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Composites Part B
journal homepage: www.elsevier.com/locate/compositesb
a r t i c l e i n f o a b s t r a c t
Article history: The mechanical properties of injection moulded short glass fibre-reinforced polyamide composites was
Received 3 April 2014 investigated using experimental techniques. The Digital Image Correlation technique was applied during
Received in revised form the tensile tests in order to obtain the stressestrain curves and to identify the fracture location at the
3 February 2015
early stages of the tests. Moreover, the thermographic technique was used during the static tests in order
Accepted 16 March 2015
to identify the fracture zone and also during the fatigue tests, carried out at different frequencies, to
Available online 23 March 2015
study the temperature evolution of the specimen. A theoretical model was developed to analyze the
temperature evolution during the fatigue test and the effect of the test frequency. The aim of this study is
Keywords:
B. Fatigue
the application of the Thermographic Method for the fatigue assessment of short glass fibre-reinforced
B. Mechanical properties polyamide composites.
D. Mechanical testing © 2015 Elsevier Ltd. All rights reserved.
1. Introduction Tensile tests were performed by Godara and Raabe [5] using
digital image correlation (DIC) for resolving the mechanical
Today, lightweight and low cost components can be obtained behaviour and spatial distribution of the plastic microstrains in an
with short fibre reinforced plastics. The recyclable nature of these epoxy resin reinforced with 35 wt% short borosilicate glass fibres.
materials by comparison to thermoset matrixes composites is also With the growing interest in lightweight structures, the short
clearly appealing. Restricted a few years ago to automotive appli- fibres reinforced plastics (SFRP) are being used increasingly in load-
cations with limited mechanical requirements, these materials, bearing applications, where the components experience cyclic
filled with glass fibres up to 50% in mass, are now used for struc- loads, so they are prone to fatigue failure in service. Thus, there is an
tural components [1e3]. increasing attention on the design of SFRP components against
Polyamide-6,6 is known for its balance of strength, modulus and fatigue and a more detailed knowledge of their fatigue behavior is
chemical resistance. Both polyamide-6,6 and short E-glass fibre needed. The fatigue mechanisms in short glass fibre reinforced
reinforced polyamide-6,6 composite have many potential applica- polyamide 6 were presented by Horst and Spoormaker [6]. The
tions, such as stressed functional automotive parts (fuel injection fatigue tests of SFRP material are even more time consuming than
rails, steering column switches), safety parts in sports and leisure the tests required for metallic materials because the viscous ma-
(snowboard bindings) and other commercial products where creep terial exhibits a high heat build-up at high frequencies [3,7].
resistance, stiffness, resistance to dynamic fatigue are demanded in Jegou et al. [8] applied a heat build-up protocol on a short fibre
addition to weight saving. reinforced plastic, used for structural automotive applications
The design of short fibre reinforced plastic components for (PA66GF50), and predicted the fatigue properties from the tem-
structural applications requires an accurate knowledge of the perature measurements. A first approach, based on the tempera-
several factors affecting the tensile properties and the fatigue life- ture measurements, was proposed, providing a good correlation to
time. The tensile strength and toughness/impact energy of short the fatigue data obtained according to the classic procedure.
fibre reinforced polymer composites would depend on a number of Esmaeillou et al. [9] performed tensionetension fatigue tests on
factors such as fibre length, interfacial adhesion and properties of SFRP composites at different applied maximum stress and analyzed
components [4]. the specimens at both microscopic and macroscopic scale. The
temperature was measured during cyclic loading using an infrared
camera and also the progressive loss of stiffness was evaluated
* Corresponding author. Tel.: þ39 347 3209239.
E-mail address: giacomo.risitano@unime.it (G. Risitano).
http://dx.doi.org/10.1016/j.compositesb.2015.03.052
1359-8368/© 2015 Elsevier Ltd. All rights reserved.
V. Crupi et al. / Composites Part B 77 (2015) 268e277 269
during the tests. Moreover, the effects of the frequency and of the and also the authors have a strong background in this filed. They
mean stress on the fatigue strength were evaluated. applied the TM for the fatigue assessment of steels in low cycle [25]
In Ref. [10], Noda et al. studied the fatigue behaviour of short high cycle [26], and very high cycle [27] fatigue regimes and also for
glass-fibre reinforced nylon 66 under stress controlled fatigue tests the fatigue analysis of metallic mechanical components [16].
on the basis of the nonlinear dynamic viscoelasticity measure- This study is the first step of a research aimed at applying the TM
ments. In order to analyze the effect of nonlinear viscoelasticity on for the fatigue assessment of composite materials, obviously taking
the fatigue behavior, quantitative measurements of nonlinear into account that the composites have different and more complex
viscoelasticity, based on Fourier analysis, were carried out. fatigue mechanisms respect to metallic materials.
Sonsino et al. [3] investigated the fatigue strength behaviour of a A review of the scientific results in literature, related to the
short-glass-fibre reinforced polyamide PA66GF35. The authors application of the thermographic techniques to composite mate-
emphasize the importance of monitoring the surface temperature rials have been presented by Vergani et al. [28].
during fatigue testing for this kind of materials. Moreover, they note De Monte et al. [29] investigated the influence of temperature,
that the surface temperature, reached by the specimen during a thickness and fibre orientation on the off-axis behaviour of
fatigue test, must not exceed the value of 35 C in order to obtain PA66GF35 under cyclic loading.
reliable values and not influenced by the possible structural The same material was considered in this study. Tensile tests
changes of the material. were carried out on specimens using a hydraulic testing machine
Handa et al. [11] investigated the temperature evolution of the and DIC and IR Camera have been used during all tests. Stress vs
specimens in PA66GF33 during fatigue tests, carried out at different strain curves and temperature evolution associated to the applied
values of load ratio and test frequency (in the range between 5 and tensile stress were determined. The trend of the surface tempera-
50 Hz). They proposed a model which correlates the stabilization of ture of the specimen during fatigue tests was analyzed at different
the surface temperature with the parameters E0 (storage modulus), test frequencies. The stress range, applied during the fatigue tests,
E00 (loss modulus) and tand (loss factor). was maintained at a constant level below the fatigue limit in order
An energy-based approach was proposed by Meneghetti and to obtain an indication on the amount of energy, which is generated
Quaresimin [12] to analyse the fatigue strength of plain and only by internal material damping.
notched specimens made of a short fibre-reinforced plastic weak-
ened by rounded notches. 2. Static tests
Full-field measurement techniques were applied in Refs. [13,14]
for the damage investigation of composites. 2.1. Material and methods
The traditional methods of fatigue assessment of metallic and
composite materials are extremely time consuming. In order to The material used in this study is a commercial polyamide-6,6
overcome the above-mentioned problems, an innovative approach containing 35 wt% glass-fibres, designed as PA66GF35. Table 1
for fatigue assessment of materials and structures has been pro- shows the mechanical and physical properties of the material;
posed in Ref. [15]: the Thermographic Method (TM). The Thermo- the values are extracted from the manufacturer's datasheet. The
graphic Method, based on thermographic analyses, allows the rapid specimens were made by injection moulding. Granulated com-
determination of the high-cycle fatigue limit [15] and the SeN mercial materials were held in a drying furnace at 60 C ÷ 80 C for
curve [16] of materials, mechanical components and structural 24 h prior to injection. For all blends, the injection parameters were
details, using a very limited number of tests. There are a lot of pa- maintained constant. Dog bone specimens (Fig. 1) were injection
pers [17e24] in literature, which confirm that the TM has been moulded (type 1A of the ISO 527-2:1993 standard) with processing
already used successfully to predict the fatigue strength of metals, conditions based on ISO 294-1:1996 and ISO 1873-2:2007. The
270 V. Crupi et al. / Composites Part B 77 (2015) 268e277
Table 1
Mechanical and physical properties of PA66GF35 according to the manufacturer's datasheet.
Fibre diameter Fibre length Density Specific heat capacity Thermal linear expansion coefficient Tensile strength Elastic modulus Failure strain
2.2. Theory/calculation a
DTs ¼ T $s ¼ Km T0 $s1 (2)
r$c 0 1
As reported in Ref. [28], there are many studies in literature on
the thermal response of composites during static tests. During where Km is the thermoelastic coefficient.
static tests of common engineering metals, the temperature evo- Clienti et al. [31] for the first time correlated the first deviation
lution on the specimen surface, detected by means of an infrared from linearity, which corresponds to the end of the phase I, to the
camera, is characterized by three phases: an initial approximately fatigue limit of plastic materials. As reported in Ref. [32] “the end of
linear decrease due to the thermoelastic effect (phase I), then the the thermoelastic phase could be related, also for composites, to a
temperature deviates from linearity until a minimum (phase II) and stress value sD, which can identify the initiation of a different kind
a very high further temperature increment until the failure (phase of damage”. This was observed for basalt [32] and glass [33] fibre
III). A typical DTeN curve, obtained by a constant-amplitude fatigue reinforced composites. The SEM analyses on glass-fibre reinforced
test, is shown in Fig. 2. specimens, tested at various load levels, and the measurements of
the fracture zone. For all stage point, the evolution of strain is
constant and gives a good prediction of the failure zone.
During some tensile tests, the temperature of the specimen
surface was detected by means of an IR camera. Fig. 4 shows the
pattern of the applied stress and the experimental temperature
increment DTS_exp, detected by means of the themocamera, during a
tensile test and some infrared images of the specimen. Comparing
the images obtained by thermographic (Fig. 4) and DIC (Fig. 3)
techniques, it is clearly evident that the infrared analysis gives less
accurate results for the prediction of the fracture zone than those
obtained by means of DIC technique. After a nonlinear initial part of
the DTS_expet curve, probably due to the stabilization of the grips of
the testing machine, an approximately linear trend is clearly visible
in the curve and its slope corresponds to the thermoelastic coeffi-
cient Km of eq. (2). A linear regression of this part of the DTS_expet
curve, relative to the phase I, was performed in order to include the
maximum number of thermal data, which allows to get the highest
correlation coefficient (R2 ¼ 0.9618). In the same graph it is re-
ported the theoretical temperature increment DTS_th, obtained
Fig. 2. Theoretical trends of stress and temperature during a static tensile test. applying eq. (1). The values of the parameters (density r, specific
heat capacity at constant pressure c and linear expansion coeffi-
cient a), used for eq. (1), are reported in Table 1. For the investigated
stiffness reduction in interrupted static tests, characterized by two
material, the DTS_expet curve has a different trend respect to the
loadingeunloading cycles, confirmed that the defects do not
linear trend of the theoretical DTS_thet curve when the applied
propagate and the global temperature trend during tensile static
stress is about 55 MPa as shown in Fig. 4.
tests is about linear until the applied stress in lower than sD [34].
Sonsino et al. [3] obtained by experimental tests that the value
of fatigue strength at Nf ¼ 1E6 cycles (R ¼ 1) for PA66GF35 (the
2.3. Results & discussion same material investigated in this study) is 55 MPa. A similar result
of fatigue strength at Nf ¼ 1E6 cycles (R ¼ 1) was obtained by De
Since the DIC technique is able to estimate the displacement Monte et al. [29] for PA66GF35 specimens with thickness t ¼ 3 mm.
field in each region of the specimen, it was applied during the
tensile tests in order to obtain the stressestrain curves and to
detect the failure zone at the early stages of the tests. Fig. 3 shows 3. Fatigue tests
an application of DIC technique during a tensile test. In the figure,
some images, obtained by DIC analysis during the tests, are showed 3.1. Material and methods
along with the stress versus strain curve in order to highlight the
evolution of strain in the fracture zone. Analysing Fig. 3, it can be The specimens, investigated under fatigue loading, have the
noted that even at low strain (about 0.4%) it's possible to identify same geometry (Fig. 1) of those used for the static tests and are
Fig. 3. Stressestrain curve and DIC images for a static tensile test.
272 V. Crupi et al. / Composites Part B 77 (2015) 268e277
Fig. 4. (a) Experimental trends of stress and temperature and IR images during a static tensile test; (b) Temperature evolution versus applied stress levels during a static tensile test.
made from the same material by injection moulding as reported in internal material damping due to the viscoelastic nature of the
paragraph 2.1. material itself.
The trend of the surface temperature of the specimen was For fatigue tests, the following parameters were used:
analyzed at five different test frequencies (1,3,6,9 and 12 Hz). The maximum stress smax ¼ 20 MPa; load ratio R ¼ 1; test frequency
stress range, applied during the tests, was maintained at a constant f ¼ 1,3,6,9 and 12 Hz.
level (20 MPa) below the fatigue limit [3] in order to obtain an As previously mentioned, the specimens were coated with black
indication on the energy amount, which is generated only by paint and during the test the surface temperature of the specimen
V. Crupi et al. / Composites Part B 77 (2015) 268e277 273
vT p
ε ¼ ε0 eiut (4) ¼b f $s0 $ε0 $sin d (12)
vt r$c
where s0 and ε0 are the stress and strain amplitudes, u is the being the number of fatigue cycles N related to frequency f and
angular velocity, d is the phase shift and t is the time. time t:
The complex modulus E* is the ratio between s and ε:
vT p
¼b $s $ε $sin d (13)
vN r$c 0 0
Then, a new parameter K can be introduced:
p
K¼b s $ε $sin d (14)
r$c 0 0
According to the definition of the parameters N* and DT*, shown
in Fig. 5, it follows:
Fig. 6. Experimental and theoretical DTdeN curves during the fatigue tests.
Table 4
for each test by means of a linear interpolation of the data relative
Theoretical and experimental values of K [K].
to the two phases of the DTdeN curves (Fig. 5), obtaining the values
of N* and DT* and the slope K. Moreover, a theoretical value of the Theoretical value Experimental value
slope K was calculated using eq. (14). The values of the parameters f ¼ 3 Hz f ¼ 6 Hz f ¼ 9 Hz f ¼ 12 Hz
(density r, specific heat capacity at constant pressure c and absor- 0.00060 0.00058 0.00065 0.00065 0.00065
bed energy factor b), used for eq. (15), are reported in Tables 1 and 3 Deviation [%] 4.7% 7.9% 7.4% 8.1%
[11]. Table 4 shows the comparison between the theoretical and
experimental values of K. A good achievement was obtained with a
percentage deviation lower than 8%. The results confirm that, as In Ref. [37], Crupi developed a theoretical model able to describe
show in Fig. 6, the slope K is almost the same for all the tests carried the temperature evolution during the phase I and phase II of the
out at different frequencies. Table 5 reports the values of N* and DT*. fatigue life:
The value of DT* increases with increasing the test frequency. Fig. 7
shows the correlation between DT* values and the corresponding f
DTd ¼ DTas $ 1 e t
N
(16)
values; as show in equation (12) and in Ref. [7], DT* is related to the
test frequency f by means of a linear relationship. These results
confirm the validity of the theoretical model applied to SFRP ma- where t is a constant; if N is t then DTd is 0.63 DTas and if N is 4t
Dt * ¼N * , then DTd is 0.98 DTas. The model was applied successfully to steels
terials. Moreover, the values of time f
required to reach the
in Ref. [37]. In order to apply eq. (16) on SFRP materials, the pa-
temperature increment DT* for each test, are reported in Table 5. It rameters N* and DT* were considered instead of Nas and DTas and it
is interesting to note that Dt* has an almost constant value for all was necessary to find the correct convergence criterion as a func-
the tests performed at different frequencies but at the same envi- tion of the relationship between N* and t parameters. Fig. 8 shows
ronmental testing conditions. the experimental DTdeN curve and other five curves, obtained
Table 3
Mechanical properties of PA66GF35 [11].
Absorbed energy ratio b [/] Storage modulus of elasticity E0 [MPa] Loss modulus of elasticity E00 [MPa] Loss factor tand [/]
Table 5
Characteristic values considered in the theoretical approach.
Test frequency Characteristic temperature increment Characteristic number of cycles Characteristic time increment
Fig. 7. Correlation between the temperature increment DT* and the frequency f with some IR images.
considering different values of the ratio between N* and t. By the Combining and developing the equation (16) with equation (15),
analysis of the results, it was found that the best convergence cri- it follows:
terion is obtained when t ¼ 1.5,N*. Applying this criterion for all
tests (Fig. 9), a good agreement between the experimental data and
DTd ¼ K$N * $ 1 e t
N
(17)
the theoretical model proposed by Crupi [37] is obtained.
Considering eq. (15) and t ¼ 1.5,N*, the equation (17) can be
written as:
p
N
DTd ¼ b s0 $ε0 $sin d$N * $ 1 e 1;5$N* (18)
r$c
Considering Dt* a constant value for all frequencies:
N* ¼ Dt * $f (19)
p N
DTd ¼ b s0 $ε0 $sin d$Dt * $f $ 1 e 1:5$Dt $f (20)
r$c
Fig. 9. Experimental data and DTdeN curves, predicted using the theoretical model proposed by Crupi [37].
conditions (stress amplitude, frequency), can be predicted by [7] Jia N, Kagan VA. Effects of time and temperature on the tensionetension fa-
tigue behavior of short fiber reinforced polyamides. Polym Compos
means of the developed eq. (20), knowing the constant value of Dt*.
1998;19(4):408e14.
[8] Jegou L, Marco Y, Le Saux V, Calloch S. Fast prediction of the Wo €hler curve
4. Conclusions from heat build-up measurements on short fiber reinforced plastic. Int J Fa-
tigue 2013;47:259e67.
[9] Esmaeillou B, Fitoussi J, Lucas A, Tcharkhtchi A. Multi-scale experimental
Digital image correlation and thermography techniques were analysis of the tensionetension fatigue behavior of a short glass fiber rein-
applied to PA66GF35 composite during static and fatigue tests. The forced polyamide composite. Procedia Eng 2011;10:2117e22.
[10] Noda K, Takahara A, Kajiyama T. Fatigue failure mechanisms of short glass-
main points of this experimental investigation are the following:
fiber reinforced nylon 66 based on nonlinear dynamic viscoelastic measure-
ment. Polymer 2001;42(13):5803e11.
DIC technique was able to predict the fracture zone already at [11] Handa K, Kato A, Narisawa I. Fatigue characteristics of a glass-fiber-reinforced
the first stage of the static tensile tests even at low values of polyamide. J Appl Polym Sci 1999;72(13):1783e93.
[12] Meneghetti G, Quaresimin M. Fatigue strength assessment of a short fiber
strain and to give more accurate results for the identification of composite based on the specific heat dissipation. Compos Part B Eng
the fracture zone than the IR analyses; 2011;42(2):217e25.
Thermographic Method was applied to PA66GF35 composite [13] Steinberger R, Valadas Leita~o TI, Ladst€
atter E, Pinter G, Billinger W, Lang RW.
Infrared thermographic techniques for non-destructive damage character-
during static tensile test; ization of carbon fibre reinforced polymers during tensile fatigue testing.
a correlation between a characteristic thermal parameter DT* J Fatigue 2006;28(10):1340e7.
and test frequency f has been proposed; [14] Goidescu C, Welemane H, Garnier C, Fazzini M, Brault R, Pe ronnet E, et al.
Damage investigation in CFRP composites using full-field measurement
a theoretical approach was developed to predict the tempera- techniques combination of digital image stereo-correlation, infrared ther-
ture evolution of SFRP composite during fatigue tests carried out mography and X-ray tomography. Compos Part B Eng 2013;48:95e105.
at different loading conditions (stress, frequency). [15] La Rosa G, Risitano A. Thermographic methodology for rapid determination of
the fatigue limit of materials and mechanical components. Int J Fatigue
2000;22(1):65e73.
References [16] Fargione G, Tringale D, Guglielmino E, Risitano G. Fatigue characterization of
mechanical components in service. Frat Integ Strut 2013;26:143e55.
[1] Bernasconi A, Davoli P, Armanni C. Fatigue strength of a clutch pedal made of [17] Luong MP. Infrared thermographic scanning of fatigue in metals. Nucl Eng Des
reprocessed short glass fibre reinforced polyamide. Int J Fatigue 2010;32(1): 1995;158(2e3):363e76.
100e7. [18] Meyendorf NGH, Ro €sner H, Kramb V, Sathish S. Thermo-acoustic fatigue
rrez-Solana F. Fatigue failure of short glass
[2] Casado J, Carrascal I, Polanco J, Gutie characterization. Ultrasonics 2002;40(1e8):427e34.
fibre reinforced PA 6.6 structural pieces for railway track fasteners. Eng Fail [19] Yang B, Liaw PK, Morrison M, Liu CT, Buchanan RA, Huang JY, et al. Temper-
Anal 2006;13(2):182e97. ature evolution during fatigue damage. Intermetallics 2005;13(3e4):419e28.
[3] Sonsino CM, Moosbrugger E. Fatigue design of highly loaded short-glass-fibre [20] Cura F, Curti G, Sesana R. A new iteration method for the thermographic
reinforced polyamide parts in engine compartments. Int J Fatigue 2008;30(7): determination of fatigue limit in steels. Int J Fatigue 2005;27(4):453e9.
1279e88. [21] Fan J, Guo X, Wu C, Zhao Y, Guo Q. Stress assessment and fatigue behavior
[4] Fu SY, Lauke B, Li RKY, Mai YW. Effects of PA6,6ePP ratio on the mechanical evaluation of components with defects based on the finite element method
properties of short glass fiber reinforced and rubber-toughened polyamide and lock-in thermography. Special Issue “Fatigue Design and Analysis in
6,6epolypropylene blends. Compos Part B Eng 2005;37(2e3):182e90. Transportation Engineering”, P I Mech Eng C J Mech. [publ. online2014].
[5] Godara A, Raabe D. Influence of fiber orientation on global mechanical [22] Starke P, Walther F, Eifler D. PHYBALea new method for lifetime prediction
behavior and mesoscale strain localization in a short glass-fiber-reinforced based on strain, temperature and electrical measurements. Int J Fatigue
epoxy polymer composite during tensile deformation investigated using 2006;28(9):1028e36.
digital image correlation. Compos Sci Technol 2007;67(11e12):2417e27. [23] Morabito AE, Chrysochoos A, Dattoma V, Galietti U. Analysis of heat sources
[6] Horst J, Spoormaker J. Mechanisms of fatigue in short glass fiber reinforced accompanying the fatigue of 2024 T3 aluminium alloys. Int J Fatigue
polyamide 6. Polym Eng Sci 1996;36(22):2718e26. 2007;29(5):977e84.
V. Crupi et al. / Composites Part B 77 (2015) 268e277 277
[24] Amiri M, Khonsari MM. Rapid determination of fatigue failure based on [30] Thomson W. On the dynamical theory of heat. Trans Roy Soc Edin 1853;20:
temperature evolution fully reversed bending load. Int J Fatigue 2010;32(2): 261e83.
382e9. [31] Clienti C, Fargione G, La Rosa G, Risitano A, Risitano G. A first approach to the
[25] Crupi V, Chiofalo G, Guglielmino E. Infrared investigations for the analysis of analysis of fatigue parameters by thermal variations in static tests on plastics.
low cycle fatigue processes in carbon steels. P I Mech Eng C e J Mech Eng Fract Mech 2010;77(11):2158e67.
2011;225(4):833e42. [32] Colombo C, Vergani L, Burman M. Static and fatigue characterization of new
[26] Wang XG, Crupi V, Guo XL, Guglielmino E. A thermography-based approach basalt fibre reinforced composites. Compos Struct 2012;94(3):1165e74.
for structural analysis and fatigue evaluation. P I Mech Eng C e J Mech [33] Harizi W, Chaki S, Bourse G, Ourak M. Mechanical damage assessment of glass
2012;26(5):1173e85. fiber-reinforced polymer composites using passive infrared thermography.
[27] Crupi V, Epasto G, Guglielmino E, Risitano G. Thermographic method for very Compos Part B Eng 2014;59:74e9.
high cycle fatigue design in transportation engineering. Special Issue “Fatigue [34] Libonati F, Vergani L. Damage assessment of composite materials by means of
Design and Analysis in Transportation Engineering”, P I Mech Eng CeJ Mech. thermographic analyses. Compos Part B Eng 2013;50:82e90.
[publ. online2014]. [35] Chandra R, Singh SP, Gupta K. A study of damping in fiber-reinforced com-
[28] Vergani L, Colombo C, Libonati F. A review of thermographic techniques for posites. J Sound Vib 2003;262(3):475e96.
damage investigation in composites. Frat Integ Strut 2014;27:1e12. [36] Rittel D. On the conversion of plastic work to heat during high strain rate
[29] De Monte M, Moosbrugger E, Quaresimin M. Influence of temperature and deformation of glassy polymers. Mech Mater 1999;31(2):131e9.
thickness on the off-axis behaviour of short glass fibre reinforced polyamide [37] Crupi V. An unifying approach to assess the structural strength. Int J Fatigue
6.6ecyclic loading. Compos Part A Appl S 2010;41:1368e79. 2008;30(79):1150e9.