Detects from ppb to very high
version of present e-Nasika system. The system has a concentrations and quickly returns to normal.
remote display unit which can be connected through • Wide Compound Library: Large library compounds
cable and can be operated remotely. The remote are possible.
display incorporates all the system display features • Low False Alarms: Use of GC and compound
and can remain at 1 km distance from main ACADA detection leads to better selectivity and low false
system. The sensing technology and specifications in alarms.
both e-Nasika and ACADA are same. (Figure 31). • Indigenous technology: >70% indigenous.
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AE sensors (320 Nos.) and DAQ System (08 for various events like snow avalanche, air turbulence
Nos.) were successfully delivered and deployed at detection, and earthquake activities, etc.
different avalanche prone sites on Manali-Leh axis
(Dhundi and Patsio, HP) and J&K (Banihal Top). SAW-based e-Nasika
The AE sensor system is working in 24x7 mode on The technological achievements of SAW-based
these avalanche prone sites and collecting AE data. e-Nasika system will be utilised for developing a
The data will be analysed by DGRE for developing a 24x7 operated CWA detector for application in places
snow avalanche prediction model. SSPL successfully of strategic and public importance and for vehicle
transferred technology to M/s Canopus Instruments, mount CWA monitoring.
Thane for AE sensors and M/s Digilogic Systems Pvt.
Ltd., Hyderabad for AE Acquisition and Analysis CNT-based Gas Sensor
(DAQ) System.
The way forward after CNT-sensor training and
Future Plans for Sensors using artificial intelligence software the sensor module
will be used for screening variety of explosives, CWAs
Landslide Early Warning System-based on AE and other toxic gases like an e-nose.
Technology
SSPL has gained experience in design and MEMS-based Acoustic Vector Sensor
development of indigenous AE sensors and DAQ Indigenously developed AVS will be utilised for
system from its past project. The experience will estimating direction of arrival of incoming acoustic
be utilised for developing AE sensor system for signal. Typical application: Gunshot localisation
monitoring landslide events and further analysing
the trends of AE behaviour leading to the real-time THz Technology
landslide event. Machine learning methods and
artificial intelligence for the post-analysis of collected SSPL has plans to develop THz detector using
AE data will be used to develop an algorithm for graphene because of its high carrier mobility, zero
Landslide Early Warning System (LEWS). bandgap and strong interband absorbance in all THz
frequency which provides wideband THz detection.
Design and Development of Indigenous Acoustic THz imaging due to non-ionising radiations is very
Vector Sensor pertinent for homeland security. THz spectroscopy
provides unique fingerprints of explosives, CWAs and
Acoustic Vector Sensor (AVS) can be used other materials. (Fig 37)
for various applications like direction of arrival
estimation, infrasonic sensing, etc. SSPL is working
towards the development of AVS
Blast Sensors
SSPL is working on development of indigenous
pressure sensors based on piezoelectric element.
Application of blast sensors will be for detection of
various shock waves, blast or explosive testing.
Infrasonic Sensors
SSPL is involved in the design and manufacturing
of infrasonic sensors. Typical application of infrasonic
sensors will be to detect and capture infrasonic waves Fig 37. THz Detector
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COOLING TECHNOLOGIES
Thermoelectric Cooler Technology
Thermoelectric Coolers are solid state cooling temperature stabilization of laser diode, Ti-based
devices based on the Peltier Effect which can provide micro-bolometer arrays, InGaAs-based SWIR
localised cooling or heating on the application of a DC detectors, cooled garments, etc. Cooler modules with
voltage. These devices find widespread use in defence sizes ranging from 10X10 to 50X50 sq mm and capable
systems and sub-systems for cooling and temperature of pumping heat in the range of 1W to 30W have been
stabilization of active devices such as laser diodes, designed and fabricated as per the requirement. The
infrared FPAs and other sensors. operating currents of these modules are in the range
of 250mA to 10A. Maximum temperature differential
SSPL has developed the technology for design
of upto 64K can be achieved across the device. Scale
and fabrication of single stage thermoelectric cooler
up of device numbers has been achieved through
modules based on Bi2Te3 alloys. The complete
interface with an industry partner.
technology development consists of thermoelectric
material optimization, device design and performance Multi-stage TE cooler modules (Fig 39) have been
simulation, and standardization of the process developed to obtain higher temperature differentials
sequence for fabrication of cooler modules reliably
and reproducibly. Polycrystalline ingots of p-type and (> 64K) .
n-type Bismuth Telluride alloys with figure of merit This develop-
> 2.5 X 10-3 /K were grown using vertical directional ment makes
freezing. Modules have been designed for different in-
it possible to
house applications based on user requirements. The
custom design
complete process sequence, which consists of several
the optimum
sub-technologies such as development of metalized Fig 38. Single Stage Cooler
modules for
alumina substrates, development of miniature
any application
thermo-elements, design of demountable assembly
based on
jigs, optimisation of soldering procedures for module
the user
assembly and testing of module characteristics has
requirements
been optimised.
and fabricate
Single stage TE cooler modules (Fig 38) have them indige-
been developed for applications such as cooling/ nously.
Fig 39. Multistage Cooler
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further enhancement in ZT values for n-type nano- Stirling Cryocooler
composites is to be carried out.
Stirling Cryocooler is used for cooling of Infrared
Focal Plane Arrays (IRFPAs) being developed at
SSPL and is also suitable for commercially available
detector arrays. These IRFPAs have to be maintained
at cryogenic temperatures of the order of 80 K for
their normal operation. Cryogenic temperatures
are produced by mechanical closed cycle Stirling
Cryocoolers. These Cryocoolers work on Stirling
Cycle and are characterized by high efficiency, fast
cool down time, smaller size, lightweight and high
reliability.
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Specifications: can be maintained at that temperature, so long as the
detector is operational. Normally, a Joule Thomson
• Cooling Capacity : 0.5 W @ 80 K
(JT) cooler is used for this purpose, as it is quite
• Cold Finger Size : 8 mm max compact, offers minimum weight (10-15 grams), have
• Cool-Down Time : < 6 minutes no moving parts and offers a very quick cool-down
• Type of Drive : Brushless DC motor time of the order of about 7 to 20 seconds.
• Feedback Control : Yes A JT cryo-cooler is fundamentally a counter
• Max. Input Power : 20 W flow heat exchanger and a nozzle which produces
• Steady State Input : 10W @ 80K refrigeration based on the joule Thomson principle
• Weight : < 450 gm of isenthalpic expansion of a refrigerant (high
purity nitrogen or argon) from a high pressure and
temperature to a lower pressure and temperature.
Cryo-coolers are often rated by their available
refrigeration capacity measured in watts, at a
particular temperature, at which the refrigeration is
available, for example 1W at 80K. A JT cooler works
on an open cycle. Another important parameter is the
power input or work required to achieve refrigeration.
The Coefficient of performance of a refrigerator is
defined as the ratio :
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Developed JT Cooler the self regulation mechanism of this JT cooler. The
exploded view of the self-regulation mechanism of
So far a Constant flow JT cooler, as shown in
the JT cooler is shown in Figure 46 and a cut section
Figure 44, has been developed at SSPL, using all
of the complete self-regulating JT cooler is shown in
indigenous parts, except fin-tube. On cooling test
Figure 47.
at Room temperature this cooler has produced the
liquid Nitrogen within the desired cool-down time of
about 30 secs with a supplied Nitrogen gas pressure
of 3000psi (208 bar).
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EMERGING TECHNOLOGIES
MEMS-based THz Detector
Terahertz (THz) waves, refer to electromagnetic
radiation in the frequency range from 0.1 to 10 THz.
(1 THz = 1012 Hz), which correspond to the wavelengths
between 3 mm and 100 μm. Explosives, like, HMX,
RDX, PETN, etc. have unique spectroscopy features
in THz frequency range. Hence THz is being widely
researched for their applications in solving security
and anti-terrorism problems. THz is non ionizing yet
can penetrate some distance through body tissue, (b)
so it is of interest as a replacement for medical
X-rays. Furthermore, the most common non-polar
substances are transparent to it and have spectral
fingerprints in the THz frequency range creating
interest for research in scientific and applied fields
including non-destructive testing, medicine etc.
THz communication is another important area of
research as it offers higher bandwidth and resolution (c) (d)
as compared to microwaves. The technology in this
spectral region is still in its infancy and generally
referred to as THz Gap.
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corrugated cardboard, clothing, shoes, bookbags, etc
in order to probe the potentially dangerous materials
contained there. Many materials of interest for
security applications including explosives, chemical
and biological agents have characteristic THz spectra
that can be used to fingerprint and thereby identify
these concealed materials.
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Graphene THz Modulator Quantum Technologies
By applying a gate voltage/optical pulse the Fermi Within the last two decades, Quantum
level in graphene can be tuned and transmission Technologies (QT) has made tremendous progress,
in graphene channel can be modulated in the moving from Noble Prize winning experiments in
THz frequency range. SSPL fabricated different quantum physics into a cross-disciplinary field of
configurations of graphene THz modulators, achieved applied research. The field essentially comprises
modulation depth upto 15-23% by electrical gating of four domains: Quantum Computation, which
and 45-55% by optical pumping. employs quantum effects to dramatically speed up
certain calculations; Quantum Communication,
Graphene THz Detector where individual or entangled photons are used to
transmit data in a secure way; Quantum Simulation,
When steady current flows in the GFET channel,
where well-controlled quantum systems are used
graphene plasmons are generated in the channel
to reproduce the behaviour of other, less accessible
which modulates gate and source/drain potential.
quantum systems and quantum sensing where the
The potential developed across the graphene channel
high sensitivity of coherent quantum systems to
is directly proportional to the intensity of incident
external perturbations is exploited to enhance the
THz beam. SSPL have fabricated graphene THz
performance of measurements of physical quantities.
detectors and achieved responsivity upto 100 mV/W
The future is quantum and nothing should stand in
and NEP upto 400 nW/Hz1/2.
the way of these quantum technologies becoming
the engine of innovations in science, economics and
THz Testing Facility
society in the 21st century.
THz testing arrangement has been created for
THz characterization of materials (graphene, MoS2, In the last few years, significant technological
InP, LT-GaAs, LT-InGaAs, etc.) and testing of the advancements have been reported in the domain of
fabricated THz devices using THz Frequency Domain quantum computing with quantum computers gaining
System (THz-FDS system) and THz Time Domain most of the headlines. However, a comparatively
System (THz-TDS). Detecting THz beam is a challenge less visible and quieter revolution in the world of
because of the low power of the incident THz beam. sensors is also on its way and is just as significant
By using different opto-mechanical components for and important. The quantum systems are highly
aligning the weak THz beam and lock-in amplifier, sensitive to external perturbations and while this
SMUs, etc. THz testing arrangement has been may prove to be a challenge and prime weakness in
improvised Figure 50, 51. quantum computing, the same serves as an advantage
while developing 'quantum sensors.' An emerging
class of quantum sensors are now being used for
measurement of several physical quantities including
time, frequency, electric and magnetic fields.
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during the past decades, yet the detection of smallest Quantum Sensing
magnetic fields with highest spatial resolution at
Development of Miniaturized Atomic
room temperature has proven to be a great scientific
Magnetometer and Miniaturized Atomic Clock
challenge. The requirement of a lightweight,
thermally stable, broad range magnetometer with SSPL is working on development of key
high spatial resolution may well be met with a components of physics package of quantum sensors
quantum magnetometer in the coming years. This i.e. VCSEL and Microfabricated AlkaliVapor Cell
includes several military areas where the sensors may (MAVC) to demonstrate their miniaturized version
be needed, for example, to provide highly accurate with low power budget. VCSEL is required as a pump
positioning data for detection of magnetic anomalies source for polarisation of Rb or Cs atoms in the vapour
produced by metallic objects such as unexploded cell. This requires wavelength to be matched at D1 or
ordinance, geophysical structures, vehicles, and D2 transition frequencies of these atoms. Fabrication
ships. of VCSEL is complex technology and requires state
of the art infrastructure. SSPL has started working
A dramatic change in the military technology
on development of these laser sources under the
landscape can therefore be envisioned in the next few
proposed project on Development of miniaturised
years by the use of these miniaturized magnetometers.
magnetometer and will also be suitable for use in
The miniaturisation and functionalisation of the
atomic clocks too. The tight tolerance required
proposed magnetometer should significantly impact
for atomic sensor applications require rigorous
and disrupt the key applications that benefit from it.
Characterization of VCSEL source. A full-fledged
Atomic clocks are among the most accurate time Characterization facility is also being set-up at SSPL.
and frequency standards which uses transition of The technology once developed will be translated to
alkali atoms as resonator. For almost a decade, an GAETEC for future production.
extensive work has been carried out world-wide to
MAVCs are sandwiched type structure in which
develop the miniaturized version of these atomic
cavities, made of silicon, are sandwiched between
clocks generally known as Chip Scale Atomic Clocks.
two glass plates. These devices are loaded with alkali
The principle of these miniaturized clocks is based
vapors and buffer gas along with an integrated heater
on Coherent Population Trapping (CPT) phenomena
to keep an optimum atomic density.
which is observed in a compact hermetically sealed
silicon vapour cell of few cubic millimetres which is At SSPL, 1400 µm (1.4 mm) thick, 4” Silicon, P Type
the heart of these quantum sources. These cells having <100> substrate which is not a conventional thickness
alkali vapours, interrogated by a high-frequency of 4” wafers (500 µm) and in fact 3x times higher has
modulated laser beam and signals are analysed. been used. Dual cavity design known as dispensing
cavity and optical cavity connected through 150µm
The frequency stability of such atomic clocks is
deep channel has been used. Hermetical Sealing of
based on transitions between the hyperfine ground
Glass/Si/Glass via Anodic bonding has been utilised
state levels of alkali atoms such as Cesium (Cs) or
to fabricate sandwich structure. The incorporation
Rubidium (Rb) whose transition frequencies are 9.91
of highly reactive Alkali metals inside deep cavities
GHz and 6.64 GHz respectively.
carried out through solid state route. The first
The advanced semiconductor processing, the prototype of Cs and Rb alkali vapour cells having a
availability of laser diodes on chip like VCSEL typical die size of ≤ 10 mmx 8mm and cavity volume
and CPT phenomena made the miniaturization of ≤5 mm3 in presence of argon as buffer gas has been
conventional atomic clock possible with typical short- demonstrated successfully. As a next immediate step,
term stability <1E-11@1000 s and aging rate <1E-8/ activation of solid-state alkali dispenser pills will
Year. be carried out using high power laser and focussing
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optics. The so obtained alkali vapours inside the cavity
will be analysed through spectroscopic measurements
whose setup are getting ready at SSPL. SSPL will also
put emphasis on Physics Package development using
mostly indigenous optical/ mechanical components.
Miniaturized control electronics and software
development will be done through an Indian Industry
to support indigenous development to a large extent
At present, the first prototype demonstration of Silicon
Alkali Vapour Cell is done at SSPL. Once the system
is developed, ready and successfully demonstrated,
India will be one of the leading countries for in-house
Fig 54. mm Deep Cavity by Laser Milling
quantum sensing technology.
Fig 53. Schematic of Silicon-based Alkali Vapour Cell Fig 56. First Prototype Demonstration of Silicon Alkali Vapour Cell